#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/29/2212904.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212904_Fobs loop_ _publ_author_name 'Jian-Lan, Cui' 'Cao, Duan-Lin' 'Cai, Jian-Bo' _publ_section_title ; (S)-Tetrahydrofuran-2-carboxamide ; _journal_coeditor_code HB2329 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1973 _journal_page_last o1974 _journal_volume 63 _journal_year 2007 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.4780 _cell_length_b 8.0568 _cell_length_c 13.6415 _exptl_crystal_F_000 248.00 _reflns_d_resolution_high 0.8001 _[local]_cod_data_source_file hb2329Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 61119D in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 86.12 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 546.59 513.16 10.82 o 4 0 0 126.38 123.20 3.07 o 6 0 0 7.39 8.69 2.45 o 1 1 0 2728.56 2396.08 24.92 o 2 1 0 245.92 247.57 3.16 o 3 1 0 109.30 105.88 1.94 o 4 1 0 1.42 0.68 0.84 o 5 1 0 0.36 0.50 0.87 o 6 1 0 4.96 5.20 1.56 o 0 2 0 682.12 741.94 14.21 o 1 2 0 702.88 625.46 8.09 o 2 2 0 235.00 250.87 3.29 o 3 2 0 38.77 39.97 1.14 o 4 2 0 2.44 2.58 0.74 o 5 2 0 15.38 16.26 1.33 o 6 2 0 1.88 -0.23 2.24 o 1 3 0 0.74 0.03 0.24 o 2 3 0 591.59 640.05 7.42 o 3 3 0 8.15 7.88 0.77 o 4 3 0 25.90 26.10 1.27 o 5 3 0 13.15 15.46 1.64 o 6 3 0 32.39 32.50 2.80 o 0 4 0 76.36 78.44 1.95 o 1 4 0 301.90 332.50 3.34 o 2 4 0 173.04 163.89 2.28 o 3 4 0 30.64 28.41 1.10 o 4 4 0 67.70 67.34 2.22 o 5 4 0 15.45 17.59 1.89 o 6 4 0 3.39 5.10 1.77 o 1 5 0 0.75 0.94 0.43 o 2 5 0 73.51 79.41 1.82 o 3 5 0 0.31 0.46 0.80 o 4 5 0 3.93 3.65 1.11 o 5 5 0 1.02 1.67 1.23 o 0 6 0 30.97 32.62 1.63 o 1 6 0 23.71 25.01 1.14 o 2 6 0 99.11 86.67 2.06 o 3 6 0 79.02 76.54 2.41 o 4 6 0 24.69 26.13 1.93 o 5 6 0 2.42 0.87 1.40 o 1 7 0 30.72 32.93 1.82 o 2 7 0 103.74 108.53 3.17 o 3 7 0 1.45 1.01 1.07 o 4 7 0 26.72 26.80 2.65 o 0 8 0 0.03 6.54 2.29 o 1 8 0 4.11 3.83 1.17 o 2 8 0 4.17 6.52 1.80 o 3 8 0 0.23 0.59 1.50 o 4 8 0 1.00 1.94 1.77 o 1 9 0 0.01 0.15 1.70 o 2 9 0 20.84 24.54 2.54 o 3 9 0 5.13 6.72 2.00 o 0 10 0 10.36 5.88 3.29 o 1 0 1 37.02 43.31 1.08 o 2 0 1 135.92 148.21 1.99 o 3 0 1 92.77 107.61 3.09 o 4 0 1 137.56 147.38 2.44 o 5 0 1 6.01 4.49 1.28 o 6 0 1 0.91 -0.97 1.41 o 0 1 1 476.71 430.02 6.58 o 1 1 1 1327.10 1276.30 10.21 o 2 1 1 681.27 695.70 5.04 o 3 1 1 163.71 158.53 1.64 o 4 1 1 24.79 23.40 0.94 o 5 1 1 9.85 11.37 0.81 o 6 1 1 3.44 6.44 1.21 o 0 2 1 74.39 63.65 0.81 o 1 2 1 530.35 535.14 4.43 o 2 2 1 307.00 317.57 2.83 o 3 2 1 11.35 11.34 0.48 o 4 2 1 10.23 10.96 0.70 o 5 2 1 9.25 11.30 0.86 o 6 2 1 1.68 2.16 1.11 o 0 3 1 390.70 381.99 3.63 o 1 3 1 731.91 757.12 7.73 o 2 3 1 405.60 427.48 3.49 o 3 3 1 77.58 76.67 1.20 o 4 3 1 92.76 91.20 1.54 o 5 3 1 36.62 38.87 1.37 o 6 3 1 11.72 15.44 1.84 o 0 4 1 97.34 101.80 1.58 o 1 4 1 86.89 94.56 0.91 o 2 4 1 25.34 26.21 0.60 o 3 4 1 32.25 29.68 0.80 o 4 4 1 79.30 80.17 1.55 o 5 4 1 36.00 39.03 1.67 o 6 4 1 10.58 8.99 1.49 o 0 5 1 14.61 11.75 0.54 o 1 5 1 3.81 3.38 0.31 o 2 5 1 33.07 30.76 0.82 o 3 5 1 4.11 4.67 0.63 o 4 5 1 6.19 6.46 0.84 o 5 5 1 4.97 4.71 1.04 o 0 6 1 113.63 104.71 2.64 o 1 6 1 200.48 199.66 2.83 o 2 6 1 24.53 26.48 0.89 o 3 6 1 12.76 13.40 0.95 o 4 6 1 4.11 3.29 0.81 o 5 6 1 0.29 0.62 1.06 o 0 7 1 448.39 446.73 6.02 o 1 7 1 80.74 76.48 1.68 o 2 7 1 28.00 29.48 1.22 o 3 7 1 1.05 1.01 0.76 o 4 7 1 0.49 -0.89 0.89 o 0 8 1 34.79 36.86 2.48 o 1 8 1 27.34 29.64 1.37 o 2 8 1 0.26 -0.45 0.82 o 3 8 1 21.36 22.39 1.64 o 4 8 1 6.45 8.25 1.41 o 0 9 1 2.58 2.33 2.19 o 1 9 1 6.70 4.18 1.25 o 2 9 1 22.05 22.78 2.18 o 3 9 1 2.16 3.33 1.34 o 0 10 1 8.50 10.27 2.37 o 0 0 2 454.54 456.18 9.78 o 1 0 2 7417.04 6569.61 80.71 o 2 0 2 34.83 35.24 0.82 o 3 0 2 3.30 1.64 0.43 o 4 0 2 68.97 72.20 1.68 o 5 0 2 6.41 7.03 1.34 o 6 0 2 15.89 18.40 2.26 o 0 1 2 1342.16 1284.70 13.09 o 1 1 2 370.14 374.60 3.21 o 2 1 2 84.87 82.02 0.90 o 3 1 2 37.30 36.30 0.67 o 4 1 2 5.31 4.24 0.55 o 5 1 2 15.00 15.24 0.93 o 6 1 2 2.44 2.06 1.05 o 0 2 2 494.34 468.40 4.62 o 1 2 2 432.14 447.62 3.86 o 2 2 2 323.10 336.60 2.98 o 3 2 2 67.24 68.35 1.14 o 4 2 2 27.39 25.28 0.85 o 5 2 2 6.57 5.76 0.75 o 6 2 2 12.23 12.04 2.65 o 0 3 2 43.40 51.71 0.85 o 1 3 2 219.55 215.24 2.79 o 2 3 2 57.71 58.06 0.84 o 3 3 2 14.45 17.65 0.66 o 4 3 2 53.92 47.68 1.13 o 5 3 2 35.79 36.62 1.36 o 6 3 2 1.00 0.60 1.16 o 0 4 2 370.58 393.34 3.89 o 1 4 2 83.71 86.49 0.98 o 2 4 2 118.11 136.06 1.65 o 3 4 2 115.86 119.65 1.81 o 4 4 2 5.15 4.81 0.70 o 5 4 2 23.49 23.64 1.35 o 6 4 2 2.13 2.17 1.24 o 0 5 2 2.89 2.86 0.44 o 1 5 2 74.57 74.98 0.95 o 2 5 2 110.02 107.11 1.49 o 3 5 2 12.08 9.92 0.79 o 4 5 2 5.76 4.76 0.81 o 5 5 2 1.36 2.03 0.95 o 0 6 2 7.38 8.44 0.69 o 1 6 2 58.05 59.67 1.24 o 2 6 2 87.48 89.47 1.60 o 3 6 2 37.79 38.73 1.26 o 4 6 2 25.08 24.78 1.27 o 5 6 2 10.61 12.63 1.30 o 0 7 2 31.34 29.33 1.33 o 1 7 2 81.72 78.71 2.31 o 2 7 2 12.10 14.04 0.98 o 3 7 2 63.48 62.12 1.84 o 4 7 2 9.71 9.90 1.08 o 0 8 2 6.04 4.45 1.95 o 1 8 2 4.80 3.40 0.84 o 2 8 2 1.17 -0.87 0.87 o 3 8 2 2.35 1.16 1.06 o 4 8 2 2.02 1.93 1.19 o 0 9 2 0.68 3.78 1.71 o 1 9 2 20.57 22.85 1.81 o 2 9 2 9.35 8.10 1.21 o 0 10 2 19.30 21.85 4.39 o 1 0 3 756.21 759.04 9.34 o 2 0 3 126.61 134.04 1.96 o 3 0 3 269.65 290.94 3.78 o 4 0 3 25.76 23.98 1.08 o 5 0 3 0.06 0.24 1.23 o 6 0 3 0.76 -0.80 1.45 o 0 1 3 910.16 850.56 10.28 o 1 1 3 1136.34 1089.20 9.32 o 2 1 3 125.77 142.82 1.48 o 3 1 3 171.09 174.08 1.79 o 4 1 3 49.11 52.83 1.20 o 5 1 3 27.32 27.47 1.25 o 6 1 3 1.31 2.59 1.28 o 0 2 3 1520.83 1409.55 13.37 o 1 2 3 316.16 344.39 2.93 o 2 2 3 307.37 310.69 2.73 o 3 2 3 126.50 116.65 1.49 o 4 2 3 14.91 12.75 0.77 o 5 2 3 1.48 0.49 0.78 o 6 2 3 1.45 0.01 1.07 o 0 3 3 719.01 770.13 7.53 o 1 3 3 224.73 229.97 2.06 o 2 3 3 230.54 236.97 1.89 o 3 3 3 280.25 300.77 3.40 o 4 3 3 5.24 6.43 0.97 o 5 3 3 37.08 37.63 1.97 o 6 3 3 7.18 4.80 1.16 o 0 4 3 211.50 201.72 2.29 o 1 4 3 139.77 148.23 1.79 o 2 4 3 28.77 29.51 0.74 o 3 4 3 105.22 103.47 1.55 o 4 4 3 73.35 74.17 2.29 o 5 4 3 23.62 19.57 1.38 o 6 4 3 1.01 -1.18 1.18 o 0 5 3 1.15 1.09 0.51 o 1 5 3 12.03 12.11 0.49 o 2 5 3 66.01 62.95 1.23 o 3 5 3 3.55 3.81 0.66 o 4 5 3 7.32 6.57 0.91 o 5 5 3 0.07 -0.04 0.94 o 0 6 3 178.84 184.91 2.72 o 1 6 3 4.88 3.69 0.58 o 2 6 3 16.29 15.53 1.23 o 3 6 3 7.13 6.14 0.82 o 4 6 3 0.34 0.26 0.80 o 5 6 3 4.11 4.17 1.13 o 0 7 3 29.82 30.37 1.36 o 1 7 3 126.90 124.44 2.14 o 2 7 3 8.82 9.53 0.88 o 3 7 3 4.04 1.55 0.91 o 4 7 3 2.01 -0.83 0.93 o 0 8 3 10.81 8.76 1.71 o 1 8 3 1.55 1.54 0.85 o 2 8 3 2.64 2.82 0.94 o 3 8 3 2.03 1.41 0.99 o 0 9 3 6.46 5.91 1.92 o 1 9 3 18.72 19.33 2.05 o 2 9 3 2.57 1.32 1.08 o 0 0 4 0.02 -0.20 0.41 o 1 0 4 1169.30 1184.57 14.34 o 2 0 4 141.75 131.58 2.01 o 3 0 4 173.39 176.04 2.34 o 4 0 4 6.25 7.24 1.16 o 5 0 4 30.86 26.98 2.08 o 6 0 4 0.00 0.20 3.32 o 0 1 4 586.52 604.70 9.38 o 1 1 4 118.73 118.59 1.59 o 2 1 4 98.21 90.56 1.12 o 3 1 4 27.60 34.86 0.75 o 4 1 4 5.02 5.02 0.70 o 5 1 4 0.92 0.43 0.68 o 6 1 4 3.19 3.09 1.22 o 0 2 4 419.21 396.53 5.21 o 1 2 4 144.84 148.82 1.73 o 2 2 4 131.83 142.10 1.54 o 3 2 4 43.48 40.55 0.82 o 4 2 4 16.11 15.07 0.83 o 5 2 4 9.20 8.71 0.91 o 6 2 4 0.45 1.55 1.51 o 0 3 4 0.27 -0.06 0.30 o 1 3 4 17.97 17.20 0.49 o 2 3 4 42.23 42.29 0.68 o 3 3 4 48.22 47.44 1.01 o 4 3 4 21.34 22.80 1.03 o 5 3 4 12.72 12.23 1.07 o 6 3 4 3.11 2.11 1.68 o 0 4 4 158.55 165.15 2.15 o 1 4 4 301.98 325.20 3.05 o 2 4 4 71.02 84.05 1.24 o 3 4 4 61.98 65.27 1.41 o 4 4 4 38.69 36.24 1.26 o 5 4 4 4.19 3.64 1.09 o 6 4 4 4.11 4.92 1.35 o 0 5 4 42.96 46.64 1.40 o 1 5 4 26.76 27.12 0.70 o 2 5 4 10.02 8.98 0.85 o 3 5 4 33.91 37.32 1.65 o 4 5 4 13.78 14.53 1.48 o 5 5 4 0.17 0.76 1.11 o 0 6 4 4.04 3.50 0.65 o 1 6 4 83.52 78.44 1.38 o 2 6 4 1.41 0.41 0.64 o 3 6 4 39.74 41.57 1.36 o 4 6 4 9.32 9.36 1.10 o 5 6 4 6.22 5.71 1.22 o 0 7 4 10.25 10.28 1.06 o 1 7 4 10.36 7.90 0.92 o 2 7 4 99.43 100.21 2.06 o 3 7 4 14.40 11.39 1.17 o 4 7 4 3.07 3.99 1.21 o 0 8 4 5.24 3.90 1.46 o 1 8 4 17.84 20.10 1.68 o 2 8 4 3.33 4.01 1.00 o 3 8 4 1.77 1.38 1.22 o 0 9 4 26.13 33.43 7.12 o 1 9 4 2.07 0.25 1.44 o 2 9 4 5.38 7.73 1.23 o 1 0 5 71.16 74.52 1.57 o 2 0 5 871.16 902.47 10.05 o 3 0 5 107.40 103.09 1.94 o 4 0 5 0.88 -0.54 0.64 o 5 0 5 20.65 18.94 1.90 o 6 0 5 0.40 1.10 2.61 o 0 1 5 27.32 27.32 1.07 o 1 1 5 762.67 817.68 8.00 o 2 1 5 4.07 4.05 0.35 o 3 1 5 59.76 61.75 1.03 o 4 1 5 30.59 31.54 1.43 o 5 1 5 13.44 11.81 0.91 o 6 1 5 4.72 5.96 1.42 o 0 2 5 66.77 62.73 1.36 o 1 2 5 151.04 141.90 1.74 o 2 2 5 11.15 10.28 0.46 o 3 2 5 8.92 10.50 1.05 o 4 2 5 38.38 40.31 1.15 o 5 2 5 0.61 0.10 0.80 o 6 2 5 3.43 2.66 1.86 o 0 3 5 25.19 22.96 1.02 o 1 3 5 408.55 413.42 3.73 o 2 3 5 165.03 170.36 2.00 o 3 3 5 42.80 37.34 1.08 o 4 3 5 70.54 70.47 1.73 o 5 3 5 10.46 10.70 1.06 o 6 3 5 0.73 0.98 1.12 o 0 4 5 178.75 186.53 2.43 o 1 4 5 129.62 127.16 1.49 o 2 4 5 49.66 51.39 1.05 o 3 4 5 97.62 92.28 1.72 o 4 4 5 8.51 6.80 0.93 o 5 4 5 7.13 6.00 1.04 o 0 5 5 93.95 109.53 2.11 o 1 5 5 62.21 50.28 1.02 o 2 5 5 6.62 5.91 0.68 o 3 5 5 15.49 18.79 0.97 o 4 5 5 2.02 1.45 0.81 o 5 5 5 3.40 2.95 1.18 o 0 6 5 36.56 34.64 1.19 o 1 6 5 21.30 21.88 0.95 o 2 6 5 11.17 14.39 1.30 o 3 6 5 7.30 5.20 0.97 o 4 6 5 7.03 5.39 1.04 o 5 6 5 5.19 7.03 1.37 o 0 7 5 30.83 30.59 1.28 o 1 7 5 101.19 98.60 2.00 o 2 7 5 20.41 17.93 1.20 o 3 7 5 8.74 9.16 1.56 o 4 7 5 0.80 2.79 1.14 o 0 8 5 1.22 0.39 4.14 o 1 8 5 0.83 1.71 0.88 o 2 8 5 5.86 5.93 0.95 o 3 8 5 0.22 -0.82 0.94 o 0 9 5 32.54 39.56 4.26 o 1 9 5 7.53 3.38 2.45 o 2 9 5 1.24 1.86 1.14 o 0 0 6 1801.52 1771.57 37.31 o 1 0 6 96.12 92.64 1.88 o 2 0 6 520.28 521.69 9.75 o 3 0 6 51.34 60.99 1.76 o 4 0 6 4.48 4.26 0.75 o 5 0 6 17.18 16.65 1.78 o 6 0 6 0.05 -0.43 1.65 o 0 1 6 167.91 195.10 3.81 o 1 1 6 271.81 282.54 3.28 o 2 1 6 28.19 26.18 0.69 o 3 1 6 53.65 49.89 0.95 o 4 1 6 8.84 8.47 0.74 o 5 1 6 7.98 8.46 0.87 o 6 1 6 0.85 1.71 1.43 o 0 2 6 815.33 792.87 10.08 o 1 2 6 67.72 65.01 1.60 o 2 2 6 15.05 19.56 0.72 o 3 2 6 15.90 19.37 0.71 o 4 2 6 4.12 4.67 0.67 o 5 2 6 0.15 0.64 0.84 o 6 2 6 3.20 1.53 2.20 o 0 3 6 1.27 0.75 0.44 o 1 3 6 157.96 167.31 1.90 o 2 3 6 7.67 6.36 0.51 o 3 3 6 128.16 128.57 2.05 o 4 3 6 5.88 5.28 0.83 o 5 3 6 7.88 7.02 1.03 o 6 3 6 9.47 11.08 1.30 o 0 4 6 21.56 24.48 0.97 o 1 4 6 93.27 95.22 1.47 o 2 4 6 125.59 121.25 1.73 o 3 4 6 27.73 27.83 1.10 o 4 4 6 24.52 21.79 1.13 o 5 4 6 3.00 2.82 1.41 o 0 5 6 7.58 6.85 0.77 o 1 5 6 7.01 6.65 0.79 o 2 5 6 28.61 30.55 1.06 o 3 5 6 12.14 11.92 0.88 o 4 5 6 5.55 4.57 0.97 o 5 5 6 1.62 0.10 1.19 o 0 6 6 77.58 72.52 1.71 o 1 6 6 111.08 107.54 2.00 o 2 6 6 36.28 35.51 1.35 o 3 6 6 32.78 30.99 1.63 o 4 6 6 3.87 4.47 1.01 o 0 7 6 0.91 0.23 0.79 o 1 7 6 22.20 23.84 1.21 o 2 7 6 64.66 61.00 1.82 o 3 7 6 0.90 0.42 0.98 o 4 7 6 2.05 2.90 1.25 o 0 8 6 1.44 0.45 1.60 o 1 8 6 22.35 21.74 1.38 o 2 8 6 1.08 1.23 0.93 o 3 8 6 1.84 -0.22 1.21 o 0 9 6 6.58 12.03 3.12 o 1 9 6 2.62 2.54 1.50 o 1 0 7 198.90 195.58 3.25 o 2 0 7 553.35 540.44 7.52 o 3 0 7 40.25 40.00 1.53 o 4 0 7 28.78 28.04 2.15 o 5 0 7 3.75 3.69 1.43 o 6 0 7 2.23 0.10 1.82 o 0 1 7 77.54 73.80 2.07 o 1 1 7 106.32 105.36 1.68 o 2 1 7 137.51 143.76 1.98 o 3 1 7 17.26 15.48 1.25 o 4 1 7 12.69 11.32 0.84 o 5 1 7 1.14 1.18 0.80 o 6 1 7 1.80 0.75 1.57 o 0 2 7 74.28 66.86 1.62 o 1 2 7 23.08 23.02 0.81 o 2 2 7 2.72 1.94 0.38 o 3 2 7 31.84 29.97 0.84 o 4 2 7 18.42 19.34 1.25 o 5 2 7 9.28 7.71 1.03 o 6 2 7 0.57 0.36 2.99 o 0 3 7 96.45 94.24 4.24 o 1 3 7 87.89 89.97 1.42 o 2 3 7 163.28 149.26 2.39 o 3 3 7 6.32 7.55 0.73 o 4 3 7 42.13 40.73 1.41 o 5 3 7 1.39 0.59 0.96 o 0 4 7 122.77 116.87 3.16 o 1 4 7 16.09 16.81 0.79 o 2 4 7 0.94 1.41 0.50 o 3 4 7 27.50 28.30 1.16 o 4 4 7 3.37 4.13 0.90 o 5 4 7 3.59 3.65 1.08 o 0 5 7 123.46 102.85 5.07 o 1 5 7 5.26 5.36 0.67 o 2 5 7 3.58 3.03 0.69 o 3 5 7 4.08 2.32 0.72 o 4 5 7 8.04 8.64 1.01 o 5 5 7 0.07 0.71 1.18 o 0 6 7 4.08 2.53 0.90 o 1 6 7 20.44 21.46 1.02 o 2 6 7 15.40 16.21 1.10 o 3 6 7 30.52 36.88 1.75 o 4 6 7 7.44 6.43 1.24 o 0 7 7 95.85 92.29 2.64 o 1 7 7 13.04 10.61 1.05 o 2 7 7 52.50 48.90 1.84 o 3 7 7 4.22 4.65 1.14 o 4 7 7 1.79 -0.06 1.24 o 0 8 7 2.13 1.21 1.70 o 1 8 7 1.18 0.20 0.90 o 2 8 7 1.16 0.95 1.02 o 3 8 7 3.79 5.13 1.35 o 0 9 7 35.10 35.20 4.63 o 1 9 7 1.81 2.22 2.20 o 0 0 8 40.05 38.79 2.22 o 1 0 8 397.65 413.12 5.96 o 2 0 8 258.98 256.23 4.31 o 3 0 8 0.37 0.17 0.73 o 4 0 8 128.82 128.41 3.05 o 5 0 8 8.88 9.67 1.72 o 6 0 8 1.32 -0.82 2.54 o 0 1 8 305.84 288.77 5.53 o 1 1 8 3.23 2.61 0.61 o 2 1 8 24.01 26.91 0.90 o 3 1 8 76.06 70.45 1.47 o 4 1 8 26.51 30.79 1.39 o 5 1 8 2.88 0.60 1.04 o 6 1 8 1.12 2.63 1.97 o 0 2 8 79.37 85.32 2.04 o 1 2 8 150.64 153.55 2.38 o 2 2 8 9.93 7.83 0.61 o 3 2 8 17.56 17.04 1.20 o 4 2 8 0.84 0.77 0.74 o 5 2 8 2.16 1.05 0.97 o 0 3 8 399.93 409.78 5.96 o 1 3 8 33.47 28.35 1.09 o 2 3 8 103.07 97.44 1.93 o 3 3 8 48.46 50.62 1.35 o 4 3 8 37.13 39.51 1.58 o 5 3 8 4.31 5.80 1.10 o 0 4 8 86.62 85.89 2.82 o 1 4 8 12.27 13.63 0.99 o 2 4 8 121.18 124.52 1.89 o 3 4 8 20.34 19.60 1.06 o 4 4 8 4.45 4.11 0.96 o 5 4 8 0.39 -0.75 1.12 o 0 5 8 1.06 1.22 1.49 o 1 5 8 9.61 10.32 0.86 o 2 5 8 5.25 4.00 0.82 o 3 5 8 3.23 2.39 0.76 o 4 5 8 2.26 2.62 0.98 o 0 6 8 33.37 34.44 3.58 o 1 6 8 17.48 16.24 1.01 o 2 6 8 79.36 84.55 2.04 o 3 6 8 0.33 0.35 0.91 o 4 6 8 8.28 9.30 1.36 o 0 7 8 2.46 0.89 1.10 o 1 7 8 25.04 26.04 1.41 o 2 7 8 2.76 1.70 0.98 o 3 7 8 9.74 10.71 3.55 o 0 8 8 0.15 -2.05 2.05 o 1 8 8 4.69 6.98 1.49 o 2 8 8 7.46 8.03 1.34 o 1 0 9 192.96 184.68 3.38 o 2 0 9 9.30 8.58 0.95 o 3 0 9 81.79 78.71 2.30 o 4 0 9 2.73 1.59 1.01 o 5 0 9 0.16 -1.56 1.56 o 0 1 9 2.75 2.24 0.75 o 1 1 9 17.08 17.37 0.85 o 2 1 9 26.98 24.62 0.92 o 3 1 9 36.51 36.04 1.15 o 4 1 9 18.14 18.73 1.36 o 5 1 9 9.20 10.70 1.44 o 0 2 9 9.28 8.47 1.28 o 1 2 9 91.18 94.28 1.76 o 2 2 9 8.73 8.42 0.69 o 3 2 9 35.28 36.90 1.27 o 4 2 9 2.82 1.09 0.95 o 5 2 9 2.24 1.14 1.26 o 0 3 9 168.12 168.20 3.21 o 1 3 9 57.97 56.45 1.38 o 2 3 9 67.35 65.26 1.83 o 3 3 9 52.50 54.08 1.81 o 4 3 9 2.01 2.05 0.91 o 5 3 9 3.67 3.32 1.15 o 0 4 9 7.36 6.93 1.22 o 1 4 9 16.93 17.22 1.21 o 2 4 9 121.40 125.30 2.12 o 3 4 9 14.41 16.54 1.04 o 4 4 9 4.10 3.60 1.36 o 5 4 9 3.36 2.60 1.17 o 0 5 9 11.53 9.69 1.85 o 1 5 9 50.08 49.67 1.70 o 2 5 9 7.92 8.89 0.94 o 3 5 9 14.88 14.41 1.18 o 4 5 9 0.64 -0.06 1.14 o 0 6 9 12.87 9.53 1.55 o 1 6 9 11.23 13.37 1.06 o 2 6 9 15.68 14.37 1.19 o 3 6 9 15.14 16.82 1.32 o 4 6 9 1.41 4.97 1.45 o 0 7 9 20.32 20.21 1.78 o 1 7 9 31.46 32.83 1.82 o 2 7 9 12.85 15.96 1.75 o 3 7 9 1.95 1.58 1.26 o 0 8 9 3.78 4.92 2.93 o 1 8 9 6.27 3.82 1.29 o 2 8 9 0.29 2.32 1.30 o 0 0 10 35.43 38.58 2.58 o 1 0 10 13.81 12.32 1.08 o 2 0 10 32.95 35.46 1.50 o 3 0 10 145.97 144.25 3.31 o 4 0 10 23.43 23.54 1.78 o 5 0 10 15.99 18.86 2.29 o 0 1 10 5.67 3.68 0.95 o 1 1 10 27.16 27.99 1.03 o 2 1 10 24.09 22.06 0.97 o 3 1 10 43.85 44.32 1.62 o 4 1 10 14.20 13.32 1.31 o 5 1 10 4.07 1.32 1.25 o 0 2 10 14.59 14.74 1.25 o 1 2 10 12.06 12.02 0.81 o 2 2 10 77.36 77.71 1.89 o 3 2 10 0.79 1.50 0.74 o 4 2 10 4.83 3.58 1.11 o 5 2 10 2.51 2.96 1.31 o 0 3 10 1.64 2.88 0.80 o 1 3 10 87.34 84.31 1.80 o 2 3 10 39.10 42.40 1.54 o 3 3 10 32.64 33.36 1.60 o 4 3 10 0.22 -1.03 1.03 o 5 3 10 2.27 1.12 1.33 o 0 4 10 7.75 5.46 1.37 o 1 4 10 113.91 113.60 2.49 o 2 4 10 7.46 9.57 1.23 o 3 4 10 23.15 25.90 1.97 o 4 4 10 0.04 0.42 1.70 o 0 5 10 11.60 13.55 2.53 o 1 5 10 2.91 1.47 0.84 o 2 5 10 2.15 0.66 0.90 o 3 5 10 4.36 3.81 1.43 o 4 5 10 6.45 6.41 1.81 o 0 6 10 0.84 0.31 1.64 o 1 6 10 6.21 8.04 1.03 o 2 6 10 3.14 4.02 1.58 o 3 6 10 15.59 16.88 1.37 o 0 7 10 0.26 1.07 1.26 o 1 7 10 1.14 0.43 1.14 o 2 7 10 2.49 1.74 1.22 o 0 8 10 0.14 4.83 2.58 o 1 8 10 1.38 0.82 1.63 o 1 0 11 1.77 0.41 0.74 o 2 0 11 23.95 30.34 1.59 o 3 0 11 4.55 4.06 1.05 o 4 0 11 1.43 0.89 1.64 o 5 0 11 11.07 6.22 2.79 o 0 1 11 173.65 165.05 6.12 o 1 1 11 26.39 28.03 1.16 o 2 1 11 0.83 0.87 0.59 o 3 1 11 14.69 15.02 1.30 o 4 1 11 20.27 20.70 1.54 o 5 1 11 1.03 0.57 1.64 o 0 2 11 58.17 56.90 1.91 o 1 2 11 24.20 27.47 1.27 o 2 2 11 82.01 81.42 1.85 o 3 2 11 2.51 2.50 0.85 o 4 2 11 2.78 2.74 1.12 o 5 2 11 0.43 -0.05 1.37 o 0 3 11 0.48 0.12 0.97 o 1 3 11 128.50 130.08 2.38 o 2 3 11 9.45 10.05 1.06 o 3 3 11 14.12 12.71 1.22 o 4 3 11 0.21 0.52 1.12 o 0 4 11 9.06 9.00 1.43 o 1 4 11 22.85 23.29 1.41 o 2 4 11 16.28 16.85 1.06 o 3 4 11 9.91 8.87 1.20 o 4 4 11 4.75 4.38 1.29 o 0 5 11 2.32 1.10 1.26 o 1 5 11 6.18 5.25 1.04 o 2 5 11 13.26 16.33 1.37 o 3 5 11 7.04 7.44 1.49 o 0 6 11 1.72 3.05 1.46 o 1 6 11 4.69 5.45 1.00 o 2 6 11 11.01 14.08 1.48 o 3 6 11 3.46 2.36 1.29 o 0 7 11 12.28 15.47 1.98 o 1 7 11 5.08 4.76 1.38 o 2 7 11 0.61 0.62 1.84 o 0 0 12 56.73 59.26 3.55 o 1 0 12 90.61 88.86 2.48 o 2 0 12 12.79 11.53 1.28 o 3 0 12 28.33 31.49 1.92 o 4 0 12 2.69 2.29 1.39 o 0 1 12 0.12 -1.09 1.09 o 1 1 12 12.77 14.23 1.25 o 2 1 12 28.30 27.99 1.19 o 3 1 12 0.03 -0.83 0.83 o 4 1 12 8.77 7.70 1.33 o 0 2 12 2.40 0.97 1.01 o 1 2 12 20.60 21.34 1.15 o 2 2 12 6.30 3.90 0.84 o 3 2 12 17.25 15.26 1.71 o 4 2 12 3.51 4.39 1.33 o 0 3 12 10.08 9.41 1.49 o 1 3 12 2.81 2.34 0.77 o 2 3 12 10.26 8.82 0.84 o 3 3 12 0.35 -1.14 1.34 o 4 3 12 1.15 -0.77 1.26 o 0 4 12 45.48 46.63 2.45 o 1 4 12 13.19 11.40 1.17 o 2 4 12 18.20 22.25 2.70 o 3 4 12 2.76 0.81 1.27 o 4 4 12 1.34 -0.81 1.33 o 0 5 12 3.96 4.88 1.50 o 1 5 12 12.26 10.62 1.22 o 2 5 12 7.86 8.80 1.36 o 3 5 12 4.75 3.02 1.51 o 0 6 12 0.05 0.15 1.66 o 1 6 12 10.41 13.42 1.29 o 2 6 12 5.30 6.92 2.11 o 0 7 12 1.20 2.34 1.84 o 1 7 12 2.26 1.94 2.27 o 1 0 13 1.54 1.82 0.96 o 2 0 13 9.09 10.66 1.30 o 3 0 13 0.34 -0.37 1.81 o 4 0 13 11.51 13.54 2.12 o 0 1 13 23.44 26.51 1.65 o 1 1 13 29.15 29.87 1.37 o 2 1 13 11.77 10.00 0.92 o 3 1 13 2.58 1.85 0.97 o 4 1 13 0.06 -0.59 1.30 o 0 2 13 0.89 -0.43 1.81 o 1 2 13 18.69 17.17 1.14 o 2 2 13 0.87 -0.17 0.83 o 3 2 13 1.52 0.45 0.97 o 4 2 13 1.13 -0.25 1.50 o 0 3 13 66.66 64.41 2.84 o 1 3 13 10.19 11.49 1.25 o 2 3 13 9.49 8.21 0.92 o 3 3 13 6.65 6.38 1.29 o 0 4 13 3.50 3.43 1.50 o 1 4 13 5.95 5.49 1.09 o 2 4 13 5.24 4.10 1.13 o 3 4 13 0.08 1.15 1.38 o 0 5 13 0.11 1.25 1.54 o 1 5 13 2.26 1.10 1.12 o 2 5 13 0.88 -0.28 1.55 o 0 6 13 0.27 -1.35 1.72 o 1 6 13 5.81 6.03 1.92 o 0 0 14 84.69 85.62 4.52 o 1 0 14 14.01 15.31 1.95 o 2 0 14 22.73 21.42 1.79 o 3 0 14 8.05 4.52 1.56 o 0 1 14 6.82 8.35 1.63 o 1 1 14 12.69 11.23 0.98 o 2 1 14 1.22 -0.45 0.89 o 3 1 14 5.98 7.06 1.17 o 0 2 14 0.57 1.69 1.48 o 1 2 14 5.75 5.49 0.95 o 2 2 14 1.32 0.19 0.93 o 3 2 14 1.47 2.29 1.21 o 0 3 14 6.20 10.05 1.75 o 1 3 14 15.52 17.89 1.50 o 2 3 14 2.63 2.95 0.93 o 3 3 14 1.96 3.43 1.30 o 0 4 14 11.22 13.59 1.88 o 1 4 14 1.02 0.97 1.09 o 2 4 14 9.13 12.45 1.50 o 0 5 14 4.48 2.94 1.84 o 1 5 14 1.59 -0.14 1.82 o 1 0 15 1.30 3.63 1.31 o 2 0 15 2.27 4.11 1.46 o 3 0 15 2.13 1.24 1.82 o 0 1 15 0.48 -1.22 1.68 o 1 1 15 2.23 0.73 0.85 o 2 1 15 1.77 1.43 1.04 o 3 1 15 0.35 0.58 1.21 o 0 2 15 5.82 3.64 1.51 o 1 2 15 10.65 15.21 1.27 o 2 2 15 2.16 1.47 1.03 o 0 3 15 30.77 33.61 2.61 o 1 3 15 1.42 1.07 1.46 o 2 3 15 18.75 19.87 1.93 o 0 4 15 0.03 -1.68 1.68 o 1 4 15 9.01 9.84 1.45 o 0 0 16 0.03 0.63 1.74 o 1 0 16 2.73 1.05 1.39 o 2 0 16 5.10 2.45 2.57 o 0 1 16 0.01 1.94 1.39 o 1 1 16 1.26 -0.45 1.07 o 2 1 16 2.12 1.39 1.17 o 0 2 16 5.65 6.10 1.93 o 1 2 16 0.01 0.02 1.18 o 0 3 16 10.66 6.11 1.81 o 1 3 16 9.34 13.86 1.71 o