#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:27:23 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181048 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/28/2212887.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212887_Fobs loop_ _publ_author_name 'Ali, Hapipah M.' 'Laila, Musalem' 'Wan Jefrey, Basirun' 'Ng, Seik Weng' _publ_section_title ; 2'-[1-(4-Chloro-2-hydroxyphenyl)ethylidene]benzenesulfonohydrazide ; _journal_coeditor_code HB2308 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1619 _journal_page_last o1620 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.253 _cell_angle_gamma 90.000 _cell_length_a 10.8711 _cell_length_b 5.7438 _cell_length_c 22.4374 _exptl_crystal_F_000 672.00 _reflns_d_resolution_high 0.7697 _cod_data_source_file hb2308Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 223.94 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 474.89 -0.74 0.49 o 2 0 0 6360.96 6582.71 77.34 o 3 0 0 0.65 -0.35 3.57 o 4 0 0 2266.25 2196.79 27.60 o 5 0 0 1659.39 1601.85 27.85 o 6 0 0 354.60 321.27 11.88 o 7 0 0 229.83 178.71 10.28 o 8 0 0 29.32 22.23 9.59 o 9 0 0 3663.11 3586.41 60.23 o 10 0 0 601.37 592.19 19.62 o 11 0 0 3.41 -3.17 10.32 o 12 0 0 19.52 8.26 11.07 o 13 0 0 1230.05 1323.57 38.68 o 14 0 0 221.39 253.62 25.53 o 1 1 0 17.13 19.11 1.03 o 2 1 0 14762.77 15633.82 112.77 o 3 1 0 3735.95 4078.63 29.59 o 4 1 0 42.65 33.03 2.86 o 5 1 0 15.95 29.72 3.33 o 6 1 0 123.75 133.45 5.96 o 7 1 0 4.48 12.65 5.03 o 8 1 0 180.71 197.85 7.40 o 9 1 0 435.15 454.97 11.00 o 10 1 0 185.14 196.03 7.76 o 11 1 0 128.05 127.35 7.55 o 12 1 0 350.59 359.07 11.91 o 13 1 0 201.74 231.91 16.67 o 0 2 0 95.00 78.66 9.85 o 1 2 0 655.83 691.32 7.50 o 2 2 0 18.11 22.39 1.61 o 3 2 0 432.15 448.61 6.15 o 4 2 0 1304.15 1426.97 14.18 o 5 2 0 286.08 345.61 6.40 o 6 2 0 407.22 387.92 7.40 o 7 2 0 516.07 473.52 9.94 o 8 2 0 218.89 231.57 8.08 o 9 2 0 5506.46 5449.15 57.07 o 10 2 0 286.75 284.20 9.60 o 11 2 0 266.58 253.97 12.17 o 12 2 0 4.52 1.73 11.59 o 13 2 0 45.90 61.73 15.92 o 1 3 0 292.26 273.03 4.53 o 2 3 0 391.62 389.99 5.99 o 3 3 0 1593.60 1636.74 15.45 o 4 3 0 340.26 341.09 6.33 o 5 3 0 705.74 720.27 9.26 o 6 3 0 2526.66 2541.90 25.49 o 7 3 0 391.54 375.85 9.00 o 8 3 0 13.38 19.39 7.96 o 9 3 0 211.03 204.09 10.83 o 10 3 0 187.89 183.14 11.09 o 11 3 0 72.60 57.41 9.43 o 12 3 0 182.93 184.67 15.24 o 0 4 0 1051.37 1062.64 44.31 o 1 4 0 1809.25 1816.21 19.19 o 2 4 0 110.40 132.45 4.19 o 3 4 0 161.58 164.30 5.29 o 4 4 0 398.17 392.19 8.70 o 5 4 0 322.39 340.16 9.85 o 6 4 0 58.33 57.51 7.79 o 7 4 0 8.93 6.84 7.54 o 8 4 0 2150.97 2099.47 34.41 o 9 4 0 275.83 296.99 12.67 o 10 4 0 91.26 123.60 18.20 o 11 4 0 278.61 246.92 13.66 o 1 5 0 7.52 0.75 4.37 o 2 5 0 68.05 66.88 3.80 o 3 5 0 105.60 114.21 5.21 o 4 5 0 8.18 8.77 6.05 o 5 5 0 47.95 47.49 7.23 o 6 5 0 33.77 36.58 9.19 o 7 5 0 396.48 389.55 14.01 o 8 5 0 166.48 159.67 10.45 o 9 5 0 21.38 18.07 9.55 o 10 5 0 3.93 1.39 9.64 o 0 6 0 487.51 516.29 36.43 o 1 6 0 817.45 830.94 31.51 o 2 6 0 210.22 210.49 9.75 o 3 6 0 7.61 10.61 5.68 o 4 6 0 149.12 161.99 8.12 o 5 6 0 42.08 40.31 9.32 o 6 6 0 11.94 16.02 7.84 o 7 6 0 141.08 170.96 10.64 o 8 6 0 198.94 201.86 12.00 o 1 7 0 39.15 34.29 17.01 o 2 7 0 1982.35 1924.65 55.88 o 3 7 0 10.31 -9.40 8.21 o 4 7 0 482.62 496.14 12.76 o -13 1 1 765.70 749.54 25.38 o -12 1 1 91.17 88.04 10.67 o -11 1 1 116.16 110.71 7.51 o -10 1 1 213.54 196.77 7.99 o -9 1 1 306.91 289.91 9.09 o -8 1 1 203.09 227.79 8.74 o -7 1 1 2205.03 2235.84 27.56 o -6 1 1 0.71 -2.09 4.52 o -5 1 1 475.31 527.00 7.96 o -4 1 1 2004.85 1869.63 17.71 o -3 1 1 5612.78 6087.08 43.53 o -2 1 1 0.22 -2.47 2.03 o -1 1 1 6227.62 6382.57 46.70 o 0 1 1 2941.92 2997.29 28.70 o 1 1 1 1651.42 1624.11 11.64 o 2 1 1 13968.91 14323.54 97.26 o 3 1 1 626.24 708.08 6.55 o 4 1 1 1071.97 1109.07 10.57 o 5 1 1 744.95 770.97 9.14 o 6 1 1 411.26 432.36 8.61 o 7 1 1 72.65 84.72 5.63 o 8 1 1 379.54 394.81 9.56 o 9 1 1 993.66 923.41 15.14 o 10 1 1 88.63 71.73 6.33 o 11 1 1 1226.56 1223.68 20.66 o 12 1 1 0.20 -13.07 8.89 o 13 1 1 127.55 135.20 14.85 o -13 2 1 151.07 132.30 15.53 o -12 2 1 182.61 208.07 15.09 o -11 2 1 22.32 3.74 14.67 o -10 2 1 131.64 142.52 8.85 o -9 2 1 1112.47 1083.04 16.41 o -8 2 1 66.66 55.88 6.49 o -7 2 1 603.19 604.38 11.40 o -6 2 1 112.04 124.88 4.69 o -5 2 1 346.50 395.36 6.73 o -4 2 1 3109.30 3133.34 29.17 o -3 2 1 1827.02 1748.39 16.88 o -2 2 1 111.78 149.17 2.59 o -1 2 1 1635.01 1598.58 15.61 o 0 2 1 313.50 312.06 6.33 o 1 2 1 396.16 405.09 5.43 o 2 2 1 881.26 885.33 7.49 o 3 2 1 488.24 459.82 6.09 o 4 2 1 2046.45 2151.67 20.84 o 5 2 1 1035.58 1093.55 11.68 o 6 2 1 1977.34 1964.37 22.10 o 7 2 1 36.53 31.41 5.10 o 8 2 1 2043.61 2009.79 24.40 o 9 2 1 88.72 78.30 6.51 o 10 2 1 462.86 431.63 12.04 o 11 2 1 1.13 -8.00 7.56 o 12 2 1 291.25 304.28 16.83 o 13 2 1 259.21 258.64 17.49 o -12 3 1 382.18 365.55 18.33 o -11 3 1 21.04 16.25 9.23 o -10 3 1 11.12 1.07 8.59 o -9 3 1 144.18 153.97 11.08 o -8 3 1 155.03 141.18 9.76 o -7 3 1 12.95 3.33 4.04 o -6 3 1 1199.59 1183.67 13.84 o -5 3 1 291.96 277.96 5.98 o -4 3 1 646.40 672.98 8.83 o -3 3 1 354.49 427.40 6.37 o -2 3 1 23.13 18.74 2.79 o -1 3 1 119.99 165.37 3.68 o 0 3 1 7.87 11.12 3.05 o 1 3 1 3359.91 3581.50 43.77 o 2 3 1 0.14 -3.92 2.61 o 3 3 1 686.80 716.74 8.29 o 4 3 1 2115.06 2141.29 19.97 o 5 3 1 39.53 34.14 3.91 o 6 3 1 1466.91 1461.43 16.03 o 7 3 1 452.99 457.43 10.25 o 8 3 1 8.99 2.22 7.84 o 9 3 1 0.52 8.69 8.12 o 10 3 1 585.19 560.16 16.47 o 11 3 1 28.99 49.43 10.15 o 12 3 1 20.54 21.34 12.64 o -11 4 1 112.34 135.30 11.65 o -10 4 1 498.69 482.89 17.22 o -9 4 1 136.92 135.10 11.69 o -8 4 1 92.37 82.22 9.17 o -7 4 1 121.11 122.10 8.99 o -6 4 1 61.58 60.56 7.94 o -5 4 1 795.52 790.14 13.30 o -4 4 1 12.34 7.53 4.74 o -3 4 1 1388.25 1413.96 15.74 o -2 4 1 1108.88 1099.09 12.48 o -1 4 1 936.07 909.36 10.19 o 0 4 1 60.21 65.67 4.56 o 1 4 1 1194.54 1346.08 21.86 o 2 4 1 364.56 348.56 6.46 o 3 4 1 543.56 515.76 8.53 o 4 4 1 162.34 161.01 5.68 o 5 4 1 1643.98 1571.89 23.82 o 6 4 1 1947.58 1836.88 29.61 o 7 4 1 211.40 210.53 10.32 o 8 4 1 168.23 186.22 10.63 o 9 4 1 16.37 14.96 9.41 o 10 4 1 81.33 66.04 9.78 o 11 4 1 94.21 110.80 11.20 o -10 5 1 6.66 -2.73 9.59 o -9 5 1 223.81 246.12 12.42 o -8 5 1 685.73 694.12 17.63 o -7 5 1 339.16 348.73 15.00 o -6 5 1 705.08 675.78 16.18 o -5 5 1 635.32 616.79 14.53 o -4 5 1 333.72 323.28 10.69 o -3 5 1 695.88 706.02 10.62 o -2 5 1 94.43 99.63 4.07 o -1 5 1 424.35 449.77 9.97 o 0 5 1 28.62 27.11 4.74 o 1 5 1 428.81 426.36 9.59 o 2 5 1 564.05 567.45 8.72 o 3 5 1 233.70 228.56 5.88 o 4 5 1 64.17 65.31 6.03 o 5 5 1 77.91 72.80 7.54 o 6 5 1 149.13 149.75 9.20 o 7 5 1 72.40 72.16 9.12 o 8 5 1 879.21 887.78 20.04 o 9 5 1 80.88 82.02 13.66 o 10 5 1 1193.46 1161.75 25.16 o -8 6 1 152.43 170.82 11.80 o -7 6 1 227.87 242.26 11.65 o -6 6 1 211.35 207.89 10.28 o -5 6 1 650.60 652.07 15.42 o -4 6 1 197.77 215.23 12.14 o -3 6 1 123.49 126.47 8.04 o -2 6 1 1034.37 1012.20 15.90 o -1 6 1 20.10 33.70 14.64 o 0 6 1 536.82 495.40 25.58 o 1 6 1 174.78 174.50 8.58 o 2 6 1 470.27 458.19 13.74 o 3 6 1 19.67 15.25 7.45 o 4 6 1 432.82 434.65 11.90 o 5 6 1 325.18 307.02 10.95 o 6 6 1 2.86 -5.45 7.54 o 7 6 1 772.54 767.55 18.40 o 8 6 1 171.43 179.04 11.58 o -4 7 1 31.16 17.91 6.87 o -3 7 1 15.47 19.22 10.18 o -2 7 1 4.19 -21.71 21.35 o -1 7 1 24.92 8.69 30.89 o 0 7 1 207.40 181.31 20.58 o 1 7 1 165.95 160.11 21.69 o 2 7 1 3.00 -1.83 16.24 o 3 7 1 33.44 21.76 9.15 o 4 7 1 159.72 162.43 11.19 o -14 0 2 138.69 160.42 24.49 o -13 0 2 1891.04 1946.22 50.37 o -12 0 2 103.45 106.05 13.19 o -11 0 2 1455.66 1446.61 32.20 o -10 0 2 45.86 59.96 10.61 o -9 0 2 200.40 225.81 13.46 o -8 0 2 410.34 405.00 15.41 o -7 0 2 847.34 1055.25 22.63 o -6 0 2 172.37 184.41 9.11 o -5 0 2 376.07 406.70 12.23 o -4 0 2 126.40 66.12 4.20 o -3 0 2 7203.79 7882.09 81.93 o -2 0 2 181.62 155.15 4.03 o -1 0 2 654.82 317.66 14.15 o 0 0 2 3017.21 -0.77 0.52 o 1 0 2 3419.58 3549.28 61.08 o 2 0 2 18.89 20.01 2.80 o 3 0 2 1755.49 1833.16 21.03 o 4 0 2 2951.35 3012.80 33.17 o 5 0 2 168.71 122.08 7.49 o 6 0 2 2734.08 2714.53 59.88 o 7 0 2 118.11 119.16 9.31 o 8 0 2 169.84 192.90 11.65 o 9 0 2 152.87 159.00 8.78 o 10 0 2 90.98 91.31 8.66 o 11 0 2 556.25 550.04 20.35 o 12 0 2 627.61 619.44 22.22 o 13 0 2 8.77 -9.19 14.47 o 14 0 2 454.29 476.16 31.01 o -13 1 2 28.79 25.87 12.78 o -12 1 2 152.05 144.76 11.03 o -11 1 2 116.80 111.41 7.65 o -10 1 2 403.19 425.67 10.69 o -9 1 2 24.13 27.44 7.40 o -8 1 2 859.43 826.59 15.18 o -7 1 2 187.61 220.22 7.80 o -6 1 2 136.58 177.68 6.45 o -5 1 2 78.95 97.94 4.13 o -4 1 2 1563.53 1524.87 14.93 o -3 1 2 683.45 673.36 6.81 o -2 1 2 1436.83 1477.15 12.31 o -1 1 2 510.16 559.13 5.97 o 0 1 2 15.23 23.48 1.32 o 1 1 2 730.42 741.38 6.13 o 2 1 2 24272.48 25550.54 173.80 o 3 1 2 8484.28 9001.33 60.08 o 4 1 2 1.16 2.55 2.35 o 5 1 2 1023.75 1103.51 11.08 o 6 1 2 77.04 80.04 4.76 o 7 1 2 553.80 551.73 10.72 o 8 1 2 0.11 -3.64 5.44 o 9 1 2 306.74 330.73 9.26 o 10 1 2 172.31 167.36 7.29 o 11 1 2 180.99 183.33 9.66 o 12 1 2 139.72 112.28 10.91 o 13 1 2 142.54 161.49 17.49 o -13 2 2 34.76 40.78 13.72 o -12 2 2 227.26 237.97 15.89 o -11 2 2 152.96 162.48 11.68 o -10 2 2 11.87 14.28 5.89 o -9 2 2 29.04 27.86 6.14 o -8 2 2 245.64 234.48 8.09 o -7 2 2 909.52 911.76 13.97 o -6 2 2 67.02 89.67 4.54 o -5 2 2 383.43 326.49 6.40 o -4 2 2 2172.55 2197.26 21.27 o -3 2 2 288.58 237.76 4.88 o -2 2 2 3804.40 3929.24 30.13 o -1 2 2 10.47 9.49 1.62 o 0 2 2 416.84 407.41 7.21 o 1 2 2 5819.49 6045.10 47.39 o 2 2 2 1294.94 1641.56 13.78 o 3 2 2 308.34 296.70 5.04 o 4 2 2 2753.47 3040.78 31.46 o 5 2 2 2509.31 2617.31 23.38 o 6 2 2 494.32 458.92 8.04 o 7 2 2 255.71 278.27 7.19 o 8 2 2 27.62 27.80 6.13 o 9 2 2 1276.00 1236.10 17.69 o 10 2 2 279.84 277.07 10.67 o 11 2 2 3.90 4.38 10.93 o 12 2 2 101.28 80.41 15.49 o 13 2 2 4.58 17.35 13.37 o -12 3 2 0.99 -8.34 9.48 o -11 3 2 150.48 154.18 11.43 o -10 3 2 128.62 149.66 10.72 o -9 3 2 275.10 298.00 12.86 o -8 3 2 977.30 973.68 20.31 o -7 3 2 6604.86 6590.10 80.48 o -6 3 2 38.58 45.24 4.93 o -5 3 2 203.69 189.13 6.92 o -4 3 2 1385.02 1331.54 24.02 o -3 3 2 1880.98 1952.04 17.96 o -2 3 2 23.32 39.73 3.04 o -1 3 2 105.06 90.46 2.79 o 0 3 2 1788.39 2013.14 28.42 o 1 3 2 2816.77 3022.94 37.49 o 2 3 2 2.26 -1.72 2.67 o 3 3 2 52.88 62.76 2.98 o 4 3 2 121.00 142.33 4.29 o 5 3 2 4007.73 4008.35 37.42 o 6 3 2 2676.37 2840.34 27.89 o 7 3 2 2776.12 2768.03 31.04 o 8 3 2 614.61 596.77 16.18 o 9 3 2 108.91 117.43 9.54 o 10 3 2 98.65 106.39 10.11 o 11 3 2 23.13 14.61 11.58 o 12 3 2 634.13 621.97 22.98 o -11 4 2 5.51 5.09 9.63 o -10 4 2 245.88 255.86 12.64 o -9 4 2 506.74 484.57 16.08 o -8 4 2 437.99 433.55 14.64 o -7 4 2 326.20 303.80 11.42 o -6 4 2 683.31 679.32 17.22 o -5 4 2 5258.71 5290.70 66.38 o -4 4 2 617.94 630.76 11.17 o -3 4 2 1125.49 1062.13 14.17 o -2 4 2 162.20 176.44 4.69 o -1 4 2 12.67 17.01 5.30 o 0 4 2 0.42 -5.32 4.54 o 1 4 2 152.80 162.14 6.31 o 2 4 2 30.20 32.67 3.54 o 3 4 2 1235.49 1307.24 14.92 o 4 4 2 1276.12 1260.39 15.05 o 5 4 2 297.38 293.47 7.98 o 6 4 2 139.56 134.26 8.92 o 7 4 2 237.94 215.00 10.19 o 8 4 2 603.75 597.92 16.46 o 9 4 2 472.27 476.85 15.36 o 10 4 2 811.14 849.14 20.23 o 11 4 2 155.06 183.00 12.36 o -10 5 2 7.33 -3.91 9.80 o -9 5 2 105.44 94.83 10.42 o -8 5 2 3.44 -2.04 8.17 o -7 5 2 37.99 37.16 8.50 o -6 5 2 573.54 558.00 14.95 o -5 5 2 733.27 699.52 15.76 o -4 5 2 369.62 364.27 11.03 o -3 5 2 157.60 167.75 5.33 o -2 5 2 803.01 802.41 10.68 o -1 5 2 330.65 331.63 11.25 o 0 5 2 374.82 370.41 13.28 o 1 5 2 0.08 -8.60 5.73 o 2 5 2 58.43 64.63 5.93 o 3 5 2 1090.02 1122.06 14.07 o 4 5 2 665.35 654.08 14.79 o 5 5 2 197.09 180.51 8.98 o 6 5 2 4.03 -3.35 7.42 o 7 5 2 441.39 422.23 13.95 o 8 5 2 0.28 5.45 9.16 o 9 5 2 624.42 632.62 18.00 o 10 5 2 0.85 0.11 10.23 o -8 6 2 91.26 104.34 12.23 o -7 6 2 20.59 18.77 8.75 o -6 6 2 43.90 48.07 8.21 o -5 6 2 0.64 -7.21 7.01 o -4 6 2 52.20 56.47 6.85 o -3 6 2 327.58 329.53 10.37 o -2 6 2 6.88 -0.59 6.74 o -1 6 2 73.76 72.50 7.42 o 0 6 2 5.85 0.38 8.40 o 1 6 2 699.42 676.11 16.54 o 2 6 2 224.49 225.18 10.46 o 3 6 2 113.84 113.24 7.82 o 4 6 2 294.01 296.31 13.58 o 5 6 2 99.28 101.86 9.03 o 6 6 2 52.77 54.17 8.33 o 7 6 2 29.78 31.94 8.93 o 8 6 2 136.82 96.15 10.56 o -4 7 2 19.60 14.23 6.83 o -3 7 2 43.72 50.48 8.55 o -2 7 2 193.73 236.46 28.45 o -1 7 2 235.81 228.87 37.78 o 0 7 2 520.65 531.10 29.11 o 1 7 2 142.19 114.31 19.13 o 2 7 2 9.75 -0.63 12.72 o 3 7 2 310.06 312.84 22.86 o 4 7 2 374.56 417.72 19.37 o -13 1 3 145.18 165.12 15.45 o -12 1 3 584.94 580.68 13.59 o -11 1 3 2285.20 2190.54 27.82 o -10 1 3 239.67 228.52 10.03 o -9 1 3 35.98 33.73 7.52 o -8 1 3 555.51 567.45 13.03 o -7 1 3 911.31 935.49 18.17 o -6 1 3 1813.52 1879.82 23.26 o -5 1 3 8.99 15.71 3.56 o -4 1 3 3618.27 3708.05 40.83 o -3 1 3 1852.73 1839.76 15.91 o -2 1 3 18701.25 19108.08 143.00 o -1 1 3 1175.31 1215.66 10.99 o 0 1 3 38.12 41.61 1.71 o 1 1 3 3360.48 3671.69 25.57 o 2 1 3 24322.31 25362.23 167.56 o 3 1 3 3927.66 4386.05 31.58 o 4 1 3 39.74 26.48 2.50 o 5 1 3 2016.69 2086.88 18.33 o 6 1 3 36.17 40.81 3.73 o 7 1 3 2152.67 2104.16 22.72 o 8 1 3 3.56 0.08 5.38 o 9 1 3 99.58 97.90 6.70 o 10 1 3 301.43 327.39 9.07 o 11 1 3 3519.33 3435.18 42.61 o 12 1 3 22.22 -1.18 9.35 o 13 1 3 31.17 22.63 13.53 o -13 2 3 34.95 29.87 13.73 o -12 2 3 52.67 48.41 9.48 o -11 2 3 14.51 7.27 8.53 o -10 2 3 615.42 614.74 12.73 o -9 2 3 602.95 598.86 12.18 o -8 2 3 1710.54 1610.75 20.99 o -7 2 3 189.62 214.28 7.35 o -6 2 3 50.86 45.57 4.28 o -5 2 3 2935.47 2971.78 26.23 o -4 2 3 90.94 73.69 3.59 o -3 2 3 77.49 94.26 3.37 o -2 2 3 1227.86 1275.99 11.57 o -1 2 3 4355.99 4481.68 36.69 o 0 2 3 673.67 691.29 6.70 o 1 2 3 1311.56 1282.69 11.43 o 2 2 3 1402.50 1393.77 11.53 o 3 2 3 2290.31 2472.99 24.19 o 4 2 3 67.73 59.97 3.52 o 5 2 3 1069.84 1115.51 11.94 o 6 2 3 26.46 38.64 4.29 o 7 2 3 247.16 227.95 7.07 o 8 2 3 272.66 271.81 8.45 o 9 2 3 455.04 454.19 10.77 o 10 2 3 4.89 3.27 6.72 o 11 2 3 21.96 25.24 12.00 o 12 2 3 2.00 -6.01 12.18 o 13 2 3 58.06 44.47 14.38 o -12 3 3 722.81 714.67 20.36 o -11 3 3 72.16 53.80 11.38 o -10 3 3 193.00 217.13 13.86 o -9 3 3 0.13 -10.69 8.02 o -8 3 3 410.96 419.61 13.97 o -7 3 3 2021.91 2009.72 24.03 o -6 3 3 3238.37 3236.95 35.70 o -5 3 3 184.75 224.80 5.34 o -4 3 3 28.18 40.33 3.63 o -3 3 3 459.19 510.71 9.19 o -2 3 3 149.12 173.50 4.63 o -1 3 3 41.72 72.02 2.85 o 0 3 3 17.46 27.09 4.16 o 1 3 3 3323.79 3771.63 46.33 o 2 3 3 223.19 244.77 4.63 o 3 3 3 1208.85 1173.25 12.56 o 4 3 3 617.68 647.21 7.87 o 5 3 3 4.87 2.69 2.30 o 6 3 3 1116.24 1196.62 13.61 o 7 3 3 956.46 971.47 15.68 o 8 3 3 1.22 17.10 7.40 o 9 3 3 172.88 180.72 10.59 o 10 3 3 230.75 237.18 11.81 o 11 3 3 28.58 14.12 11.43 o 12 3 3 340.12 344.05 18.73 o -11 4 3 93.20 91.87 11.10 o -10 4 3 308.70 310.00 13.57 o -9 4 3 156.18 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