#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/28/2212889.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212889_Fobs loop_ _publ_author_name 'Lerner, Hans-Wolfram' 'Bolte, Michael' _publ_section_title ; {\m~4~-3,3'-Bi[tricyclo[2.2.1.0^2,6^]heptaphosphane](4{-})}tetrakis[bis(1,2-dimethoxyethane)sodium(I)] ; _journal_coeditor_code HB2311 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1013 _journal_page_last m1014 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.320 _cell_angle_gamma 90.000 _cell_length_a 12.4440 _cell_length_b 20.2640 _cell_length_c 12.8740 _exptl_crystal_F_000 1308.00 _reflns_d_resolution_high 0.8366 _[local]_cod_data_source_file hb2311Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' wa166 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 227.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 2637.43 2648.04 272.82 o 4 0 0 977.07 807.89 258.02 o 5 0 0 1392.01 1309.79 215.29 o 6 0 0 2412.65 2447.06 328.17 o 7 0 0 1503.74 1118.00 166.45 o 8 0 0 16188.25 15307.25 793.62 o 9 0 0 8187.06 7882.63 302.30 o 10 0 0 1242.40 1148.66 132.58 o 11 0 0 343.08 326.19 164.89 o 12 0 0 523.84 591.12 134.72 o 13 0 0 3746.54 3754.57 170.35 o 14 0 0 921.15 830.37 146.98 o 2 1 0 9241.44 10077.64 506.00 o 3 1 0 3208.05 3246.35 191.96 o 4 1 0 4017.90 3778.31 167.42 o 5 1 0 1090.83 819.03 142.96 o 6 1 0 6152.45 5972.36 163.65 o 7 1 0 67.54 109.25 112.56 o 8 1 0 317.02 273.46 102.55 o 9 1 0 271.50 267.79 116.73 o 10 1 0 57.37 44.72 113.98 o 11 1 0 1.75 55.82 92.40 o 12 1 0 28.84 175.27 83.64 o 13 1 0 1.72 -71.53 110.81 o 14 1 0 2.16 -18.48 242.90 o 2 2 0 2077.96 1776.60 227.53 o 3 2 0 5278.01 5821.91 208.38 o 4 2 0 63.85 89.41 190.88 o 5 2 0 16187.00 16028.17 382.57 o 6 2 0 5379.93 5469.03 155.44 o 7 2 0 568.23 496.97 151.01 o 8 2 0 5612.59 5230.31 206.75 o 9 2 0 1654.52 1829.51 115.59 o 10 2 0 163.73 344.25 110.37 o 11 2 0 6.11 52.41 89.90 o 12 2 0 296.99 238.52 93.93 o 13 2 0 1610.24 1572.75 105.21 o 14 2 0 250.97 319.65 100.38 o 2 3 0 2663.96 3010.01 230.20 o 3 3 0 1207.05 726.84 216.89 o 4 3 0 1031.04 823.20 161.19 o 5 3 0 31.03 136.56 148.34 o 6 3 0 8180.33 7965.19 245.60 o 7 3 0 4641.83 4626.53 251.96 o 8 3 0 2806.63 2653.44 124.42 o 9 3 0 333.28 256.60 116.26 o 10 3 0 599.79 714.24 107.68 o 11 3 0 21.69 107.96 100.66 o 12 3 0 17.37 33.22 86.27 o 13 3 0 32.14 88.86 92.50 o 14 3 0 14.15 31.23 83.82 o 0 4 0 10275.16 10548.30 454.03 o 1 4 0 8260.88 7746.15 277.68 o 2 4 0 3720.41 3927.19 228.26 o 3 4 0 4247.98 4424.34 263.25 o 4 4 0 20.90 -172.61 190.33 o 5 4 0 2605.06 2694.60 152.18 o 6 4 0 1512.61 1297.41 132.66 o 7 4 0 525.20 507.23 120.08 o 8 4 0 16.00 55.99 113.70 o 9 4 0 377.60 325.11 116.12 o 10 4 0 1450.16 1292.25 107.26 o 11 4 0 437.00 463.35 92.14 o 12 4 0 21.35 55.37 89.31 o 13 4 0 189.36 287.14 84.80 o 14 4 0 12.75 49.67 90.96 o 1 5 0 7235.82 7567.48 289.67 o 2 5 0 3688.43 4073.87 360.79 o 3 5 0 626.78 812.38 207.64 o 4 5 0 1454.25 1312.34 212.15 o 5 5 0 10114.76 10740.73 375.75 o 6 5 0 362.80 361.34 139.85 o 7 5 0 2608.79 2481.74 124.16 o 8 5 0 456.43 321.32 133.73 o 9 5 0 863.42 748.08 127.04 o 10 5 0 22.30 139.83 126.72 o 11 5 0 142.07 232.97 98.94 o 12 5 0 78.17 179.37 86.54 o 13 5 0 26.27 88.62 80.40 o 14 5 0 31.32 155.63 79.67 o 0 6 0 37708.87 42844.63 1164.23 o 1 6 0 7045.68 7622.27 255.99 o 2 6 0 913.29 773.15 211.71 o 3 6 0 14246.93 14884.85 421.81 o 4 6 0 197.30 288.40 206.68 o 5 6 0 3600.58 3584.59 199.02 o 6 6 0 506.55 227.08 135.26 o 7 6 0 0.10 104.94 147.11 o 8 6 0 156.30 126.49 132.39 o 9 6 0 2199.43 2246.06 131.05 o 10 6 0 4764.18 4589.78 138.34 o 11 6 0 84.44 91.91 102.46 o 12 6 0 563.66 511.23 86.06 o 13 6 0 82.09 106.16 81.27 o 14 6 0 18.13 122.35 75.99 o 1 7 0 1278.82 1199.45 208.26 o 2 7 0 180.10 197.84 181.43 o 3 7 0 93.92 -112.27 180.12 o 4 7 0 146.05 150.28 225.92 o 5 7 0 12139.73 12272.74 191.84 o 6 7 0 0.96 -195.66 195.66 o 7 7 0 2847.29 2947.22 157.12 o 8 7 0 919.79 873.87 122.02 o 9 7 0 0.51 35.98 120.22 o 10 7 0 230.69 248.97 109.87 o 11 7 0 3.58 56.52 92.98 o 12 7 0 130.34 243.90 87.71 o 13 7 0 106.36 171.16 87.23 o 0 8 0 3755.34 3598.93 204.10 o 1 8 0 337.61 189.61 163.99 o 2 8 0 517.63 331.14 146.67 o 3 8 0 2235.80 2400.16 202.65 o 4 8 0 17.78 46.67 168.73 o 5 8 0 5912.36 5335.70 183.03 o 6 8 0 24.27 149.17 355.72 o 7 8 0 165.59 61.38 138.84 o 8 8 0 379.51 347.26 118.04 o 9 8 0 94.92 91.77 120.37 o 10 8 0 659.84 697.95 103.00 o 11 8 0 739.71 753.19 93.20 o 12 8 0 79.30 140.18 84.51 o 13 8 0 3.13 135.75 84.76 o 1 9 0 2145.30 2372.11 180.12 o 2 9 0 2301.89 2227.24 144.41 o 3 9 0 6632.28 6741.13 244.47 o 4 9 0 841.59 435.07 183.92 o 5 9 0 312.56 232.35 180.04 o 6 9 0 1471.03 1689.09 187.26 o 7 9 0 80.37 204.35 160.99 o 8 9 0 226.27 432.42 118.16 o 9 9 0 305.15 288.85 107.95 o 10 9 0 1188.40 1225.30 174.22 o 11 9 0 853.27 787.18 89.96 o 12 9 0 12.47 -35.47 89.91 o 13 9 0 0.58 10.32 90.80 o 0 10 0 837.54 638.10 204.99 o 1 10 0 2234.77 2206.54 175.84 o 2 10 0 5577.53 5730.59 261.47 o 3 10 0 215.85 272.08 140.06 o 4 10 0 946.52 647.54 201.26 o 5 10 0 5292.33 5846.18 514.13 o 6 10 0 124.37 131.68 160.02 o 7 10 0 25.95 369.20 276.08 o 8 10 0 1777.13 1966.98 111.44 o 9 10 0 1338.24 1523.08 127.94 o 10 10 0 89.39 86.46 108.18 o 11 10 0 444.18 434.97 99.88 o 12 10 0 261.34 346.83 88.62 o 13 10 0 114.29 234.28 85.41 o 1 11 0 63.84 139.10 209.78 o 2 11 0 10071.16 9457.77 447.78 o 3 11 0 1988.84 1766.51 134.55 o 4 11 0 93.38 -69.53 144.85 o 5 11 0 2396.97 2421.81 167.15 o 6 11 0 12.38 112.36 148.15 o 7 11 0 5.36 241.03 281.54 o 8 11 0 517.90 928.19 365.77 o 9 11 0 137.77 183.35 108.94 o 10 11 0 1967.74 2095.46 140.10 o 11 11 0 1392.31 1435.59 196.91 o 12 11 0 143.35 88.09 91.84 o 0 12 0 2994.19 2991.96 385.72 o 1 12 0 10049.41 10059.49 577.53 o 2 12 0 3349.55 3379.55 177.04 o 3 12 0 1261.69 1389.87 122.60 o 4 12 0 12.34 159.60 131.02 o 5 12 0 321.87 208.15 158.39 o 6 12 0 1203.67 1208.58 151.72 o 7 12 0 1433.84 1411.28 140.84 o 8 12 0 2382.79 2123.86 134.19 o 9 12 0 1134.28 1092.98 117.29 o 10 12 0 434.74 383.12 187.55 o 11 12 0 0.55 86.46 96.24 o 12 12 0 280.44 136.68 85.29 o 1 13 0 75.98 -21.28 135.00 o 2 13 0 1401.38 1466.23 130.82 o 3 13 0 1191.86 927.54 129.12 o 4 13 0 479.04 652.02 192.90 o 5 13 0 17.44 -101.66 152.87 o 6 13 0 0.05 259.34 153.15 o 7 13 0 59.35 48.50 136.53 o 8 13 0 37.17 333.23 150.61 o 9 13 0 230.13 354.84 110.90 o 10 13 0 1395.03 1214.56 99.09 o 11 13 0 109.69 116.23 93.63 o 12 13 0 351.10 309.89 89.12 o 0 14 0 2188.08 2239.85 237.18 o 1 14 0 1017.55 783.85 140.87 o 2 14 0 522.59 501.72 123.30 o 3 14 0 66.90 17.12 130.85 o 4 14 0 497.29 453.12 128.36 o 5 14 0 13.17 175.83 140.95 o 6 14 0 183.90 151.84 146.31 o 7 14 0 187.83 389.74 126.20 o 8 14 0 264.29 314.56 125.84 o 9 14 0 104.05 62.70 99.18 o 10 14 0 299.81 364.84 98.50 o 11 14 0 7.87 -3.56 90.29 o 1 15 0 135.24 130.78 134.42 o 2 15 0 640.80 699.10 130.66 o 3 15 0 1741.10 1971.34 128.87 o 4 15 0 1246.86 1291.90 117.21 o 5 15 0 754.26 960.12 123.92 o 6 15 0 212.28 234.87 163.60 o 7 15 0 331.72 388.50 126.06 o 8 15 0 115.00 -23.79 134.41 o 9 15 0 329.26 377.48 127.91 o 10 15 0 592.71 634.58 161.14 o 11 15 0 18.32 1.19 90.50 o 0 16 0 45.65 220.65 232.74 o 1 16 0 20.43 -51.22 117.24 o 2 16 0 210.55 229.95 135.85 o 3 16 0 57.25 33.98 121.84 o 4 16 0 108.37 175.93 124.08 o 5 16 0 188.76 125.06 115.83 o 6 16 0 0.06 -4.42 118.50 o 7 16 0 23.28 -32.68 193.51 o 8 16 0 78.74 170.76 185.91 o 9 16 0 103.22 7.63 111.83 o 10 16 0 7.97 20.20 88.86 o 1 17 0 283.50 272.64 108.20 o 2 17 0 7.37 127.65 115.74 o 3 17 0 1620.99 1685.68 119.64 o 4 17 0 2557.72 2679.28 125.32 o 5 17 0 2331.02 2171.52 114.81 o 6 17 0 195.41 253.54 108.47 o 7 17 0 795.38 699.01 103.51 o 8 17 0 1359.19 1459.68 124.34 o 9 17 0 79.72 210.96 109.26 o 10 17 0 74.02 38.64 87.26 o 0 18 0 304.88 242.92 154.75 o 1 18 0 350.84 391.07 102.27 o 2 18 0 648.68 610.43 106.33 o 3 18 0 517.44 367.75 110.48 o 4 18 0 104.11 63.43 110.00 o 5 18 0 1045.24 1145.21 127.67 o 6 18 0 99.69 235.45 102.60 o 7 18 0 3.94 0.53 93.63 o 8 18 0 707.47 766.21 96.22 o 9 18 0 343.60 362.37 90.77 o 1 19 0 32.06 -3.54 122.22 o 2 19 0 435.83 570.02 105.28 o 3 19 0 500.18 390.16 92.15 o 4 19 0 397.25 285.68 110.13 o 5 19 0 437.50 465.37 106.63 o 6 19 0 112.38 122.02 100.07 o 7 19 0 148.44 167.90 92.94 o 8 19 0 255.92 260.43 109.95 o 0 20 0 789.45 645.31 152.88 o 1 20 0 135.28 256.20 111.22 o 2 20 0 1.90 27.52 92.57 o 3 20 0 126.94 252.02 105.24 o 4 20 0 174.33 281.69 115.83 o 5 20 0 504.61 450.09 152.07 o 6 20 0 50.37 -24.81 95.94 o 7 20 0 96.82 130.54 85.58 o 8 20 0 313.24 287.69 157.71 o 1 21 0 623.62 490.78 95.92 o 2 21 0 446.55 329.68 88.87 o 3 21 0 30.13 54.26 89.43 o 4 21 0 0.07 102.59 93.05 o 5 21 0 140.80 196.03 94.47 o 6 21 0 42.48 306.94 139.53 o 7 21 0 13.03 110.92 84.04 o 0 22 0 152.45 268.49 153.61 o 1 22 0 2.80 92.25 111.34 o 2 22 0 83.40 199.42 103.52 o 3 22 0 32.49 109.71 86.65 o 4 22 0 19.83 102.20 93.65 o 5 22 0 2.40 55.61 80.73 o 6 22 0 120.84 48.82 189.33 o 1 23 0 296.82 369.75 112.19 o 2 23 0 296.02 330.21 113.52 o 3 23 0 0.01 96.63 89.24 o 4 23 0 88.85 83.79 83.32 o 0 24 0 0.17 -100.45 164.43 o 1 24 0 17.13 42.80 126.27 o -14 1 1 243.49 335.48 104.66 o -13 1 1 127.76 142.14 90.81 o -12 1 1 895.51 975.51 182.48 o -11 1 1 265.93 234.24 105.05 o -10 1 1 74.46 260.28 105.62 o -9 1 1 5633.77 5808.34 272.25 o -8 1 1 2658.40 2559.83 117.10 o -7 1 1 148.15 61.31 121.82 o -6 1 1 688.34 736.79 118.74 o -5 1 1 6439.69 6530.87 222.29 o -4 1 1 3403.27 3356.31 172.84 o -3 1 1 11303.78 11952.74 198.32 o -2 1 1 12254.77 13845.14 387.28 o 2 1 1 9044.64 9394.62 755.47 o 3 1 1 2098.76 1885.28 203.33 o 4 1 1 51710.08 54026.83 1585.30 o 5 1 1 9809.84 9930.12 238.03 o 6 1 1 2323.63 2344.79 149.48 o 7 1 1 1897.15 1521.96 138.63 o 8 1 1 56.67 23.50 127.51 o 9 1 1 321.45 268.04 121.18 o 10 1 1 988.37 902.81 108.06 o 11 1 1 1455.07 1441.84 193.62 o 12 1 1 8459.95 7928.43 801.18 o 13 1 1 1595.52 1300.61 147.38 o 14 1 1 58.51 191.76 91.64 o -14 2 1 7.53 278.59 87.79 o -13 2 1 0.07 145.43 114.64 o -12 2 1 88.56 -22.29 97.09 o -11 2 1 73.39 201.77 111.93 o -10 2 1 697.74 678.87 120.66 o -9 2 1 1496.76 1460.96 115.45 o -8 2 1 2202.88 2024.14 157.55 o -7 2 1 1551.20 1456.92 128.13 o -6 2 1 1843.09 1587.02 124.51 o -5 2 1 1049.66 873.05 145.38 o -4 2 1 30.89 112.04 147.05 o -3 2 1 254.97 185.83 198.82 o -2 2 1 9002.09 9751.99 469.89 o 2 2 1 1924.39 2235.28 248.12 o 3 2 1 5883.71 6012.73 244.99 o 4 2 1 6403.97 6447.99 187.76 o 5 2 1 34.18 147.45 158.40 o 6 2 1 4521.31 4452.36 152.67 o 7 2 1 2264.41 2031.53 135.96 o 8 2 1 978.90 835.02 135.73 o 9 2 1 2971.45 3044.11 190.70 o 10 2 1 690.82 710.14 118.83 o 11 2 1 78.97 10.05 86.61 o 12 2 1 18.75 112.73 81.77 o 13 2 1 27.41 90.13 89.72 o 14 2 1 8.31 110.49 90.07 o -14 3 1 157.14 226.97 96.97 o -13 3 1 89.54 115.69 96.94 o -12 3 1 705.59 724.08 100.43 o -11 3 1 10.28 113.30 97.36 o -10 3 1 1755.69 1595.48 127.58 o -9 3 1 525.13 608.86 114.68 o -8 3 1 3022.71 2901.30 160.77 o -7 3 1 4652.10 4777.60 164.31 o -6 3 1 190.91 195.28 146.49 o -5 3 1 2578.35 2522.42 218.97 o -4 3 1 1848.51 1672.53 171.69 o -3 3 1 1559.67 1354.68 197.39 o -2 3 1 14929.45 15527.19 464.19 o -1 3 1 9444.11 8885.99 307.86 o 1 3 1 2957.80 3041.60 274.61 o 2 3 1 17453.12 17222.71 1360.60 o 3 3 1 242.97 222.85 242.76 o 4 3 1 892.70 917.76 175.74 o 5 3 1 4488.54 4541.35 378.71 o 6 3 1 7325.66 7558.44 316.32 o 7 3 1 127.50 153.03 125.84 o 8 3 1 0.54 57.93 116.56 o 9 3 1 872.17 976.73 121.19 o 10 3 1 461.76 406.17 106.37 o 11 3 1 864.74 850.44 99.50 o 12 3 1 1124.71 955.23 90.95 o 13 3 1 119.13 167.13 106.81 o 14 3 1 162.79 207.04 92.92 o -14 4 1 265.38 162.88 87.30 o -13 4 1 17.39 26.91 102.09 o -12 4 1 268.45 230.37 105.38 o -11 4 1 59.37 73.74 102.75 o -10 4 1 10.60 151.09 113.96 o -9 4 1 3175.16 3046.97 130.13 o -8 4 1 1829.60 1819.19 124.13 o -7 4 1 2266.48 2497.35 146.00 o -6 4 1 1248.00 1121.62 145.36 o -5 4 1 1093.65 1084.15 184.09 o -4 4 1 2532.84 2231.07 167.98 o -3 4 1 9721.10 10532.60 256.70 o -2 4 1 104.93 166.23 253.92 o -1 4 1 974.65 920.80 214.71 o 0 4 1 3927.99 3697.27 222.11 o 1 4 1 2064.67 1728.90 244.60 o 2 4 1 1706.50 1730.69 252.76 o 3 4 1 1705.22 1178.83 200.74 o 4 4 1 814.18 757.43 222.20 o 5 4 1 6692.42 7015.08 362.39 o 6 4 1 2849.92 2554.31 205.23 o 7 4 1 3977.75 3998.25 217.30 o 8 4 1 16.57 209.09 130.61 o 9 4 1 792.57 630.74 118.62 o 10 4 1 77.07 170.66 109.88 o 11 4 1 52.13 39.38 99.07 o 12 4 1 3.35 139.00 91.14 o 13 4 1 12.06 167.67 84.91 o 14 4 1 35.21 144.46 78.99 o -14 5 1 20.71 47.05 83.79 o -13 5 1 375.08 478.26 97.82 o -12 5 1 25.71 163.20 98.33 o -11 5 1 697.95 596.56 95.03 o -10 5 1 1786.49 1595.42 105.20 o -9 5 1 362.99 626.56 122.42 o -8 5 1 26.97 107.86 125.53 o -7 5 1 1637.91 1700.62 139.51 o -6 5 1 2570.28 2378.95 218.20 o -5 5 1 10364.23 9942.12 160.03 o -4 5 1 368.71 92.50 185.57 o -3 5 1 1000.40 1032.45 270.35 o -2 5 1 4373.87 4356.52 343.04 o -1 5 1 3950.30 3975.80 335.05 o 0 5 1 5142.97 5152.84 234.72 o 1 5 1 676.71 983.84 243.97 o 2 5 1 3257.26 3449.95 270.52 o 3 5 1 349.46 27.47 183.53 o 4 5 1 3920.97 3884.32 204.66 o 5 5 1 516.25 515.27 174.24 o 6 5 1 908.77 807.08 138.10 o 7 5 1 239.50 275.62 124.71 o 8 5 1 344.77 304.49 131.36 o 9 5 1 790.11 884.54 109.69 o 10 5 1 104.26 135.83 125.62 o 11 5 1 40.05 6.28 88.57 o 12 5 1 378.88 433.83 88.21 o 13 5 1 81.65 218.52 84.81 o 14 5 1 275.02 140.51 135.94 o -14 6 1 182.32 312.26 94.38 o -13 6 1 17.08 8.35 93.23 o -12 6 1 7.37 -10.70 85.86 o -11 6 1 126.59 348.94 95.68 o -10 6 1 724.83 660.25 114.59 o -9 6 1 237.59 189.75 119.62 o -8 6 1 23.40 65.24 126.28 o -7 6 1 354.34 317.38 169.58 o -6 6 1 1983.14 1693.00 148.36 o -5 6 1 7.97 115.11 188.08 o -4 6 1 3532.32 3495.22 212.59 o -3 6 1 5951.56 6199.13 253.33 o -2 6 1 6964.15 6325.76 208.57 o -1 6 1 7996.31 8478.07 205.91 o 0 6 1 3004.45 3475.90 422.03 o 1 6 1 941.05 1021.39 296.57 o 2 6 1 13.49 108.06 202.77 o 3 6 1 629.10 497.35 174.85 o 4 6 1 1366.76 1641.75 200.18 o 5 6 1 3.51 -25.04 160.21 o 6 6 1 244.60 388.01 157.80 o 7 6 1 3710.73 3650.84 264.91 o 8 6 1 266.17 236.36 121.64 o 9 6 1 57.28 -13.32 113.08 o 10 6 1 2.10 194.35 96.64 o 11 6 1 0.20 34.02 94.84 o 12 6 1 33.25 136.91 95.46 o 13 6 1 44.56 110.23 82.30 o -14 7 1 11.55 99.42 111.88 o -13 7 1 83.67 95.23 91.84 o -12 7 1 19.74 27.49 92.10 o -11 7 1 1432.77 1343.44 101.13 o -10 7 1 795.23 890.45 112.62 o -9 7 1 434.03 432.99 117.41 o -8 7 1 3186.90 3223.98 143.53 o -7 7 1 856.70 728.65 152.28 o -6 7 1 6155.94 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