#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/29/2212971.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212971_Fobs loop_ _publ_author_name 'Mtshali, Thato N.' 'Purcell, Walter' 'Visser, Hendrik G.' 'Basson, Stephen S.' _publ_section_title ; Bis(tetraphenylarsonium) tricyanidonitrido(quinoline-2-carboxylato-\k^2^N,O)rhenate(V) dihydrate ; _journal_coeditor_code NG2227 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1037 _journal_page_last m1038 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 72.831 _cell_angle_beta 88.917 _cell_angle_gamma 65.473 _cell_length_a 13.3672 _cell_length_b 13.3695 _cell_length_c 17.0828 _exptl_crystal_F_000 1248.00 _reflns_d_resolution_high 0.7569 _[local]_cod_data_source_file ng2227Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 5m_wp1_a in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 315.38 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 62.34 78.31 13.55 o 2 0 0 10370.17 10901.67 97.26 o 3 0 0 66868.59 64924.34 884.56 o 4 0 0 20818.69 21740.21 260.86 o 5 0 0 6318.21 5707.59 307.95 o 6 0 0 3880.93 3958.30 109.64 o 7 0 0 20768.43 20256.47 836.45 o 8 0 0 828.25 881.39 81.86 o 9 0 0 573.33 576.52 84.70 o 10 0 0 7136.73 6883.81 622.00 o 11 0 0 766.92 630.06 100.37 o 12 0 0 837.26 955.97 215.80 o 13 0 0 437.72 449.24 108.86 o 14 0 0 1697.46 1785.51 153.97 o 15 0 0 23.26 -34.05 122.38 o -15 1 0 168.31 144.32 189.04 o -14 1 0 311.85 456.68 191.07 o -13 1 0 831.88 825.67 123.60 o -12 1 0 2414.11 2469.41 163.94 o -11 1 0 10.69 42.76 82.60 o -10 1 0 22.60 -16.26 82.66 o -9 1 0 3332.37 3078.38 141.79 o -8 1 0 2722.86 2801.26 342.51 o -7 1 0 559.26 526.56 71.10 o -6 1 0 475.91 659.02 67.55 o -5 1 0 11189.78 10259.86 144.69 o -4 1 0 18.00 56.56 40.72 o -3 1 0 1457.50 1369.99 73.54 o -2 1 0 12992.37 13265.28 168.71 o -1 1 0 24686.83 23608.54 823.58 o 0 1 0 1358.18 1700.44 47.86 o 1 1 0 1391.65 1303.05 23.73 o 2 1 0 23435.88 24770.28 355.02 o 3 1 0 1739.28 2084.43 62.34 o 4 1 0 5638.70 5986.64 281.87 o 5 1 0 22637.18 21033.84 1127.12 o 6 1 0 12934.76 13530.14 865.24 o 7 1 0 6376.93 5858.59 359.45 o 8 1 0 4243.35 4531.75 189.04 o 9 1 0 20194.16 19251.93 614.21 o 10 1 0 692.76 741.43 97.20 o 11 1 0 806.12 711.22 100.13 o 12 1 0 8648.53 8796.47 220.97 o 13 1 0 704.84 701.12 117.83 o 14 1 0 2306.31 2665.02 329.97 o 15 1 0 1034.03 1411.09 194.80 o 16 1 0 2042.01 2219.88 182.04 o -14 2 0 1637.97 1384.93 208.01 o -13 2 0 102.03 255.44 156.52 o -12 2 0 4764.30 5007.85 272.38 o -11 2 0 481.73 349.59 137.21 o -10 2 0 2509.10 2721.77 162.61 o -9 2 0 5174.57 4903.42 290.33 o -8 2 0 463.96 468.19 113.83 o -7 2 0 17484.57 16992.16 408.91 o -6 2 0 19.42 155.94 78.26 o -5 2 0 11838.65 10799.27 150.36 o -4 2 0 7276.44 7355.89 125.69 o -3 2 0 13582.32 12444.87 132.46 o -2 2 0 19151.33 20006.14 777.50 o -1 2 0 23242.39 23802.90 783.94 o 0 2 0 19617.99 21750.95 288.98 o 1 2 0 3464.45 3459.08 80.68 o 2 2 0 1068.76 1364.14 45.01 o 3 2 0 22609.92 22242.46 142.89 o 4 2 0 3699.76 4086.94 82.58 o 5 2 0 14071.04 13572.08 271.94 o 6 2 0 794.28 888.58 60.60 o 7 2 0 12878.76 11998.22 526.13 o 8 2 0 325.22 538.63 73.18 o 9 2 0 49.52 83.52 119.59 o 10 2 0 1711.64 1897.79 139.18 o 11 2 0 196.86 183.53 94.18 o 12 2 0 213.57 211.02 93.51 o 13 2 0 69.73 5.54 97.63 o 14 2 0 1247.61 1411.61 140.60 o 15 2 0 682.09 489.62 126.99 o 16 2 0 189.22 95.53 126.24 o -14 3 0 398.46 255.44 191.75 o -13 3 0 1097.02 951.29 202.59 o -12 3 0 353.90 513.59 166.00 o -11 3 0 63.90 65.02 90.79 o -10 3 0 4091.93 4250.27 161.66 o -9 3 0 18.22 88.92 79.05 o -8 3 0 6738.05 6580.47 257.47 o -7 3 0 4615.57 4005.74 201.91 o -6 3 0 1627.54 1546.19 155.16 o -5 3 0 22598.35 22144.71 301.51 o -4 3 0 194.33 246.69 57.25 o -3 3 0 27499.89 26834.50 886.93 o -2 3 0 1957.43 2076.51 87.74 o -1 3 0 61299.87 63462.71 495.16 o 0 3 0 83010.53 88490.19 1799.82 o 1 3 0 13903.72 14297.03 228.42 o 2 3 0 40253.41 41489.49 754.69 o 3 3 0 14762.45 14019.59 116.41 o 4 3 0 46164.48 46806.78 573.28 o 5 3 0 17585.21 15568.17 263.48 o 6 3 0 8787.54 8512.77 183.79 o 7 3 0 41765.83 40951.28 1077.47 o 8 3 0 840.87 971.80 67.51 o 9 3 0 8557.76 7883.61 604.38 o 10 3 0 4181.47 4267.91 395.70 o 11 3 0 470.07 358.42 93.67 o 12 3 0 6015.20 6135.87 194.03 o 13 3 0 303.92 254.11 106.94 o 14 3 0 1455.15 1650.01 140.86 o 15 3 0 1512.05 1556.23 149.56 o 16 3 0 759.44 732.87 142.05 o 17 3 0 140.10 -21.36 187.35 o -13 4 0 138.03 406.54 201.24 o -12 4 0 3425.85 3868.87 273.06 o -11 4 0 29.85 -64.37 136.19 o -10 4 0 28.14 -4.87 88.06 o -9 4 0 3323.96 3463.01 222.92 o -8 4 0 1415.36 1490.64 107.52 o -7 4 0 407.68 350.76 81.12 o -6 4 0 158.96 244.00 70.83 o -5 4 0 7399.83 7028.56 141.10 o -4 4 0 229.61 244.83 55.48 o -3 4 0 1970.47 2173.84 143.98 o -2 4 0 2558.19 3111.06 71.89 o -1 4 0 10093.91 10562.36 156.22 o 0 4 0 19163.10 20988.59 162.95 o 1 4 0 2319.58 2913.35 69.14 o 2 4 0 20778.08 21862.27 579.42 o 3 4 0 6538.44 7726.24 179.67 o 4 4 0 4267.48 3931.83 85.07 o 5 4 0 1160.68 1173.35 68.33 o 6 4 0 21061.62 20971.94 494.14 o 7 4 0 1441.06 1306.17 83.42 o 8 4 0 1269.71 1196.59 91.35 o 9 4 0 15461.90 14821.40 529.63 o 10 4 0 13.38 135.62 79.99 o 11 4 0 4699.36 4461.67 175.80 o 12 4 0 2390.57 2652.37 160.02 o 13 4 0 1726.09 1560.77 128.30 o 14 4 0 2611.67 2591.27 177.65 o 15 4 0 82.02 58.95 107.31 o 16 4 0 1711.71 1884.28 167.11 o 17 4 0 763.69 932.50 159.93 o -11 5 0 62.94 -90.79 157.19 o -10 5 0 5714.87 5924.59 287.96 o -9 5 0 4.75 122.64 134.83 o -8 5 0 1410.12 1535.63 111.86 o -7 5 0 14895.70 14814.89 373.67 o -6 5 0 3735.15 3741.52 140.13 o -5 5 0 6994.75 6947.76 260.52 o -4 5 0 1945.19 2312.90 89.70 o -3 5 0 22858.31 22433.77 198.25 o -2 5 0 2452.72 2748.59 82.17 o -1 5 0 861.59 937.94 50.43 o 0 5 0 46538.09 48991.82 919.76 o 1 5 0 1182.17 1293.67 68.68 o 2 5 0 5046.20 4978.10 83.94 o 3 5 0 1586.83 1479.72 70.12 o 4 5 0 12435.48 12501.68 282.99 o 5 5 0 1392.53 1426.71 77.47 o 6 5 0 445.61 510.08 51.97 o 7 5 0 2130.21 1837.51 148.36 o 8 5 0 1282.75 1517.90 95.66 o 9 5 0 1423.96 1269.39 102.76 o 10 5 0 2209.25 2387.83 150.15 o 11 5 0 1269.13 1234.32 129.88 o 12 5 0 362.81 437.95 104.01 o 13 5 0 592.14 628.77 111.59 o 14 5 0 932.64 953.15 126.03 o 15 5 0 350.20 155.96 136.87 o 16 5 0 458.07 505.80 130.48 o 17 5 0 14.68 -92.62 129.52 o -12 6 0 1310.51 1643.08 227.66 o -11 6 0 145.11 122.64 157.19 o -10 6 0 37.53 50.82 136.19 o -9 6 0 21.92 -27.60 91.70 o -8 6 0 3316.17 3728.08 164.57 o -7 6 0 113.17 29.90 63.76 o -6 6 0 2695.35 2619.41 114.24 o -5 6 0 7166.56 7227.82 137.44 o -4 6 0 4684.99 4448.42 117.20 o -3 6 0 10112.32 10447.49 184.34 o -2 6 0 3376.59 3675.46 96.93 o -1 6 0 31154.26 32406.29 344.98 o 0 6 0 6442.36 7375.26 235.73 o 1 6 0 3701.40 3946.47 89.44 o 2 6 0 34466.38 36438.80 742.23 o 3 6 0 3207.59 3537.97 94.60 o 4 6 0 13094.77 13627.11 164.15 o 5 6 0 10332.23 9816.40 213.34 o 6 6 0 33198.86 33005.14 801.91 o 7 6 0 9965.49 9586.90 140.23 o 8 6 0 1.47 8.48 53.76 o 9 6 0 23810.53 22606.20 226.84 o 10 6 0 224.16 215.96 95.39 o 11 6 0 1196.83 1321.58 97.91 o 12 6 0 4179.34 4403.89 230.07 o 13 6 0 1802.40 1860.95 146.28 o 14 6 0 1422.98 1562.16 172.10 o 15 6 0 161.54 5.76 107.80 o 16 6 0 1988.16 2185.04 190.42 o 17 6 0 205.24 250.61 141.34 o -11 7 0 115.99 281.87 197.17 o -10 7 0 2663.76 2971.78 295.42 o -9 7 0 431.36 597.61 177.52 o -8 7 0 874.76 911.32 174.81 o -7 7 0 2041.89 1933.76 222.92 o -6 7 0 1284.32 1389.37 151.77 o -5 7 0 870.34 1021.99 79.17 o -4 7 0 1698.07 1920.26 109.72 o -3 7 0 3355.91 3616.53 113.52 o -2 7 0 654.51 642.14 61.93 o -1 7 0 68.63 137.25 49.92 o 0 7 0 9271.42 9959.79 265.67 o 1 7 0 12587.44 13249.73 180.46 o 2 7 0 550.43 629.06 50.24 o 3 7 0 1547.11 1445.87 83.73 o 4 7 0 7285.24 6808.11 114.20 o 5 7 0 3892.14 4565.62 132.50 o 6 7 0 200.23 190.35 54.25 o 7 7 0 4984.09 4858.62 116.01 o 8 7 0 20126.12 19119.35 363.81 o 9 7 0 971.14 917.46 78.43 o 10 7 0 3.37 -0.85 71.40 o 11 7 0 7024.62 6704.95 162.08 o 12 7 0 96.95 15.00 76.76 o 13 7 0 1434.67 1379.86 111.39 o 14 7 0 3181.91 3577.54 188.07 o 15 7 0 1889.26 1710.54 154.44 o 16 7 0 1072.70 989.58 148.39 o 17 7 0 367.10 386.25 142.05 o -10 8 0 1122.67 1045.48 215.46 o -9 8 0 9.75 -155.84 155.84 o -8 8 0 7222.66 7061.54 319.81 o -7 8 0 801.02 1052.25 167.36 o -6 8 0 1962.54 2076.72 219.53 o -5 8 0 7395.26 7691.67 287.29 o -4 8 0 2644.85 2578.64 147.31 o -3 8 0 8672.98 8948.54 184.93 o -2 8 0 2994.11 3333.07 115.54 o -1 8 0 11220.96 11737.92 164.21 o 0 8 0 2357.62 2761.36 106.17 o 1 8 0 405.34 429.99 55.33 o 2 8 0 9805.65 10169.17 294.09 o 3 8 0 2166.11 2423.91 97.01 o 4 8 0 5951.53 6100.72 117.94 o 5 8 0 5203.51 4936.01 114.12 o 6 8 0 5283.92 5233.06 124.03 o 7 8 0 1167.30 1098.42 75.80 o 8 8 0 1396.63 1420.14 84.58 o 9 8 0 4164.87 3887.57 131.90 o 10 8 0 660.70 686.56 81.35 o 11 8 0 100.37 133.28 77.90 o 12 8 0 1276.28 1468.52 104.63 o 13 8 0 363.11 516.34 91.32 o 14 8 0 15.32 0.82 90.79 o 15 8 0 94.05 114.24 113.78 o 16 8 0 1456.32 1925.82 166.00 o 17 8 0 302.22 149.70 145.89 o -9 9 0 172.19 86.73 190.39 o -8 9 0 1259.84 1378.16 211.40 o -7 9 0 0.71 78.60 162.61 o -6 9 0 2341.01 2319.97 255.44 o -5 9 0 1784.60 1853.13 199.88 o -4 9 0 3130.65 3044.28 229.69 o -3 9 0 5650.58 5841.25 261.54 o -2 9 0 17.26 196.80 106.72 o -1 9 0 5349.04 5839.07 210.72 o 0 9 0 935.39 1174.34 74.56 o 1 9 0 10365.25 10594.64 148.28 o 2 9 0 4216.20 4354.82 249.10 o 3 9 0 960.12 1078.65 89.43 o 4 9 0 10475.91 10450.92 359.86 o 5 9 0 368.83 494.74 64.06 o 6 9 0 10658.17 10455.08 411.15 o 7 9 0 2172.57 2069.80 115.29 o 8 9 0 13212.47 12780.08 184.92 o 9 9 0 5087.32 4641.02 140.26 o 10 9 0 5.71 73.86 72.51 o 11 9 0 8783.28 8781.41 176.90 o 12 9 0 466.96 542.80 89.53 o 13 9 0 2536.41 2607.39 142.74 o 14 9 0 2938.86 3241.67 158.43 o 15 9 0 871.59 703.59 133.29 o 16 9 0 902.43 874.74 148.51 o 17 9 0 558.82 771.55 235.79 o -8 10 0 791.28 472.26 201.91 o -7 10 0 923.36 701.95 195.82 o -6 10 0 2168.69 2456.83 256.12 o -5 10 0 1957.38 2113.99 235.79 o -4 10 0 41.08 12.87 132.80 o -3 10 0 2774.25 2672.98 224.27 o -2 10 0 6.80 16.26 115.86 o -1 10 0 353.30 276.59 108.41 o 0 10 0 323.88 358.53 167.70 o 1 10 0 674.92 923.03 108.07 o 2 10 0 715.11 762.56 101.14 o 3 10 0 387.65 496.91 67.97 o 4 10 0 1658.86 1654.46 102.50 o 5 10 0 615.45 750.75 74.57 o 6 10 0 812.73 898.05 81.41 o 7 10 0 41.36 -27.82 68.28 o 8 10 0 4352.59 4117.56 175.36 o 9 10 0 1031.14 1035.71 89.49 o 10 10 0 243.97 182.25 74.77 o 11 10 0 1001.38 1096.70 117.45 o 12 10 0 96.14 53.83 81.36 o 13 10 0 3345.55 3721.84 158.49 o 14 10 0 69.63 124.04 90.68 o 15 10 0 1980.72 2052.93 161.41 o 16 10 0 985.49 1126.75 152.34 o 17 10 0 552.30 359.55 146.75 o -7 11 0 87.81 4.07 186.33 o -6 11 0 1680.77 1851.77 230.37 o -5 11 0 1434.40 1525.19 205.98 o -4 11 0 4239.30 3925.11 275.77 o -3 11 0 3208.47 3116.10 254.76 o -2 11 0 152.78 187.68 136.19 o -1 11 0 10677.64 11231.92 365.21 o 0 11 0 59.99 -21.68 125.35 o 1 11 0 4247.68 4597.65 180.35 o 2 11 0 3333.61 3609.34 174.64 o 3 11 0 1801.69 2129.03 144.76 o 4 11 0 2721.02 2717.96 178.26 o 5 11 0 2306.45 2186.20 115.09 o 6 11 0 4094.22 4218.52 150.93 o 7 11 0 141.55 150.95 71.40 o 8 11 0 286.39 255.88 75.22 o 9 11 0 1035.85 1092.39 92.18 o 10 11 0 589.78 456.08 84.86 o 11 11 0 549.37 536.94 96.21 o 12 11 0 355.57 407.27 90.38 o 13 11 0 430.84 443.80 98.48 o 14 11 0 7.48 -6.61 90.98 o 15 11 0 62.14 9.40 123.75 o 16 11 0 274.99 417.54 138.42 o 17 11 0 4.68 -57.29 145.67 o -5 12 0 78.51 -151.77 169.39 o -4 12 0 541.59 651.14 184.97 o -3 12 0 1689.44 1695.26 221.56 o -2 12 0 2056.41 2139.06 266.28 o -1 12 0 143.92 35.23 140.26 o 0 12 0 18.90 -129.41 132.80 o 1 12 0 9809.96 9665.40 336.07 o 2 12 0 31.74 -76.94 106.04 o 3 12 0 2409.93 2638.84 171.48 o 4 12 0 4190.22 4361.35 196.18 o 5 12 0 2214.02 2303.93 155.20 o 6 12 0 1819.74 1746.57 131.54 o 7 12 0 350.62 198.17 114.17 o 8 12 0 7988.10 7920.94 170.59 o 9 12 0 1942.22 1806.42 117.88 o 10 12 0 940.02 1099.82 97.89 o 11 12 0 5434.92 5207.33 161.91 o 12 12 0 555.88 468.86 97.63 o 13 12 0 1958.07 1999.07 135.55 o 14 12 0 827.96 921.66 117.02 o 15 12 0 1354.93 1378.35 158.22 o 16 12 0 575.79 480.88 162.61 o -4 13 0 1201.21 1125.43 248.66 o -3 13 0 1276.53 1435.75 233.76 o -2 13 0 132.64 159.90 161.26 o -1 13 0 1590.61 1691.87 215.46 o 0 13 0 164.53 134.83 158.55 o 1 13 0 148.51 23.71 147.03 o 2 13 0 704.90 605.06 163.29 o 3 13 0 1638.11 1812.47 199.20 o 4 13 0 114.62 205.60 118.54 o 5 13 0 23.56 -35.84 106.78 o 6 13 0 1855.94 1760.48 148.64 o 7 13 0 1330.64 1512.23 139.44 o 8 13 0 832.86 894.46 136.58 o 9 13 0 957.93 983.59 138.10 o 10 13 0 1244.63 1318.31 258.83 o 11 13 0 54.40 29.28 85.37 o 12 13 0 4.22 48.23 90.66 o 13 13 0 1373.53 1344.06 123.76 o 14 13 0 481.89 517.36 116.38 o 15 13 0 555.21 505.01 147.38 o 16 13 0 261.82 221.67 149.01 o -2 14 0 949.24 1027.86 226.98 o -1 14 0 1078.92 1148.47 216.14 o 0 14 0 32.56 174.13 172.78 o 1 14 0 5640.08 5385.25 317.10 o 2 14 0 84.32 170.07 160.58 o 3 14 0 959.75 1197.93 195.14 o 4 14 0 4807.40 4502.39 306.26 o 5 14 0 726.92 679.70 140.89 o 6 14 0 782.67 972.81 145.53 o 7 14 0 1103.79 947.95 143.39 o 8 14 0 2971.52 2899.09 200.95 o 9 14 0 46.64 -123.86 123.86 o 10 14 0 4.27 -115.54 115.54 o 11 14 0 1834.84 1919.56 165.90 o 12 14 0 95.93 80.64 131.29 o 13 14 0 49.17 -139.56 139.56 o 14 14 0 460.38 672.72 154.87 o 15 14 0 748.05 606.42 244.60 o 0 15 0 899.98 654.52 215.46 o 1 15 0 1025.46 1394.42 225.63 o 2 15 0 17.24 90.79 178.20 o 3 15 0 1772.30 2101.12 243.24 o 4 15 0 22.92 12.20 172.10 o 5 15 0 495.45 363.17 183.62 o 6 15 0 2182.84 2162.77 237.82 o 7 15 0 1416.69 1428.34 169.21 o 8 15 0 1523.44 1746.77 177.49 o 9 15 0 328.59 440.90 142.43 o 10 15 0 3467.75 3509.30 224.58 o 11 15 0 159.97 286.03 140.49 o 12 15 0 134.40 307.63 222.58 o 13 15 0 3371.48 3256.19 239.71 o 14 15 0 115.44 160.62 156.18 o 3 16 0 537.66 380.11 231.73 o 4 16 0 289.19 473.61 204.62 o 5 16 0 30.15 -176.84 176.84 o 6 16 0 60.73 35.91 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