#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2212873.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212873_Fobs loop_ _publ_author_name 'Portilla, Jaime' 'Cobo, Justo' 'Torre, Jos\'e M. de la' 'Low, John N.' 'Glidewell, Christopher' _publ_section_title ; N,N'-Bis(isonicotinoyl)hydrazine dihydrate at 120(2)K: a three-dimensional framework built from N---H···O, O---H···O, O---H···N and C---H···O hydrogen bonds ; _journal_coeditor_code GG3079 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1687 _journal_page_last o1690 _journal_volume 63 _journal_year 2007 _space_group_IT_number 43 _symmetry_space_group_name_Hall 'F 2 -2d' _symmetry_space_group_name_H-M 'F d d 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 28.1492 _cell_length_b 24.1628 _cell_length_c 3.7181 _exptl_crystal_F_000 1168.00 _reflns_d_resolution_high 0.7689 _[local]_cod_data_source_file gg3079Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Compound X Fdd2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 323.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x+1/4, y+1/4, z+1/4' 'x+3/4, -y+3/4, z+1/4' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' '-x+1/4, y+3/4, z+3/4' 'x+3/4, -y+5/4, z+3/4' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' '-x+3/4, y+1/4, z+3/4' 'x+5/4, -y+3/4, z+3/4' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' '-x+3/4, y+3/4, z+1/4' 'x+5/4, -y+5/4, z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 8 0 0 4142.36 3767.61 55.89 o 12 0 0 9921.88 10560.21 113.92 o 16 0 0 282.55 181.86 12.28 o 20 0 0 5354.24 4534.81 73.86 o 24 0 0 15748.39 17439.49 299.39 o 28 0 0 5324.18 6806.00 239.10 o 32 0 0 389.23 497.49 73.69 o 36 0 0 2682.22 3315.52 237.41 o 6 2 0 7157.93 6000.05 43.95 o 8 2 0 2113.73 1894.46 18.39 o 10 2 0 231.99 182.55 5.77 o 12 2 0 41723.61 41142.35 290.53 o 14 2 0 890.61 864.91 14.47 o 16 2 0 4533.06 4211.13 41.38 o 18 2 0 29.77 18.49 8.01 o 20 2 0 2605.71 2613.26 36.46 o 22 2 0 6533.40 6632.94 83.99 o 24 2 0 4132.21 4248.19 61.23 o 26 2 0 8.19 5.40 18.32 o 28 2 0 1.86 -16.33 24.39 o 30 2 0 425.43 522.20 42.54 o 32 2 0 114.41 101.10 35.65 o 34 2 0 115.14 71.55 64.44 o 36 2 0 218.51 290.53 78.19 o 4 4 0 7749.54 7043.36 58.70 o 6 4 0 2748.61 2535.58 25.98 o 8 4 0 8289.21 6581.55 51.95 o 10 4 0 5793.28 5900.27 48.60 o 12 4 0 9787.96 9445.09 72.52 o 14 4 0 4625.05 4215.64 39.19 o 16 4 0 1730.25 1776.93 26.28 o 18 4 0 41.02 52.30 8.94 o 20 4 0 3014.83 2915.93 43.41 o 22 4 0 854.87 795.39 26.24 o 24 4 0 5555.97 5457.45 80.91 o 26 4 0 249.32 229.58 22.95 o 28 4 0 369.15 405.54 32.39 o 30 4 0 2.71 29.33 28.55 o 32 4 0 18.70 -32.21 39.27 o 34 4 0 263.67 297.61 52.83 o 36 4 0 751.69 1102.84 85.01 o 2 6 0 231.45 156.95 5.22 o 4 6 0 17621.43 16976.33 137.67 o 6 6 0 4.41 -0.08 4.02 o 8 6 0 31584.80 31024.80 230.37 o 10 6 0 3067.25 2877.21 30.16 o 12 6 0 19544.02 19774.94 150.71 o 14 6 0 153.12 194.75 8.26 o 16 6 0 75.60 58.84 7.47 o 18 6 0 4013.68 3702.65 43.94 o 20 6 0 465.75 515.57 17.00 o 22 6 0 77.45 69.60 12.28 o 24 6 0 4069.11 5147.57 81.42 o 26 6 0 65.37 14.59 20.88 o 28 6 0 8.13 9.61 23.78 o 30 6 0 4.85 29.95 31.48 o 32 6 0 1092.80 1592.70 82.96 o 34 6 0 0.80 25.25 50.74 o 0 8 0 6583.87 6374.52 77.91 o 2 8 0 9784.99 9368.43 76.34 o 4 8 0 10209.99 9948.00 83.85 o 6 8 0 1084.25 815.17 14.47 o 8 8 0 8480.51 8551.85 74.71 o 10 8 0 1561.45 1416.67 20.83 o 12 8 0 3787.08 4337.91 45.00 o 14 8 0 1562.16 1359.97 23.48 o 16 8 0 2813.08 2701.07 35.39 o 18 8 0 171.84 118.91 12.19 o 20 8 0 3964.53 4308.87 64.52 o 22 8 0 271.03 223.26 18.91 o 24 8 0 7351.88 7696.38 116.70 o 26 8 0 11.48 12.46 21.74 o 28 8 0 111.01 32.27 28.96 o 30 8 0 192.40 119.47 35.58 o 32 8 0 64.28 49.21 38.03 o 34 8 0 218.33 288.89 79.96 o 2 10 0 3918.93 4035.98 38.44 o 4 10 0 16059.32 17155.43 135.66 o 6 10 0 6758.45 6518.07 59.35 o 8 10 0 2416.16 2332.03 29.85 o 10 10 0 435.87 505.81 13.27 o 12 10 0 12231.43 13650.44 116.78 o 14 10 0 1193.79 1069.00 23.17 o 16 10 0 327.49 337.16 15.43 o 18 10 0 856.25 738.68 31.52 o 20 10 0 1.86 27.00 13.66 o 22 10 0 1047.44 901.47 31.04 o 24 10 0 1207.86 1112.49 37.48 o 26 10 0 123.58 60.96 26.68 o 28 10 0 600.96 600.65 41.08 o 30 10 0 68.96 -22.62 35.72 o 32 10 0 73.05 -2.65 43.27 o 34 10 0 654.74 720.77 99.99 o 0 12 0 6483.90 6974.07 93.77 o 2 12 0 491.33 624.59 12.48 o 4 12 0 5339.39 6149.18 60.93 o 6 12 0 6018.55 5740.51 65.11 o 8 12 0 466.76 460.05 13.24 o 10 12 0 1818.79 1555.55 26.30 o 12 12 0 279.20 228.53 13.59 o 14 12 0 4452.53 4934.42 62.64 o 16 12 0 11.43 9.36 11.34 o 18 12 0 728.89 642.06 23.94 o 20 12 0 238.27 95.37 18.79 o 22 12 0 0.04 8.34 16.94 o 24 12 0 230.49 85.66 22.09 o 26 12 0 4.08 12.61 27.50 o 28 12 0 4.62 -11.10 33.69 o 30 12 0 411.35 386.45 48.13 o 32 12 0 384.55 321.36 60.60 o 2 14 0 45.11 40.56 6.89 o 4 14 0 2039.10 2453.67 32.52 o 6 14 0 1453.88 1149.54 22.60 o 8 14 0 481.84 412.43 13.66 o 10 14 0 216.55 198.97 13.46 o 12 14 0 93.80 57.37 11.81 o 14 14 0 2293.11 2162.01 38.64 o 16 14 0 3615.13 3531.35 63.62 o 18 14 0 1885.08 1802.16 44.32 o 20 14 0 86.37 53.76 19.05 o 22 14 0 125.03 78.57 20.69 o 24 14 0 71.07 14.30 23.78 o 26 14 0 483.58 552.36 42.59 o 28 14 0 3.02 11.00 36.62 o 30 14 0 0.80 4.90 42.98 o 32 14 0 89.39 104.16 52.20 o 0 16 0 18042.33 22981.73 312.30 o 2 16 0 9.99 -2.38 7.90 o 4 16 0 903.75 920.60 21.59 o 6 16 0 3565.50 3585.16 46.52 o 8 16 0 1471.32 1308.13 26.59 o 10 16 0 35.47 45.98 13.54 o 12 16 0 5656.66 5760.94 74.82 o 14 16 0 1206.48 1242.89 35.69 o 16 16 0 2724.45 3318.51 59.74 o 18 16 0 40.98 39.86 17.97 o 20 16 0 115.04 69.75 21.66 o 22 16 0 985.03 861.23 44.12 o 24 16 0 1260.01 1054.32 53.12 o 26 16 0 42.40 13.62 31.59 o 28 16 0 712.56 956.12 67.34 o 30 16 0 12.72 15.70 45.36 o 2 18 0 1248.40 1198.21 32.99 o 4 18 0 7.94 16.85 10.71 o 6 18 0 0.08 -0.75 9.85 o 8 18 0 267.85 192.78 15.33 o 10 18 0 5946.32 6834.82 86.24 o 12 18 0 14756.01 17734.36 213.88 o 14 18 0 1685.58 1831.32 43.38 o 16 18 0 23.87 16.59 20.40 o 18 18 0 704.28 684.05 34.49 o 20 18 0 110.77 49.88 24.86 o 22 18 0 363.53 280.07 35.26 o 24 18 0 1118.63 1371.84 58.45 o 26 18 0 44.55 -30.57 42.68 o 28 18 0 8.97 46.66 47.83 o 0 20 0 27.08 16.79 21.84 o 2 20 0 7.43 21.74 18.52 o 4 20 0 500.99 470.36 21.02 o 6 20 0 93.08 57.42 16.35 o 8 20 0 936.24 1091.76 30.07 o 10 20 0 7804.08 9628.60 132.20 o 12 20 0 268.80 187.78 26.16 o 14 20 0 1326.59 1556.48 46.26 o 16 20 0 520.35 515.52 36.44 o 18 20 0 1042.57 1130.21 45.99 o 20 20 0 132.49 39.65 31.17 o 22 20 0 18.21 29.44 30.42 o 24 20 0 64.24 34.71 43.23 o 26 20 0 723.22 979.92 70.81 o 28 20 0 80.42 56.57 62.11 o 2 22 0 4354.90 4982.89 129.50 o 4 22 0 490.76 448.29 31.61 o 6 22 0 104.47 69.63 21.44 o 8 22 0 1149.16 1411.99 41.18 o 10 22 0 1145.26 1448.25 44.30 o 12 22 0 5941.75 7482.59 123.30 o 14 22 0 104.55 41.07 29.67 o 16 22 0 451.44 470.99 39.30 o 18 22 0 309.61 303.09 37.80 o 20 22 0 85.01 25.18 40.16 o 22 22 0 122.09 122.36 49.27 o 24 22 0 921.73 1160.45 75.93 o 26 22 0 777.63 981.74 104.23 o 0 24 0 1971.16 2232.23 131.01 o 2 24 0 496.10 350.07 36.85 o 4 24 0 44.68 44.65 30.17 o 6 24 0 1.06 -2.97 30.36 o 8 24 0 0.18 17.87 30.24 o 10 24 0 0.03 -10.81 30.78 o 12 24 0 1000.69 1109.22 56.91 o 14 24 0 4.87 20.15 32.88 o 16 24 0 425.16 491.39 52.80 o 18 24 0 579.12 606.50 53.00 o 20 24 0 379.06 271.67 93.51 o 22 24 0 87.72 -23.65 50.10 o 2 26 0 13.22 52.24 33.63 o 4 26 0 41.97 17.04 34.95 o 6 26 0 404.57 262.72 46.25 o 8 26 0 715.00 650.16 50.36 o 10 26 0 773.70 874.71 64.11 o 12 26 0 55.28 -18.94 37.62 o 14 26 0 349.12 390.93 47.44 o 16 26 0 47.89 76.26 45.50 o 18 26 0 319.77 225.58 79.37 o 20 26 0 42.25 21.67 52.18 o 0 28 0 1174.35 1196.02 125.29 o 2 28 0 992.52 1175.32 76.19 o 4 28 0 16.93 -27.42 37.77 o 6 28 0 575.79 474.11 47.13 o 8 28 0 105.00 -17.46 45.45 o 10 28 0 266.84 226.96 50.16 o 12 28 0 8.71 41.49 43.89 o 14 28 0 610.40 589.87 129.22 o 16 28 0 169.93 45.44 55.05 o 2 30 0 229.18 202.80 60.02 o 4 30 0 402.83 477.76 68.75 o 6 30 0 558.38 649.79 72.16 o 8 30 0 220.44 83.46 48.96 o 10 30 0 85.24 65.34 49.45 o 1 1 1 35626.30 33054.00 154.02 o 3 1 1 22590.14 21884.75 109.10 o 5 1 1 1745.61 1484.60 11.40 o 7 1 1 10562.77 10459.79 53.86 o 9 1 1 3395.21 2927.06 19.82 o 11 1 1 3558.13 3601.45 25.55 o 13 1 1 4002.05 3980.03 28.17 o 15 1 1 1287.82 1184.47 14.84 o 17 1 1 2899.52 2856.55 27.20 o 19 1 1 4469.10 4607.50 40.07 o 21 1 1 2613.62 2643.07 29.53 o 23 1 1 4641.09 4784.57 50.98 o 25 1 1 21.74 22.11 14.30 o 27 1 1 347.37 340.26 23.96 o 29 1 1 113.13 96.70 22.40 o 31 1 1 59.50 60.70 24.38 o 33 1 1 1.88 13.18 29.75 o 35 1 1 509.07 493.39 53.77 o 1 3 1 104971.34 96063.79 468.93 o 3 3 1 8509.23 8404.69 47.24 o 5 3 1 19657.68 19057.05 99.29 o 7 3 1 3079.57 2960.22 20.52 o 9 3 1 15117.30 15298.56 80.88 o 11 3 1 2551.10 2430.31 18.91 o 13 3 1 5508.97 5741.23 36.38 o 15 3 1 3185.53 3149.10 25.06 o 17 3 1 934.71 727.81 13.29 o 19 3 1 1360.77 1346.82 19.61 o 21 3 1 2664.10 2723.69 34.06 o 23 3 1 9303.88 10898.91 97.76 o 25 3 1 1150.49 1226.86 33.80 o 27 3 1 420.10 502.58 25.56 o 29 3 1 570.26 581.86 33.93 o 31 3 1 315.37 329.63 29.54 o 33 3 1 483.99 683.21 40.57 o 35 3 1 577.22 598.13 52.57 o 1 5 1 10740.51 10119.85 50.84 o 3 5 1 31013.88 29971.35 145.14 o 5 5 1 1160.40 1059.41 9.97 o 7 5 1 2771.21 2771.09 20.33 o 9 5 1 491.26 454.97 7.79 o 11 5 1 17808.47 19322.52 100.78 o 13 5 1 2886.29 2570.78 22.14 o 15 5 1 229.07 179.94 7.25 o 17 5 1 728.41 649.34 13.95 o 19 5 1 960.64 940.68 17.86 o 21 5 1 705.24 655.53 16.17 o 23 5 1 3810.29 4110.32 48.85 o 25 5 1 4023.09 4747.74 58.73 o 27 5 1 702.09 756.38 25.60 o 29 5 1 88.00 68.16 21.70 o 31 5 1 768.51 949.12 57.05 o 33 5 1 102.20 108.41 30.36 o 35 5 1 364.62 354.57 49.97 o 1 7 1 1783.65 1662.01 12.92 o 3 7 1 6445.26 6339.26 35.65 o 5 7 1 1034.35 956.91 10.21 o 7 7 1 325.90 251.46 5.64 o 9 7 1 1425.24 1346.34 12.96 o 11 7 1 11163.83 11947.47 68.76 o 13 7 1 5527.94 5797.75 40.66 o 15 7 1 382.91 282.04 8.80 o 17 7 1 1290.19 1289.16 18.58 o 19 7 1 507.33 446.66 13.00 o 21 7 1 593.04 549.36 20.03 o 23 7 1 804.41 663.81 21.25 o 25 7 1 1697.17 1756.35 38.17 o 27 7 1 1049.19 1104.57 31.77 o 29 7 1 75.19 22.30 12.52 o 31 7 1 113.36 81.54 26.95 o 33 7 1 226.92 215.34 35.08 o 1 9 1 276.71 207.89 5.16 o 3 9 1 7053.36 7801.17 44.72 o 5 9 1 3908.23 4132.99 27.43 o 7 9 1 78.83 72.75 4.46 o 9 9 1 5135.58 5276.64 33.94 o 11 9 1 7208.15 7150.43 46.01 o 13 9 1 804.26 878.38 13.79 o 15 9 1 125.04 80.81 7.43 o 17 9 1 275.60 277.37 10.90 o 19 9 1 102.58 114.17 10.46 o 21 9 1 825.55 645.14 18.49 o 23 9 1 14.32 20.60 13.44 o 25 9 1 188.17 186.44 19.85 o 27 9 1 278.34 235.41 24.66 o 29 9 1 142.48 75.60 25.05 o 31 9 1 381.33 405.41 33.45 o 33 9 1 180.85 155.50 33.52 o 1 11 1 6142.85 7451.38 46.24 o 3 11 1 348.67 363.23 7.31 o 5 11 1 803.26 747.65 10.46 o 7 11 1 609.93 493.67 8.92 o 9 11 1 193.41 130.85 6.03 o 11 11 1 848.89 685.41 11.57 o 13 11 1 903.26 968.31 17.50 o 15 11 1 7007.66 7628.35 67.31 o 17 11 1 930.66 961.36 25.64 o 19 11 1 26.08 10.28 11.71 o 21 11 1 567.75 536.13 20.98 o 23 11 1 421.58 331.39 20.67 o 25 11 1 763.40 754.77 37.02 o 27 11 1 657.51 532.82 34.27 o 29 11 1 152.70 93.96 29.07 o 31 11 1 118.89 77.72 29.93 o 33 11 1 71.34 77.86 37.05 o 1 13 1 9653.63 11065.39 68.40 o 3 13 1 509.74 402.45 9.23 o 5 13 1 2145.58 2217.27 22.45 o 7 13 1 848.86 827.45 14.73 o 9 13 1 1225.68 1218.97 18.43 o 11 13 1 301.27 317.06 9.52 o 13 13 1 6052.15 6664.07 70.41 o 15 13 1 826.92 947.22 18.29 o 17 13 1 770.63 724.82 21.53 o 19 13 1 264.24 171.32 17.16 o 21 13 1 919.95 786.10 30.93 o 23 13 1 2164.22 2317.70 65.04 o 25 13 1 178.88 133.78 22.51 o 27 13 1 331.29 301.79 30.00 o 29 13 1 344.99 291.90 31.08 o 31 13 1 20.48 0.54 30.58 o 1 15 1 3589.20 3966.92 38.20 o 3 15 1 530.42 518.71 11.96 o 5 15 1 210.40 174.34 9.23 o 7 15 1 2386.91 2380.36 27.95 o 9 15 1 1526.25 1491.28 21.53 o 11 15 1 2762.21 2832.15 30.82 o 13 15 1 6587.34 7562.36 66.24 o 15 15 1 467.01 496.40 18.99 o 17 15 1 412.35 414.51 17.69 o 19 15 1 381.01 301.53 19.79 o 21 15 1 287.26 171.36 22.35 o 23 15 1 528.78 460.98 27.52 o 25 15 1 75.07 35.52 22.53 o 27 15 1 37.79 4.23 24.86 o 29 15 1 338.02 151.59 38.45 o 31 15 1 116.92 140.28 40.55 o 1 17 1 262.70 232.23 10.60 o 3 17 1 144.73 121.54 10.35 o 5 17 1 321.45 244.86 11.89 o 7 17 1 2846.05 3177.56 34.81 o 9 17 1 2162.41 2214.68 29.85 o 11 17 1 1981.84 2131.49 29.78 o 13 17 1 5901.49 7225.61 71.23 o 15 17 1 863.02 935.03 22.75 o 17 17 1 879.27 847.07 23.77 o 19 17 1 1234.37 1223.66 34.83 o 21 17 1 336.99 219.05 22.57 o 23 17 1 109.43 25.86 21.13 o 25 17 1 451.02 452.58 34.57 o 27 17 1 138.66 91.60 28.67 o 29 17 1 229.40 220.64 40.98 o 1 19 1 16.01 28.26 9.91 o 3 19 1 1708.16 1673.47 27.75 o 5 19 1 1887.05 1896.84 30.69 o 7 19 1 3642.82 4297.77 48.66 o 9 19 1 1887.60 1963.35 31.79 o 11 19 1 2022.12 2309.34 36.40 o 13 19 1 2694.41 3341.11 47.89 o 15 19 1 805.92 882.98 31.05 o 17 19 1 44.37 32.25 18.47 o 19 19 1 302.42 322.45 25.12 o 21 19 1 586.01 680.42 31.82 o 23 19 1 571.63 489.18 48.04 o 25 19 1 399.20 379.08 39.27 o 27 19 1 41.66 30.34 36.63 o 1 21 1 174.29 112.33 13.88 o 3 21 1 587.73 583.30 20.66 o 5 21 1 259.99 248.30 16.63 o 7 21 1 660.78 663.75 23.57 o 9 21 1 696.92 694.97 24.71 o 11 21 1 5310.06 7006.76 84.87 o 13 21 1 790.05 947.63 29.96 o 15 21 1 206.75 182.81 20.68 o 17 21 1 418.36 526.08 28.80 o 19 21 1 399.01 378.36 29.43 o 21 21 1 173.64 104.55 25.37 o 23 21 1 109.16 57.04 28.69 o 25 21 1 517.11 622.50 43.25 o 1 23 1 128.95 56.84 16.22 o 3 23 1 128.17 74.97 15.29 o 5 23 1 1635.40 1793.45 40.42 o 7 23 1 37.55 4.31 19.75 o 9 23 1 982.62 1086.70 42.58 o 11 23 1 1403.76 1693.45 46.68 o 13 23 1 201.71 158.06 22.54 o 15 23 1 373.97 397.08 30.87 o 17 23 1 318.13 249.41 31.66 o 19 23 1 328.98 331.60 36.87 o 21 23 1 41.35 -22.46 31.87 o 23 23 1 2.83 -24.28 36.14 o 1 25 1 1950.32 2334.06 48.25 o 3 25 1 269.13 241.60 25.49 o 5 25 1 2.61 -9.45 22.74 o 7 25 1 463.02 452.80 30.10 o 9 25 1 97.32 40.73 26.79 o 11 25 1 1248.46 1529.23 59.66 o 13 25 1 828.34 827.05 63.44 o 15 25 1 245.00 233.77 32.67 o 17 25 1 34.78 34.93 29.75 o 19 25 1 270.88 160.30 40.04 o 1 27 1 1051.70 1075.47 41.22 o 3 27 1 55.24 26.39 25.29 o 5 27 1 134.71 134.07 29.07 o 7 27 1 182.26 102.80 30.09 o 9 27 1 140.70 93.92 29.73 o 11 27 1 222.56 221.68 38.86 o 13 27 1 62.57 42.42 33.78 o 15 27 1 389.78 460.05 42.78 o 17 27 1 314.72 356.13 55.37 o 1 29 1 1.57 -33.64 33.64 o 3 29 1 85.86 48.95 31.41 o 5 29 1 167.15 110.37 35.47 o 7 29 1 8.54 9.34 33.08 o 9 29 1 136.05 93.06 37.90 o 11 29 1 150.09 54.98 37.96 o 2 0 2 103.23 91.08 6.56 o 6 0 2 3929.33 4213.39 45.34 o 10 0 2 8480.63 9852.57 88.00 o 14 0 2 2368.46 2581.55 36.88 o 18 0 2 328.16 317.29 18.92 o 22 0 2 8095.43 10079.89 159.56 o 26 0 2 196.19 286.02 38.01 o 30 0 2 151.89 86.81 40.21 o 0 2 2 27234.55 31788.99 214.49 o 2 2 2 11586.62 12597.31 67.50 o 4 2 2 2868.66 2697.84 21.64 o 6 2 2 2293.15 2301.72 20.06 o 8 2 2 4889.88 5000.32 34.93 o 10 2 2 2006.08 1938.90 19.98 o 12 2 2 1188.93 1141.06 15.88 o 14 2 2 438.19 473.82 10.92 o 16 2 2 2001.84 2155.57 29.56 o 18 2 2 502.75 531.36 16.70 o 20 2 2 4201.25 5061.32 60.67 o 22 2 2 469.12 535.83 24.30 o 24 2 2 2355.50 2806.35 52.33 o 26 2 2 284.63 294.77 25.16 o 28 2 2 51.19 43.22 24.18 o 30 2 2 210.61 162.56 32.40 o 32 2 2 102.00 77.72 36.77 o 2 4 2 7489.60 7760.81 48.10 o 4 4 2 1283.03 1091.66 13.41 o 6 4 2 2110.04 2235.76 19.63 o 8 4 2 1872.18 1882.98 19.22 o 10 4 2 809.53 898.78 15.35 o 12 4 2 2956.53 3209.97 30.58 o 14 4 2 466.71 441.24 12.80 o 16 4 2 545.45 514.76 13.60 o 18 4 2 847.97 831.36 18.09 o 20 4 2 1805.27 2071.07 36.24 o 22 4 2 372.53 351.87 19.99 o 24 4 2 635.21 796.01 30.23 o 26 4 2 1166.98 1443.02 50.60 o 28 4 2 26.14 69.34 24.26 o 30 4 2 128.55 118.11 31.00 o 32 4 2 395.59 363.33 55.01 o 0 6 2 3769.64 3733.86 38.44 o 2 6 2 4650.76 5001.57 34.75 o 4 6 2 6781.35 7956.76 49.64 o 6 6 2 1211.96 1068.34 14.05 o 8 6 2 795.20 886.13 14.66 o 10 6 2 1763.66 1748.71 21.58 o 12 6 2 701.67 576.19 12.13 o 14 6 2 3550.31 4178.80 38.40 o 16 6 2 668.89 711.45 16.78 o 18 6 2 718.37 703.52 17.22 o 20 6 2 1587.90 1526.38 28.11 o 22 6 2 784.10 993.07 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o 5 1 3 489.11 448.44 15.38 o 7 1 3 941.44 1153.38 23.18 o 9 1 3 1799.29 2143.74 30.50 o 11 1 3 215.27 171.31 17.28 o 13 1 3 232.67 212.20 15.77 o 15 1 3 1637.67 1992.89 36.19 o 17 1 3 37.21 -16.91 16.91 o 19 1 3 244.33 205.53 20.51 o 21 1 3 1943.14 2842.87 72.54 o 23 1 3 140.98 121.50 25.49 o 25 1 3 181.91 158.19 28.64 o 27 1 3 203.45 137.68 32.86 o 1 3 3 119.91 90.46 8.57 o 3 3 3 450.35 419.82 13.00 o 5 3 3 59.73 39.56 9.82 o 7 3 3 22.27 15.92 8.96 o 9 3 3 37.49 14.10 10.72 o 11 3 3 258.65 223.83 16.71 o 13 3 3 1525.99 1929.07 35.85 o 15 3 3 196.15 138.77 19.54 o 17 3 3 296.45 198.31 20.06 o 19 3 3 468.05 478.12 28.64 o 21 3 3 417.05 405.90 25.72 o 23 3 3 854.96 1050.03 45.49 o 25 3 3 45.21 32.22 31.15 o 27 3 3 375.91 369.77 48.05 o 1 5 3 5421.23 6951.02 62.03 o 3 5 3 2179.39 2489.62 30.68 o 5 5 3 481.29 527.17 14.50 o 7 5 3 129.47 142.92 12.08 o 9 5 3 346.62 382.12 16.26 o 11 5 3 186.11 181.51 15.86 o 13 5 3 254.03 252.44 17.45 o 15 5 3 232.05 192.13 17.92 o 17 5 3 67.29 33.61 18.38 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34.78 o 7 11 3 3409.90 4476.05 54.73 o 9 11 3 843.45 959.68 25.29 o 11 11 3 78.50 16.40 16.04 o 13 11 3 894.72 974.32 27.76 o 15 11 3 727.76 777.14 30.06 o 17 11 3 543.78 559.87 29.16 o 19 11 3 122.90 96.86 24.13 o 21 11 3 944.09 1268.26 47.15 o 23 11 3 252.55 195.77 38.44 o 25 11 3 79.64 27.52 39.93 o 1 13 3 611.69 641.09 24.86 o 3 13 3 181.25 129.19 16.81 o 5 13 3 153.26 114.14 16.26 o 7 13 3 333.43 301.64 21.03 o 9 13 3 1229.26 1435.60 34.39 o 11 13 3 770.37 953.22 29.25 o 13 13 3 166.98 114.23 18.35 o 15 13 3 879.67 1053.97 37.44 o 17 13 3 70.96 52.28 22.49 o 19 13 3 60.37 14.23 27.10 o 21 13 3 1.02 38.14 29.89 o 23 13 3 345.56 232.19 48.29 o 1 15 3 199.78 140.19 21.96 o 3 15 3 18.39 35.55 17.71 o 5 15 3 428.69 514.09 25.26 o 7 15 3 998.80 1148.83 32.12 o 9 15 3 544.48 674.27 30.13 o 11 15 3 544.79 443.68 29.28 o 13 15 3 692.13 802.89 38.15 o 15 15 3 315.25 260.49 27.59 o 17 15 3 43.01 28.41 26.04 o 19 15 3 28.17 31.69 29.30 o 21 15 3 245.36 109.79 34.19 o 1 17 3 82.72 53.91 18.20 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o 8 8 4 136.12 101.84 24.14 o 10 8 4 66.07 68.72 24.48 o 12 8 4 178.77 93.73 26.48 o 14 8 4 8.79 -19.12 27.55 o 16 8 4 249.94 219.47 42.33 o 18 8 4 222.33 350.49 48.99 o 2 10 4 208.78 165.60 25.37 o 4 10 4 169.38 81.32 26.02 o 6 10 4 330.11 301.05 33.08 o 8 10 4 88.29 21.46 17.68 o 10 10 4 114.62 34.10 25.55 o 12 10 4 649.16 750.35 44.49 o 14 10 4 78.86 34.62 29.03 o 16 10 4 59.65 47.24 37.51 o 0 12 4 129.05 85.09 41.03 o 2 12 4 33.50 4.93 27.06 o 4 12 4 273.66 157.32 31.82 o 6 12 4 1006.83 1422.12 79.52 o 8 12 4 215.77 139.32 40.90 o 10 12 4 232.10 117.53 30.95 o 12 12 4 105.83 42.83 32.87 o 14 12 4 241.94 203.34 64.22 o 2 14 4 329.49 286.54 42.02 o 4 14 4 92.26 26.52 30.41 o 6 14 4 93.00 56.40 33.17 o 8 14 4 1041.21 1201.69 74.05 o 10 14 4 149.00 60.09 36.27 o 12 14 4 360.80 513.23 96.24 o 0 16 4 68.69 15.80 47.82 o 2 16 4 203.59 109.83 35.37 o 4 16 4 53.60 7.91 34.26 o 6 16 4 703.35 1067.24 73.74 o 8 16 4 45.28 80.04 44.41 o