#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/28/2212893.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212893_Fobs loop_ _publ_author_name 'Nesterov, Vladimir N.' 'Sarkisov, Sergey S.' 'Curley, Michael J.' 'Urbas, Augustine' _publ_section_title ; An orthorhombic polymorph of 3,5-bis[4-(dimethylamino)benzylidene]-1-methyl-4-piperidone ; _journal_coeditor_code HB2316 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1785 _journal_page_last o1787 _journal_volume 63 _journal_year 2007 _space_group_IT_number 33 _symmetry_space_group_name_Hall 'P 2c -2n' _symmetry_space_group_name_H-M 'P n a 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.0395 _cell_length_b 22.2979 _cell_length_c 7.6686 _exptl_crystal_F_000 808.00 _reflns_d_resolution_high 0.7600 _[local]_cod_data_source_file hb2316Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' n59 in Pna2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 295.07 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 321.70 306.58 14.47 o 4 0 0 470.99 466.73 20.44 o 6 0 0 780.25 717.96 28.39 o 8 0 0 598.51 652.37 32.39 o 10 0 0 2619.27 2587.40 79.38 o 12 0 0 412.86 334.94 68.32 o 14 0 0 7.08 16.54 64.01 o 1 1 0 3032.66 2742.11 26.93 o 2 1 0 174.63 164.38 6.73 o 3 1 0 3506.53 3170.41 34.35 o 4 1 0 1182.42 1106.58 19.64 o 5 1 0 205.34 195.79 12.52 o 6 1 0 702.83 746.82 20.57 o 7 1 0 106.49 88.64 13.98 o 8 1 0 42.43 38.69 15.59 o 9 1 0 348.30 349.29 21.89 o 10 1 0 3.83 -21.66 21.66 o 11 1 0 87.83 115.96 28.98 o 12 1 0 610.90 691.70 54.28 o 13 1 0 23.72 74.41 44.78 o 14 1 0 329.26 371.74 86.75 o 15 1 0 102.83 140.66 56.73 o 0 2 0 730.63 653.90 11.72 o 1 2 0 91.93 93.83 4.28 o 2 2 0 555.88 488.84 12.69 o 3 2 0 35.27 15.92 16.06 o 4 2 0 1911.29 1796.65 25.14 o 5 2 0 147.57 139.83 11.73 o 6 2 0 295.10 294.65 15.72 o 7 2 0 450.50 506.42 22.39 o 8 2 0 8.61 -14.74 14.74 o 9 2 0 30.58 24.74 17.68 o 10 2 0 487.40 480.95 30.25 o 11 2 0 262.59 272.98 37.26 o 12 2 0 149.90 104.58 48.41 o 13 2 0 53.70 64.50 46.46 o 14 2 0 14.38 -44.25 44.29 o 15 2 0 7.71 -18.35 68.36 o 1 3 0 5618.84 4956.59 43.95 o 2 3 0 2176.55 2001.03 24.39 o 3 3 0 89.09 79.27 12.76 o 4 3 0 38.12 53.67 12.24 o 5 3 0 1779.59 1820.71 28.10 o 6 3 0 60.15 56.42 12.88 o 7 3 0 5.82 -8.26 13.11 o 8 3 0 9.53 -3.14 15.37 o 9 3 0 0.07 -4.21 17.51 o 10 3 0 232.28 220.51 26.27 o 11 3 0 2.78 -28.81 32.00 o 12 3 0 50.81 46.18 40.94 o 13 3 0 1.22 38.01 43.35 o 14 3 0 1.98 84.13 78.54 o 15 3 0 2.58 5.07 58.50 o 0 4 0 145.01 156.39 9.97 o 1 4 0 2.70 -0.01 6.78 o 2 4 0 14.58 25.70 10.77 o 3 4 0 300.33 321.99 13.27 o 4 4 0 245.03 263.49 13.41 o 5 4 0 297.21 290.42 20.18 o 6 4 0 1003.95 1041.92 23.94 o 7 4 0 2253.04 2150.47 39.77 o 8 4 0 177.74 174.79 21.91 o 9 4 0 408.76 429.62 28.34 o 10 4 0 43.93 4.97 23.78 o 11 4 0 58.90 0.96 22.99 o 12 4 0 37.45 56.82 59.47 o 13 4 0 145.73 180.80 46.87 o 14 4 0 103.30 49.43 62.13 o 15 4 0 1.92 -54.61 78.61 o 1 5 0 310.71 301.94 17.18 o 2 5 0 1302.82 1292.91 21.74 o 3 5 0 111.03 100.18 12.83 o 4 5 0 1339.31 1324.32 27.79 o 5 5 0 35.56 67.96 12.84 o 6 5 0 2618.07 2764.54 49.80 o 7 5 0 886.43 935.66 25.53 o 8 5 0 203.79 205.49 19.73 o 9 5 0 139.31 159.03 24.76 o 10 5 0 122.48 135.11 26.42 o 11 5 0 3.64 -10.55 23.46 o 12 5 0 13.54 18.37 40.29 o 13 5 0 53.89 80.86 76.86 o 14 5 0 112.00 145.11 49.81 o 15 5 0 55.29 43.06 52.13 o 0 6 0 81.74 85.23 15.61 o 1 6 0 79.62 86.11 10.81 o 2 6 0 18.42 28.71 10.16 o 3 6 0 142.14 136.93 12.01 o 4 6 0 1943.99 1936.26 29.06 o 5 6 0 4.66 -10.03 12.62 o 6 6 0 0.27 16.26 13.44 o 7 6 0 23.85 -0.28 15.17 o 8 6 0 117.67 117.33 20.37 o 9 6 0 1.92 20.89 23.36 o 10 6 0 169.19 205.37 27.56 o 11 6 0 0.25 -25.08 31.63 o 12 6 0 156.61 203.32 45.75 o 13 6 0 55.31 20.83 42.92 o 14 6 0 28.75 74.55 48.03 o 15 6 0 20.54 11.53 71.64 o 1 7 0 770.21 704.83 17.18 o 2 7 0 0.56 1.88 9.89 o 3 7 0 848.83 801.18 19.39 o 4 7 0 465.30 485.16 17.74 o 5 7 0 72.57 54.22 13.86 o 6 7 0 374.78 406.57 19.50 o 7 7 0 92.97 71.80 17.27 o 8 7 0 319.15 298.50 28.79 o 9 7 0 95.13 105.45 26.41 o 10 7 0 732.20 691.57 34.56 o 11 7 0 332.25 351.73 33.78 o 12 7 0 133.12 69.14 46.11 o 13 7 0 34.54 29.06 43.17 o 14 7 0 1.65 85.05 53.61 o 15 7 0 34.32 23.57 53.22 o 0 8 0 1070.99 992.86 27.41 o 1 8 0 678.39 700.88 17.38 o 2 8 0 1126.32 1091.44 21.85 o 3 8 0 1578.21 1607.65 26.93 o 4 8 0 35.92 24.82 12.95 o 5 8 0 1343.65 1353.47 28.29 o 6 8 0 382.29 411.27 20.37 o 7 8 0 0.57 -16.42 16.42 o 8 8 0 29.31 -6.21 22.85 o 9 8 0 31.96 49.24 25.80 o 10 8 0 171.07 175.38 34.79 o 11 8 0 32.82 80.90 25.92 o 12 8 0 36.73 21.63 37.20 o 13 8 0 268.16 292.98 51.00 o 14 8 0 113.06 73.46 58.97 o 15 8 0 6.45 3.20 52.79 o 1 9 0 2148.80 2108.14 29.07 o 2 9 0 354.35 378.01 15.32 o 3 9 0 2164.00 2093.49 31.73 o 4 9 0 479.81 516.23 19.55 o 5 9 0 441.41 489.58 20.35 o 6 9 0 29.84 23.00 16.13 o 7 9 0 39.20 53.48 18.52 o 8 9 0 2.87 -21.21 23.02 o 9 9 0 1238.62 1305.07 47.36 o 10 9 0 555.13 525.98 33.04 o 11 9 0 802.39 861.89 41.78 o 12 9 0 72.22 45.63 33.60 o 13 9 0 0.65 26.65 46.97 o 14 9 0 59.37 197.67 52.95 o 15 9 0 14.05 14.14 54.37 o 0 10 0 175.75 167.81 18.26 o 1 10 0 8304.23 7949.24 75.72 o 2 10 0 636.13 646.19 22.37 o 3 10 0 611.46 619.32 20.67 o 4 10 0 155.29 169.08 15.98 o 5 10 0 216.08 273.24 18.74 o 6 10 0 0.66 13.67 16.77 o 7 10 0 42.89 50.26 19.54 o 8 10 0 36.69 6.84 24.73 o 9 10 0 35.45 40.07 26.20 o 10 10 0 24.00 -24.47 24.83 o 11 10 0 7.85 -18.32 26.31 o 12 10 0 128.14 74.60 38.05 o 13 10 0 104.98 27.18 44.78 o 14 10 0 89.16 47.10 59.38 o 2 11 0 2530.57 2594.95 35.97 o 3 11 0 2.78 19.83 13.33 o 4 11 0 90.83 95.88 15.91 o 5 11 0 459.55 549.14 23.09 o 6 11 0 586.40 643.89 26.03 o 7 11 0 540.73 579.70 31.66 o 8 11 0 470.59 465.46 33.00 o 9 11 0 2.01 32.20 25.59 o 10 11 0 29.85 31.77 26.48 o 11 11 0 281.97 354.91 33.89 o 12 11 0 206.09 229.85 39.22 o 13 11 0 68.94 83.85 46.26 o 14 11 0 56.20 65.71 61.45 o 0 12 0 60.03 89.76 19.23 o 2 12 0 99.10 126.52 14.07 o 3 12 0 332.53 338.27 18.19 o 4 12 0 3.68 -5.00 15.10 o 5 12 0 5.89 -11.36 16.91 o 6 12 0 86.21 62.61 19.32 o 7 12 0 2.44 -4.02 24.54 o 8 12 0 1441.57 1453.04 45.18 o 9 12 0 1.87 17.21 25.87 o 10 12 0 14.52 19.21 26.87 o 11 12 0 306.19 343.37 41.30 o 12 12 0 30.26 -8.35 33.63 o 13 12 0 41.34 123.79 45.12 o 14 12 0 1.44 -58.19 58.19 o 1 13 0 2.92 6.30 13.02 o 2 13 0 12.37 9.91 13.05 o 3 13 0 173.36 169.97 16.89 o 4 13 0 14.19 -6.08 16.14 o 5 13 0 110.75 113.93 20.14 o 6 13 0 132.12 155.82 22.11 o 7 13 0 235.70 250.27 29.36 o 8 13 0 280.84 363.40 31.81 o 9 13 0 10.61 -4.68 26.00 o 10 13 0 1.78 -5.60 31.69 o 11 13 0 18.36 8.27 33.93 o 12 13 0 34.02 77.96 45.12 o 13 13 0 0.01 14.87 44.16 o 14 13 0 182.84 78.05 78.58 o 0 14 0 0.62 25.33 20.36 o 1 14 0 0.00 -13.72 13.73 o 2 14 0 502.88 524.60 20.87 o 3 14 0 148.17 170.16 18.01 o 4 14 0 30.50 28.11 17.78 o 5 14 0 20.19 20.77 19.58 o 6 14 0 60.62 85.82 22.44 o 7 14 0 491.77 499.41 39.03 o 8 14 0 419.93 376.00 37.49 o 9 14 0 0.81 -3.27 31.34 o 10 14 0 88.51 154.98 47.58 o 11 14 0 37.31 1.41 35.63 o 12 14 0 1.28 5.64 41.70 o 13 14 0 89.22 84.67 52.04 o 1 15 0 7.21 -7.43 15.21 o 2 15 0 11.65 -10.73 20.51 o 3 15 0 115.23 126.43 23.76 o 4 15 0 136.14 160.61 25.62 o 5 15 0 1842.36 1848.89 45.85 o 6 15 0 81.64 46.42 25.98 o 7 15 0 1389.73 1311.64 49.89 o 8 15 0 200.76 181.27 34.84 o 9 15 0 79.35 79.25 34.35 o 10 15 0 0.18 -32.00 32.00 o 11 15 0 1.05 2.69 36.02 o 12 15 0 72.74 40.61 45.18 o 13 15 0 0.51 59.39 89.80 o 0 16 0 717.26 709.42 55.60 o 1 16 0 8.26 -14.60 21.07 o 2 16 0 254.09 256.86 26.00 o 3 16 0 266.32 265.56 27.33 o 4 16 0 77.00 62.11 25.27 o 5 16 0 135.11 116.88 27.64 o 6 16 0 26.44 11.68 25.35 o 7 16 0 603.36 559.63 60.27 o 8 16 0 54.03 56.10 32.88 o 9 16 0 2.31 21.24 34.31 o 10 16 0 16.50 21.74 35.41 o 11 16 0 3.11 44.79 39.18 o 12 16 0 35.83 51.06 49.96 o 13 16 0 27.67 -48.67 48.67 o 1 17 0 512.89 511.05 35.04 o 2 17 0 519.55 549.08 30.57 o 3 17 0 180.72 185.32 27.69 o 4 17 0 5.03 -9.09 25.81 o 5 17 0 982.89 971.31 49.61 o 6 17 0 474.68 456.45 38.54 o 7 17 0 57.00 51.81 53.17 o 8 17 0 103.63 102.70 45.09 o 9 17 0 159.41 217.39 39.14 o 10 17 0 70.22 90.47 37.30 o 11 17 0 1.16 -15.48 41.11 o 12 17 0 24.89 32.86 49.89 o 0 18 0 790.93 814.16 62.39 o 1 18 0 282.52 304.96 33.06 o 2 18 0 18.53 10.55 29.24 o 3 18 0 9.73 -7.74 28.85 o 4 18 0 39.39 27.52 26.25 o 5 18 0 245.96 276.11 36.90 o 6 18 0 26.46 -29.66 29.66 o 7 18 0 61.81 46.87 34.16 o 8 18 0 20.71 12.67 34.47 o 9 18 0 0.22 -21.24 34.30 o 10 18 0 15.45 58.55 39.21 o 11 18 0 6.45 0.22 42.32 o 12 18 0 5.13 40.90 52.47 o 1 19 0 92.94 87.56 32.53 o 2 19 0 1474.59 1426.81 53.19 o 3 19 0 228.07 218.91 32.78 o 4 19 0 65.81 15.44 32.63 o 5 19 0 385.19 413.24 36.47 o 6 19 0 34.88 17.01 32.37 o 7 19 0 0.00 17.17 34.25 o 8 19 0 15.55 4.48 34.67 o 9 19 0 1.44 23.08 37.19 o 10 19 0 0.22 -34.05 38.51 o 11 19 0 36.01 46.78 46.12 o 12 19 0 47.95 -13.84 53.89 o 0 20 0 315.66 271.00 47.32 o 1 20 0 444.06 423.32 36.76 o 2 20 0 220.77 288.45 38.95 o 3 20 0 0.71 -6.10 28.77 o 4 20 0 374.25 382.78 51.86 o 5 20 0 18.59 -11.13 29.19 o 6 20 0 148.86 72.56 38.24 o 7 20 0 59.01 33.92 42.61 o 8 20 0 1.81 -32.86 51.65 o 9 20 0 10.37 -36.63 61.38 o 10 20 0 53.33 53.38 68.73 o 11 20 0 4.34 37.20 46.48 o 1 21 0 93.34 61.22 30.70 o 2 21 0 8.25 -29.17 29.17 o 3 21 0 3.52 9.18 29.98 o 4 21 0 2.83 28.50 30.77 o 5 21 0 4.22 -35.28 35.28 o 6 21 0 3.56 1.34 41.18 o 7 21 0 4.03 -45.61 45.61 o 8 21 0 22.17 -11.22 66.33 o 9 21 0 43.16 89.14 80.42 o 10 21 0 1.77 -18.98 83.28 o 11 21 0 2.78 61.28 97.90 o 0 22 0 10.19 -24.49 78.50 o 1 22 0 84.66 19.69 31.21 o 2 22 0 343.21 333.33 37.00 o 3 22 0 18.73 -4.75 31.25 o 4 22 0 100.21 74.34 33.89 o 5 22 0 6.16 -28.26 39.11 o 6 22 0 3.79 6.28 42.08 o 7 22 0 22.62 22.89 44.05 o 8 22 0 79.72 124.43 49.31 o 9 22 0 2.00 18.16 83.16 o 10 22 0 0.40 -56.23 65.37 o 1 23 0 13.65 7.95 32.38 o 2 23 0 0.00 -31.17 31.17 o 3 23 0 24.55 16.25 36.78 o 4 23 0 10.42 15.55 43.04 o 5 23 0 20.16 30.97 44.22 o 6 23 0 4.28 -1.79 52.68 o 7 23 0 28.64 13.69 45.81 o 8 23 0 7.94 2.91 80.89 o 9 23 0 6.81 -16.09 50.35 o 0 24 0 55.31 -3.96 46.40 o 1 24 0 2.96 -13.26 32.55 o 2 24 0 0.01 12.13 34.23 o 3 24 0 12.07 -32.65 32.65 o 4 24 0 18.11 5.26 35.75 o 5 24 0 26.64 -2.15 43.97 o 6 24 0 16.26 2.67 57.59 o 7 24 0 8.70 6.91 47.40 o 8 24 0 0.01 10.21 79.07 o 9 24 0 57.09 36.40 53.10 o 1 25 0 18.67 -36.09 36.09 o 2 25 0 16.53 -21.16 33.94 o 3 25 0 2.43 -26.84 36.79 o 4 25 0 174.32 192.29 51.12 o 5 25 0 0.96 -42.81 42.81 o 6 25 0 16.30 -29.77 98.35 o 7 25 0 2.26 -13.10 48.10 o 8 25 0 0.64 -53.13 53.13 o 0 26 0 1.00 -47.97 47.97 o 1 26 0 0.50 -33.82 33.82 o 2 26 0 0.09 -48.05 48.05 o 3 26 0 27.61 21.29 42.61 o 4 26 0 0.17 -36.65 52.67 o 5 26 0 83.17 -22.77 46.47 o 6 26 0 11.24 -47.85 50.24 o 7 26 0 23.29 -48.97 48.97 o 1 27 0 29.70 -26.24 44.39 o 2 27 0 0.95 -42.74 42.74 o 3 27 0 0.02 -38.93 38.93 o 4 27 0 59.06 73.82 83.99 o 5 27 0 56.34 -82.33 93.60 o 6 27 0 0.65 -49.08 78.54 o 0 28 0 0.09 -78.37 105.05 o 1 28 0 24.14 30.48 47.86 o 2 28 0 36.45 63.95 43.67 o 3 28 0 9.44 -13.44 67.40 o 4 28 0 1.58 -43.82 55.01 o 1 29 0 21.31 -18.93 50.05 o 2 29 0 1.02 0.47 47.81 o 2 0 1 20432.50 18761.44 162.38 o 4 0 1 206.65 229.69 11.33 o 6 0 1 5915.05 6036.64 65.91 o 8 0 1 1160.04 1107.52 28.98 o 10 0 1 11.80 31.35 23.47 o 12 0 1 773.95 767.24 48.47 o 14 0 1 22.23 74.59 47.85 o 0 1 1 692.31 665.75 10.06 o 1 1 1 4374.76 4184.47 26.97 o 2 1 1 22745.90 20672.44 122.73 o 3 1 1 3073.23 2871.95 22.71 o 4 1 1 2384.45 2259.66 20.68 o 5 1 1 397.17 420.42 10.49 o 6 1 1 584.26 595.41 13.21 o 7 1 1 914.42 893.37 16.33 o 8 1 1 1107.76 1110.54 19.57 o 9 1 1 0.72 0.00 13.27 o 10 1 1 758.18 790.76 23.73 o 11 1 1 64.67 56.80 20.64 o 12 1 1 631.91 617.34 33.57 o 13 1 1 31.22 30.76 26.08 o 14 1 1 34.52 42.79 40.77 o 15 1 1 30.10 17.10 59.59 o 1 2 1 3508.58 3199.62 22.51 o 2 2 1 4819.15 4364.78 31.68 o 3 2 1 329.01 319.75 9.78 o 4 2 1 356.38 353.97 10.36 o 5 2 1 417.34 449.64 12.02 o 6 2 1 237.83 254.29 10.70 o 7 2 1 190.77 198.11 10.88 o 8 2 1 199.23 221.36 12.71 o 9 2 1 426.35 437.95 17.85 o 10 2 1 178.49 160.57 23.30 o 11 2 1 18.13 20.30 20.64 o 12 2 1 143.49 125.15 25.50 o 13 2 1 145.29 123.01 28.02 o 14 2 1 11.46 -30.43 30.43 o 15 2 1 23.29 -21.74 41.15 o 0 3 1 7781.23 7078.28 61.49 o 1 3 1 169.58 163.15 6.92 o 2 3 1 126.44 139.93 10.50 o 3 3 1 484.59 498.00 11.33 o 4 3 1 1728.26 1565.18 19.05 o 5 3 1 254.96 298.57 11.33 o 6 3 1 151.37 178.73 13.68 o 7 3 1 23.86 16.12 10.70 o 8 3 1 52.61 72.94 13.05 o 9 3 1 112.35 114.95 15.20 o 10 3 1 199.21 211.31 17.38 o 11 3 1 37.41 27.94 20.34 o 12 3 1 142.93 139.21 26.04 o 13 3 1 9.58 -2.35 24.91 o 14 3 1 154.30 189.04 35.25 o 15 3 1 27.47 82.48 48.75 o 1 4 1 869.81 810.55 12.89 o 2 4 1 54.81 57.34 7.66 o 3 4 1 269.88 224.69 9.69 o 4 4 1 410.76 420.19 11.93 o 5 4 1 1528.01 1542.18 20.19 o 6 4 1 343.74 356.63 13.59 o 7 4 1 187.81 194.10 13.09 o 8 4 1 31.63 19.73 12.90 o 9 4 1 582.93 593.35 20.05 o 10 4 1 245.15 201.37 19.74 o 11 4 1 102.90 90.54 21.43 o 12 4 1 19.54 32.56 21.85 o 13 4 1 34.36 79.61 26.43 o 14 4 1 2.95 33.63 33.37 o 15 4 1 80.56 103.41 67.16 o 0 5 1 7552.01 6891.41 62.84 o 1 5 1 1624.24 1463.84 17.02 o 2 5 1 1085.62 1019.44 13.92 o 3 5 1 560.95 555.12 11.26 o 4 5 1 909.36 864.29 15.45 o 5 5 1 219.75 219.43 11.76 o 6 5 1 27.25 19.63 10.65 o 7 5 1 160.28 163.20 15.05 o 8 5 1 126.67 115.79 14.82 o 9 5 1 352.20 381.04 18.68 o 10 5 1 274.46 269.18 20.73 o 11 5 1 152.29 123.80 22.29 o 12 5 1 71.79 47.56 22.50 o 13 5 1 37.90 46.88 26.48 o 14 5 1 21.51 9.37 32.09 o 15 5 1 21.87 49.87 36.50 o 1 6 1 2.65 17.42 7.45 o 2 6 1 1652.21 1561.54 19.07 o 3 6 1 835.77 816.92 13.49 o 4 6 1 3097.31 3015.99 28.30 o 5 6 1 228.22 265.38 12.74 o 6 6 1 1201.12 1210.04 20.80 o 7 6 1 258.23 274.88 16.47 o 8 6 1 381.42 392.91 17.83 o 9 6 1 438.15 459.68 20.00 o 10 6 1 958.41 1004.21 38.38 o 11 6 1 117.82 111.84 22.50 o 12 6 1 207.11 206.94 25.40 o 13 6 1 16.18 55.01 26.58 o 14 6 1 34.18 57.15 35.22 o 15 6 1 16.76 16.22 37.12 o 0 7 1 2788.30 2685.69 35.70 o 1 7 1 341.15 360.86 10.31 o 2 7 1 632.18 652.23 12.14 o 3 7 1 1832.87 1786.97 19.53 o 4 7 1 505.84 515.19 13.29 o 5 7 1 476.48 501.97 14.84 o 6 7 1 101.08 107.28 12.63 o 7 7 1 23.93 2.64 13.12 o 8 7 1 276.03 287.62 17.42 o 9 7 1 239.47 241.91 19.93 o 10 7 1 331.97 356.50 21.93 o 11 7 1 123.16 84.66 20.73 o 12 7 1 4.65 2.46 22.46 o 13 7 1 154.51 143.16 28.59 o 14 7 1 49.59 9.48 42.92 o 15 7 1 1.57 -38.29 38.29 o 1 8 1 712.87 759.53 13.89 o 2 8 1 109.39 132.22 9.44 o 3 8 1 1359.77 1329.28 20.21 o 4 8 1 89.49 82.04 9.87 o 5 8 1 401.73 413.44 13.19 o 6 8 1 6.48 -8.16 9.89 o 7 8 1 5.78 14.42 13.73 o 8 8 1 200.86 210.50 17.33 o 9 8 1 925.38 884.56 26.38 o 10 8 1 22.56 12.07 18.13 o 11 8 1 379.85 373.64 24.87 o 12 8 1 26.81 -3.15 22.92 o 13 8 1 98.63 87.43 30.25 o 14 8 1 36.46 85.28 41.99 o 15 8 1 39.75 -12.64 66.71 o 0 9 1 0.25 10.70 15.43 o 1 9 1 1447.81 1425.93 18.40 o 2 9 1 661.34 696.34 14.81 o 3 9 1 2537.68 2591.41 25.40 o 4 9 1 485.40 496.74 13.93 o 5 9 1 826.42 862.26 17.30 o 6 9 1 25.75 23.97 10.99 o 7 9 1 10.15 -2.45 14.57 o 8 9 1 217.15 232.22 19.15 o 9 9 1 321.00 341.52 22.42 o 10 9 1 40.69 16.87 19.09 o 11 9 1 584.17 608.39 31.97 o 12 9 1 92.39 111.20 25.01 o 13 9 1 101.18 71.62 26.92 o 14 9 1 17.61 0.40 33.71 o 1 10 1 57.23 61.28 9.76 o 2 10 1 223.42 235.64 11.90 o 3 10 1 52.02 61.93 9.69 o 4 10 1 582.88 638.23 15.34 o 5 10 1 46.47 57.79 11.40 o 6 10 1 188.27 188.46 13.64 o 7 10 1 821.83 836.03 22.62 o 8 10 1 580.73 590.91 22.44 o 9 10 1 28.60 14.69 18.25 o 10 10 1 252.71 274.31 22.08 o 11 10 1 89.94 90.56 21.69 o 12 10 1 84.99 49.59 24.13 o 13 10 1 48.68 0.53 25.78 o 14 10 1 140.50 186.54 40.73 o 0 11 1 1453.32 1487.08 31.58 o 1 11 1 278.04 283.47 12.42 o 2 11 1 423.38 463.48 14.41 o 3 11 1 502.85 541.45 13.96 o 4 11 1 190.99 246.47 15.99 o 5 11 1 15.17 2.72 11.48 o 6 11 1 186.31 204.35 14.62 o 7 11 1 64.35 70.32 16.43 o 8 11 1 389.41 402.84 23.16 o 9 11 1 722.36 683.28 25.32 o 10 11 1 160.57 165.32 21.17 o 11 11 1 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