#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/28/2212803.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212803_Fobs loop_ _publ_author_name 'Klap\"otke, Thomas M.' 'Krumm, Burkhard' 'Scherr, Matthias' _publ_section_title ; 1,3-Bis[chlorobis(dimethylphenylsilyl)methyl]triselane ; _journal_coeditor_code BT2303 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1965 _journal_page_last o1966 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 94.688 _cell_angle_beta 107.801 _cell_angle_gamma 91.108 _cell_length_a 11.2970 _cell_length_b 13.0120 _cell_length_c 13.7510 _exptl_crystal_F_000 880.00 _reflns_d_resolution_high 0.8106 _[local]_cod_data_source_file bt2303Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' p-1 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 237.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k 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0 4509.31 4700.72 272.59 o 8 1 0 1671.87 1648.58 243.11 o 9 1 0 1502.65 1583.97 291.54 o 10 1 0 692.99 940.01 341.66 o 11 1 0 358.43 495.32 301.15 o 12 1 0 5.69 21.32 126.13 o 13 1 0 1.94 -53.07 481.26 o -13 2 0 0.06 8.84 988.73 o -12 2 0 216.32 118.26 398.58 o -11 2 0 1727.62 1781.48 364.97 o -10 2 0 1113.25 1093.68 313.76 o -9 2 0 297.64 720.53 266.37 o -8 2 0 2214.29 2106.27 221.54 o -7 2 0 5798.62 5629.42 396.63 o -6 2 0 1122.76 859.00 178.71 o -5 2 0 1328.05 885.77 167.52 o -4 2 0 8082.16 8016.65 200.98 o -3 2 0 2.14 -15.63 67.81 o -2 2 0 4222.38 4396.76 205.50 o 2 2 0 5120.08 5658.77 200.07 o 3 2 0 305.66 383.01 84.94 o 4 2 0 3512.50 3486.69 196.17 o 5 2 0 1.40 15.81 22.72 o 6 2 0 91.67 14.69 42.09 o 7 2 0 4079.37 3960.03 228.79 o 8 2 0 1351.15 1211.07 221.76 o 9 2 0 357.09 382.07 271.79 o 10 2 0 1410.48 1657.00 293.47 o 11 2 0 1326.33 1420.29 512.11 o 12 2 0 184.86 -11.69 490.96 o 13 2 0 4.50 82.16 1705.47 o -13 3 0 68.35 -214.98 486.55 o -12 3 0 436.36 397.58 518.03 o -11 3 0 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17087.19 16298.49 308.41 o -3 4 0 427.05 374.10 143.89 o -2 4 0 3831.74 4236.47 204.38 o -1 4 0 2807.22 2983.63 125.30 o 0 4 0 10654.41 14730.29 364.74 o 1 4 0 1804.31 2015.68 162.71 o 2 4 0 2016.13 2209.52 166.76 o 3 4 0 3486.70 2909.88 167.58 o 4 4 0 14296.30 14662.41 354.45 o 5 4 0 1172.68 993.40 236.34 o 6 4 0 1308.95 1188.35 177.69 o 7 4 0 932.89 827.95 212.74 o 8 4 0 674.03 953.24 261.68 o 9 4 0 2993.57 3378.77 411.31 o 10 4 0 1225.82 1781.16 436.13 o 11 4 0 368.55 69.65 649.70 o 12 4 0 1226.81 1177.78 619.42 o -12 5 0 401.32 312.39 542.55 o -11 5 0 405.78 249.51 607.80 o -10 5 0 2512.59 2281.33 501.05 o -9 5 0 2454.95 3044.65 386.42 o -8 5 0 949.19 997.34 342.57 o -7 5 0 325.94 355.30 164.95 o -6 5 0 8.03 35.95 71.40 o -5 5 0 2173.32 2210.18 249.30 o -4 5 0 1559.75 1427.88 214.36 o -3 5 0 1430.86 1314.40 211.73 o -2 5 0 4.74 11.70 68.13 o -1 5 0 990.85 944.46 103.34 o 0 5 0 7848.96 9993.76 449.85 o 1 5 0 178.27 318.18 72.43 o 2 5 0 2.08 11.12 38.00 o 3 5 0 313.19 287.64 89.23 o 4 5 0 2594.12 1945.03 221.97 o 5 5 0 1121.92 1646.44 230.32 o 6 5 0 412.31 534.64 180.78 o 7 5 0 2052.08 2382.28 284.32 o 8 5 0 1222.25 1890.64 329.89 o 9 5 0 1057.22 765.26 443.48 o 10 5 0 1820.16 1726.11 481.46 o 11 5 0 412.31 347.47 514.62 o 12 5 0 10.70 -138.96 826.20 o -12 6 0 57.92 250.18 1060.03 o -11 6 0 336.33 150.45 436.40 o -10 6 0 630.54 772.93 454.76 o -9 6 0 234.55 563.26 476.57 o -8 6 0 4232.13 4305.55 441.94 o -7 6 0 5211.36 4810.74 421.93 o -6 6 0 33.79 131.76 163.84 o -5 6 0 42.22 12.69 207.57 o -4 6 0 50.25 85.06 219.59 o -3 6 0 2355.52 2246.32 213.17 o -2 6 0 1771.38 1733.54 118.05 o -1 6 0 1105.88 1139.12 110.54 o 0 6 0 1791.35 1990.08 144.08 o 1 6 0 1782.29 1700.83 135.36 o 2 6 0 5307.47 5016.73 164.08 o 3 6 0 1074.54 834.77 128.33 o 4 6 0 66.78 74.18 116.06 o 5 6 0 101.28 64.55 247.94 o 6 6 0 700.34 762.53 261.42 o 7 6 0 5277.63 5426.04 453.52 o 8 6 0 1280.25 1766.79 345.69 o 9 6 0 7.73 382.45 406.24 o 10 6 0 156.93 281.21 746.05 o 11 6 0 2.38 129.00 410.05 o 12 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396.09 328.07 245.51 o -3 8 0 809.68 661.59 112.62 o -2 8 0 2124.29 1776.77 148.03 o -1 8 0 13159.71 13791.58 325.96 o 0 8 0 20211.31 27038.68 479.80 o 1 8 0 4344.37 6614.77 419.15 o 2 8 0 930.28 995.28 156.24 o 3 8 0 6.17 -7.88 221.87 o 4 8 0 2257.01 2217.04 169.88 o 5 8 0 6390.45 5907.36 418.62 o 6 8 0 4848.29 5050.50 587.26 o 7 8 0 783.82 995.33 381.07 o 8 8 0 1553.07 2065.91 414.03 o 9 8 0 843.88 1435.58 464.48 o 10 8 0 29.13 -50.24 313.85 o 11 8 0 20.97 0.64 16.95 o -11 9 0 192.94 118.17 353.03 o -10 9 0 2.32 -103.85 457.71 o -9 9 0 1269.12 1120.35 471.25 o -8 9 0 1119.94 1112.29 469.80 o -7 9 0 667.61 759.85 419.78 o -6 9 0 5298.27 4753.26 393.69 o -5 9 0 5402.68 4879.35 840.81 o -4 9 0 1581.83 1095.27 285.29 o -3 9 0 237.01 192.66 157.42 o -2 9 0 735.16 515.28 155.28 o -1 9 0 5269.75 5169.60 234.13 o 0 9 0 7241.17 8982.58 297.15 o 1 9 0 2066.02 2623.81 196.27 o 2 9 0 27.07 67.95 160.83 o 3 9 0 629.42 564.11 161.35 o 4 9 0 2773.76 2746.24 425.26 o 5 9 0 1783.49 1648.78 348.79 o 6 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399.36 o -1 -13 1 10.38 60.26 264.56 o 0 -13 1 32.03 74.95 191.75 o 1 -13 1 48.34 55.82 160.93 o 2 -13 1 351.17 179.71 310.81 o 3 -13 1 658.60 381.69 336.89 o 4 -13 1 690.99 905.01 519.59 o 5 -13 1 405.71 462.80 478.62 o 6 -13 1 284.92 502.81 587.44 o 7 -13 1 50.60 180.63 542.00 o 8 -13 1 431.99 538.50 638.52 o -8 -12 1 1302.66 1152.95 603.66 o -7 -12 1 165.29 102.23 315.78 o -6 -12 1 1057.85 1072.61 475.17 o -5 -12 1 1013.08 1091.66 517.24 o -4 -12 1 1923.69 2023.48 442.71 o -3 -12 1 4669.45 5328.44 442.48 o -2 -12 1 814.92 1523.30 380.55 o -1 -12 1 15.67 80.62 193.43 o 0 -12 1 108.52 -0.97 124.62 o 1 -12 1 14.35 27.87 239.71 o 2 -12 1 174.96 297.38 276.71 o 3 -12 1 5641.35 5553.43 887.95 o 4 -12 1 3597.70 3372.15 418.64 o 5 -12 1 669.01 753.89 438.27 o 6 -12 1 2374.51 2645.26 500.18 o 7 -12 1 74.49 342.92 470.35 o 8 -12 1 1477.24 1530.78 559.91 o 9 -12 1 1302.29 1473.76 690.34 o -9 -11 1 1291.51 1583.73 621.18 o -8 -11 1 229.77 71.45 358.93 o -7 -11 1 70.07 -2.17 176.60 o -6 -11 1 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