#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:26:43 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181046 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/26/2212676.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212676_Fobs loop_ _publ_author_name 'Yan, Chao-Guo' 'Liu, Li' 'Han, Jun' _publ_section_title ; (1-Ferrocenylbutane-1,3-dionato)[tris(2-aminoethyl)amine]cobalt(II) chloride tetraphenylborate acetone solvate ; _journal_coeditor_code SF2006 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m683 _journal_page_last m684 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.463 _cell_angle_gamma 90.000 _cell_length_a 15.0945 _cell_length_b 12.0255 _cell_length_c 25.4724 _exptl_crystal_F_000 1864.00 _reflns_d_resolution_high 0.8107 _cod_data_source_file sf2006Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Z060324WUTX_0m in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 395.54 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 53041.87 54196.10 683.30 o 4 0 0 889.05 1127.74 34.41 o 6 0 0 19248.67 19037.00 277.92 o 8 0 0 19492.80 19738.51 236.96 o 10 0 0 142.36 111.28 24.35 o 12 0 0 1.08 -14.13 30.06 o 14 0 0 1368.90 1427.92 125.81 o 16 0 0 269.57 349.61 86.13 o 18 0 0 1.05 -38.03 58.47 o 1 1 0 29870.51 29030.21 211.69 o 2 1 0 40479.53 42873.93 334.67 o 3 1 0 5017.80 4814.24 49.06 o 4 1 0 24128.08 24938.15 176.27 o 5 1 0 13521.08 13685.99 114.61 o 6 1 0 4583.04 4237.79 62.34 o 7 1 0 829.05 836.75 27.58 o 8 1 0 2770.12 2966.79 52.46 o 9 1 0 1082.60 950.76 32.42 o 10 1 0 1574.51 1606.06 51.87 o 11 1 0 360.43 257.82 62.45 o 12 1 0 495.75 534.89 56.26 o 13 1 0 0.63 -3.16 27.77 o 14 1 0 117.52 102.55 38.53 o 15 1 0 199.01 214.43 49.77 o 16 1 0 551.71 499.53 90.33 o 17 1 0 37.46 11.17 41.61 o 18 1 0 112.97 112.56 53.66 o 0 2 0 23326.40 23593.96 224.67 o 1 2 0 23223.73 23057.53 336.24 o 2 2 0 17879.95 19070.41 156.30 o 3 2 0 101.61 37.77 9.59 o 4 2 0 785.35 782.05 24.32 o 5 2 0 4373.05 4244.73 49.24 o 6 2 0 3008.11 2954.31 42.33 o 7 2 0 326.91 364.23 17.55 o 8 2 0 599.22 572.00 26.58 o 9 2 0 2939.53 3050.69 50.44 o 10 2 0 236.64 186.70 17.58 o 11 2 0 1335.36 1367.35 75.95 o 12 2 0 1373.75 1343.31 114.91 o 13 2 0 788.85 883.96 72.42 o 14 2 0 493.53 582.00 99.05 o 15 2 0 4.42 20.13 35.01 o 16 2 0 134.56 63.95 43.50 o 17 2 0 109.21 69.00 47.40 o 18 2 0 159.53 17.33 50.48 o 1 3 0 51690.64 53175.21 338.01 o 2 3 0 5709.20 5881.40 72.51 o 3 3 0 614.58 576.11 22.06 o 4 3 0 458.00 442.81 21.60 o 5 3 0 305.07 192.81 16.53 o 6 3 0 108.94 113.46 14.70 o 7 3 0 14528.18 14705.77 140.87 o 8 3 0 5217.42 5485.49 79.59 o 9 3 0 350.60 353.19 23.90 o 10 3 0 220.61 238.15 24.32 o 11 3 0 177.23 170.31 39.26 o 12 3 0 1044.98 1203.73 115.59 o 13 3 0 1441.12 1651.73 93.11 o 14 3 0 350.78 440.74 61.09 o 15 3 0 427.75 348.84 80.87 o 16 3 0 603.53 615.15 78.51 o 17 3 0 3.41 -48.86 35.50 o 18 3 0 66.61 45.93 50.90 o 0 4 0 26934.95 28719.28 232.73 o 1 4 0 2373.94 2476.36 35.72 o 2 4 0 4009.89 3955.65 63.24 o 3 4 0 82.13 43.87 16.94 o 4 4 0 30.37 50.11 13.30 o 5 4 0 21.06 32.83 10.21 o 6 4 0 1067.67 1184.53 39.16 o 7 4 0 1556.59 1364.47 70.60 o 8 4 0 1754.06 1832.65 46.91 o 9 4 0 126.11 110.96 20.43 o 10 4 0 656.99 747.97 35.74 o 11 4 0 60.62 16.65 26.44 o 12 4 0 214.58 277.19 46.95 o 13 4 0 60.10 15.61 29.59 o 14 4 0 99.74 143.76 66.36 o 15 4 0 189.97 275.59 56.75 o 16 4 0 23.27 -3.92 39.87 o 17 4 0 424.51 367.69 71.33 o 1 5 0 14981.22 14819.49 124.87 o 2 5 0 7989.81 8166.66 106.47 o 3 5 0 381.54 454.79 25.77 o 4 5 0 4488.50 4178.90 74.13 o 5 5 0 1319.33 1189.90 40.58 o 6 5 0 11.07 26.03 11.82 o 7 5 0 312.11 357.56 29.86 o 8 5 0 1160.51 1177.29 44.55 o 9 5 0 77.46 81.10 16.44 o 10 5 0 931.89 1006.84 41.79 o 11 5 0 2300.94 2176.17 72.36 o 12 5 0 420.55 413.37 54.32 o 13 5 0 272.32 250.64 48.19 o 14 5 0 11.31 20.74 32.34 o 15 5 0 108.19 112.06 59.67 o 16 5 0 42.53 -3.56 37.12 o 17 5 0 100.71 71.57 49.62 o 0 6 0 457.38 485.86 22.61 o 1 6 0 9770.54 10550.62 102.92 o 2 6 0 4274.07 4005.21 160.41 o 3 6 0 2031.55 2221.60 56.20 o 4 6 0 98.73 119.66 17.87 o 5 6 0 2071.88 1984.20 55.22 o 6 6 0 18.02 35.16 17.50 o 7 6 0 621.14 552.51 34.42 o 8 6 0 1004.21 911.00 43.73 o 9 6 0 1883.96 1776.58 86.46 o 10 6 0 438.85 467.30 33.00 o 11 6 0 67.42 37.64 21.20 o 12 6 0 22.08 -21.50 37.35 o 13 6 0 7.40 36.84 33.36 o 14 6 0 0.25 6.22 33.08 o 15 6 0 274.76 267.88 57.83 o 16 6 0 129.00 197.89 57.25 o 1 7 0 10473.83 10819.42 96.08 o 2 7 0 5656.89 5647.54 98.70 o 3 7 0 2788.07 3002.23 70.45 o 4 7 0 4164.93 4338.17 87.56 o 5 7 0 9.42 10.04 19.87 o 6 7 0 1679.90 1570.50 54.25 o 7 7 0 5256.14 4997.13 112.06 o 8 7 0 239.61 241.57 28.65 o 9 7 0 270.15 235.72 30.16 o 10 7 0 2.01 30.78 20.37 o 11 7 0 5.45 -5.80 20.95 o 12 7 0 268.31 340.23 56.12 o 13 7 0 325.66 413.38 82.22 o 14 7 0 43.19 88.62 44.37 o 15 7 0 99.53 166.33 58.10 o 16 7 0 17.86 -3.12 45.29 o 0 8 0 976.86 1056.68 56.76 o 1 8 0 2556.35 2503.65 68.17 o 2 8 0 2495.10 2348.73 66.31 o 3 8 0 12324.90 12387.41 166.72 o 4 8 0 44.05 17.38 14.01 o 5 8 0 5118.55 4950.02 100.63 o 6 8 0 9.02 13.51 19.21 o 7 8 0 53.16 46.88 18.32 o 8 8 0 347.52 294.57 33.80 o 9 8 0 665.52 716.08 46.86 o 10 8 0 34.82 34.37 21.98 o 11 8 0 942.47 1037.94 61.95 o 12 8 0 43.07 39.40 35.75 o 13 8 0 25.13 -5.96 36.02 o 14 8 0 8.60 51.26 44.10 o 15 8 0 2.01 -42.49 40.64 o 1 9 0 703.40 738.64 78.23 o 2 9 0 1591.09 1497.10 57.34 o 3 9 0 18.47 56.31 18.94 o 4 9 0 535.03 554.94 40.95 o 5 9 0 671.89 658.88 43.01 o 6 9 0 483.80 449.17 37.99 o 7 9 0 41.89 22.70 18.83 o 8 9 0 738.55 775.27 49.49 o 9 9 0 810.74 871.58 53.79 o 10 9 0 323.90 318.88 41.22 o 11 9 0 348.09 265.23 50.29 o 12 9 0 75.92 81.06 84.10 o 13 9 0 84.03 85.17 46.87 o 14 9 0 0.99 -11.43 42.16 o 0 10 0 3161.37 3062.81 150.76 o 1 10 0 399.02 446.48 39.60 o 2 10 0 855.06 811.88 49.65 o 3 10 0 247.56 231.42 31.17 o 4 10 0 150.12 175.78 29.65 o 5 10 0 524.77 453.79 42.19 o 6 10 0 996.17 1109.71 61.43 o 7 10 0 241.37 230.85 42.73 o 8 10 0 369.21 399.20 42.06 o 9 10 0 101.68 114.34 28.70 o 10 10 0 493.02 476.17 60.09 o 11 10 0 21.24 11.47 34.45 o 12 10 0 38.74 72.00 55.91 o 13 10 0 5.07 -11.27 50.05 o 1 11 0 157.82 71.75 31.45 o 2 11 0 467.20 422.02 71.50 o 3 11 0 1.56 -7.12 22.17 o 4 11 0 2394.02 2493.82 105.98 o 5 11 0 5.43 -11.30 20.83 o 6 11 0 27.87 18.09 21.80 o 7 11 0 27.69 30.96 24.25 o 8 11 0 9.45 -11.11 27.36 o 9 11 0 369.26 382.27 54.94 o 10 11 0 489.84 550.73 64.39 o 11 11 0 68.48 -36.07 46.29 o 12 11 0 18.82 74.55 67.79 o 0 12 0 263.26 280.17 66.59 o 1 12 0 6.51 -12.03 26.08 o 2 12 0 244.57 280.32 39.66 o 3 12 0 0.79 3.42 24.00 o 4 12 0 264.54 195.02 45.28 o 5 12 0 50.09 49.41 34.21 o 6 12 0 13.54 13.00 46.07 o 7 12 0 0.18 26.87 31.46 o 8 12 0 43.87 11.04 32.58 o 9 12 0 97.29 76.38 39.86 o 10 12 0 0.38 27.21 53.21 o 1 13 0 95.60 63.64 34.49 o 2 13 0 136.71 62.56 38.74 o 3 13 0 1.77 -36.19 24.12 o 4 13 0 130.00 144.50 41.27 o 5 13 0 2.64 10.30 27.09 o 6 13 0 1.19 4.59 31.42 o 7 13 0 9.76 -41.43 32.39 o 8 13 0 252.03 160.79 73.35 o 0 14 0 405.98 293.55 82.52 o 1 14 0 20.65 -45.08 33.63 o 2 14 0 36.00 16.09 34.08 o 3 14 0 68.58 16.49 35.37 o 4 14 0 0.25 -40.90 29.59 o 5 14 0 83.23 72.31 50.13 o 6 14 0 177.25 247.68 62.38 o -17 0 1 243.95 257.78 87.33 o -15 0 1 636.59 482.34 93.64 o -13 0 1 153.70 146.40 58.92 o -11 0 1 718.84 774.53 82.52 o -9 0 1 77.88 59.09 17.22 o -7 0 1 284.05 238.84 35.47 o -5 0 1 26993.33 26346.56 261.78 o -3 0 1 245.84 530.58 35.25 o 3 0 1 101294.94 102386.56 889.10 o 5 0 1 10723.67 11252.40 142.88 o 7 0 1 1126.72 1016.41 61.02 o 9 0 1 9342.42 9206.08 168.12 o 11 0 1 3114.92 3093.69 90.09 o 13 0 1 12.96 45.39 41.94 o 15 0 1 128.64 93.19 62.83 o 17 0 1 590.29 544.41 107.77 o -18 1 1 9.52 -29.53 59.15 o -17 1 1 88.39 58.17 47.23 o -16 1 1 2.11 -3.57 43.59 o -15 1 1 184.16 180.37 50.73 o -14 1 1 69.50 52.26 33.15 o -13 1 1 155.28 100.57 36.79 o -12 1 1 707.79 745.78 62.43 o -11 1 1 406.13 384.43 66.29 o -10 1 1 17.65 16.40 11.32 o -9 1 1 1068.92 1017.06 43.65 o -8 1 1 1114.61 951.97 29.31 o -7 1 1 15456.38 15787.97 135.37 o -6 1 1 4577.00 5174.04 61.25 o -5 1 1 7556.19 7752.96 74.99 o -4 1 1 11431.49 12230.02 86.09 o -3 1 1 14210.22 14486.29 94.02 o -2 1 1 298.31 383.15 15.78 o -1 1 1 13875.65 13823.19 108.91 o 0 1 1 6400.72 6343.31 168.42 o 1 1 1 91153.52 84786.37 519.60 o 2 1 1 21264.37 20828.57 162.72 o 3 1 1 3074.05 2660.95 40.38 o 4 1 1 5889.00 5590.06 83.35 o 5 1 1 2525.69 2727.86 43.41 o 6 1 1 199.85 253.56 16.47 o 7 1 1 17096.08 16984.25 149.07 o 8 1 1 3.78 2.42 9.83 o 9 1 1 707.80 603.74 28.62 o 10 1 1 6411.84 6344.90 89.90 o 11 1 1 3513.72 3464.35 81.74 o 12 1 1 498.97 539.96 57.38 o 13 1 1 1369.88 1377.11 85.38 o 14 1 1 32.14 -2.45 28.94 o 15 1 1 155.14 119.09 42.37 o 16 1 1 16.07 -49.91 37.89 o 17 1 1 41.13 26.80 44.26 o 18 1 1 180.86 110.81 100.41 o -18 2 1 0.03 -10.77 46.71 o -17 2 1 530.78 440.35 74.07 o -16 2 1 7.32 41.05 40.69 o -15 2 1 263.56 320.27 58.87 o -14 2 1 18.91 36.24 34.04 o -13 2 1 69.07 70.90 35.42 o -12 2 1 7.12 5.69 24.78 o -11 2 1 2803.07 2356.95 94.79 o -10 2 1 148.38 155.20 15.26 o -9 2 1 7175.24 6778.66 75.65 o -8 2 1 91.18 57.66 12.03 o -7 2 1 45.66 30.34 9.94 o -6 2 1 3434.34 3485.64 59.04 o -5 2 1 353.19 327.04 21.15 o -4 2 1 118.03 95.48 10.49 o -3 2 1 2871.50 2879.41 42.81 o -2 2 1 11557.99 12661.58 112.36 o -1 2 1 20381.08 20252.26 162.20 o 0 2 1 15447.53 16762.75 169.29 o 1 2 1 16599.20 17587.08 122.68 o 2 2 1 3121.76 4105.39 52.47 o 3 2 1 997.52 1008.94 53.43 o 4 2 1 7864.10 7165.53 84.28 o 5 2 1 808.01 776.44 23.33 o 6 2 1 8513.32 8329.50 80.36 o 7 2 1 362.63 382.66 20.37 o 8 2 1 4956.22 4835.08 63.79 o 9 2 1 465.61 494.15 29.14 o 10 2 1 296.51 293.29 23.99 o 11 2 1 1090.31 1162.63 50.63 o 12 2 1 1579.29 1514.57 82.77 o 13 2 1 346.31 298.84 49.38 o 14 2 1 361.09 437.53 60.30 o 15 2 1 99.54 99.72 42.01 o 16 2 1 312.39 438.33 68.65 o 17 2 1 409.56 557.46 77.83 o 18 2 1 1.29 28.62 47.77 o -18 3 1 44.53 19.77 48.98 o -17 3 1 154.65 111.88 53.50 o -16 3 1 100.96 128.60 56.52 o -15 3 1 324.09 450.48 64.51 o -14 3 1 426.87 459.29 62.72 o -13 3 1 1844.54 1974.84 98.74 o -12 3 1 72.36 44.71 30.16 o -11 3 1 2131.85 2124.71 106.27 o -10 3 1 2.54 25.63 13.06 o -9 3 1 589.20 562.84 37.08 o -8 3 1 2700.16 2909.32 55.08 o -7 3 1 1349.13 1400.59 37.51 o -6 3 1 12.63 25.01 8.18 o -5 3 1 6068.91 6023.08 80.99 o -4 3 1 4990.30 4889.45 76.02 o -3 3 1 630.52 771.73 48.90 o -2 3 1 28553.66 27840.29 258.74 o -1 3 1 1274.16 1228.42 29.91 o 0 3 1 6586.01 7191.83 109.37 o 1 3 1 7728.79 8067.25 71.80 o 2 3 1 3331.51 3127.18 49.56 o 3 3 1 655.19 558.58 22.33 o 4 3 1 5.50 7.44 7.49 o 5 3 1 6359.63 6083.74 135.50 o 6 3 1 123.94 274.19 20.79 o 7 3 1 533.52 600.65 25.33 o 8 3 1 2956.63 2919.19 50.36 o 9 3 1 35.58 62.53 12.91 o 10 3 1 2250.38 2262.08 48.68 o 11 3 1 479.34 542.95 38.77 o 12 3 1 740.85 831.49 67.91 o 13 3 1 227.50 187.10 43.49 o 14 3 1 297.54 262.34 56.97 o 15 3 1 0.16 0.73 33.79 o 16 3 1 351.27 385.80 66.31 o 17 3 1 24.75 68.90 51.65 o -17 4 1 79.63 62.07 68.84 o -16 4 1 1.56 35.96 36.95 o -15 4 1 989.07 1015.63 87.89 o -14 4 1 749.53 867.52 77.97 o -13 4 1 23.93 22.89 30.84 o -12 4 1 2930.85 3233.24 179.32 o -11 4 1 257.45 166.34 37.10 o -10 4 1 934.66 920.72 37.62 o -9 4 1 4432.19 4666.74 77.77 o -8 4 1 155.96 113.71 15.95 o -7 4 1 2253.70 2150.17 52.60 o -6 4 1 5434.78 5223.96 99.83 o -5 4 1 204.69 266.49 20.26 o -4 4 1 3695.62 3658.93 80.32 o -3 4 1 5.49 -1.32 12.60 o -2 4 1 2330.29 2450.23 49.69 o -1 4 1 24337.97 25241.77 218.78 o 0 4 1 5638.50 5846.45 57.50 o 1 4 1 29573.58 31570.84 219.70 o 2 4 1 13422.54 14815.09 121.31 o 3 4 1 496.15 448.51 22.73 o 4 4 1 1033.03 1114.68 35.02 o 5 4 1 120.53 105.54 21.46 o 6 4 1 911.88 852.55 76.42 o 7 4 1 327.66 426.42 27.41 o 8 4 1 267.79 341.61 27.27 o 9 4 1 680.95 729.52 34.06 o 10 4 1 27.84 43.78 16.92 o 11 4 1 178.38 259.79 39.21 o 12 4 1 444.89 445.26 60.12 o 13 4 1 0.64 -11.50 35.62 o 14 4 1 33.64 8.16 39.00 o 15 4 1 215.69 83.60 44.20 o 16 4 1 13.48 -41.57 62.90 o 17 4 1 0.71 -49.48 39.80 o -17 5 1 26.90 13.02 52.31 o -16 5 1 447.88 582.65 77.86 o -15 5 1 126.07 164.52 48.13 o -14 5 1 546.45 680.79 74.47 o -13 5 1 44.93 50.15 34.06 o -12 5 1 237.21 228.97 66.89 o -11 5 1 50.13 29.55 35.10 o -10 5 1 4510.31 4593.66 83.50 o -9 5 1 45.73 23.49 12.75 o -8 5 1 2682.17 2615.43 64.40 o -7 5 1 438.13 515.87 47.30 o -6 5 1 7561.47 7681.80 110.84 o -5 5 1 411.98 404.03 26.07 o -4 5 1 1585.79 1536.11 66.36 o -3 5 1 433.77 510.29 26.99 o -2 5 1 341.43 322.15 22.18 o -1 5 1 436.36 542.24 24.19 o 0 5 1 14609.91 15315.29 161.89 o 1 5 1 2387.59 2549.07 46.99 o 2 5 1 200.20 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