#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:27:23 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181048 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/28/2212828.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212828_Fobs loop_ _publ_author_name 'Zhu, Yu-Lin' 'Wang, Long-Sheng' 'Li, Qiang' 'Wei, Yong-Ge' _publ_section_title ; Bis(tetrabutylammonium) di-\m-bromido-bis[dibromidopalladate(II)] ; _journal_coeditor_code CV2197 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1004 _journal_page_last m1005 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.190 _cell_angle_gamma 90.000 _cell_length_a 13.6408 _cell_length_b 14.8687 _cell_length_c 22.4765 _exptl_crystal_F_000 2320.00 _reflns_d_resolution_high 0.7706 _cod_data_source_file cv2197Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' w in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 686.34 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2526.74 2516.50 32.43 o 3 0 0 98.05 83.71 17.34 o 4 0 0 96894.05 90870.68 4079.03 o 5 0 0 40679.04 40118.00 861.54 o 6 0 0 8731.86 8862.10 135.26 o 7 0 0 4915.63 4519.19 102.89 o 8 0 0 627.74 760.59 49.00 o 9 0 0 5730.45 5901.18 205.97 o 10 0 0 202.87 165.81 50.33 o 11 0 0 4.15 34.29 43.19 o 12 0 0 3839.72 3697.55 107.96 o 13 0 0 584.04 622.28 55.19 o 14 0 0 397.21 300.81 57.50 o 15 0 0 84.29 85.66 48.42 o 16 0 0 18.58 26.77 77.54 o 17 0 0 4123.24 4531.51 398.93 o 2 1 0 600.85 477.98 16.93 o 3 1 0 35879.42 38362.55 430.22 o 4 1 0 6189.81 5687.26 53.80 o 5 1 0 190424.50 172129.28 6986.53 o 6 1 0 5147.63 5669.01 89.96 o 7 1 0 22219.45 22306.65 453.96 o 8 1 0 178.18 175.61 24.45 o 9 1 0 2795.36 2830.62 91.14 o 10 1 0 826.22 857.05 41.04 o 11 1 0 100.93 115.06 32.15 o 12 1 0 8142.66 8043.57 131.69 o 13 1 0 125.48 117.95 33.11 o 14 1 0 1677.42 1875.04 96.33 o 15 1 0 0.54 56.27 41.65 o 16 1 0 37.75 85.88 55.79 o 17 1 0 0.23 -20.44 124.98 o 1 2 0 5215.24 4869.97 48.93 o 2 2 0 2252.29 2027.29 44.79 o 3 2 0 101.70 124.64 12.88 o 4 2 0 25262.69 25245.55 249.23 o 5 2 0 49.02 122.12 37.13 o 6 2 0 25219.03 25344.58 333.42 o 7 2 0 8785.04 8034.20 207.12 o 8 2 0 422.05 352.42 32.52 o 9 2 0 4177.03 3768.59 184.31 o 10 2 0 4588.16 4616.11 95.00 o 11 2 0 3.87 -12.69 27.61 o 12 2 0 279.36 284.02 41.07 o 13 2 0 1222.77 1323.14 47.43 o 14 2 0 232.03 246.71 54.42 o 15 2 0 3.62 -31.55 31.55 o 16 2 0 4.15 17.81 49.34 o 17 2 0 1838.78 1066.59 592.93 o 1 3 0 3270.91 3118.74 47.24 o 2 3 0 123793.83 113724.13 3078.76 o 3 3 0 17.56 27.68 16.59 o 4 3 0 24978.25 25533.58 297.64 o 5 3 0 62494.00 62567.44 1139.52 o 6 3 0 8945.22 8659.91 92.66 o 7 3 0 97.97 51.67 21.53 o 8 3 0 1280.48 1083.27 66.03 o 9 3 0 2101.27 2264.88 51.90 o 10 3 0 0.54 40.79 26.01 o 11 3 0 2463.67 1893.28 265.79 o 12 3 0 2290.66 2425.15 86.88 o 13 3 0 168.34 178.59 52.50 o 14 3 0 5.30 -28.56 60.15 o 15 3 0 71.45 120.89 51.88 o 16 3 0 47.06 0.67 83.36 o 17 3 0 479.73 360.73 107.76 o 0 4 0 767.91 904.80 44.14 o 1 4 0 62174.66 61504.44 1229.61 o 2 4 0 526.58 525.02 29.40 o 3 4 0 1965.24 1930.07 39.12 o 4 4 0 70.72 80.43 23.77 o 5 4 0 63193.39 66028.54 1249.94 o 6 4 0 11817.79 11351.60 130.47 o 7 4 0 3673.93 3585.42 51.38 o 8 4 0 81.90 42.83 23.30 o 9 4 0 6307.11 5983.78 207.08 o 10 4 0 11131.11 10915.83 234.58 o 11 4 0 72.31 122.60 57.58 o 12 4 0 5393.59 5234.43 203.77 o 13 4 0 297.66 294.83 60.82 o 14 4 0 413.39 333.99 66.93 o 15 4 0 24.44 -43.33 67.73 o 16 4 0 273.54 256.08 122.20 o 17 4 0 0.05 153.68 88.48 o 1 5 0 4853.70 4660.75 82.23 o 2 5 0 8884.53 8609.65 172.56 o 3 5 0 4068.96 4090.21 69.18 o 4 5 0 26306.85 27329.77 425.76 o 5 5 0 851.51 1032.64 42.40 o 6 5 0 32385.14 29505.84 944.83 o 7 5 0 13914.71 14193.18 184.58 o 8 5 0 1.71 18.87 22.36 o 9 5 0 1276.91 1213.02 38.88 o 10 5 0 4490.72 4402.03 158.66 o 11 5 0 7441.11 7513.31 196.09 o 12 5 0 3.12 -4.53 74.96 o 13 5 0 2676.14 3020.66 151.73 o 14 5 0 9.11 80.21 56.24 o 15 5 0 299.09 371.65 70.30 o 16 5 0 35.24 38.06 108.85 o 0 6 0 29541.49 28276.71 620.95 o 1 6 0 71.15 34.18 29.28 o 2 6 0 736.95 735.78 41.84 o 3 6 0 2484.20 2359.58 66.18 o 4 6 0 234.86 263.38 36.65 o 5 6 0 30945.43 30876.02 522.50 o 6 6 0 3.81 -6.78 37.93 o 7 6 0 3266.15 3218.41 56.57 o 8 6 0 4390.25 4807.43 81.25 o 9 6 0 609.97 620.21 45.12 o 10 6 0 45.46 78.71 44.41 o 11 6 0 1513.94 1868.21 131.68 o 12 6 0 6335.11 6981.04 224.18 o 13 6 0 201.02 126.22 71.58 o 14 6 0 20.75 31.90 61.71 o 15 6 0 102.26 40.24 70.30 o 16 6 0 801.94 739.13 137.33 o 1 7 0 31.17 83.62 38.64 o 2 7 0 38.63 50.65 34.53 o 3 7 0 11102.34 11381.82 179.74 o 4 7 0 155.70 147.95 38.92 o 5 7 0 20391.18 20178.33 333.14 o 6 7 0 3417.88 3331.20 83.56 o 7 7 0 6498.35 6766.56 114.94 o 8 7 0 1038.24 995.81 77.15 o 9 7 0 1306.99 1339.86 53.38 o 10 7 0 5802.77 5808.16 131.46 o 11 7 0 393.09 410.06 95.40 o 12 7 0 1807.55 1783.52 141.84 o 13 7 0 1343.58 1438.12 117.94 o 14 7 0 2.76 -23.69 77.33 o 15 7 0 176.84 178.91 81.25 o 16 7 0 3.44 23.88 89.37 o 0 8 0 17830.39 17972.28 485.75 o 1 8 0 1719.43 1553.37 62.38 o 2 8 0 4740.75 4569.60 97.64 o 3 8 0 752.16 843.10 59.56 o 4 8 0 24.40 35.05 44.82 o 5 8 0 29.60 97.82 43.63 o 6 8 0 3534.73 3617.44 109.29 o 7 8 0 3651.48 3754.37 154.71 o 8 8 0 1315.31 1364.49 109.21 o 9 8 0 168.74 195.27 30.87 o 10 8 0 3359.54 3075.82 180.52 o 11 8 0 234.80 171.43 53.92 o 12 8 0 1739.62 1801.75 131.61 o 13 8 0 1216.71 1095.55 104.53 o 14 8 0 109.25 238.53 85.82 o 15 8 0 184.70 334.77 183.25 o 1 9 0 3335.73 3546.51 106.25 o 2 9 0 4310.73 4228.29 105.95 o 3 9 0 81.09 144.46 61.58 o 4 9 0 2675.99 2882.43 106.74 o 5 9 0 12633.82 13106.89 314.48 o 6 9 0 3335.73 3231.60 117.09 o 7 9 0 3723.21 4102.80 124.90 o 8 9 0 1424.78 1385.12 66.32 o 9 9 0 104.14 52.07 38.24 o 10 9 0 314.35 309.64 35.99 o 11 9 0 431.61 367.83 64.65 o 12 9 0 3426.24 3512.05 354.06 o 13 9 0 11.95 -12.63 83.32 o 14 9 0 66.53 52.98 97.99 o 15 9 0 71.39 -125.21 174.96 o 0 10 0 16002.91 16540.86 460.92 o 1 10 0 118.35 178.30 55.90 o 2 10 0 5412.65 5480.24 144.66 o 3 10 0 610.20 633.16 62.90 o 4 10 0 77.97 46.97 53.16 o 5 10 0 917.40 973.46 74.24 o 6 10 0 148.63 192.49 75.94 o 7 10 0 16077.91 16316.00 354.90 o 8 10 0 1.66 -13.62 52.65 o 9 10 0 448.53 533.03 56.62 o 10 10 0 2787.32 2680.67 70.21 o 11 10 0 154.13 60.63 43.48 o 12 10 0 295.27 458.26 163.27 o 13 10 0 191.97 105.91 204.55 o 14 10 0 5.58 -0.23 133.86 o 1 11 0 704.98 712.17 80.05 o 2 11 0 7644.45 7662.26 190.19 o 3 11 0 4.87 22.60 62.27 o 4 11 0 19.97 129.91 65.99 o 5 11 0 2739.61 2790.32 116.98 o 6 11 0 1651.47 2043.58 130.07 o 7 11 0 384.22 354.32 68.37 o 8 11 0 1480.70 1328.95 71.32 o 9 11 0 52.71 17.54 64.83 o 10 11 0 1473.80 1466.52 104.10 o 11 11 0 1455.81 1425.26 130.46 o 12 11 0 852.52 658.92 108.90 o 13 11 0 155.94 87.84 190.04 o 14 11 0 614.27 721.29 131.90 o 0 12 0 7157.39 7895.98 438.71 o 1 12 0 862.90 1018.49 87.81 o 2 12 0 209.48 213.26 77.74 o 3 12 0 5133.34 5359.66 219.44 o 4 12 0 318.96 193.09 76.26 o 5 12 0 967.12 1005.30 89.39 o 6 12 0 1339.08 1583.17 125.17 o 7 12 0 4975.87 5370.76 197.33 o 8 12 0 1084.62 1059.22 123.05 o 9 12 0 1374.02 1187.31 118.67 o 10 12 0 851.07 729.81 89.80 o 11 12 0 553.31 618.88 100.18 o 12 12 0 681.37 472.29 131.15 o 13 12 0 14.48 -89.27 157.34 o 1 13 0 197.14 231.15 88.34 o 2 13 0 7013.75 7005.53 214.66 o 3 13 0 6.31 -39.30 77.11 o 4 13 0 6.06 -71.45 79.42 o 5 13 0 832.95 777.17 91.05 o 6 13 0 2392.95 2482.95 130.79 o 7 13 0 1534.21 1689.33 146.97 o 8 13 0 337.82 371.00 93.13 o 9 13 0 0.51 57.41 59.54 o 10 13 0 835.67 669.68 86.99 o 11 13 0 551.47 559.44 88.43 o 12 13 0 46.30 21.90 91.98 o 0 14 0 562.05 727.73 223.60 o 1 14 0 2198.14 2466.78 156.90 o 2 14 0 1087.44 1196.91 125.75 o 3 14 0 2484.06 2360.53 178.20 o 4 14 0 21.95 82.97 88.56 o 5 14 0 878.25 1057.23 209.41 o 6 14 0 1043.42 1184.82 147.68 o 7 14 0 117.01 211.18 86.80 o 8 14 0 172.59 -36.42 79.22 o 9 14 0 416.66 314.85 89.25 o 10 14 0 168.97 133.79 74.99 o 11 14 0 95.47 77.67 77.37 o 1 15 0 1451.27 1658.88 172.41 o 2 15 0 2053.03 2139.31 155.28 o 3 15 0 35.04 71.75 98.82 o 4 15 0 9.24 28.17 112.95 o 5 15 0 74.06 -87.03 87.03 o 6 15 0 320.72 276.20 126.41 o 7 15 0 651.97 737.37 136.94 o 8 15 0 53.77 265.79 117.34 o 9 15 0 283.60 390.09 135.64 o 10 15 0 23.30 -93.68 93.68 o 0 16 0 16.66 14.04 125.41 o 1 16 0 127.25 -61.35 90.90 o 2 16 0 815.86 976.51 136.89 o 3 16 0 1.70 -24.29 111.88 o 4 16 0 501.95 579.78 119.11 o 5 16 0 86.85 106.96 101.75 o 6 16 0 379.97 214.09 173.96 o 7 16 0 67.61 102.10 97.51 o 8 16 0 10.98 31.69 99.21 o 9 16 0 107.48 361.49 106.58 o 1 17 0 750.46 1020.22 194.48 o 2 17 0 163.09 -6.31 149.26 o 3 17 0 435.31 374.06 113.66 o 4 17 0 64.87 119.60 115.98 o 5 17 0 72.71 98.96 98.43 o 6 17 0 106.49 198.43 124.06 o 7 17 0 22.24 -12.97 105.25 o 8 17 0 0.04 -87.89 111.15 o 0 18 0 436.44 277.76 164.95 o 1 18 0 139.33 885.34 292.22 o 2 18 0 12.38 163.13 123.15 o 3 18 0 205.65 44.36 194.94 o 4 18 0 899.79 915.23 135.78 o 5 18 0 104.20 88.66 103.58 o 6 18 0 0.07 333.39 219.93 o 1 19 0 320.98 301.94 165.02 o 2 19 0 690.14 827.73 226.61 o -17 1 1 563.69 691.53 226.24 o -16 1 1 5.55 45.81 46.64 o -15 1 1 11.30 -1.49 46.09 o -14 1 1 258.51 233.76 43.52 o -13 1 1 1176.27 1164.06 56.35 o -12 1 1 268.42 240.33 45.68 o -11 1 1 10.31 28.45 32.27 o -10 1 1 46.92 59.88 23.46 o -9 1 1 3120.10 2911.33 116.36 o -8 1 1 116.03 95.80 22.31 o -7 1 1 10694.15 10294.95 128.39 o -6 1 1 978.06 1066.66 42.74 o -5 1 1 21033.87 20649.71 275.09 o -4 1 1 13462.41 13748.82 174.79 o -3 1 1 3481.26 3905.54 108.89 o -2 1 1 2731.49 2768.46 27.46 o 2 1 1 11.81 21.98 6.38 o 3 1 1 1026.76 888.23 18.45 o 4 1 1 26610.59 26124.74 434.79 o 5 1 1 317.40 343.56 20.72 o 6 1 1 15740.85 16390.21 309.83 o 7 1 1 5106.66 4897.46 59.35 o 8 1 1 336.31 337.23 29.47 o 9 1 1 3853.60 3854.49 108.99 o 10 1 1 1717.17 1829.01 51.60 o 11 1 1 890.46 912.89 40.55 o 12 1 1 1035.10 1054.27 50.50 o 13 1 1 50.88 61.31 37.35 o 14 1 1 493.83 491.94 42.15 o 15 1 1 39.87 -28.86 33.71 o 16 1 1 66.12 135.56 61.23 o 17 1 1 136.29 86.72 168.92 o -17 2 1 787.46 1080.47 154.61 o -16 2 1 392.69 364.28 82.83 o -15 2 1 66.71 66.68 29.43 o -14 2 1 11.79 28.05 49.11 o -13 2 1 521.33 530.43 35.46 o -12 2 1 5793.08 6113.05 173.12 o -11 2 1 23.02 -3.68 24.07 o -10 2 1 166.83 231.80 53.31 o -9 2 1 1131.87 1119.92 46.00 o -8 2 1 148.52 159.15 23.99 o -7 2 1 24.02 21.83 27.37 o -6 2 1 10516.15 11723.47 219.18 o -5 2 1 9734.35 10503.72 122.65 o -4 2 1 16103.21 15823.54 192.49 o -3 2 1 22832.72 23892.79 287.55 o -2 2 1 13994.98 13133.80 125.53 o -1 2 1 18063.97 17623.73 280.45 o 1 2 1 98651.26 87406.88 1910.37 o 2 2 1 5113.38 4586.61 83.92 o 3 2 1 10217.66 9781.48 164.12 o 4 2 1 2039.24 1959.13 29.75 o 5 2 1 176541.22 166409.77 5216.40 o 6 2 1 8366.07 7967.94 85.42 o 7 2 1 1687.16 1694.28 31.94 o 8 2 1 680.39 693.36 37.93 o 9 2 1 159.04 201.25 25.86 o 10 2 1 5194.96 5015.13 79.14 o 11 2 1 167.54 194.26 33.05 o 12 2 1 454.74 526.58 55.37 o 13 2 1 565.86 623.47 38.85 o 14 2 1 92.64 68.44 43.85 o 15 2 1 4.36 -1.15 35.56 o 16 2 1 0.89 3.21 91.19 o 17 2 1 990.81 707.59 75.46 o -17 3 1 2186.77 2752.93 360.66 o -16 3 1 68.76 4.25 89.43 o -15 3 1 15.22 -1.68 53.38 o -14 3 1 785.94 1036.58 74.45 o -13 3 1 3499.11 3936.63 108.94 o -12 3 1 285.05 433.46 66.95 o -11 3 1 7.63 1.33 48.80 o -10 3 1 1.75 -5.96 44.17 o -9 3 1 2541.36 2365.56 184.95 o -8 3 1 2009.46 1739.84 127.63 o -7 3 1 5838.81 5866.33 217.21 o -6 3 1 812.29 719.39 27.95 o -5 3 1 78953.89 79047.08 1586.26 o -4 3 1 6456.66 5758.58 127.60 o -3 3 1 11871.16 11412.67 165.67 o -2 3 1 35032.23 33818.86 474.37 o -1 3 1 98823.04 90694.59 2118.25 o 0 3 1 97556.16 89618.74 2097.92 o 1 3 1 23023.84 23344.43 281.83 o 2 3 1 306.02 342.27 22.69 o 3 3 1 14383.24 14395.84 151.66 o 4 3 1 21730.10 21497.98 230.03 o 5 3 1 53.01 80.70 31.45 o 6 3 1 53634.40 53889.71 1017.31 o 7 3 1 2434.37 2215.15 43.75 o 8 3 1 74.40 107.57 23.16 o 9 3 1 1901.17 2026.89 46.79 o 10 3 1 12685.26 13123.79 198.08 o 11 3 1 986.60 1064.67 43.28 o 12 3 1 5312.11 5195.81 122.17 o 13 3 1 335.80 302.89 53.50 o 14 3 1 510.96 583.78 68.37 o 15 3 1 48.75 82.59 58.45 o 16 3 1 106.95 88.64 82.45 o 17 3 1 809.71 990.63 150.36 o -17 4 1 1118.04 1228.10 148.09 o -16 4 1 133.24 132.17 90.52 o -15 4 1 19.45 -20.13 56.61 o -14 4 1 138.14 161.39 59.90 o -13 4 1 1812.08 1891.67 178.80 o -12 4 1 18806.06 19971.52 473.26 o -11 4 1 265.83 241.59 59.60 o -10 4 1 4510.61 4577.81 180.20 o -9 4 1 419.93 501.32 121.50 o -8 4 1 5181.67 5349.83 133.25 o -7 4 1 112.86 142.08 18.05 o -6 4 1 33300.42 34996.09 511.11 o -5 4 1 26016.62 27054.41 340.39 o -4 4 1 6878.91 6528.45 86.61 o -3 4 1 1770.89 1699.51 39.74 o -2 4 1 3441.78 3465.37 62.10 o -1 4 1 10473.13 10168.58 186.24 o 0 4 1 165564.47 146485.36 4764.76 o 1 4 1 64896.00 64294.34 1307.74 o 2 4 1 8513.85 8430.26 97.84 o 3 4 1 9916.63 8956.05 103.13 o 4 4 1 5914.45 6360.74 77.84 o 5 4 1 108767.84 105503.32 2529.99 o 6 4 1 66.19 47.16 20.81 o 7 4 1 3050.14 2654.97 56.02 o 8 4 1 498.67 532.30 31.89 o 9 4 1 80.83 137.25 32.60 o 10 4 1 2190.19 2287.90 101.88 o 11 4 1 7415.07 8007.58 194.89 o 12 4 1 1102.21 1235.72 68.63 o 13 4 1 1565.29 1648.02 100.76 o 14 4 1 17.19 78.54 58.17 o 15 4 1 251.64 228.31 59.71 o 16 4 1 20.45 -1.20 91.93 o -16 5 1 69.53 32.59 73.37 o -15 5 1 63.90 152.63 61.10 o -14 5 1 3.84 60.79 64.99 o -13 5 1 3511.41 3881.66 176.00 o -12 5 1 4458.14 4667.43 213.41 o -11 5 1 111.39 196.71 108.89 o -10 5 1 96.50 116.21 67.96 o -9 5 1 2042.62 2289.46 81.25 o -8 5 1 995.14 1086.45 36.64 o -7 5 1 13768.59 13569.11 167.53 o -6 5 1 15044.69 14305.13 192.17 o -5 5 1 104507.27 105276.02 2959.31 o -4 5 1 6607.27 6621.69 96.25 o -3 5 1 5763.56 5322.99 86.62 o -2 5 1 0.15 15.43 25.69 o -1 5 1 11182.89 11322.43 184.94 o 0 5 1 65840.77 63342.30 1293.75 o 1 5 1 969.25 1059.10 40.96 o 2 5 1 7689.20 7260.27 130.18 o 3 5 1 278.31 278.65 26.91 o 4 5 1 5521.09 5611.04 103.08 o 5 5 1 14527.83 14272.53 191.44 o 6 5 1 13656.50 13346.42 170.08 o 7 5 1 25.52 46.02 22.40 o 8 5 1 1581.88 1454.44 68.07 o 9 5 1 1532.93 1599.65 133.23 o 10 5 1 20633.97 20906.14 345.90 o 11 5 1 1216.18 1207.21 91.51 o 12 5 1 2469.87 2549.41 119.93 o 13 5 1 1397.93 1593.16 105.47 o 14 5 1 112.29 32.95 57.43 o 15 5 1 47.41 50.73 68.02 o 16 5 1 104.67 107.16 70.51 o -16 6 1 0.48 -91.27 91.27 o -15 6 1 49.35 37.54 79.74 o -14 6 1 77.74 26.69 71.17 o -13 6 1 4583.56 4798.07 176.57 o -12 6 1 7322.69 7667.13 227.96 o -11 6 1 2647.44 2829.43 145.93 o -10 6 1 9625.99 9726.67 287.52 o -9 6 1 417.97 394.38 39.14 o -8 6 1 6642.16 6407.37 233.78 o -7 6 1 14979.96 14949.55 210.95 o -6 6 1 11592.89 11372.09 143.45 o -5 6 1 35623.23 35187.86 659.62 o -4 6 1 569.41 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92.08 o -5 3 27 222.84 109.17 75.43 o -4 3 27 48.06 62.62 73.43 o -3 3 27 55.42 64.44 73.70 o -2 3 27 118.42 38.26 58.64 o -1 3 27 82.96 -120.39 183.08 o 0 3 27 88.68 18.62 67.58 o 1 3 27 242.27 181.33 137.14 o 2 3 27 103.48 59.77 82.01 o 3 3 27 3.90 -66.59 234.51 o -8 4 27 6.11 42.17 91.44 o -7 4 27 1188.76 1062.27 91.00 o -6 4 27 342.02 395.87 76.05 o -5 4 27 301.33 343.24 61.66 o -4 4 27 0.34 42.19 50.61 o -3 4 27 185.07 -4.86 49.81 o -2 4 27 346.73 235.74 66.78 o -1 4 27 316.30 321.94 98.34 o 0 4 27 47.33 209.74 127.71 o 1 4 27 83.38 150.54 85.88 o 2 4 27 137.30 61.44 81.11 o -7 5 27 12.44 114.99 122.76 o -6 5 27 1906.61 1953.74 169.89 o -5 5 27 0.03 99.16 58.65 o -4 5 27 42.01 78.70 62.93 o -3 5 27 9.68 87.42 55.98 o -2 5 27 1099.50 1119.21 141.69 o -1 5 27 111.14 299.59 108.69 o 0 5 27 94.74 106.87 93.68 o 1 5 27 348.53 378.48 92.58 o -6 6 27 26.94 63.68 77.91 o -5 6 27 838.35 672.43 75.81 o -4 6 27 76.60 23.95 62.42 o -3 6 27 95.36 -106.82 161.81 o -2 6 27 15.50 -120.64 120.64 o 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109.69 o -5 3 28 13.10 -26.38 72.39 o -4 3 28 38.44 34.93 64.91 o -3 3 28 7.77 14.98 71.39 o -2 3 28 354.44 479.27 112.48 o -1 3 28 369.20 206.28 95.89 o 0 3 28 81.15 40.86 104.34 o 1 3 28 63.04 -5.48 68.25 o -6 4 28 64.85 20.36 60.89 o -5 4 28 534.74 528.54 101.70 o -4 4 28 1.20 53.19 58.75 o -3 4 28 16.16 -16.74 55.09 o -2 4 28 1.27 125.71 108.84 o -1 4 28 454.06 680.86 130.24 o 0 4 28 233.57 116.74 102.74 o -4 5 28 309.33 254.43 73.45 o -3 5 28 47.91 -31.00 87.87 o -2 5 28 136.67 171.69 96.87 o -4 1 29 82.69 146.47 97.93 o -3 1 29 39.63 -81.40 116.68 o -2 1 29 200.40 95.02 66.47 o -3 2 29 27.14 -47.51 214.17 o