#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/27/2212782.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212782_Fobs loop_ _publ_author_name 'Grigoriev, Mikhail S.' 'Krot, Nikolai N.' _publ_section_title ; Tricaesium dihydroxotetraoxoplutonate(VII) trihydrate ; _journal_coeditor_code BR2033 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i108 _journal_page_last i110 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.391 _cell_angle_gamma 90.000 _cell_length_a 12.5381 _cell_length_b 11.4983 _cell_length_c 8.0195 _exptl_crystal_F_000 1356.00 _reflns_d_resolution_high 0.5026 _[local]_cod_data_source_file br2033Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' PP in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 768.61 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 347129.53 367969.19 10223.37 o 6 0 0 2198.63 2437.49 137.78 o 8 0 0 5522.07 5771.69 119.54 o 10 0 0 15572.14 15883.43 227.31 o 12 0 0 18667.50 18931.96 398.58 o 14 0 0 1834.05 1866.85 97.37 o 16 0 0 39664.16 40195.87 685.75 o 18 0 0 17930.63 17813.64 454.87 o 20 0 0 17317.87 16284.94 606.68 o 22 0 0 4616.20 4158.10 290.76 o 24 0 0 2944.97 3226.89 391.18 o 1 1 0 2999.21 3279.47 70.97 o 3 1 0 131172.48 140859.67 1750.61 o 5 1 0 10939.84 10799.43 184.19 o 7 1 0 67372.31 69979.82 839.29 o 9 1 0 2094.07 2191.45 51.67 o 11 1 0 6.98 31.62 17.86 o 13 1 0 22845.83 23025.70 292.04 o 15 1 0 2642.11 2632.31 84.41 o 17 1 0 6353.49 6142.53 148.63 o 19 1 0 174.26 190.57 62.95 o 21 1 0 32.25 63.76 83.73 o 23 1 0 1137.12 1115.16 148.42 o 0 2 0 7492.77 8583.87 300.54 o 2 2 0 101623.87 107315.12 1580.85 o 4 2 0 12919.23 13403.50 157.31 o 6 2 0 198612.89 209350.06 3697.92 o 8 2 0 39605.69 40371.17 436.17 o 10 2 0 108319.01 112145.56 1034.53 o 12 2 0 26544.67 26849.20 268.27 o 14 2 0 26143.86 26184.88 337.03 o 16 2 0 3717.92 3780.96 111.99 o 18 2 0 6338.33 6386.78 170.25 o 20 2 0 860.47 802.71 122.81 o 22 2 0 3011.56 3165.46 218.02 o 24 2 0 1509.15 1895.08 224.20 o 1 3 0 655.01 640.54 53.63 o 5 3 0 211.77 263.64 31.56 o 7 3 0 1129.10 1089.37 39.64 o 9 3 0 289.10 298.61 39.44 o 11 3 0 1590.35 1631.04 48.74 o 13 3 0 0.28 53.66 32.37 o 15 3 0 494.62 484.69 50.25 o 17 3 0 12.34 11.74 43.99 o 19 3 0 17.80 121.67 61.07 o 21 3 0 64.28 77.58 85.41 o 23 3 0 0.71 143.33 241.72 o 0 4 0 659.48 897.23 93.69 o 2 4 0 8263.08 8338.21 151.42 o 4 4 0 45253.97 45673.36 546.62 o 6 4 0 82208.62 83438.06 839.77 o 8 4 0 119558.24 121836.54 991.18 o 10 4 0 87446.24 89786.22 720.15 o 12 4 0 37758.25 37882.23 344.16 o 14 4 0 17035.39 17074.55 217.32 o 16 4 0 4008.40 3884.49 192.23 o 18 4 0 1593.49 1733.61 112.95 o 20 4 0 1648.92 1540.95 163.60 o 22 4 0 2006.91 2164.55 189.66 o 24 4 0 2052.11 2236.68 502.99 o 1 5 0 602.54 617.57 44.87 o 3 5 0 83805.58 84614.96 1094.61 o 5 5 0 26038.25 26368.60 318.79 o 7 5 0 54852.98 54966.75 535.54 o 9 5 0 1.48 28.69 13.87 o 11 5 0 202.09 314.72 41.35 o 13 5 0 13815.22 14278.62 189.36 o 15 5 0 4469.04 4447.91 107.89 o 17 5 0 3572.72 3570.25 158.43 o 19 5 0 30.29 63.21 64.26 o 21 5 0 132.96 84.61 89.30 o 23 5 0 973.21 771.42 163.88 o 0 6 0 294053.00 284006.16 15587.74 o 2 6 0 128989.16 125854.99 2477.28 o 4 6 0 142375.02 139191.58 1784.69 o 6 6 0 208.61 261.22 23.13 o 8 6 0 9637.83 9738.98 108.40 o 10 6 0 3269.56 3206.20 48.70 o 12 6 0 4699.40 4862.11 85.46 o 14 6 0 6553.58 6528.69 126.71 o 16 6 0 24465.25 25105.70 375.68 o 18 6 0 12872.70 13023.80 328.28 o 20 6 0 16426.13 16450.38 463.39 o 22 6 0 4085.33 3770.08 422.14 o 24 6 0 2183.25 1925.44 346.59 o 1 7 0 5806.47 5741.05 114.74 o 3 7 0 71513.02 72690.79 1037.50 o 5 7 0 6172.20 6377.01 92.43 o 7 7 0 33877.17 34497.65 338.48 o 9 7 0 2011.63 1937.95 52.23 o 11 7 0 492.64 608.15 29.55 o 13 7 0 14430.56 14230.44 188.26 o 15 7 0 722.86 742.01 60.24 o 17 7 0 2768.53 2932.14 132.58 o 19 7 0 88.38 135.53 121.84 o 21 7 0 12.78 -48.55 97.81 o 23 7 0 789.65 973.53 257.64 o 0 8 0 788.49 865.17 59.49 o 2 8 0 72069.30 71688.20 732.43 o 4 8 0 5070.91 5270.18 81.63 o 6 8 0 51022.45 51573.14 518.07 o 8 8 0 12023.35 12281.95 139.01 o 10 8 0 46734.68 47229.65 427.47 o 12 8 0 8859.41 8731.92 143.03 o 14 8 0 25937.45 25782.17 359.95 o 16 8 0 4163.73 4360.57 139.95 o 18 8 0 6932.11 6492.79 414.06 o 20 8 0 1702.79 1822.22 213.85 o 22 8 0 2132.64 2190.15 342.52 o 1 9 0 7807.60 7499.76 113.50 o 3 9 0 548.47 663.17 42.53 o 5 9 0 15273.31 14839.92 193.08 o 7 9 0 431.08 485.14 30.02 o 9 9 0 3175.56 3113.00 58.38 o 11 9 0 2016.61 1954.12 51.70 o 13 9 0 18.66 38.15 36.05 o 15 9 0 1596.84 1542.87 86.63 o 17 9 0 167.17 160.06 51.60 o 19 9 0 98.41 24.57 90.11 o 21 9 0 324.45 448.50 184.29 o 0 10 0 3888.28 4034.54 95.70 o 2 10 0 19.27 107.54 23.75 o 4 10 0 25333.59 25538.33 264.10 o 6 10 0 28457.21 28608.42 295.05 o 8 10 0 66422.27 66376.41 629.71 o 10 10 0 34501.51 34490.47 333.23 o 12 10 0 31332.99 30992.50 301.98 o 14 10 0 6010.89 6346.45 129.02 o 16 10 0 3378.38 3428.31 164.67 o 18 10 0 477.93 467.60 95.99 o 20 10 0 956.56 542.72 198.21 o 22 10 0 798.10 671.30 228.55 o 1 11 0 2712.52 2562.62 60.42 o 3 11 0 16030.76 15632.43 180.80 o 5 11 0 23397.14 23084.90 264.24 o 7 11 0 6495.65 6308.31 109.35 o 9 11 0 318.01 387.35 49.32 o 11 11 0 2891.46 2843.10 68.41 o 13 11 0 6102.40 6023.76 134.50 o 15 11 0 4343.88 4511.54 180.09 o 17 11 0 1044.71 1073.09 99.05 o 19 11 0 24.61 17.63 125.74 o 21 11 0 294.89 524.73 200.72 o 0 12 0 84926.34 82887.32 1219.48 o 2 12 0 45614.41 45316.36 470.03 o 4 12 0 32451.71 32318.55 332.55 o 6 12 0 8373.15 8364.29 125.64 o 8 12 0 1894.71 1915.22 61.29 o 10 12 0 192.01 186.43 32.27 o 12 12 0 2438.11 2410.57 70.02 o 14 12 0 2586.82 2563.45 96.25 o 16 12 0 7611.01 7320.25 226.77 o 18 12 0 7056.53 7207.62 229.62 o 20 12 0 5240.37 4886.08 411.18 o 1 13 0 5.05 64.11 31.09 o 3 13 0 9230.45 8905.61 135.86 o 5 13 0 1050.53 1256.27 72.09 o 7 13 0 7735.32 7719.44 126.01 o 9 13 0 39.13 78.74 31.33 o 11 13 0 7.94 52.61 29.48 o 13 13 0 1366.18 1379.12 63.08 o 15 13 0 292.95 303.83 51.74 o 17 13 0 737.39 706.65 93.28 o 19 13 0 35.02 135.40 115.76 o 0 14 0 8737.72 8535.28 257.61 o 2 14 0 22622.43 21745.43 264.29 o 4 14 0 5599.42 5500.75 126.91 o 6 14 0 17341.91 17763.23 223.04 o 8 14 0 3483.85 3485.89 93.35 o 10 14 0 11540.26 11465.05 176.66 o 12 14 0 4178.39 4253.01 98.51 o 14 14 0 7041.65 7255.46 173.89 o 16 14 0 2946.03 2839.08 156.02 o 18 14 0 3377.39 3711.77 240.26 o 1 15 0 3647.99 3572.90 100.62 o 3 15 0 95.19 34.52 36.37 o 5 15 0 6268.29 6179.37 141.47 o 7 15 0 10.00 -15.29 33.32 o 9 15 0 636.55 653.74 54.40 o 11 15 0 2003.51 1953.94 76.38 o 13 15 0 66.05 99.42 32.79 o 15 15 0 1093.47 1126.04 86.13 o 17 15 0 5.32 -33.43 75.19 o 0 16 0 2333.49 2585.33 153.81 o 2 16 0 259.84 339.09 49.70 o 4 16 0 9326.33 9613.97 188.33 o 6 16 0 7384.36 7275.83 160.68 o 8 16 0 20644.42 20742.89 315.79 o 10 16 0 10758.67 10529.14 223.79 o 12 16 0 10431.60 10324.05 208.82 o 14 16 0 2329.32 2429.10 118.07 o 16 16 0 1572.59 1616.25 150.69 o 1 17 0 2099.16 2180.43 87.49 o 3 17 0 2004.04 1965.01 94.74 o 5 17 0 7332.41 7554.79 161.34 o 7 17 0 1254.86 1239.36 92.56 o 9 17 0 520.33 548.83 77.29 o 11 17 0 1092.76 1192.60 86.56 o 13 17 0 760.13 789.30 76.64 o 15 17 0 1586.69 1686.26 193.84 o 0 18 0 12551.18 12910.94 311.59 o 2 18 0 13274.09 13838.37 308.24 o 4 18 0 6472.42 6489.71 159.84 o 6 18 0 3090.03 3318.53 126.42 o 8 18 0 944.62 912.49 78.33 o 10 18 0 686.24 617.82 73.83 o 12 18 0 537.37 483.12 99.90 o 14 18 0 1589.64 1755.22 139.90 o 1 19 0 0.46 24.47 49.23 o 3 19 0 122.16 113.60 53.79 o 5 19 0 303.85 278.30 60.59 o 7 19 0 98.09 16.77 60.35 o 9 19 0 81.71 138.13 61.15 o 11 19 0 8.98 -42.37 60.13 o 13 19 0 61.90 33.12 57.64 o 0 20 0 2988.87 2611.53 205.95 o 2 20 0 4717.13 4726.33 181.44 o 4 20 0 2189.03 2328.07 126.94 o 6 20 0 2778.03 2730.10 153.07 o 8 20 0 1350.52 1310.60 114.91 o 10 20 0 1875.53 2212.39 138.00 o 12 20 0 1244.62 1285.17 128.38 o 1 21 0 259.70 90.14 85.71 o 3 21 0 361.75 245.35 69.71 o 5 21 0 1293.89 1480.92 206.08 o 7 21 0 92.91 37.41 70.77 o 9 21 0 41.71 117.97 79.68 o 0 22 0 508.72 487.74 177.88 o 2 22 0 106.28 208.46 106.19 o 4 22 0 1799.93 1949.80 139.40 o 6 22 0 1929.58 1984.01 172.27 o -23 1 1 2004.49 2329.93 234.86 o -21 1 1 910.55 913.32 122.28 o -19 1 1 3657.20 3786.77 137.99 o -17 1 1 3773.17 3780.66 127.96 o -15 1 1 16676.52 16723.36 259.63 o -13 1 1 27134.84 27097.47 282.39 o -11 1 1 69574.46 71671.92 631.43 o -9 1 1 47910.41 49396.29 472.29 o -7 1 1 106268.54 112327.73 1444.56 o -5 1 1 20140.55 21444.31 256.64 o 3 1 1 38045.02 39143.99 802.87 o 5 1 1 158782.61 161499.73 2612.60 o 7 1 1 89793.54 91508.07 1119.43 o 9 1 1 130318.98 133725.75 1276.07 o 11 1 1 48186.92 48848.33 479.69 o 13 1 1 35473.30 35307.03 393.16 o 15 1 1 6431.74 6373.93 142.08 o 17 1 1 5418.99 5659.74 156.00 o 19 1 1 1528.32 1732.24 114.99 o 21 1 1 2754.45 2625.97 167.14 o 23 1 1 2103.19 1991.46 231.60 o -24 2 1 696.05 831.07 169.07 o -22 2 1 222.35 181.70 149.05 o -20 2 1 136.08 112.70 69.95 o -18 2 1 4515.06 4717.47 146.65 o -16 2 1 2589.88 2655.83 96.68 o -14 2 1 21742.73 21753.64 277.64 o -12 2 1 1272.47 1380.45 44.85 o -8 2 1 61837.64 64104.43 670.61 o -6 2 1 28565.34 30167.11 355.80 o -4 2 1 268770.69 285018.47 3884.29 o -2 2 1 2162.93 2262.94 82.30 o 0 2 1 783.35 860.49 40.57 o 2 2 1 126775.92 124460.09 2817.50 o 4 2 1 58423.64 61026.63 765.76 o 6 2 1 85466.74 86403.81 1221.54 o 8 2 1 8332.57 8458.75 120.09 o 10 2 1 46.48 53.53 25.72 o 12 2 1 35001.29 35844.99 370.33 o 14 2 1 5654.27 5543.99 124.01 o 16 2 1 4173.37 4232.48 116.72 o 18 2 1 285.64 410.44 69.70 o 20 2 1 172.95 146.82 66.55 o 22 2 1 2383.27 2693.77 206.56 o 24 2 1 190.68 248.02 142.60 o -23 3 1 3574.32 3874.47 283.56 o -21 3 1 13465.25 13431.89 358.39 o -19 3 1 11850.66 11960.34 315.83 o -17 3 1 23324.43 23746.09 385.67 o -15 3 1 3629.63 3773.13 101.89 o -13 3 1 8747.04 8852.79 121.88 o -11 3 1 4851.01 4817.10 79.79 o -9 3 1 11359.04 11433.47 148.67 o -7 3 1 535.24 560.98 26.17 o -5 3 1 171715.11 184487.11 2298.07 o -3 3 1 143669.63 150832.23 2670.35 o -1 3 1 590756.69 587001.81 12588.97 o 1 3 1 156257.66 160317.16 3498.39 o 3 3 1 302031.22 283836.91 5574.05 o 5 3 1 1854.15 1895.60 50.65 o 7 3 1 18033.72 18050.86 229.36 o 9 3 1 7082.01 7114.67 105.65 o 11 3 1 11317.97 11534.02 142.12 o 13 3 1 3068.19 3300.62 78.34 o 15 3 1 40196.09 41518.61 527.79 o 17 3 1 18194.98 18366.43 319.66 o 19 3 1 24312.32 24865.93 522.49 o 21 3 1 6467.76 6297.85 275.90 o 23 3 1 3826.62 3643.59 392.79 o -24 4 1 987.77 1095.22 182.17 o -22 4 1 7.73 125.67 100.85 o -20 4 1 203.21 176.78 76.71 o -18 4 1 2402.73 2527.41 147.41 o -16 4 1 1576.59 1589.09 78.29 o -14 4 1 14787.89 14705.74 196.48 o -12 4 1 811.19 880.19 36.12 o -10 4 1 6543.64 6520.78 86.30 o -8 4 1 54738.63 56186.68 516.98 o -6 4 1 6346.11 6653.63 82.93 o -4 4 1 65807.04 68912.04 1000.83 o -2 4 1 7469.12 7764.40 359.76 o 0 4 1 7160.46 6914.47 144.12 o 2 4 1 239596.38 232349.70 5067.74 o 4 4 1 2648.08 2718.77 105.42 o 6 4 1 87916.55 85506.30 1266.78 o 8 4 1 1144.47 1141.33 36.41 o 10 4 1 2.96 29.11 17.82 o 12 4 1 26055.85 26051.00 278.60 o 14 4 1 1193.36 1324.47 57.21 o 16 4 1 10019.46 10118.82 211.90 o 18 4 1 433.66 556.46 85.69 o 20 4 1 4.30 -67.41 67.41 o 22 4 1 1027.11 1175.92 151.89 o 24 4 1 227.66 113.53 169.24 o -23 5 1 2000.35 1597.91 304.57 o -21 5 1 1462.96 1651.72 167.70 o -19 5 1 4808.01 4641.84 193.02 o -17 5 1 2975.20 2808.29 147.86 o -15 5 1 23697.52 23188.45 322.65 o -13 5 1 13809.12 13942.43 172.59 o -11 5 1 68523.70 69868.97 626.72 o -9 5 1 34025.74 34880.67 312.84 o -7 5 1 91286.71 95490.76 804.35 o -5 5 1 10750.13 11157.22 195.92 o -3 5 1 74808.23 75953.58 1106.45 o -1 5 1 21.92 99.09 33.27 o 1 5 1 70512.08 67565.81 1016.77 o 3 5 1 14219.45 14078.93 216.02 o 5 5 1 112248.26 109131.52 1566.85 o 7 5 1 31511.11 31632.70 291.49 o 9 5 1 93860.45 95073.41 897.96 o 11 5 1 15461.36 15304.68 160.26 o 13 5 1 29735.25 29738.41 318.85 o 15 5 1 4123.82 4121.50 123.10 o 17 5 1 7869.19 8255.71 215.66 o 19 5 1 1465.55 1499.17 130.16 o 21 5 1 4143.20 4560.51 274.19 o 23 5 1 1406.49 1181.55 195.11 o -24 6 1 27.36 185.29 186.63 o -22 6 1 296.22 96.35 174.53 o -20 6 1 6.23 -58.99 90.22 o -18 6 1 188.19 182.02 114.31 o -16 6 1 1300.52 1373.95 76.77 o -14 6 1 26.93 9.11 26.61 o -12 6 1 3065.46 2991.72 69.62 o -10 6 1 1455.93 1533.30 48.83 o -8 6 1 599.35 621.62 45.74 o -6 6 1 19666.64 20179.92 234.85 o -4 6 1 821.16 876.91 56.29 o -2 6 1 10384.19 10409.39 229.65 o 0 6 1 19020.15 19249.65 321.68 o 2 6 1 209.32 378.83 68.07 o 4 6 1 26355.57 26108.85 318.69 o 6 6 1 970.42 988.22 34.30 o 8 6 1 2939.99 2937.72 48.04 o 10 6 1 6974.92 6724.23 102.50 o 12 6 1 3.40 46.53 27.34 o 14 6 1 2390.17 2389.79 87.10 o 16 6 1 162.76 286.01 55.29 o 18 6 1 31.79 -23.95 66.50 o 20 6 1 433.92 307.31 102.55 o 22 6 1 1.39 -105.36 105.36 o -23 7 1 963.65 989.87 255.85 o -21 7 1 1272.94 1172.90 148.39 o -19 7 1 962.43 1158.27 140.59 o -17 7 1 4008.78 4087.05 138.87 o -15 7 1 11040.34 11117.30 234.03 o -13 7 1 28887.97 28587.13 348.76 o -11 7 1 50126.49 50954.80 457.36 o -9 7 1 73859.96 74942.88 679.77 o -7 7 1 46682.51 48782.72 484.88 o -5 7 1 38498.44 39178.63 446.59 o -3 7 1 7420.27 7890.99 127.48 o -1 7 1 3518.89 3478.41 76.90 o 1 7 1 5545.59 5688.86 101.11 o 3 7 1 23233.89 23110.09 259.43 o 5 7 1 42582.84 43088.74 428.93 o 7 7 1 80726.69 79599.91 669.79 o 9 7 1 58139.74 58087.00 469.64 o 11 7 1 41728.67 41410.18 420.75 o 13 7 1 13999.77 13635.20 203.20 o 15 7 1 5238.80 5199.70 123.07 o 17 7 1 1218.71 1329.20 109.10 o 19 7 1 1285.52 1126.84 136.07 o 21 7 1 1438.84 1232.31 186.89 o 23 7 1 2219.45 2600.82 364.68 o -22 8 1 179.15 488.07 195.69 o -20 8 1 1.33 -42.89 81.96 o -18 8 1 1180.73 1391.77 103.23 o -16 8 1 4956.02 4870.51 151.98 o -14 8 1 7222.16 7347.86 144.97 o -12 8 1 1897.41 1839.85 45.04 o -10 8 1 0.47 11.53 20.50 o -8 8 1 17190.90 17131.31 181.43 o -6 8 1 30868.38 30831.95 343.62 o -4 8 1 24856.52 24966.71 282.57 o -2 8 1 5603.62 5604.07 107.88 o 0 8 1 3907.24 3764.73 80.44 o 2 8 1 48587.26 46901.63 496.74 o 4 8 1 32471.63 31604.73 348.56 o 6 8 1 23674.33 23108.88 269.83 o 8 8 1 1298.60 1264.81 37.57 o 10 8 1 4468.21 4520.77 65.49 o 12 8 1 10756.25 11068.49 155.22 o 14 8 1 6335.43 6176.53 146.35 o 16 8 1 3427.56 3596.71 125.19 o 18 8 1 1.50 -55.75 70.96 o 20 8 1 433.34 375.90 159.20 o 22 8 1 655.37 955.00 247.22 o -19 9 1 8196.80 8593.28 322.89 o -17 9 1 13705.62 14081.94 293.90 o -15 9 1 3714.77 3726.45 135.90 o -13 9 1 4040.09 4104.15 100.24 o -11 9 1 96.11 153.66 23.33 o -9 9 1 2934.26 3154.39 68.64 o -7 9 1 2657.67 2764.89 60.06 o -5 9 1 77193.43 79080.76 721.14 o -3 9 1 68136.02 69521.11 673.21 o -1 9 1 198312.44 201636.84 2276.29 o 1 9 1 82921.99 82219.89 789.62 o 3 9 1 69423.98 68455.08 679.18 o 5 9 1 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