#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/26/2212638.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212638_Fobs loop_ _publ_author_name 'Ouellette, Wayne' 'Zubieta, Jon' _publ_section_title ; Aqua[2,6-bis(pyridin-2-yl)pyridin-4-ol]sulfatocopper(II) dihydrate ; _journal_coeditor_code LH2311 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m908 _journal_page_last m909 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.201 _cell_angle_gamma 90.000 _cell_length_a 13.2197 _cell_length_b 18.4067 _cell_length_c 6.9874 _exptl_crystal_F_000 948.00 _reflns_d_resolution_high 0.7101 _[local]_cod_data_source_file lh2311Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21_c in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 250.16 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 20703.50 20582.71 1373.44 o 3 0 0 4268.75 4848.17 58.03 o 4 0 0 8075.00 8588.05 97.00 o 5 0 0 2922.51 3001.05 57.35 o 6 0 0 19495.10 19894.99 284.29 o 7 0 0 18966.77 21590.85 232.57 o 8 0 0 4935.60 4732.96 70.07 o 9 0 0 53.48 67.09 13.52 o 10 0 0 1016.38 1038.92 33.12 o 11 0 0 11733.70 11804.23 185.24 o 12 0 0 4247.02 4019.16 133.56 o 13 0 0 721.11 847.10 46.11 o 14 0 0 3296.48 3192.92 87.10 o 15 0 0 95.69 112.21 29.41 o 16 0 0 1501.45 1534.78 63.61 o 17 0 0 672.22 630.41 82.01 o 18 0 0 188.37 219.55 28.11 o 1 1 0 12635.56 14515.40 176.61 o 2 1 0 130.12 163.63 6.15 o 3 1 0 1117.10 1132.91 15.04 o 4 1 0 4429.73 4847.08 42.95 o 5 1 0 42.88 85.55 7.05 o 6 1 0 4051.32 4512.77 44.28 o 7 1 0 1748.40 1778.44 25.54 o 8 1 0 12.62 41.26 8.73 o 9 1 0 1204.23 1105.11 22.66 o 10 1 0 502.72 475.66 17.02 o 11 1 0 215.77 201.27 15.92 o 12 1 0 100.32 93.40 13.41 o 13 1 0 1.49 0.51 13.78 o 14 1 0 60.76 61.25 16.17 o 15 1 0 811.13 779.50 34.42 o 16 1 0 0.26 12.80 13.42 o 17 1 0 453.04 481.47 30.34 o 18 1 0 203.16 245.48 25.97 o 0 2 0 7634.99 9031.44 191.18 o 1 2 0 1.50 14.47 2.59 o 2 2 0 2237.33 2487.19 25.33 o 3 2 0 36837.70 41574.90 407.74 o 4 2 0 55.35 65.47 7.28 o 5 2 0 1367.21 1277.22 18.44 o 6 2 0 2936.09 3019.04 33.17 o 7 2 0 247.23 299.45 11.33 o 8 2 0 2186.46 2077.31 29.12 o 9 2 0 1585.56 1566.52 26.48 o 10 2 0 114.73 134.95 11.17 o 11 2 0 790.44 688.64 23.91 o 12 2 0 0.39 23.08 10.92 o 13 2 0 1136.70 1088.05 34.47 o 14 2 0 1313.51 1330.39 46.24 o 15 2 0 110.14 129.55 18.11 o 16 2 0 293.98 313.56 24.74 o 17 2 0 368.02 371.80 32.03 o 18 2 0 5.87 26.99 29.20 o 1 3 0 1788.99 1752.60 19.73 o 2 3 0 112.47 75.19 5.39 o 3 3 0 76.17 113.20 9.53 o 4 3 0 739.33 696.39 15.23 o 5 3 0 6670.46 7099.81 98.44 o 6 3 0 972.80 868.86 20.67 o 7 3 0 2327.16 2239.79 28.31 o 8 3 0 730.36 722.06 16.98 o 9 3 0 2014.64 1954.54 25.56 o 10 3 0 352.32 363.90 18.65 o 11 3 0 377.25 337.38 21.11 o 12 3 0 624.36 642.03 24.62 o 13 3 0 4.22 4.69 11.29 o 14 3 0 1384.20 1314.94 39.63 o 15 3 0 576.32 554.99 35.29 o 16 3 0 109.27 145.48 22.64 o 17 3 0 46.18 70.65 18.84 o 18 3 0 132.34 100.78 28.88 o 0 4 0 42.30 79.44 7.14 o 1 4 0 224.59 276.05 7.88 o 2 4 0 205.57 193.71 7.14 o 3 4 0 2663.48 2845.01 45.77 o 4 4 0 335.10 362.20 11.90 o 5 4 0 73.65 95.18 8.25 o 6 4 0 3.04 -0.97 9.60 o 7 4 0 677.07 637.27 18.35 o 8 4 0 94.73 79.51 10.36 o 9 4 0 271.00 261.02 18.02 o 10 4 0 12.65 19.58 10.26 o 11 4 0 63.52 86.60 13.35 o 12 4 0 2.14 0.24 10.44 o 13 4 0 897.07 896.55 29.54 o 14 4 0 495.80 470.86 27.78 o 15 4 0 175.07 164.87 23.99 o 16 4 0 85.59 134.92 26.63 o 17 4 0 36.77 27.86 24.93 o 18 4 0 147.81 150.04 26.74 o 1 5 0 850.73 783.36 15.63 o 2 5 0 51.50 63.95 5.58 o 3 5 0 564.19 629.83 13.29 o 4 5 0 11.17 16.41 6.53 o 5 5 0 2318.64 2452.79 38.41 o 6 5 0 274.58 276.17 12.66 o 7 5 0 47.55 40.20 8.29 o 8 5 0 18.36 42.86 9.36 o 9 5 0 158.18 152.13 14.30 o 10 5 0 869.36 844.32 32.08 o 11 5 0 1001.49 976.73 28.52 o 12 5 0 936.57 962.12 36.82 o 13 5 0 16.52 9.23 11.74 o 14 5 0 99.45 103.74 18.09 o 15 5 0 299.13 315.10 29.94 o 16 5 0 20.86 45.86 18.87 o 17 5 0 1.70 -18.15 18.15 o 18 5 0 14.20 24.73 15.26 o 0 6 0 3893.80 3973.86 52.74 o 1 6 0 7604.62 8048.80 65.56 o 2 6 0 44.86 90.39 6.19 o 3 6 0 9421.92 9163.17 74.16 o 4 6 0 38.08 36.85 7.22 o 5 6 0 4679.91 4405.49 62.88 o 6 6 0 790.29 856.15 20.10 o 7 6 0 4.67 11.39 7.77 o 8 6 0 3036.16 2908.00 42.57 o 9 6 0 3692.19 3467.82 49.08 o 10 6 0 5918.65 5785.15 70.73 o 11 6 0 7861.30 7593.31 142.01 o 12 6 0 219.66 216.08 17.64 o 13 6 0 1372.55 1278.26 49.69 o 14 6 0 2567.06 2422.54 71.50 o 15 6 0 77.66 52.47 19.10 o 16 6 0 2114.77 2008.73 61.09 o 17 6 0 98.70 83.85 28.68 o 18 6 0 441.88 452.18 71.65 o 1 7 0 5563.08 5559.19 49.70 o 2 7 0 458.14 495.66 11.83 o 3 7 0 5312.99 6589.94 57.66 o 4 7 0 10047.06 11209.56 90.60 o 5 7 0 13056.08 13882.95 122.31 o 6 7 0 2187.43 2179.22 32.88 o 7 7 0 9245.06 9184.32 138.66 o 8 7 0 33.47 22.35 9.30 o 9 7 0 222.02 220.80 20.43 o 10 7 0 10075.84 10060.42 134.44 o 11 7 0 88.02 107.68 14.06 o 12 7 0 3131.62 2870.72 72.39 o 13 7 0 184.75 187.08 20.94 o 14 7 0 427.43 409.64 28.36 o 15 7 0 517.32 527.08 36.24 o 16 7 0 820.91 831.49 48.91 o 17 7 0 364.49 339.84 31.54 o 0 8 0 4687.83 4093.86 57.35 o 1 8 0 573.84 558.08 13.00 o 2 8 0 8035.93 9028.98 84.50 o 3 8 0 1266.28 1186.01 19.00 o 4 8 0 287.69 215.82 8.81 o 5 8 0 569.56 834.56 20.90 o 6 8 0 1400.93 1306.66 25.24 o 7 8 0 621.61 576.82 18.85 o 8 8 0 5826.78 5573.81 66.01 o 9 8 0 486.01 508.46 20.74 o 10 8 0 1472.27 1372.31 31.38 o 11 8 0 104.76 123.06 18.08 o 12 8 0 831.54 797.14 42.92 o 13 8 0 1545.31 1396.99 53.08 o 14 8 0 2407.43 2209.87 54.00 o 15 8 0 0.05 31.82 15.20 o 16 8 0 205.48 196.45 25.74 o 17 8 0 114.09 136.95 22.22 o 1 9 0 8728.82 8928.49 76.08 o 2 9 0 7467.15 7681.30 67.78 o 3 9 0 1774.59 1820.67 24.98 o 4 9 0 13230.80 13444.14 108.59 o 5 9 0 1554.37 1481.10 21.56 o 6 9 0 106.57 107.05 10.06 o 7 9 0 11761.07 11777.72 112.78 o 8 9 0 190.05 187.21 13.95 o 9 9 0 3648.16 3511.79 59.92 o 10 9 0 1168.30 1196.77 40.15 o 11 9 0 156.90 144.78 18.97 o 12 9 0 1525.57 1505.14 43.28 o 13 9 0 2073.01 2029.33 51.04 o 14 9 0 297.26 329.29 27.09 o 15 9 0 1378.82 1342.30 44.33 o 16 9 0 156.28 169.51 26.35 o 17 9 0 346.03 334.22 31.34 o 0 10 0 443.82 479.38 19.56 o 1 10 0 1443.49 1775.70 25.95 o 2 10 0 3195.86 3543.01 39.43 o 3 10 0 14.96 15.20 8.15 o 4 10 0 971.59 1008.63 19.21 o 5 10 0 1372.41 1342.17 28.43 o 6 10 0 94.75 69.15 9.16 o 7 10 0 150.47 177.34 12.41 o 8 10 0 372.10 340.10 21.92 o 9 10 0 118.98 155.68 17.80 o 10 10 0 846.82 738.12 30.45 o 11 10 0 174.02 178.88 20.20 o 12 10 0 129.30 123.22 19.11 o 13 10 0 16.19 12.70 15.04 o 14 10 0 161.20 195.19 22.54 o 15 10 0 97.76 104.44 19.83 o 16 10 0 137.82 168.88 20.82 o 17 10 0 20.76 55.90 17.13 o 1 11 0 1312.83 1226.93 23.13 o 2 11 0 1035.45 1081.64 20.58 o 3 11 0 487.90 468.37 19.17 o 4 11 0 3941.37 4012.41 48.64 o 5 11 0 535.68 547.69 16.90 o 6 11 0 79.17 89.75 11.33 o 7 11 0 3146.27 2918.12 98.73 o 8 11 0 2316.41 2435.43 88.54 o 9 11 0 14.56 37.32 13.88 o 10 11 0 383.51 405.86 25.83 o 11 11 0 1.36 -9.48 13.71 o 12 11 0 1043.72 1028.79 39.05 o 13 11 0 162.38 205.26 23.27 o 14 11 0 119.39 146.77 21.43 o 15 11 0 1837.98 1670.84 56.24 o 16 11 0 33.35 56.05 19.45 o 0 12 0 3998.04 3918.19 62.80 o 1 12 0 897.02 847.48 19.31 o 2 12 0 3319.92 3149.99 45.80 o 3 12 0 1558.10 1556.04 25.48 o 4 12 0 111.71 92.60 11.41 o 5 12 0 1100.35 1064.66 22.95 o 6 12 0 194.54 177.12 17.02 o 7 12 0 106.74 163.17 17.83 o 8 12 0 615.73 593.98 36.59 o 9 12 0 3.50 12.68 13.06 o 10 12 0 231.38 174.54 19.98 o 11 12 0 943.20 943.09 36.83 o 12 12 0 20.03 31.14 15.04 o 13 12 0 215.62 283.78 27.06 o 14 12 0 269.77 280.54 25.72 o 15 12 0 5.42 37.06 15.56 o 16 12 0 276.10 327.47 27.49 o 1 13 0 111.92 109.45 10.05 o 2 13 0 411.53 446.92 15.61 o 3 13 0 2883.92 2880.51 37.71 o 4 13 0 5206.48 5037.16 54.25 o 5 13 0 7.36 -3.64 13.40 o 6 13 0 1909.04 1699.26 59.45 o 7 13 0 1230.16 1216.11 39.36 o 8 13 0 359.25 411.11 25.08 o 9 13 0 503.30 532.14 28.64 o 10 13 0 270.54 324.61 25.13 o 11 13 0 619.46 561.79 31.40 o 12 13 0 39.66 29.51 16.19 o 13 13 0 204.57 229.41 34.76 o 14 13 0 12.86 19.47 15.75 o 15 13 0 439.58 469.62 31.88 o 16 13 0 278.17 363.26 27.78 o 0 14 0 1014.16 1008.06 31.66 o 1 14 0 3034.89 2908.77 38.93 o 2 14 0 109.41 99.37 10.22 o 3 14 0 831.46 846.05 19.82 o 4 14 0 429.53 430.53 26.55 o 5 14 0 46.30 49.19 13.78 o 6 14 0 494.95 406.42 23.81 o 7 14 0 0.41 10.08 12.76 o 8 14 0 1290.32 1209.69 37.47 o 9 14 0 58.51 48.25 16.06 o 10 14 0 207.67 202.21 22.45 o 11 14 0 93.82 72.79 18.23 o 12 14 0 31.19 62.24 17.34 o 13 14 0 11.21 -0.25 15.65 o 14 14 0 229.95 337.48 27.41 o 15 14 0 126.02 137.67 20.15 o 1 15 0 1080.92 1160.13 29.85 o 2 15 0 8049.05 7890.42 84.25 o 3 15 0 1056.87 1049.35 27.89 o 4 15 0 4985.51 4694.35 147.72 o 5 15 0 4.68 13.55 12.68 o 6 15 0 3047.27 3076.80 57.75 o 7 15 0 3821.40 3797.82 66.25 o 8 15 0 499.79 450.01 27.52 o 9 15 0 4147.59 3840.57 81.22 o 10 15 0 2600.86 2463.92 57.97 o 11 15 0 10.68 -9.47 14.16 o 12 15 0 2158.29 2161.59 64.44 o 13 15 0 651.55 708.90 37.31 o 14 15 0 407.53 363.16 29.08 o 15 15 0 410.40 403.25 29.78 o 0 16 0 244.47 242.23 20.47 o 1 16 0 303.37 313.24 15.61 o 2 16 0 4.25 14.97 10.75 o 3 16 0 4967.32 4996.69 128.89 o 4 16 0 836.49 666.65 32.57 o 5 16 0 296.23 335.02 26.65 o 6 16 0 2.68 -7.01 12.59 o 7 16 0 116.08 87.18 17.60 o 8 16 0 1149.54 1102.21 37.81 o 9 16 0 1383.27 1256.36 48.34 o 10 16 0 220.96 181.86 22.13 o 11 16 0 696.99 772.04 37.52 o 12 16 0 87.37 139.45 21.18 o 13 16 0 312.88 343.16 35.57 o 14 16 0 168.50 196.81 22.94 o 1 17 0 4724.60 4537.53 62.30 o 2 17 0 837.27 823.59 26.34 o 3 17 0 2454.61 2318.33 55.15 o 4 17 0 2513.04 2465.60 77.78 o 5 17 0 268.63 272.81 21.68 o 6 17 0 1811.07 1630.72 44.59 o 7 17 0 1385.15 1382.87 44.76 o 8 17 0 15.32 34.72 16.15 o 9 17 0 1119.60 1107.84 39.21 o 10 17 0 243.97 247.74 24.31 o 11 17 0 26.40 8.30 19.88 o 12 17 0 617.52 526.17 33.89 o 13 17 0 659.14 704.38 43.90 o 14 17 0 210.41 273.81 30.92 o 0 18 0 940.24 1016.60 48.13 o 1 18 0 165.77 207.39 16.83 o 2 18 0 1066.10 1076.97 29.68 o 3 18 0 2643.21 2531.02 61.10 o 4 18 0 98.16 118.78 18.92 o 5 18 0 2464.15 2342.90 61.45 o 6 18 0 647.53 604.17 30.89 o 7 18 0 215.88 258.64 23.37 o 8 18 0 2696.06 2726.94 60.11 o 9 18 0 565.56 607.75 33.46 o 10 18 0 256.30 273.64 25.66 o 11 18 0 633.19 670.08 37.09 o 12 18 0 14.45 19.88 21.87 o 13 18 0 287.21 293.99 26.53 o 1 19 0 10.75 18.79 13.96 o 2 19 0 151.13 143.09 17.79 o 3 19 0 267.73 228.99 29.46 o 4 19 0 25.86 20.23 16.95 o 5 19 0 4.36 6.96 13.01 o 6 19 0 17.01 21.87 14.59 o 7 19 0 78.56 81.50 17.27 o 8 19 0 2.28 3.65 14.28 o 9 19 0 25.52 17.51 15.28 o 10 19 0 10.19 31.33 24.80 o 11 19 0 6.79 1.65 15.78 o 12 19 0 29.08 47.52 16.10 o 0 20 0 322.36 376.90 37.24 o 1 20 0 36.57 34.20 15.22 o 2 20 0 9.62 21.84 17.03 o 3 20 0 28.18 25.24 13.36 o 4 20 0 0.24 -5.96 13.08 o 5 20 0 205.41 212.50 21.65 o 6 20 0 59.43 70.95 16.96 o 7 20 0 13.21 15.87 19.63 o 8 20 0 157.70 171.59 21.20 o 9 20 0 114.65 143.32 30.11 o 10 20 0 58.19 72.92 17.38 o 11 20 0 163.99 208.63 24.06 o 1 21 0 914.49 963.99 41.71 o 2 21 0 663.40 714.48 39.70 o 3 21 0 321.62 352.68 30.56 o 4 21 0 563.98 551.58 30.10 o 5 21 0 116.10 170.43 20.45 o 6 21 0 264.80 297.50 25.04 o 7 21 0 527.12 552.15 32.63 o 8 21 0 113.66 165.64 20.67 o 9 21 0 274.00 304.09 26.69 o 10 21 0 183.00 163.15 20.34 o 0 22 0 605.55 598.45 48.21 o 1 22 0 322.70 392.73 31.83 o 2 22 0 1290.89 1284.36 56.41 o 3 22 0 740.31 739.98 41.61 o 4 22 0 42.49 51.09 19.32 o 5 22 0 399.43 457.34 29.25 o 6 22 0 900.42 1056.02 53.02 o 7 22 0 0.30 -1.64 19.28 o 8 22 0 1102.04 1171.40 42.63 o 9 22 0 331.35 332.21 26.75 o 1 23 0 106.52 98.11 36.05 o 2 23 0 5.50 31.50 19.61 o 3 23 0 22.68 56.65 19.01 o 4 23 0 1097.75 1067.24 66.48 o 5 23 0 674.66 704.83 42.85 o 6 23 0 391.53 495.96 37.13 o 7 23 0 13.07 40.73 14.28 o 8 23 0 273.70 296.88 25.55 o 0 24 0 631.65 645.27 65.28 o 1 24 0 333.82 358.23 35.91 o 2 24 0 576.59 523.22 36.52 o 3 24 0 1856.97 1952.77 61.04 o 4 24 0 332.99 353.78 31.94 o 5 24 0 2033.71 2002.62 66.98 o 6 24 0 1359.11 1252.48 53.15 o 7 24 0 58.15 68.95 25.40 o 1 25 0 24.50 73.44 21.65 o 2 25 0 73.13 94.95 20.24 o 3 25 0 0.51 55.33 19.37 o 4 25 0 16.59 65.04 25.15 o -18 1 1 500.68 495.86 45.73 o -17 1 1 17.22 8.88 15.12 o -16 1 1 1917.25 1849.92 57.23 o -15 1 1 133.46 118.64 17.73 o -14 1 1 701.52 704.00 32.27 o -13 1 1 1191.99 1172.77 44.48 o -12 1 1 214.28 208.90 24.01 o -11 1 1 4424.15 4350.62 126.74 o -10 1 1 1956.95 1841.86 31.44 o -9 1 1 731.79 636.97 18.87 o -8 1 1 6571.87 6735.72 65.37 o -7 1 1 51.98 51.04 7.41 o -6 1 1 2309.65 2256.89 28.03 o -5 1 1 3477.47 3208.44 33.22 o -4 1 1 483.47 477.66 9.89 o -3 1 1 614.37 784.58 11.47 o -2 1 1 13743.82 15910.55 115.15 o -1 1 1 81.29 112.47 3.94 o 0 1 1 12876.65 14105.49 265.95 o 1 1 1 5810.51 6689.48 56.38 o 2 1 1 979.27 1270.51 14.39 o 3 1 1 15937.93 18057.09 131.57 o 4 1 1 6168.21 6659.17 55.42 o 5 1 1 4377.07 4416.13 41.65 o 6 1 1 11478.79 12067.00 96.82 o 7 1 1 119.08 96.03 8.20 o 8 1 1 1256.68 1216.02 22.07 o 9 1 1 3935.61 4018.75 46.02 o 10 1 1 679.76 688.37 19.36 o 11 1 1 110.78 137.87 14.64 o 12 1 1 91.55 93.73 14.30 o 13 1 1 173.79 182.80 19.14 o 14 1 1 1050.69 984.18 35.22 o 15 1 1 173.61 162.32 19.93 o 16 1 1 404.70 411.84 28.39 o 17 1 1 501.89 514.52 31.23 o 18 1 1 23.63 92.09 21.41 o -18 2 1 503.83 544.67 43.21 o -17 2 1 395.48 401.67 36.12 o -16 2 1 282.64 300.89 29.09 o -15 2 1 1921.65 1898.12 51.52 o -14 2 1 105.41 134.22 18.24 o -13 2 1 1626.85 1563.45 41.10 o -12 2 1 145.31 167.74 16.12 o -11 2 1 391.71 382.26 20.19 o -10 2 1 5693.09 5725.00 87.21 o -9 2 1 1496.03 1418.74 28.72 o -8 2 1 130.91 215.65 11.72 o -7 2 1 2643.32 2490.77 31.70 o -6 2 1 2466.14 2442.97 29.31 o -5 2 1 176.81 155.89 8.33 o -4 2 1 7530.52 7626.90 57.48 o -3 2 1 5942.83 6724.56 54.15 o -2 2 1 11993.69 13871.85 123.92 o -1 2 1 14712.77 16631.15 119.76 o 0 2 1 3304.15 4018.54 32.44 o 1 2 1 7540.63 8621.74 71.97 o 2 2 1 2414.23 2362.43 22.54 o 3 2 1 9467.58 10360.51 79.39 o 4 2 1 1153.80 998.42 15.26 o 5 2 1 297.65 291.41 9.49 o 6 2 1 1581.27 1662.25 25.00 o 7 2 1 3939.46 3666.76 40.36 o 8 2 1 43.03 44.47 7.56 o 9 2 1 8993.58 8882.21 81.09 o 10 2 1 1859.22 1740.49 29.09 o 11 2 1 2.44 8.02 10.14 o 12 2 1 1947.68 1787.72 36.90 o 13 2 1 843.33 810.27 31.29 o 14 2 1 2824.13 2571.93 54.74 o 15 2 1 1535.99 1536.61 45.57 o 16 2 1 247.26 270.91 23.96 o 17 2 1 853.95 867.17 38.58 o 18 2 1 809.21 874.60 45.24 o -18 3 1 8.95 -8.95 29.45 o -17 3 1 36.79 80.39 20.11 o -16 3 1 42.72 59.89 18.81 o -15 3 1 0.07 11.71 16.37 o -14 3 1 70.30 61.85 14.05 o -13 3 1 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