#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/26/2212637.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212637_Fobs loop_ _publ_author_name 'Wu, Zi-Sheng' 'Liu, Chong-Bo' 'Wang, Yuan-Xing' 'Fang, Zhi-Jie' 'Wen, Hui-Liang' _publ_section_title ; 2-[(2R,3S,4S,5S)-3,4-Benzyloxy-2,5-bis(trityloxymethyl)tetrahydrofuran-2-yloxy]-3,4,5-tribenzyloxy-6-(trityloxymethyl)tetrahydropyran--methanol--2-butanone (1/1/0.75) ; _journal_coeditor_code LH2308 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1471 _journal_page_last o1472 _journal_volume 63 _journal_year 2007 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.322 _cell_angle_gamma 90.000 _cell_length_a 12.9897 _cell_length_b 24.0016 _cell_length_c 15.9688 _exptl_crystal_F_000 1708.00 _reflns_d_resolution_high 0.8106 _[local]_cod_data_source_file lh2308Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' _R70117a' _shelx_refln_list_code 4 _shelx_f_calc_maximum 196.93 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 687.24 449.66 12.67 o 3 0 0 81.45 96.00 4.28 o 4 0 0 142.94 177.22 6.89 o 5 0 0 172.57 202.30 10.78 o 6 0 0 202.44 176.61 25.90 o 7 0 0 1993.69 1953.97 49.34 o 8 0 0 254.21 213.66 27.44 o 9 0 0 288.75 331.46 16.40 o 10 0 0 46.30 44.57 9.25 o 11 0 0 1246.19 1204.57 72.48 o 12 0 0 122.87 128.58 52.40 o 13 0 0 65.72 56.07 26.56 o 1 1 0 367.20 14.64 2.63 o 2 1 0 2809.96 4573.82 59.12 o 3 1 0 2737.68 3807.84 75.27 o 4 1 0 830.13 754.49 16.71 o 5 1 0 111.25 91.12 5.23 o 6 1 0 480.91 436.67 9.18 o 7 1 0 93.74 82.43 9.71 o 8 1 0 142.28 160.77 11.95 o 9 1 0 527.08 474.72 13.37 o 10 1 0 1022.96 971.22 38.92 o 11 1 0 153.48 147.03 24.50 o 12 1 0 59.87 50.27 18.71 o 13 1 0 48.65 36.03 18.12 o 1 2 0 6252.63 2920.98 114.90 o 2 2 0 7602.58 7852.25 149.62 o 3 2 0 16716.27 16044.93 149.03 o 4 2 0 5033.97 3915.25 51.83 o 5 2 0 1468.62 1147.64 20.41 o 6 2 0 793.80 766.07 9.70 o 7 2 0 29.71 19.58 3.80 o 8 2 0 34.05 39.41 5.23 o 9 2 0 55.98 53.22 7.11 o 10 2 0 894.80 838.62 66.63 o 11 2 0 52.41 65.01 13.93 o 12 2 0 180.61 176.83 59.68 o 13 2 0 97.28 106.78 39.51 o 1 3 0 11466.33 6580.49 63.75 o 2 3 0 5254.31 3189.54 42.30 o 3 3 0 2198.31 1498.53 27.71 o 4 3 0 6683.44 6511.50 110.03 o 5 3 0 1968.35 2285.70 35.43 o 6 3 0 374.06 362.39 14.24 o 7 3 0 414.74 336.76 14.31 o 8 3 0 264.84 277.82 9.95 o 9 3 0 58.15 69.72 8.39 o 10 3 0 1431.91 1340.17 36.06 o 11 3 0 291.48 400.92 16.46 o 12 3 0 308.40 334.62 97.46 o 13 3 0 220.51 161.31 103.45 o 14 3 0 143.63 111.13 62.67 o 0 4 0 6605.50 7541.02 124.47 o 1 4 0 1599.76 1444.90 23.92 o 2 4 0 11933.23 10452.17 76.04 o 3 4 0 1862.08 1959.12 30.08 o 4 4 0 2499.75 2689.09 33.71 o 5 4 0 3107.55 3536.03 24.71 o 6 4 0 1388.05 1314.68 28.32 o 7 4 0 195.10 235.72 8.82 o 8 4 0 637.54 709.13 21.62 o 9 4 0 315.28 305.15 8.25 o 10 4 0 615.31 625.97 28.59 o 11 4 0 208.88 206.02 16.84 o 12 4 0 351.62 388.08 27.47 o 13 4 0 49.95 13.28 22.57 o 14 4 0 32.48 63.87 24.58 o 2 5 0 2751.44 2065.86 32.28 o 3 5 0 6008.03 5844.57 65.87 o 4 5 0 1655.43 1887.47 29.74 o 5 5 0 750.59 779.90 13.97 o 6 5 0 955.29 889.14 27.71 o 7 5 0 1546.51 1687.65 31.84 o 8 5 0 392.20 376.15 18.49 o 9 5 0 310.68 275.92 15.28 o 10 5 0 1993.55 1925.68 66.98 o 11 5 0 16.49 18.88 6.95 o 12 5 0 64.64 74.33 16.34 o 13 5 0 254.84 208.64 70.33 o 14 5 0 71.14 49.11 31.74 o 0 6 0 5423.07 6475.84 100.82 o 1 6 0 10346.95 10755.18 171.01 o 2 6 0 7536.93 6864.15 83.31 o 3 6 0 731.41 739.33 16.48 o 4 6 0 981.76 1041.66 21.38 o 5 6 0 3318.46 3794.59 45.20 o 6 6 0 1194.60 1173.46 28.70 o 7 6 0 726.31 709.39 21.28 o 8 6 0 88.93 103.43 13.60 o 9 6 0 7.04 8.93 3.45 o 10 6 0 157.44 173.16 25.94 o 11 6 0 26.50 27.36 8.46 o 12 6 0 366.05 345.54 72.43 o 13 6 0 74.93 67.28 26.18 o 14 6 0 6.76 27.72 21.09 o 1 7 0 283.19 225.00 12.21 o 2 7 0 9901.11 9943.03 137.33 o 3 7 0 1603.66 1268.76 21.44 o 4 7 0 1479.17 1425.85 30.39 o 5 7 0 564.99 613.83 19.37 o 6 7 0 1095.31 1332.01 32.46 o 7 7 0 175.79 199.05 8.08 o 8 7 0 17.97 11.69 3.21 o 9 7 0 153.88 229.24 39.76 o 10 7 0 1538.84 1581.78 57.34 o 11 7 0 150.91 161.44 26.21 o 12 7 0 9.67 13.27 9.22 o 13 7 0 0.27 9.53 23.97 o 14 7 0 114.31 69.96 30.40 o 1 8 0 4607.58 4295.20 62.68 o 2 8 0 210.26 183.39 5.03 o 3 8 0 346.34 387.05 14.21 o 4 8 0 2844.32 2572.41 42.93 o 5 8 0 356.60 357.98 10.99 o 6 8 0 218.98 198.20 7.23 o 7 8 0 270.93 256.09 10.94 o 8 8 0 116.56 119.59 16.98 o 9 8 0 1832.64 1886.33 50.54 o 10 8 0 1250.26 1229.16 50.55 o 11 8 0 129.74 123.80 24.36 o 12 8 0 490.56 541.96 57.92 o 13 8 0 22.20 40.07 32.70 o 14 8 0 220.76 178.56 71.39 o 1 9 0 3895.18 4023.26 73.65 o 2 9 0 147.56 33.47 18.13 o 3 9 0 3571.04 3775.09 44.85 o 4 9 0 917.11 1000.33 26.25 o 5 9 0 121.30 72.91 4.26 o 6 9 0 1188.79 1222.05 41.85 o 7 9 0 115.89 152.80 15.35 o 8 9 0 1228.27 1343.54 47.16 o 9 9 0 217.68 185.71 27.60 o 10 9 0 176.36 127.99 18.38 o 11 9 0 240.83 211.22 25.88 o 12 9 0 410.62 472.41 47.03 o 13 9 0 33.97 36.16 32.54 o 14 9 0 128.30 111.64 49.21 o 0 10 0 3884.45 3892.25 114.32 o 1 10 0 3882.89 4027.77 75.58 o 2 10 0 397.20 379.40 12.09 o 3 10 0 939.31 1037.40 26.92 o 4 10 0 897.20 850.39 22.70 o 5 10 0 110.54 85.17 7.29 o 6 10 0 657.69 678.17 24.06 o 7 10 0 474.68 433.33 18.81 o 8 10 0 916.63 914.89 39.74 o 9 10 0 153.93 146.23 18.75 o 10 10 0 316.12 360.29 25.46 o 11 10 0 19.71 16.29 8.62 o 12 10 0 352.64 394.21 67.18 o 13 10 0 8.19 23.46 6.16 o 1 11 0 720.60 791.11 27.36 o 2 11 0 961.77 967.27 25.36 o 3 11 0 52.35 47.00 6.35 o 4 11 0 276.74 339.30 6.13 o 5 11 0 414.09 382.64 12.81 o 6 11 0 62.26 42.19 9.91 o 7 11 0 7.30 12.11 5.84 o 8 11 0 3365.48 3579.70 41.78 o 9 11 0 1142.86 1124.18 46.34 o 10 11 0 99.48 142.19 26.04 o 11 11 0 15.08 18.64 7.73 o 12 11 0 404.69 447.77 31.84 o 13 11 0 6.17 6.33 31.76 o 0 12 0 869.42 836.70 31.69 o 1 12 0 54.44 64.43 7.48 o 2 12 0 1871.52 1871.40 42.57 o 3 12 0 752.96 876.85 24.97 o 4 12 0 711.11 754.64 21.61 o 5 12 0 1045.91 1063.96 35.80 o 6 12 0 638.87 729.49 29.51 o 7 12 0 1038.06 1024.97 43.99 o 8 12 0 784.64 731.21 31.81 o 9 12 0 685.11 676.63 29.95 o 10 12 0 174.10 177.92 28.71 o 11 12 0 175.69 151.57 25.63 o 12 12 0 58.66 62.46 13.78 o 13 12 0 150.94 136.79 40.69 o 1 13 0 152.86 171.16 23.50 o 2 13 0 2999.35 3213.37 71.08 o 3 13 0 1883.86 1842.74 33.60 o 4 13 0 1573.79 1392.83 29.88 o 5 13 0 1794.75 1599.43 38.41 o 6 13 0 637.08 730.64 34.36 o 7 13 0 175.28 155.21 24.03 o 8 13 0 1418.00 1401.96 50.87 o 9 13 0 1902.11 2030.05 69.55 o 10 13 0 85.46 63.88 11.18 o 11 13 0 286.33 260.88 37.61 o 12 13 0 40.97 41.05 14.15 o 13 13 0 41.10 48.21 13.84 o 0 14 0 285.89 329.47 17.96 o 1 14 0 418.66 368.11 9.27 o 2 14 0 979.01 986.88 19.39 o 3 14 0 682.66 624.55 24.65 o 4 14 0 215.19 210.63 9.60 o 5 14 0 486.86 461.05 24.87 o 6 14 0 759.63 830.26 36.87 o 7 14 0 243.22 226.05 27.14 o 8 14 0 355.12 408.50 21.09 o 9 14 0 209.14 184.91 24.55 o 10 14 0 61.32 72.05 14.43 o 11 14 0 151.42 148.15 20.17 o 12 14 0 158.88 197.95 34.96 o 13 14 0 7.61 -5.83 11.75 o 2 15 0 139.15 132.66 11.80 o 3 15 0 226.44 191.99 10.27 o 4 15 0 1229.52 1329.80 35.09 o 5 15 0 128.06 164.47 23.75 o 6 15 0 123.15 75.53 21.43 o 7 15 0 46.60 57.05 9.17 o 8 15 0 2043.25 2119.78 75.51 o 9 15 0 437.81 497.50 41.45 o 10 15 0 197.09 186.07 33.99 o 11 15 0 10.21 -6.63 11.22 o 12 15 0 178.74 140.49 28.22 o 1 16 0 524.15 479.13 15.89 o 2 16 0 132.99 89.90 13.14 o 3 16 0 216.88 183.05 11.23 o 4 16 0 30.90 21.39 4.79 o 5 16 0 132.82 134.84 17.58 o 6 16 0 120.28 120.31 16.18 o 7 16 0 153.92 130.97 19.24 o 8 16 0 652.86 792.82 36.45 o 9 16 0 189.93 185.92 29.95 o 10 16 0 212.77 215.73 37.06 o 11 16 0 12.82 26.98 9.18 o 12 16 0 6.62 18.93 9.96 o 1 17 0 19.75 10.17 3.50 o 2 17 0 411.36 415.32 15.08 o 3 17 0 1383.71 1450.10 45.15 o 4 17 0 126.56 124.10 18.70 o 5 17 0 813.25 793.11 25.91 o 6 17 0 6.72 20.13 6.99 o 7 17 0 336.42 355.23 46.19 o 8 17 0 37.33 47.29 10.69 o 9 17 0 157.27 138.64 24.56 o 10 17 0 51.57 57.51 19.05 o 11 17 0 27.64 13.38 7.26 o 12 17 0 51.15 60.60 18.32 o 0 18 0 900.27 1045.98 36.49 o 2 18 0 361.11 323.05 12.53 o 3 18 0 158.82 120.00 19.74 o 4 18 0 579.99 553.51 34.08 o 5 18 0 1274.27 1342.69 82.38 o 6 18 0 802.13 717.87 35.47 o 7 18 0 389.37 403.67 23.49 o 8 18 0 67.54 61.82 12.35 o 9 18 0 201.47 147.67 22.11 o 10 18 0 58.31 45.39 10.61 o 11 18 0 1.75 -6.54 14.56 o 1 19 0 113.66 74.80 29.00 o 2 19 0 954.87 1038.04 35.65 o 3 19 0 464.03 497.10 64.01 o 4 19 0 543.12 516.47 18.01 o 5 19 0 37.24 53.65 12.14 o 6 19 0 93.30 99.22 17.87 o 7 19 0 107.52 101.47 16.43 o 8 19 0 122.79 133.15 15.98 o 9 19 0 37.23 19.14 10.42 o 10 19 0 44.86 50.68 14.92 o 11 19 0 22.15 21.80 8.78 o 0 20 0 91.95 115.52 17.79 o 1 20 0 71.91 59.57 8.96 o 2 20 0 720.49 723.69 30.22 o 3 20 0 408.45 352.85 55.49 o 4 20 0 86.22 75.53 13.78 o 5 20 0 320.50 304.26 38.75 o 6 20 0 510.07 551.47 29.43 o 7 20 0 118.76 86.46 21.20 o 8 20 0 147.33 149.78 20.77 o 9 20 0 113.72 108.98 19.96 o 10 20 0 94.05 97.26 25.09 o 1 21 0 99.50 85.78 21.55 o 2 21 0 437.69 509.97 15.47 o 3 21 0 411.71 380.37 37.39 o 4 21 0 10.20 14.01 7.59 o 5 21 0 578.29 600.82 33.35 o 6 21 0 143.52 178.74 25.03 o 7 21 0 14.12 27.09 9.48 o 8 21 0 50.21 40.13 11.02 o 9 21 0 12.57 3.83 8.11 o 10 21 0 84.43 71.24 16.92 o 0 22 0 557.83 602.78 38.29 o 1 22 0 140.71 102.28 32.52 o 2 22 0 182.91 194.27 13.59 o 3 22 0 18.13 26.76 7.32 o 4 22 0 662.96 683.76 44.76 o 5 22 0 18.30 9.98 11.11 o 6 22 0 263.88 254.78 36.94 o 7 22 0 5.88 12.66 8.38 o 8 22 0 40.96 37.25 10.28 o 9 22 0 35.14 35.36 12.69 o 1 23 0 84.69 60.23 15.39 o 2 23 0 70.79 69.87 13.78 o 3 23 0 106.99 111.38 16.51 o 4 23 0 158.22 115.42 19.93 o 5 23 0 340.92 388.67 28.94 o 6 23 0 62.79 59.68 13.14 o 7 23 0 26.87 24.83 7.08 o 8 23 0 94.65 130.78 28.84 o 9 23 0 21.35 21.19 17.88 o 0 24 0 707.14 777.84 40.02 o 1 24 0 213.22 206.02 30.16 o 2 24 0 45.06 48.30 11.23 o 3 24 0 39.61 34.76 8.15 o 4 24 0 266.93 267.39 39.57 o 5 24 0 207.42 213.99 41.15 o 6 24 0 42.64 37.67 10.65 o 7 24 0 29.67 26.36 10.34 o 8 24 0 222.94 200.96 39.84 o 1 25 0 26.88 27.45 7.77 o 2 25 0 76.70 65.49 19.09 o 3 25 0 13.06 14.93 6.59 o 4 25 0 193.94 198.73 30.59 o 5 25 0 20.78 23.36 10.28 o 6 25 0 55.15 66.28 15.35 o 7 25 0 105.93 122.08 26.69 o 0 26 0 1193.12 1353.80 215.49 o 1 26 0 120.61 121.96 19.73 o 2 26 0 4.52 2.48 8.95 o 3 26 0 15.07 16.67 9.98 o 4 26 0 2.04 12.13 7.85 o 5 26 0 33.80 43.33 9.54 o 6 26 0 68.01 73.66 21.23 o 7 26 0 66.90 58.35 13.45 o 1 27 0 17.98 16.52 8.29 o 2 27 0 15.96 24.48 9.76 o 3 27 0 112.63 131.17 24.71 o 4 27 0 134.29 124.16 28.76 o 5 27 0 175.14 145.29 30.81 o 6 27 0 76.84 66.68 16.83 o 0 28 0 40.52 40.93 23.74 o 1 28 0 67.15 77.61 18.92 o 2 28 0 139.31 168.01 34.39 o 3 28 0 16.62 24.84 11.46 o 4 28 0 1.64 29.55 10.80 o 1 29 0 12.73 35.60 13.13 o 2 29 0 10.84 22.35 10.76 o -11 0 1 227.65 256.18 23.28 o -10 0 1 1006.82 960.77 43.50 o -9 0 1 110.55 108.93 18.87 o -8 0 1 614.37 687.98 29.74 o -7 0 1 109.70 127.84 6.18 o -6 0 1 87.33 95.02 5.88 o -5 0 1 486.78 769.13 24.15 o -4 0 1 38.54 9.18 5.08 o -3 0 1 30.21 11.45 7.67 o -2 0 1 6808.89 4120.21 105.08 o -1 0 1 77.80 331.26 11.57 o 1 0 1 948.56 70.45 4.02 o 2 0 1 24492.65 23962.09 334.24 o 3 0 1 8984.29 10387.07 98.10 o 4 0 1 1560.74 1308.03 32.02 o 5 0 1 3587.48 3488.09 144.16 o 6 0 1 2777.56 2908.76 68.28 o 7 0 1 1145.09 916.04 35.80 o 8 0 1 1783.14 1856.95 48.09 o 9 0 1 1541.04 1425.27 58.79 o 10 0 1 793.32 850.70 49.87 o 11 0 1 500.61 423.86 19.47 o 12 0 1 116.80 125.07 47.24 o 13 0 1 64.73 55.49 29.44 o -13 1 1 3.22 24.35 12.42 o -11 1 1 296.39 355.64 21.76 o -10 1 1 649.51 627.01 18.00 o -9 1 1 58.26 53.02 5.44 o -8 1 1 697.30 661.33 20.33 o -7 1 1 1173.31 1199.66 29.08 o -6 1 1 1225.85 1285.31 27.39 o -5 1 1 845.80 1039.43 17.61 o -4 1 1 4186.76 3639.26 44.30 o -3 1 1 30421.09 30995.31 206.98 o -2 1 1 6176.77 7371.22 63.34 o -1 1 1 16005.23 11171.65 110.35 o 0 1 1 6766.84 4116.05 46.36 o 1 1 1 13620.58 11828.33 170.46 o 2 1 1 877.11 1411.44 23.82 o 3 1 1 3360.71 2427.07 53.06 o 4 1 1 7612.13 6919.92 84.41 o 5 1 1 881.06 767.75 13.02 o 6 1 1 2909.82 2807.70 48.96 o 7 1 1 466.13 542.36 16.33 o 8 1 1 449.47 458.09 14.08 o 9 1 1 117.82 141.45 15.80 o 10 1 1 37.19 38.39 6.69 o 11 1 1 442.24 481.51 23.28 o 12 1 1 347.00 215.12 59.02 o 13 1 1 11.74 30.43 18.81 o -13 2 1 62.09 109.94 43.45 o -12 2 1 31.48 37.67 16.37 o -11 2 1 501.45 546.14 22.01 o -10 2 1 361.87 307.37 8.68 o -9 2 1 100.91 88.28 9.80 o -8 2 1 159.98 174.96 7.75 o -7 2 1 802.72 894.57 24.98 o -6 2 1 1297.85 1367.47 29.65 o -5 2 1 703.09 674.98 16.12 o -4 2 1 1485.38 1533.89 27.09 o -3 2 1 20494.86 18827.55 155.97 o -2 2 1 2663.18 2465.43 42.15 o -1 2 1 3024.35 477.63 14.18 o 0 2 1 8010.02 9426.28 126.12 o 1 2 1 4695.59 3165.82 43.25 o 2 2 1 10486.83 10149.59 219.74 o 3 2 1 2538.64 2411.48 58.15 o 4 2 1 1089.08 1117.85 19.26 o 5 2 1 626.57 640.58 17.81 o 6 2 1 2107.55 2020.34 41.47 o 7 2 1 2306.28 2341.13 43.36 o 8 2 1 1260.17 1215.75 27.96 o 9 2 1 28.48 29.20 4.98 o 10 2 1 405.53 405.25 13.68 o 11 2 1 505.13 457.66 16.78 o 12 2 1 18.99 11.09 6.38 o 13 2 1 18.33 22.63 21.08 o 14 2 1 59.34 44.42 28.49 o -14 3 1 60.24 14.17 17.99 o -13 3 1 79.16 134.61 37.19 o -12 3 1 233.32 216.56 50.60 o -11 3 1 245.87 254.42 18.83 o -10 3 1 383.22 443.27 16.90 o -9 3 1 248.64 239.93 7.15 o -8 3 1 15.88 13.78 5.76 o -7 3 1 2346.99 2588.29 45.57 o -6 3 1 8265.16 8575.75 97.90 o -5 3 1 7094.51 7187.16 57.14 o -4 3 1 1529.78 1407.78 23.47 o -3 3 1 11500.72 10060.22 140.42 o -2 3 1 13902.02 12630.10 224.97 o -1 3 1 5471.14 5740.46 87.41 o 0 3 1 3897.58 2430.70 62.17 o 1 3 1 12722.29 9269.52 160.68 o 2 3 1 8796.57 9339.50 245.68 o 3 3 1 1254.85 1582.37 25.79 o 4 3 1 1452.58 1290.46 21.60 o 5 3 1 3266.64 2954.96 48.58 o 6 3 1 1715.34 1692.28 35.14 o 7 3 1 667.98 584.30 19.22 o 8 3 1 602.49 566.12 19.51 o 9 3 1 251.81 226.65 10.00 o 10 3 1 423.03 430.63 9.94 o 11 3 1 55.52 52.72 9.73 o 12 3 1 285.34 304.25 50.96 o 13 3 1 37.97 61.48 19.54 o 14 3 1 110.83 69.23 37.78 o -14 4 1 59.44 61.65 36.49 o -13 4 1 70.50 105.62 33.58 o -12 4 1 131.38 112.48 41.95 o -11 4 1 128.56 127.89 25.37 o -10 4 1 32.83 45.34 6.84 o -9 4 1 438.37 420.01 16.58 o -8 4 1 1269.99 1210.20 18.70 o -7 4 1 179.80 233.33 10.90 o -6 4 1 881.07 900.99 23.77 o -5 4 1 524.60 537.70 13.83 o -4 4 1 894.26 739.05 16.71 o -3 4 1 580.11 604.94 17.73 o -2 4 1 25768.00 26798.32 300.90 o -1 4 1 2610.27 2152.63 33.85 o 0 4 1 13975.08 15225.96 279.04 o 1 4 1 6493.71 6482.49 66.54 o 2 4 1 2431.86 2201.99 39.33 o 3 4 1 1623.56 1520.60 50.73 o 5 4 1 3261.40 3147.25 56.54 o 6 4 1 1256.77 1323.95 33.28 o 7 4 1 3034.72 3223.30 58.81 o 8 4 1 910.13 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