#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/28/2212845.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212845_Fobs loop_ _publ_author_name 'Zhai, Jun' 'Yin, Han-Dong' 'Li, Feng' 'Chen, Shao-Wen' 'Wang, Da-Qi' _publ_section_title ; Bis(N,N-dibenzylthiocarbamoyl) disulfide ; _journal_coeditor_code CV2217 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1969 _journal_page_last o1970 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 115.860 _cell_angle_gamma 90.000 _cell_length_a 19.5460 _cell_length_b 14.3253 _cell_length_c 21.9582 _exptl_crystal_F_000 2288.00 _reflns_d_resolution_high 0.8406 _[local]_cod_data_source_file cv2217Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 061214b in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 643.28 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 127563.57 133935.64 1237.28 o 4 0 0 54136.25 57498.50 859.95 o 6 0 0 50045.13 49456.10 496.06 o 8 0 0 14921.19 15201.78 218.84 o 10 0 0 1960.72 1652.05 90.91 o 12 0 0 1258.80 1238.24 107.91 o 14 0 0 5056.63 4944.77 155.32 o 16 0 0 53.29 -53.14 108.35 o 18 0 0 0.23 -126.20 110.84 o 20 0 0 42.90 -153.60 123.29 o 1 1 0 6966.83 7079.74 86.28 o 3 1 0 481.19 485.92 62.46 o 5 1 0 61913.32 62054.68 619.81 o 7 1 0 12103.56 12201.95 127.56 o 9 1 0 5608.60 5731.49 91.90 o 11 1 0 2118.12 1987.49 89.09 o 13 1 0 891.47 941.66 63.12 o 15 1 0 32.39 33.93 54.80 o 17 1 0 15.55 -68.85 70.30 o 19 1 0 4.56 -41.87 84.34 o 0 2 0 36344.63 36838.23 354.91 o 2 2 0 3114.96 3230.57 91.54 o 4 2 0 425.18 364.61 41.84 o 6 2 0 8946.41 8605.20 103.06 o 8 2 0 718.26 782.02 39.70 o 10 2 0 3.05 -28.18 25.76 o 12 2 0 1396.10 1295.37 95.45 o 14 2 0 18.42 33.98 55.37 o 16 2 0 359.28 378.92 70.53 o 18 2 0 274.15 177.64 97.26 o 20 2 0 263.27 303.31 111.15 o 1 3 0 30673.22 32834.96 201.51 o 3 3 0 3554.83 3231.44 53.13 o 5 3 0 4856.57 4578.49 66.25 o 7 3 0 312.28 378.08 29.26 o 9 3 0 446.21 434.50 34.89 o 11 3 0 1029.69 1095.22 76.38 o 13 3 0 1183.71 1160.19 139.04 o 15 3 0 1669.33 1701.69 102.42 o 17 3 0 580.44 566.63 82.82 o 19 3 0 195.06 288.65 100.70 o 0 4 0 122.31 193.73 36.86 o 2 4 0 1854.86 2034.02 34.33 o 4 4 0 4895.62 5075.41 74.84 o 6 4 0 1212.44 1114.60 70.52 o 8 4 0 212.42 135.90 27.33 o 10 4 0 2932.58 2699.03 91.57 o 12 4 0 2.56 -59.14 44.40 o 14 4 0 1140.90 1204.42 93.64 o 16 4 0 77.31 233.32 69.38 o 18 4 0 90.06 118.06 95.94 o 20 4 0 52.38 -9.29 91.17 o 1 5 0 532.37 498.19 24.99 o 3 5 0 29213.43 29784.06 263.47 o 5 5 0 3875.12 3957.77 103.17 o 7 5 0 3.80 -63.41 42.38 o 9 5 0 6038.61 5631.08 158.40 o 11 5 0 1337.90 1357.45 121.92 o 13 5 0 224.27 172.39 63.58 o 15 5 0 240.54 135.04 66.39 o 17 5 0 278.66 328.91 80.80 o 19 5 0 1075.34 1200.52 220.00 o 0 6 0 213.64 172.71 32.07 o 2 6 0 1986.57 1980.91 42.32 o 4 6 0 81.31 36.75 23.18 o 6 6 0 6917.74 7306.03 300.08 o 8 6 0 4788.89 5258.57 155.05 o 10 6 0 3856.65 3792.95 146.39 o 12 6 0 3324.33 3446.78 123.52 o 14 6 0 597.49 500.07 76.48 o 16 6 0 23.85 -30.27 78.76 o 18 6 0 223.55 136.07 75.10 o 1 7 0 214.39 206.84 25.12 o 3 7 0 699.47 772.24 34.94 o 5 7 0 7142.03 7522.09 145.84 o 7 7 0 4332.40 3950.11 165.41 o 9 7 0 398.24 415.52 88.42 o 11 7 0 1131.42 1096.76 114.33 o 13 7 0 872.51 990.65 91.17 o 15 7 0 105.09 71.84 65.58 o 17 7 0 8.29 -33.73 67.76 o 19 7 0 1.15 -30.71 94.98 o 0 8 0 11116.65 11513.99 162.07 o 2 8 0 292.92 338.92 30.59 o 4 8 0 8362.12 8810.45 145.08 o 6 8 0 826.03 797.06 49.78 o 8 8 0 64.24 26.44 66.04 o 10 8 0 2608.18 2548.56 237.02 o 12 8 0 84.29 32.37 75.49 o 14 8 0 692.16 792.30 89.91 o 16 8 0 78.65 -22.88 91.84 o 18 8 0 39.98 -95.70 95.11 o 1 9 0 617.52 688.31 39.52 o 3 9 0 272.58 226.38 30.85 o 5 9 0 773.88 722.11 57.93 o 7 9 0 656.14 649.24 67.24 o 9 9 0 337.08 242.94 62.98 o 11 9 0 1.21 -55.95 74.81 o 13 9 0 501.04 436.26 104.52 o 15 9 0 39.80 -73.92 79.35 o 17 9 0 27.54 -26.03 88.52 o 0 10 0 921.98 912.33 67.30 o 2 10 0 0.40 -39.39 26.26 o 4 10 0 50.57 -21.38 34.68 o 6 10 0 439.38 415.01 67.68 o 8 10 0 212.28 205.91 65.49 o 10 10 0 15.94 -72.22 52.90 o 12 10 0 153.28 151.66 83.46 o 14 10 0 331.51 470.18 120.59 o 16 10 0 771.97 600.05 123.18 o 1 11 0 267.96 136.98 35.66 o 3 11 0 9265.54 9068.05 117.56 o 5 11 0 1889.93 1828.43 79.23 o 7 11 0 1570.16 1556.25 101.26 o 9 11 0 37.46 11.53 58.90 o 11 11 0 1323.25 1600.74 119.98 o 13 11 0 656.46 831.10 95.64 o 15 11 0 15.98 -89.87 89.61 o 0 12 0 101.32 54.19 74.50 o 2 12 0 49.40 1.30 33.99 o 4 12 0 36.01 -7.01 49.59 o 6 12 0 1544.04 1641.81 106.96 o 8 12 0 63.26 47.55 61.36 o 10 12 0 25.61 -35.91 59.53 o 12 12 0 525.00 524.28 89.34 o 14 12 0 535.65 758.62 136.92 o 1 13 0 80.32 64.21 38.94 o 3 13 0 310.99 323.85 60.09 o 5 13 0 332.75 340.00 84.64 o 7 13 0 506.88 614.07 84.70 o 9 13 0 270.07 230.55 75.85 o 11 13 0 49.33 -5.93 85.56 o 13 13 0 30.15 -68.65 85.21 o 0 14 0 56.74 -78.01 69.61 o 2 14 0 148.05 53.44 49.50 o 4 14 0 246.19 207.64 62.14 o 6 14 0 11.42 -60.78 58.83 o 8 14 0 10.40 -91.79 61.19 o 10 14 0 505.29 611.52 124.82 o 1 15 0 253.84 233.91 73.32 o 3 15 0 332.11 293.50 80.02 o 5 15 0 76.20 68.81 88.49 o 7 15 0 158.22 243.66 99.34 o 9 15 0 7.77 -127.84 85.23 o 0 16 0 189.26 156.08 136.98 o 2 16 0 98.02 38.83 89.48 o 4 16 0 531.32 379.90 118.48 o 6 16 0 3.53 -68.91 135.75 o 1 17 0 58.84 -208.60 139.07 o -21 1 1 2.02 -107.82 83.99 o -19 1 1 5.12 -62.78 78.80 o -17 1 1 303.92 101.88 79.04 o -15 1 1 363.54 326.61 63.31 o -13 1 1 7773.17 7439.48 127.33 o -11 1 1 6876.59 6612.18 107.60 o -9 1 1 1890.45 1597.07 55.67 o -7 1 1 31764.29 31323.62 291.77 o -5 1 1 16711.38 16964.55 144.18 o -3 1 1 45710.76 47968.45 429.62 o -1 1 1 20789.17 22319.72 337.41 o 1 1 1 30884.66 32107.38 1004.00 o 3 1 1 71023.73 75735.01 580.48 o 5 1 1 11696.14 11965.35 116.18 o 7 1 1 2967.36 2998.43 61.32 o 9 1 1 5253.36 5024.82 99.77 o 11 1 1 9652.51 9261.92 132.79 o 13 1 1 5289.58 5177.94 131.64 o 15 1 1 570.95 603.73 100.10 o 17 1 1 273.20 205.60 91.12 o 19 1 1 417.77 370.43 108.96 o -20 2 1 216.56 309.87 97.86 o -18 2 1 89.56 -3.11 80.84 o -16 2 1 1076.29 938.98 86.42 o -14 2 1 335.52 264.32 62.73 o -12 2 1 1265.70 1251.74 81.12 o -10 2 1 965.78 976.79 47.53 o -8 2 1 34.05 34.33 22.52 o -6 2 1 1929.21 1878.38 42.66 o -4 2 1 24237.24 24715.33 218.19 o -2 2 1 425.14 405.33 18.62 o 0 2 1 17865.28 17552.31 112.48 o 2 2 1 3608.09 3417.54 72.42 o 4 2 1 18623.26 18943.16 236.40 o 6 2 1 38633.36 39561.21 1022.08 o 8 2 1 13760.53 13952.80 146.73 o 10 2 1 63.04 80.01 31.56 o 12 2 1 492.80 500.31 66.39 o 14 2 1 3559.26 3374.99 116.54 o 16 2 1 0.06 -50.65 69.62 o 18 2 1 362.41 328.56 101.37 o 20 2 1 18.60 -37.33 83.56 o -19 3 1 45.46 -68.36 82.10 o -17 3 1 100.28 132.26 65.25 o -15 3 1 94.99 48.65 58.69 o -13 3 1 110.44 37.23 50.99 o -11 3 1 164.27 171.48 35.52 o -9 3 1 2990.49 3425.84 67.65 o -7 3 1 13569.36 12959.94 130.07 o -5 3 1 75.16 85.65 18.89 o -3 3 1 1651.00 1470.85 44.64 o -1 3 1 101679.66 103720.39 542.62 o 1 3 1 3212.64 3284.50 42.54 o 3 3 1 17323.89 17466.07 221.58 o 5 3 1 11.83 -29.65 32.30 o 7 3 1 755.28 627.65 31.97 o 9 3 1 4522.50 4221.26 75.40 o 11 3 1 230.44 274.71 56.47 o 13 3 1 256.78 362.98 64.58 o 15 3 1 1.10 -77.76 51.84 o 17 3 1 776.20 709.12 115.60 o 19 3 1 180.16 57.07 97.15 o -20 4 1 112.25 -3.76 94.36 o -18 4 1 1413.30 1661.34 119.49 o -16 4 1 2111.32 2265.15 124.53 o -14 4 1 118.35 32.57 52.70 o -12 4 1 2278.92 2102.39 90.97 o -10 4 1 5722.88 5363.34 89.64 o -8 4 1 1266.53 1044.85 47.54 o -6 4 1 12985.72 13267.69 274.17 o -4 4 1 4516.21 4472.41 65.11 o -2 4 1 633.46 732.55 29.95 o 0 4 1 990.60 1160.00 28.18 o 2 4 1 3152.12 3083.41 47.02 o 4 4 1 567.99 833.42 95.25 o 6 4 1 4063.31 4263.26 119.61 o 8 4 1 13267.62 13002.08 322.14 o 10 4 1 5671.17 5455.74 126.97 o 12 4 1 516.89 563.86 72.44 o 14 4 1 894.57 860.91 122.10 o 16 4 1 90.27 28.38 66.37 o 18 4 1 151.51 14.82 146.53 o -19 5 1 48.48 84.61 70.45 o -17 5 1 79.11 -18.48 64.44 o -15 5 1 399.71 361.60 116.93 o -13 5 1 6836.70 6898.74 158.27 o -11 5 1 9075.91 8755.20 162.41 o -9 5 1 7.82 -3.79 28.85 o -7 5 1 6269.90 6459.19 74.54 o -5 5 1 32381.79 33361.39 546.76 o -3 5 1 154.22 152.19 21.38 o -1 5 1 14248.44 14821.76 113.29 o 1 5 1 5261.64 5488.39 61.75 o 3 5 1 32477.18 32398.99 326.92 o 5 5 1 6513.94 6464.47 146.60 o 7 5 1 327.61 280.98 59.62 o 9 5 1 2928.72 2824.03 121.31 o 11 5 1 45.44 -44.87 44.44 o 13 5 1 29.26 42.41 54.42 o 15 5 1 274.27 361.08 75.65 o 17 5 1 622.13 793.44 101.57 o 19 5 1 669.02 971.37 174.36 o -18 6 1 27.20 44.51 70.54 o -16 6 1 1317.21 1657.73 114.32 o -14 6 1 180.32 203.37 64.16 o -12 6 1 187.91 172.28 58.53 o -10 6 1 497.75 630.56 87.91 o -8 6 1 6884.38 7489.06 144.14 o -6 6 1 1.27 14.02 27.27 o -4 6 1 18958.34 19553.38 171.71 o -2 6 1 19980.85 20536.46 150.66 o 0 6 1 11485.86 11689.73 104.55 o 2 6 1 127.75 49.17 19.18 o 4 6 1 12519.99 12297.10 168.85 o 6 6 1 17518.86 18010.32 720.05 o 8 6 1 9988.91 9647.62 382.96 o 10 6 1 330.20 471.81 88.64 o 12 6 1 5687.68 5684.39 147.11 o 14 6 1 203.32 77.79 61.58 o 16 6 1 384.70 277.38 81.85 o 18 6 1 617.05 505.57 94.84 o -19 7 1 94.73 95.36 103.15 o -17 7 1 758.80 1005.12 138.65 o -15 7 1 2.91 -83.67 56.70 o -13 7 1 1910.41 1835.21 199.29 o -11 7 1 1008.84 933.75 108.16 o -9 7 1 2934.41 2738.10 127.98 o -7 7 1 44.04 98.03 34.40 o -5 7 1 6782.59 6392.36 102.11 o -3 7 1 590.05 593.06 33.54 o -1 7 1 2927.50 3006.79 54.36 o 1 7 1 377.83 373.86 30.64 o 3 7 1 1088.44 1153.98 43.01 o 5 7 1 536.38 549.25 41.46 o 7 7 1 228.01 167.74 64.85 o 9 7 1 72.30 24.71 66.21 o 11 7 1 409.07 519.65 97.05 o 13 7 1 5.73 -34.65 55.97 o 15 7 1 206.50 185.43 70.06 o 17 7 1 386.42 392.84 85.08 o -18 8 1 41.24 -27.66 87.59 o -16 8 1 213.15 89.43 107.30 o -14 8 1 1487.39 1506.72 141.05 o -12 8 1 1482.22 1867.97 135.89 o -10 8 1 805.33 809.01 101.81 o -8 8 1 3538.61 3497.77 114.05 o -6 8 1 3939.55 3952.50 86.72 o -4 8 1 3564.17 3406.88 70.46 o -2 8 1 215.61 221.75 27.76 o 0 8 1 922.28 999.45 41.67 o 2 8 1 3271.39 3215.17 59.37 o 4 8 1 516.17 428.65 41.67 o 6 8 1 13.20 -20.06 48.76 o 8 8 1 54.10 73.58 65.56 o 10 8 1 507.47 526.52 98.94 o 12 8 1 4.02 -97.96 113.95 o 14 8 1 121.20 -8.02 66.31 o 16 8 1 62.22 47.73 71.79 o 18 8 1 3.31 -137.71 91.81 o -17 9 1 140.08 -67.12 86.42 o -15 9 1 339.63 368.01 104.20 o -13 9 1 151.75 96.33 84.57 o -11 9 1 36.63 13.42 74.80 o -9 9 1 965.57 955.67 81.56 o -7 9 1 713.81 806.67 73.48 o -5 9 1 508.67 601.56 47.10 o -3 9 1 589.98 448.36 35.95 o -1 9 1 60.22 15.36 25.15 o 1 9 1 958.04 984.25 43.49 o 3 9 1 1492.73 1508.13 54.56 o 5 9 1 2.66 -59.49 39.66 o 7 9 1 1035.20 978.65 79.89 o 9 9 1 2468.07 2544.55 239.72 o 11 9 1 137.28 57.38 80.06 o 13 9 1 1182.71 1366.73 193.85 o 15 9 1 57.01 100.31 94.03 o 17 9 1 15.04 -71.68 85.26 o -16 10 1 9.28 11.58 92.98 o -14 10 1 866.47 912.03 134.76 o -12 10 1 104.84 198.53 93.19 o -10 10 1 8.68 -59.16 55.21 o -8 10 1 113.89 99.23 66.15 o -6 10 1 2420.18 2309.95 120.71 o -4 10 1 2648.77 2584.88 77.47 o -2 10 1 1360.14 1416.56 53.59 o 0 10 1 43.94 -13.19 27.59 o 2 10 1 2386.63 2403.66 61.28 o 4 10 1 2060.93 1910.49 77.01 o 6 10 1 1843.31 1805.93 90.10 o 8 10 1 1719.98 1814.37 108.02 o 10 10 1 396.81 373.44 70.88 o 12 10 1 210.40 317.55 97.95 o 14 10 1 166.09 147.35 103.12 o 16 10 1 487.17 341.57 123.21 o -13 11 1 1216.13 1438.62 112.71 o -11 11 1 182.43 202.46 67.55 o -9 11 1 381.65 399.58 73.56 o -7 11 1 337.94 345.25 70.62 o -5 11 1 180.22 187.51 52.65 o -3 11 1 1556.07 1475.59 55.54 o -1 11 1 953.12 939.42 58.58 o 1 11 1 433.94 375.70 40.82 o 3 11 1 515.16 653.84 63.17 o 5 11 1 309.20 429.65 72.48 o 7 11 1 2136.15 2141.68 100.99 o 9 11 1 1393.57 1376.93 102.82 o 11 11 1 5.20 -65.48 56.84 o 13 11 1 1535.73 1826.62 117.86 o 15 11 1 1058.12 1285.08 156.91 o -14 12 1 433.13 365.50 116.83 o -12 12 1 170.52 20.03 91.28 o -10 12 1 513.74 611.98 85.85 o -8 12 1 732.80 886.54 88.76 o -6 12 1 1082.18 1205.70 108.06 o -4 12 1 2091.53 2027.11 92.46 o -2 12 1 119.05 62.35 36.17 o 0 12 1 2377.01 2146.49 65.25 o 2 12 1 40.02 -38.57 36.09 o 4 12 1 2234.89 2155.45 88.24 o 6 12 1 2657.99 2473.57 109.35 o 8 12 1 825.07 808.80 90.21 o 10 12 1 607.81 765.27 95.08 o 12 12 1 456.91 403.01 88.31 o 14 12 1 73.89 189.48 79.76 o -13 13 1 179.84 68.98 97.84 o -11 13 1 457.16 600.99 228.71 o -9 13 1 141.86 154.75 86.77 o -7 13 1 2.29 -85.48 56.99 o -5 13 1 7.63 -3.87 50.18 o -3 13 1 358.87 378.32 62.66 o -1 13 1 566.07 616.50 59.48 o 1 13 1 2.33 -53.71 35.81 o 3 13 1 116.60 137.83 52.08 o 5 13 1 193.30 96.71 62.33 o 7 13 1 157.36 164.58 68.37 o 9 13 1 133.04 258.18 73.33 o 11 13 1 233.56 110.03 72.73 o 13 13 1 143.31 255.19 111.26 o -12 14 1 127.66 172.95 103.36 o -10 14 1 46.02 91.34 97.88 o -8 14 1 20.44 -25.98 77.13 o -6 14 1 216.91 177.98 69.48 o -4 14 1 557.99 467.85 76.33 o -2 14 1 262.32 148.07 55.49 o 0 14 1 118.39 90.39 65.22 o 2 14 1 17.93 0.94 63.46 o 4 14 1 636.37 439.30 132.90 o 6 14 1 63.56 31.65 62.74 o 8 14 1 131.53 43.20 159.39 o 10 14 1 70.66 3.65 88.86 o -9 15 1 164.76 148.73 192.40 o -7 15 1 1.88 -66.87 91.12 o -5 15 1 146.24 153.73 75.86 o -3 15 1 1.01 -21.63 69.12 o -1 15 1 26.14 19.06 75.33 o 1 15 1 44.09 -68.33 65.99 o 3 15 1 199.40 212.87 77.97 o 5 15 1 8.58 -98.88 83.36 o 7 15 1 82.74 44.92 71.66 o 9 15 1 301.66 427.78 215.03 o -6 16 1 85.65 64.34 136.98 o -4 16 1 110.46 210.64 106.58 o -2 16 1 0.35 42.75 149.02 o 0 16 1 29.80 -106.57 84.84 o 2 16 1 0.02 72.25 76.27 o 4 16 1 243.27 233.26 111.16 o 6 16 1 2.01 -160.24 128.69 o -1 17 1 98.69 -29.89 139.47 o -20 0 2 15.64 12.87 126.61 o -18 0 2 167.91 228.31 132.00 o -16 0 2 2604.36 2129.89 173.53 o -14 0 2 49.43 -26.47 52.13 o -12 0 2 1490.84 1493.04 145.30 o -10 0 2 1432.56 1499.22 96.93 o -8 0 2 57622.05 60255.07 703.86 o -6 0 2 30500.85 30296.48 328.02 o -4 0 2 198.47 194.80 29.58 o -2 0 2 1840.75 1812.10 28.00 o 0 0 2 22186.79 21369.04 305.12 o 2 0 2 33617.39 32760.32 453.74 o 4 0 2 413805.13 404642.91 11719.03 o 6 0 2 9213.39 8807.48 148.30 o 8 0 2 7090.24 6775.32 142.09 o 10 0 2 40229.09 40309.76 475.87 o 12 0 2 17184.65 17034.66 282.21 o 14 0 2 3145.54 2966.30 210.47 o 16 0 2 877.74 1049.38 169.79 o 18 0 2 421.76 341.21 153.59 o 20 0 2 0.01 -114.99 124.96 o -21 1 2 62.04 -32.79 90.42 o -19 1 2 538.00 425.16 106.85 o -17 1 2 603.48 561.06 100.15 o -15 1 2 13.56 24.20 51.05 o -13 1 2 34.79 -43.57 35.21 o -11 1 2 100.62 113.61 32.11 o -9 1 2 1426.11 1389.40 48.00 o -7 1 2 849.13 755.80 36.04 o -5 1 2 159.69 133.19 21.90 o -3 1 2 9418.07 10217.93 87.29 o -1 1 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