#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/29/2212901.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212901_Fobs loop_ _publ_author_name 'Hu, Tong-Liang' 'Tian, Jin-Lei' _publ_section_title ; trans-Bis[(2E)-3-(N,N-dimethylamino)-1-(2-pyridyl)prop-2-en-1-one-\k^2^N,O]bis(perchlorato-\kO)cadmium(II) ; _journal_coeditor_code HB2326 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1092 _journal_page_last m1093 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 78.656 _cell_angle_beta 79.377 _cell_angle_gamma 71.775 _cell_length_a 7.3648 _cell_length_b 9.3606 _cell_length_c 9.8394 _exptl_crystal_F_000 334.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file hb2326Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 187.32 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1872.29 1579.95 58.30 o 2 0 0 40.09 44.14 2.09 o 3 0 0 2330.15 2484.89 88.84 o 4 0 0 610.84 711.13 26.26 o 5 0 0 20.94 20.43 1.96 o 6 0 0 60.55 63.76 2.46 o 8 0 0 0.69 3.58 1.41 o -6 1 0 624.74 625.48 20.95 o -5 1 0 489.46 522.93 13.12 o -2 1 0 3573.92 3228.41 84.33 o -1 1 0 18.70 27.19 1.30 o 0 1 0 2576.50 2256.89 55.02 o 1 1 0 5152.27 5527.80 200.42 o 2 1 0 16.81 20.18 1.25 o 3 1 0 2030.64 2215.18 79.40 o 4 1 0 2182.43 2214.26 79.58 o 5 1 0 84.60 101.98 4.96 o 6 1 0 22.94 18.56 2.11 o 7 1 0 84.80 98.28 5.37 o -6 2 0 33.95 29.81 2.31 o -5 2 0 479.02 493.77 16.74 o -4 2 0 479.86 477.57 16.02 o -3 2 0 656.23 712.72 17.25 o -2 2 0 2334.96 2114.58 80.13 o -1 2 0 2662.02 2590.16 81.45 o 0 2 0 2433.12 2382.61 56.65 o 1 2 0 3679.47 3923.82 94.15 o 2 2 0 4765.87 4683.12 169.75 o 3 2 0 31.46 40.06 2.31 o 4 2 0 623.77 652.35 24.36 o 5 2 0 1530.73 1565.38 56.97 o 6 2 0 406.13 404.83 13.44 o 7 2 0 7.74 8.42 1.58 o 8 2 0 167.48 189.48 9.07 o -6 3 0 15.94 12.85 1.58 o -5 3 0 62.19 55.04 3.06 o -4 3 0 525.49 446.66 15.25 o -3 3 0 578.27 546.82 18.21 o -2 3 0 137.30 143.20 5.49 o -1 3 0 1335.41 1362.13 43.40 o 0 3 0 345.96 325.27 8.04 o 1 3 0 181.03 199.75 5.19 o 2 3 0 176.02 178.11 6.58 o 3 3 0 268.87 217.15 4.36 o 4 3 0 200.69 196.55 5.12 o 5 3 0 971.16 940.99 36.33 o 6 3 0 774.18 785.37 29.75 o 7 3 0 1.99 0.94 1.09 o 8 3 0 74.80 81.28 5.13 o -6 4 0 79.17 82.58 4.27 o -5 4 0 0.84 0.17 0.78 o -4 4 0 57.64 56.13 3.08 o -3 4 0 802.53 734.54 24.36 o -2 4 0 607.00 642.61 21.39 o -1 4 0 595.39 558.93 18.63 o 0 4 0 955.40 902.46 21.73 o 1 4 0 2223.11 2245.83 53.14 o 2 4 0 42.75 45.65 1.78 o 3 4 0 1496.24 1501.59 35.91 o 4 4 0 1959.03 2096.42 49.86 o 5 4 0 232.22 244.24 10.37 o 6 4 0 526.86 506.92 19.98 o 7 4 0 411.01 378.25 15.72 o 8 4 0 16.44 27.42 2.94 o -6 5 0 82.56 78.76 4.40 o -5 5 0 58.06 56.03 3.41 o -4 5 0 31.69 33.66 2.46 o -3 5 0 318.95 347.39 12.57 o -2 5 0 965.54 952.55 31.33 o -1 5 0 259.60 265.47 9.77 o 0 5 0 1296.58 1352.29 32.29 o 1 5 0 2183.54 2276.18 54.04 o 2 5 0 932.89 1007.04 24.39 o 3 5 0 148.47 177.64 14.76 o 4 5 0 913.40 874.77 40.16 o 5 5 0 331.53 333.24 8.84 o 6 5 0 0.23 -0.54 0.80 o 7 5 0 214.51 196.45 9.30 o 8 5 0 25.11 27.56 2.95 o -5 6 0 73.89 66.91 3.98 o -4 6 0 200.02 205.45 8.46 o -3 6 0 46.69 46.15 3.05 o -2 6 0 395.20 384.46 13.93 o -1 6 0 247.23 262.26 9.99 o 0 6 0 78.15 70.08 3.64 o 1 6 0 278.10 275.56 7.32 o 2 6 0 1516.02 1563.67 37.58 o 3 6 0 632.58 683.48 17.05 o 4 6 0 305.89 299.07 8.81 o 5 6 0 659.65 628.04 15.87 o 6 6 0 9.98 6.98 1.37 o 7 6 0 9.24 8.01 1.62 o 8 6 0 136.59 130.29 7.28 o -4 7 0 130.35 123.12 6.02 o -3 7 0 179.24 183.29 7.95 o -2 7 0 52.39 49.19 3.33 o -1 7 0 467.08 522.53 18.54 o 0 7 0 138.10 126.12 5.82 o 1 7 0 33.18 28.26 2.26 o 2 7 0 1033.14 1055.29 25.82 o 3 7 0 181.91 187.42 5.53 o 4 7 0 14.35 9.51 0.96 o 5 7 0 57.05 59.37 2.49 o 6 7 0 404.02 382.10 10.34 o 7 7 0 32.28 30.51 3.05 o -3 8 0 29.72 39.57 3.26 o -2 8 0 6.68 6.15 1.47 o -1 8 0 23.45 23.81 2.46 o 0 8 0 287.44 309.74 12.07 o 1 8 0 103.57 99.12 5.04 o 2 8 0 237.81 236.67 9.36 o 3 8 0 206.28 205.23 6.09 o 4 8 0 53.86 51.16 2.40 o 5 8 0 55.02 55.12 2.52 o 6 8 0 226.61 210.42 6.41 o 7 8 0 91.43 89.67 5.73 o -2 9 0 128.99 148.01 7.40 o -1 9 0 27.96 26.99 2.81 o 0 9 0 23.28 30.04 2.90 o 1 9 0 251.73 277.02 11.21 o 2 9 0 45.03 42.25 3.15 o 3 9 0 261.71 239.43 9.77 o 4 9 0 328.66 324.39 9.14 o 5 9 0 138.83 133.56 4.63 o 6 9 0 32.46 34.77 2.10 o -1 10 0 123.35 149.65 7.74 o 0 10 0 12.73 13.80 2.21 o 1 10 0 74.56 78.74 4.95 o 2 10 0 55.97 58.91 4.07 o 3 10 0 64.26 61.57 4.11 o 4 10 0 28.25 24.00 2.53 o 5 10 0 60.51 60.37 2.97 o -5 -10 1 34.95 33.11 2.10 o -4 -10 1 6.16 5.67 1.50 o -3 -10 1 163.81 170.34 8.02 o -2 -10 1 237.49 232.86 10.12 o -1 -10 1 2.48 2.98 1.34 o 0 -10 1 12.63 12.85 2.18 o -6 -9 1 57.64 52.88 2.68 o -5 -9 1 188.85 189.90 6.07 o -4 -9 1 148.76 138.31 4.72 o -3 -9 1 84.67 83.03 4.72 o -2 -9 1 502.88 523.38 18.92 o -1 -9 1 54.10 52.40 3.69 o 0 -9 1 0.96 1.73 1.12 o 1 -9 1 128.58 148.87 7.45 o 2 -9 1 45.79 53.89 4.10 o -7 -8 1 94.18 89.08 5.68 o -6 -8 1 58.21 55.39 2.67 o -5 -8 1 106.73 107.35 3.93 o -4 -8 1 134.69 124.02 4.25 o -3 -8 1 5.88 8.64 1.00 o -2 -8 1 0.51 5.22 1.28 o -1 -8 1 354.47 355.07 13.31 o 0 -8 1 152.20 206.02 8.73 o 1 -8 1 10.79 7.13 1.52 o 2 -8 1 151.14 168.75 7.87 o 3 -8 1 52.95 46.41 3.57 o -7 -7 1 134.31 135.37 7.38 o -6 -7 1 270.20 260.62 7.58 o -5 -7 1 111.51 98.32 4.73 o -4 -7 1 220.17 209.29 6.18 o -3 -7 1 598.25 611.46 15.57 o -2 -7 1 7.06 6.49 1.04 o -1 -7 1 228.78 205.65 8.23 o 0 -7 1 266.14 277.97 10.72 o 1 -7 1 8.82 7.40 1.47 o 2 -7 1 175.13 181.33 7.90 o 3 -7 1 394.18 446.05 16.40 o 4 -7 1 105.46 105.42 5.51 o -8 -6 1 47.60 47.14 3.99 o -7 -6 1 0.15 0.24 0.93 o -6 -6 1 118.87 121.80 6.49 o -5 -6 1 563.43 539.29 13.92 o -4 -6 1 52.11 53.63 3.84 o -3 -6 1 1198.50 1271.34 30.86 o -2 -6 1 519.52 484.52 16.81 o -1 -6 1 251.89 214.42 6.24 o 0 -6 1 301.53 313.01 11.47 o 1 -6 1 320.00 336.30 12.37 o 2 -6 1 132.39 129.93 5.90 o 3 -6 1 23.59 22.49 2.14 o 4 -6 1 157.76 150.22 6.70 o 5 -6 1 17.25 17.06 2.04 o -8 -5 1 148.58 135.72 7.39 o -7 -5 1 32.66 25.35 2.76 o -6 -5 1 37.98 34.51 2.99 o -5 -5 1 1137.08 1150.30 28.04 o -4 -5 1 298.34 265.62 7.26 o -3 -5 1 33.62 30.11 1.48 o -2 -5 1 2554.18 2639.78 62.51 o -1 -5 1 1257.90 1323.71 31.71 o 0 -5 1 1135.13 1247.54 40.28 o 1 -5 1 942.74 1020.05 33.33 o 2 -5 1 387.96 406.64 14.34 o 3 -5 1 33.29 30.54 2.27 o 4 -5 1 21.59 26.01 2.15 o 5 -5 1 193.81 188.30 7.80 o 6 -5 1 2.00 2.98 1.05 o -8 -4 1 147.80 138.95 7.42 o -7 -4 1 282.61 266.89 11.81 o -6 -4 1 289.89 262.98 11.44 o -5 -4 1 223.38 223.42 9.73 o -4 -4 1 1289.98 1305.51 31.47 o -3 -4 1 53.29 52.74 1.98 o -2 -4 1 1809.95 1977.47 47.04 o -1 -4 1 2633.40 2597.71 48.21 o 0 -4 1 312.01 295.72 10.30 o 1 -4 1 703.84 816.39 19.81 o 2 -4 1 167.02 139.25 5.61 o 3 -4 1 264.43 266.55 9.79 o 4 -4 1 36.95 38.07 2.50 o 5 -4 1 95.12 101.09 4.73 o 6 -4 1 66.36 63.04 3.66 o -8 -3 1 27.04 32.71 3.13 o -7 -3 1 290.07 287.98 12.49 o -6 -3 1 623.41 665.70 25.65 o -5 -3 1 10.93 10.92 1.68 o -4 -3 1 373.52 377.15 14.83 o -3 -3 1 249.48 201.16 5.45 o -2 -3 1 15.94 14.00 0.81 o -1 -3 1 1588.52 1556.55 29.06 o 0 -3 1 2891.10 3005.88 94.50 o 1 -3 1 420.24 397.31 9.82 o 2 -3 1 268.99 310.04 10.74 o 3 -3 1 1331.18 1443.63 46.20 o 4 -3 1 475.85 482.36 16.37 o 5 -3 1 9.65 7.15 1.11 o 6 -3 1 111.14 114.17 5.12 o -7 -2 1 155.07 165.83 8.04 o -6 -2 1 107.90 113.44 5.79 o -5 -2 1 357.85 321.60 13.04 o -4 -2 1 1133.51 1158.36 42.43 o -3 -2 1 3209.65 3680.53 131.45 o -2 -2 1 904.92 962.40 23.13 o -1 -2 1 78.81 77.34 1.67 o 1 -2 1 1.69 6.98 0.67 o 3 -2 1 1553.09 1716.42 76.43 o 4 -2 1 2294.78 2329.31 73.60 o 5 -2 1 50.97 44.39 2.46 o 6 -2 1 11.52 7.90 1.16 o 7 -2 1 272.84 265.36 10.26 o -6 -1 1 141.84 161.71 7.53 o -5 -1 1 432.55 469.07 18.18 o -4 -1 1 1446.89 1645.72 59.58 o -3 -1 1 1317.58 1499.51 54.16 o -2 -1 1 2211.03 2385.35 85.34 o -1 -1 1 5416.21 5696.54 137.37 o 0 -1 1 791.01 734.69 26.64 o 1 -1 1 2296.17 2532.42 60.52 o 2 -1 1 2033.95 1977.55 46.57 o 3 -1 1 7.27 15.24 2.34 o 4 -1 1 1256.40 1218.58 38.84 o 5 -1 1 785.47 763.45 24.87 o 6 -1 1 144.99 139.17 5.60 o 7 -1 1 138.51 139.20 6.39 o 8 -1 1 89.77 94.92 5.27 o -7 0 1 278.38 259.30 9.83 o -6 0 1 158.49 162.79 7.47 o -4 0 1 1227.62 1266.81 46.09 o -3 0 1 2001.65 2047.25 73.52 o -2 0 1 487.31 537.43 19.79 o -1 0 1 10906.07 12339.88 446.14 o 0 0 1 3376.24 3034.93 111.74 o 1 0 1 794.78 836.51 24.25 o 2 0 1 5768.08 5557.39 119.19 o 3 0 1 258.51 234.44 8.85 o 4 0 1 103.51 111.58 3.20 o 5 0 1 691.31 770.16 36.35 o 6 0 1 164.76 168.95 6.67 o 7 0 1 92.50 93.63 4.88 o 8 0 1 24.60 29.56 2.82 o -7 1 1 131.69 132.13 5.87 o -6 1 1 692.73 757.32 25.36 o -5 1 1 0.55 1.08 0.48 o -4 1 1 208.34 215.54 8.84 o -3 1 1 4727.59 4779.48 170.17 o -2 1 1 769.27 767.24 27.81 o -1 1 1 137.27 140.74 3.90 o 0 1 1 1294.92 1377.38 67.38 o 1 1 1 2222.28 2230.31 52.46 o 3 1 1 2320.85 2372.94 54.63 o 4 1 1 1003.62 1056.63 28.83 o 5 1 1 91.49 89.67 2.99 o 6 1 1 140.27 144.36 3.51 o 7 1 1 33.53 33.56 2.83 o 8 1 1 61.91 64.91 4.15 o -7 2 1 0.24 0.72 0.94 o -6 2 1 318.91 299.74 11.10 o -5 2 1 345.04 330.26 11.79 o -4 2 1 9.04 13.47 1.73 o -3 2 1 1698.56 1679.54 39.84 o -2 2 1 2166.41 1949.68 46.05 o -1 2 1 72.95 67.77 1.98 o 0 2 1 885.28 963.90 22.95 o 2 2 1 1034.43 1055.42 24.42 o 3 2 1 20.75 19.77 1.02 o 4 2 1 960.94 835.83 19.74 o 5 2 1 133.44 117.44 3.61 o 6 2 1 3.24 1.19 1.16 o 7 2 1 313.27 339.28 17.94 o -7 3 1 42.18 43.76 3.03 o -6 3 1 10.92 10.73 1.55 o -5 3 1 495.19 519.97 17.88 o -4 3 1 280.22 272.76 9.90 o -3 3 1 85.50 93.32 4.02 o -2 3 1 1206.31 1068.89 25.63 o -1 3 1 55.64 46.14 2.25 o 0 3 1 63.36 70.46 2.78 o 1 3 1 553.24 524.76 12.72 o 2 3 1 6466.17 7051.19 168.36 o 3 3 1 1627.21 1654.87 30.87 o 4 3 1 1.33 0.74 0.44 o 5 3 1 1657.04 1667.21 38.95 o 6 3 1 128.99 123.32 3.94 o 7 3 1 101.89 93.63 5.23 o 8 3 1 123.87 138.10 7.21 o -6 4 1 7.49 7.94 1.40 o -5 4 1 12.62 11.74 1.54 o -4 4 1 964.70 937.73 30.81 o -3 4 1 119.39 97.70 4.33 o -2 4 1 350.66 344.29 12.02 o -1 4 1 1457.77 1433.65 34.15 o 0 4 1 2394.85 2484.66 58.84 o 1 4 1 1470.07 1605.01 42.17 o 2 4 1 1140.77 1182.05 28.28 o 3 4 1 3783.74 4110.82 96.74 o 4 4 1 16.49 20.59 0.80 o 5 4 1 532.59 466.46 18.19 o 6 4 1 1204.06 1191.45 44.22 o 7 4 1 36.92 31.78 2.89 o 8 4 1 11.68 9.74 1.68 o -6 5 1 157.43 151.63 6.88 o -5 5 1 64.67 64.42 3.70 o -4 5 1 75.49 67.13 3.69 o -3 5 1 624.04 605.94 20.61 o -2 5 1 147.10 167.47 6.75 o -1 5 1 907.99 936.36 30.69 o 0 5 1 1023.62 958.08 23.18 o 1 5 1 986.62 1121.03 26.95 o 2 5 1 183.42 191.32 5.24 o 3 5 1 376.90 354.30 15.25 o 4 5 1 1341.34 1422.74 105.16 o 5 5 1 6.98 4.98 1.03 o 6 5 1 490.62 468.38 18.75 o 7 5 1 116.10 124.05 6.60 o 8 5 1 0.84 0.17 1.04 o -5 6 1 149.97 138.55 6.47 o -4 6 1 6.84 3.76 1.15 o -3 6 1 328.58 334.76 12.42 o -2 6 1 1246.44 1272.33 41.57 o -1 6 1 506.91 517.57 17.93 o 0 6 1 30.85 18.79 1.76 o 1 6 1 730.43 705.44 17.41 o 2 6 1 941.23 1010.89 24.58 o 3 6 1 0.56 0.40 1.13 o 4 6 1 688.71 699.88 17.37 o 5 6 1 191.00 180.73 5.29 o 6 6 1 88.24 67.00 4.33 o 7 6 1 257.49 229.33 10.61 o 8 6 1 103.43 98.08 5.94 o -4 7 1 29.19 22.80 2.36 o -3 7 1 9.69 9.38 1.54 o -2 7 1 209.21 201.71 8.39 o -1 7 1 477.30 475.33 16.98 o 0 7 1 45.39 41.60 2.83 o 1 7 1 500.68 527.91 13.40 o 2 7 1 893.39 965.59 23.67 o 3 7 1 0.55 3.33 0.90 o 4 7 1 9.90 8.96 2.15 o 5 7 1 218.10 202.29 5.93 o 6 7 1 101.79 94.92 5.56 o 7 7 1 45.44 38.57 3.42 o 8 7 1 73.00 67.74 4.85 o -3 8 1 0.66 0.81 0.94 o -2 8 1 7.64 7.00 1.48 o -1 8 1 199.55 218.58 9.24 o 0 8 1 361.86 360.98 13.67 o 1 8 1 0.24 -0.20 0.69 o 2 8 1 254.86 261.63 7.34 o 3 8 1 1082.44 1157.61 28.41 o 4 8 1 185.60 198.02 6.23 o 5 8 1 286.03 297.34 8.36 o 6 8 1 211.22 218.37 10.26 o 7 8 1 37.26 32.58 3.22 o -2 9 1 70.71 67.07 4.41 o -1 9 1 57.48 62.45 4.25 o 0 9 1 249.41 280.52 11.51 o 1 9 1 12.30 11.40 1.84 o 2 9 1 0.46 4.91 1.30 o 3 9 1 766.84 803.06 20.30 o 4 9 1 249.84 257.06 7.50 o 5 9 1 17.44 20.56 1.57 o 6 9 1 89.08 99.63 5.93 o -1 10 1 24.21 24.48 2.87 o 0 10 1 56.16 71.02 4.75 o 1 10 1 200.36 211.29 9.44 o 2 10 1 77.44 80.51 4.82 o 3 10 1 29.86 31.41 2.85 o 4 10 1 217.25 215.53 9.17 o 5 10 1 62.16 64.65 2.94 o 2 11 1 152.70 166.10 8.10 o 3 11 1 2.94 6.10 1.66 o -4 -10 2 92.65 97.58 5.49 o -3 -10 2 156.33 146.99 7.25 o -2 -10 2 72.37 65.96 4.48 o -1 -10 2 16.15 13.41 2.21 o 0 -10 2 66.30 69.25 4.74 o -5 -9 2 100.11 91.28 5.02 o -4 -9 2 14.43 14.73 1.99 o -3 -9 2 50.05 53.02 3.66 o -2 -9 2 99.45 96.57 5.30 o -1 -9 2 81.78 80.34 4.76 o 0 -9 2 67.05 70.69 4.49 o 1 -9 2 82.29 87.54 5.35 o 2 -9 2 0.77 0.58 1.16 o -6 -8 2 54.22 51.74 3.45 o -5 -8 2 292.57 269.59 7.91 o -4 -8 2 1.51 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219.06 242.78 11.09 o 2 -2 9 7.83 7.54 1.49 o 3 -2 9 0.96 1.25 1.23 o 4 -2 9 11.48 11.72 2.14 o -4 -1 9 55.80 52.14 4.32 o -3 -1 9 51.98 53.12 4.41 o -2 -1 9 145.38 151.69 8.15 o -1 -1 9 183.95 204.86 10.09 o 0 -1 9 32.35 41.36 3.69 o 1 -1 9 24.87 24.48 2.72 o 2 -1 9 151.39 160.55 5.24 o 3 -1 9 16.65 17.79 1.63 o 4 -1 9 15.96 19.05 2.38 o 5 -1 9 20.88 20.39 2.65 o -4 0 9 91.21 96.49 6.25 o -3 0 9 292.63 273.73 12.73 o -2 0 9 3.09 3.39 1.50 o -1 0 9 113.37 112.73 6.60 o 0 0 9 365.92 413.27 17.44 o 1 0 9 6.28 5.05 1.47 o 2 0 9 148.39 130.78 6.75 o 3 0 9 180.77 172.48 5.58 o 4 0 9 60.99 57.69 2.76 o 5 0 9 8.26 12.25 2.15 o -4 1 9 105.37 118.33 7.10 o -3 1 9 370.92 367.49 16.21 o -2 1 9 250.61 262.48 12.27 o -1 1 9 72.98 75.63 5.13 o 0 1 9 353.11 351.52 15.16 o 1 1 9 198.54 201.69 9.52 o 2 1 9 40.10 38.67 3.19 o 3 1 9 222.44 227.27 11.98 o 4 1 9 188.07 190.26 6.06 o 5 1 9 4.23 4.52 1.02 o 6 1 9 6.65 8.86 2.10 o -3 2 9 85.58 107.40 6.59 o -2 2 9 624.90 635.55 25.57 o -1 2 9 206.84 207.84 10.07 o 0 2 9 2.85 1.67 1.16 o 1 2 9 582.40 603.14 23.90 o 2 2 9 161.34 150.83 7.58 o 3 2 9 0.45 5.85 1.38 o 4 2 9 22.56 18.88 1.65 o 5 2 9 100.40 97.92 3.94 o 6 2 9 6.76 7.62 1.32 o -3 3 9 43.96 58.84 3.05 o -2 3 9 164.49 180.39 9.18 o -1 3 9 393.99 401.51 16.99 o 0 3 9 16.45 11.14 1.80 o 1 3 9 223.45 232.64 10.62 o 2 3 9 396.53 394.52 16.41 o 3 3 9 69.54 60.96 4.13 o 4 3 9 7.87 7.33 1.42 o 5 3 9 132.07 139.39 7.35 o 6 3 9 23.54 24.41 2.25 o -3 4 9 147.37 159.23 5.76 o -2 4 9 75.88 84.99 3.66 o -1 4 9 111.36 124.12 5.61 o 0 4 9 150.83 149.48 4.96 o 1 4 9 5.22 5.42 1.35 o 2 4 9 67.64 66.60 4.39 o 3 4 9 305.88 309.49 13.37 o 4 4 9 47.96 50.26 3.79 o 5 4 9 2.17 1.16 1.05 o 6 4 9 63.40 65.09 5.98 o -2 5 9 157.09 161.52 5.61 o -1 5 9 103.94 102.93 3.98 o 0 5 9 482.97 490.94 13.06 o 1 5 9 213.72 200.35 9.50 o 2 5 9 175.41 170.26 8.34 o 3 5 9 162.44 147.08 7.53 o 4 5 9 94.37 99.39 5.89 o 5 5 9 3.21 4.09 1.42 o 6 5 9 36.79 34.23 3.45 o -1 6 9 144.43 128.49 4.65 o 0 6 9 227.40 224.71 10.45 o 1 6 9 226.94 224.81 10.39 o 2 6 9 242.13 217.28 10.13 o 3 6 9 76.36 78.10 5.03 o 4 6 9 105.63 99.65 5.97 o 5 6 9 85.03 85.09 5.49 o 6 6 9 0.95 0.85 1.07 o 0 7 9 103.85 101.90 5.87 o 1 7 9 60.17 65.26 4.38 o 2 7 9 131.86 132.83 7.08 o 3 7 9 167.37 166.33 8.45 o 4 7 9 89.70 82.37 5.33 o 5 7 9 88.63 82.79 5.57 o 1 8 9 60.62 54.78 4.01 o 2 8 9 27.12 29.03 2.99 o 3 8 9 71.51 70.31 4.84 o 4 8 9 40.88 42.20 3.67 o -1 -3 10 15.02 17.86 2.84 o 0 -3 10 59.94 68.74 4.99 o 1 -3 10 22.59 30.95 3.30 o 2 -3 10 10.54 14.56 2.24 o -2 -2 10 12.66 12.92 2.39 o -1 -2 10 27.72 33.47 3.65 o 0 -2 10 47.83 49.79 4.26 o 1 -2 10 20.02 22.49 2.94 o 2 -2 10 26.43 24.97 2.71 o 3 -2 10 24.19 22.59 2.69 o -2 -1 10 86.15 97.43 6.41 o -1 -1 10 71.89 88.63 6.09 o 0 -1 10 5.53 4.05 1.56 o 1 -1 10 16.78 17.31 2.61 o 2 -1 10 46.56 48.14 3.86 o 3 -1 10 6.56 6.24 1.61 o 4 -1 10 28.21 31.58 3.16 o -3 0 10 24.77 27.27 3.36 o -2 0 10 124.42 141.14 8.14 o -1 0 10 190.35 202.30 10.26 o 0 0 10 56.26 61.83 4.75 o 1 0 10 148.08 147.12 7.81 o 2 0 10 154.38 150.54 7.85 o 3 0 10 46.22 46.79 2.55 o 4 0 10 4.26 3.86 1.00 o -3 1 10 174.04 178.84 9.66 o -2 1 10 160.02 179.38 9.51 o -1 1 10 97.14 102.31 6.50 o 0 1 10 166.07 221.99 10.82 o 1 1 10 194.52 212.84 10.24 o 2 1 10 54.85 56.22 4.27 o 3 1 10 84.98 80.50 5.16 o 4 1 10 0.10 0.19 0.86 o 5 1 10 4.10 4.67 1.30 o -2 2 10 99.57 103.09 6.59 o -1 2 10 34.09 42.96 4.00 o 0 2 10 227.33 228.74 10.93 o 1 2 10 291.33 301.91 13.51 o 2 2 10 42.74 45.97 3.86 o 3 2 10 50.21 45.18 3.64 o 4 2 10 56.40 49.32 3.81 o 5 2 10 4.08 4.96 1.05 o -2 3 10 163.29 183.50 9.64 o -1 3 10 185.23 178.67 9.24 o 0 3 10 33.36 31.67 3.30 o 1 3 10 2.44 4.09 1.48 o 2 3 10 113.25 102.43 6.11 o 3 3 10 27.70 30.46 3.00 o 4 3 10 95.68 84.72 5.27 o 5 3 10 59.27 56.17 4.24 o -2 4 10 125.02 150.76 5.55 o -1 4 10 296.82 312.17 9.28 o 0 4 10 69.84 66.62 4.88 o 1 4 10 10.76 6.20 1.54 o 2 4 10 148.87 137.27 7.36 o 3 4 10 95.11 95.55 5.76 o 4 4 10 2.06 8.07 1.64 o 5 4 10 41.67 45.43 3.86 o -1 5 10 178.47 188.35 6.28 o 0 5 10 380.25 357.62 15.61 o 1 5 10 240.32 217.28 10.44 o 2 5 10 57.25 60.02 4.34 o 3 5 10 187.39 179.10 8.93 o 4 5 10 54.57 49.15 3.98 o 5 5 10 0.53 0.75 1.09 o 0 6 10 91.73 102.85 6.25 o 1 6 10 233.79 207.52 10.06 o 2 6 10 14.01 11.90 1.92 o 3 6 10 67.03 66.52 4.70 o 4 6 10 300.94 283.84 13.03 o 5 6 10 27.01 22.74 2.82 o 1 7 10 143.28 148.05 7.85 o 2 7 10 128.22 118.12 6.71 o 3 7 10 19.35 25.24 2.88 o 4 7 10 68.80 67.47 4.93 o 0 -1 11 24.26 24.72 3.43 o 1 -1 11 61.09 75.03 5.39 o 2 -1 11 0.45 -0.44 1.18 o -1 0 11 93.36 114.92 7.33 o 0 0 11 52.57 55.65 4.73 o 1 0 11 100.29 97.03 6.20 o 2 0 11 29.21 34.83 3.59 o 3 0 11 7.61 6.18 1.58 o -1 1 11 224.26 250.54 12.42 o 0 1 11 68.25 79.57 5.66 o 1 1 11 5.28 5.68 1.74 o 2 1 11 152.63 154.31 8.34 o 3 1 11 14.79 18.04 2.58 o -1 2 11 81.41 98.27 6.60 o 0 2 11 120.86 128.16 7.56 o 1 2 11 5.92 7.35 1.87 o 2 2 11 128.54 133.26 7.57 o 3 2 11 94.44 81.84 5.43 o 4 2 11 12.96 16.18 2.40 o 0 3 11 33.16 36.92 3.77 o 1 3 11 20.00 19.57 2.83 o 2 3 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