#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2212995.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212995_Fobs loop_ _publ_author_name 'Yathirajan, H. S.' 'Ashok, M. A.' 'Narayana Achar, B.' 'Bolte, Michael' _publ_section_title ; Chlorpromazinium picrate ; _journal_coeditor_code SG2144 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1795 _journal_page_last o1797 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 108.758 _cell_angle_beta 104.675 _cell_angle_gamma 100.922 _cell_length_a 12.3355 _cell_length_b 14.6631 _cell_length_c 15.5340 _exptl_crystal_F_000 1136.00 _reflns_d_resolution_high 0.8400 _[local]_cod_data_source_file sg2144Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' yat75 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 242.69 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 0.74 48.28 52.52 o 3 0 0 1609.75 1647.66 62.78 o 4 0 0 5363.43 6364.80 102.17 o 5 0 0 481.16 534.12 36.20 o 6 0 0 120.09 128.09 25.52 o 7 0 0 0.87 -6.25 24.08 o 8 0 0 254.24 281.58 29.78 o 9 0 0 8.84 67.08 28.78 o 10 0 0 1171.02 1067.26 40.09 o 11 0 0 138.94 148.58 30.07 o 12 0 0 46.50 66.19 32.13 o 13 0 0 3.65 21.52 28.62 o -13 1 0 3.09 29.13 31.87 o -12 1 0 0.07 37.28 31.20 o -11 1 0 189.48 187.23 29.39 o -10 1 0 52.27 54.98 24.45 o -9 1 0 71.70 112.03 28.73 o -8 1 0 328.37 310.00 26.69 o -7 1 0 163.03 155.97 27.79 o -6 1 0 4444.05 4763.77 142.69 o -5 1 0 1543.67 1554.95 54.17 o -4 1 0 62.99 104.23 43.30 o -3 1 0 14210.95 14088.15 641.65 o 2 1 0 7567.13 6972.58 304.94 o 3 1 0 1216.40 1162.69 47.30 o 4 1 0 461.72 445.27 34.63 o 5 1 0 1383.29 1454.35 48.23 o 6 1 0 442.09 398.28 29.42 o 7 1 0 6.42 0.39 22.36 o 8 1 0 21.74 15.63 21.75 o 9 1 0 1633.95 1506.61 101.95 o 10 1 0 461.49 484.06 27.60 o 11 1 0 46.28 22.28 25.17 o 12 1 0 12.57 11.43 26.55 o 13 1 0 7.29 16.02 27.78 o -13 2 0 4.60 36.11 33.10 o -12 2 0 18.22 5.78 32.63 o -11 2 0 198.15 170.08 26.35 o -10 2 0 924.37 873.01 86.07 o -9 2 0 268.82 258.04 30.78 o -8 2 0 1.00 44.35 27.42 o -7 2 0 12.60 42.97 32.64 o -6 2 0 727.80 727.68 46.84 o -5 2 0 6.79 18.98 39.96 o -4 2 0 611.41 575.91 55.96 o -3 2 0 88.28 141.29 55.98 o -2 2 0 365.66 654.73 75.69 o 1 2 0 1876.68 2375.22 228.69 o 2 2 0 3268.94 4036.52 292.58 o 3 2 0 760.58 841.28 44.42 o 4 2 0 34.14 -1.36 28.71 o 5 2 0 81.84 98.05 26.30 o 6 2 0 1195.93 1156.60 150.47 o 7 2 0 1130.80 1138.63 45.69 o 8 2 0 103.86 88.36 37.99 o 9 2 0 19.34 34.95 23.37 o 10 2 0 10.18 6.13 27.05 o 11 2 0 36.95 25.22 28.87 o 12 2 0 199.52 132.53 27.92 o -14 3 0 14.44 21.06 40.42 o -13 3 0 34.62 8.59 40.95 o -12 3 0 22.27 49.16 30.66 o -11 3 0 92.79 42.05 26.37 o -10 3 0 868.88 830.92 33.82 o -9 3 0 516.34 458.43 35.91 o -8 3 0 281.56 320.53 58.73 o -7 3 0 131.75 136.79 36.76 o -6 3 0 1013.66 1124.07 52.10 o -5 3 0 2452.86 2111.87 66.77 o -4 3 0 829.75 724.42 55.68 o -3 3 0 2810.59 1900.90 118.86 o -2 3 0 3701.10 3704.91 130.56 o 0 3 0 424.41 364.32 60.66 o 1 3 0 257.51 260.30 34.16 o 2 3 0 3407.30 2507.14 260.94 o 3 3 0 37.59 222.41 33.71 o 4 3 0 6.21 25.35 30.13 o 5 3 0 1092.74 1151.62 77.40 o 6 3 0 0.12 21.15 26.50 o 7 3 0 8.57 -1.71 21.21 o 8 3 0 0.63 -11.08 28.72 o 9 3 0 1307.14 1070.04 45.04 o 10 3 0 399.11 349.23 30.06 o 11 3 0 13.49 37.28 28.50 o 12 3 0 9.64 50.32 26.39 o -14 4 0 14.10 42.49 33.50 o -13 4 0 35.33 72.54 31.89 o -12 4 0 75.90 40.62 48.05 o -11 4 0 38.27 45.34 26.28 o -10 4 0 64.85 72.39 36.03 o -9 4 0 52.11 120.99 37.33 o -8 4 0 2889.01 2633.60 80.67 o -7 4 0 47.58 6.20 34.84 o -6 4 0 869.93 947.96 48.99 o -5 4 0 133.68 161.15 45.80 o -4 4 0 505.35 590.94 54.19 o -3 4 0 1979.73 1799.02 101.05 o -2 4 0 1225.61 659.06 73.80 o 0 4 0 5426.21 3381.03 354.06 o 1 4 0 188.14 100.94 32.30 o 2 4 0 3455.05 3369.18 330.80 o 3 4 0 1855.90 1787.08 128.19 o 4 4 0 16.55 50.06 25.55 o 5 4 0 238.10 406.30 33.81 o 6 4 0 275.97 210.57 39.04 o 7 4 0 193.94 221.88 22.83 o 8 4 0 344.22 322.17 28.30 o 9 4 0 159.21 175.69 37.84 o 10 4 0 36.25 54.59 23.15 o 11 4 0 2.50 -13.59 25.59 o 12 4 0 8.93 7.38 30.72 o -14 5 0 10.23 6.81 33.45 o -13 5 0 1.55 38.84 32.59 o -12 5 0 153.33 126.40 47.34 o -11 5 0 5.38 -44.19 44.19 o -10 5 0 50.34 45.50 39.20 o -9 5 0 16.04 14.19 34.82 o -8 5 0 42.11 84.99 34.45 o -7 5 0 163.46 142.63 36.18 o -6 5 0 529.45 694.23 45.36 o -5 5 0 158.01 381.43 43.06 o -4 5 0 3352.95 2133.42 150.58 o -3 5 0 540.49 521.82 74.04 o -2 5 0 203.09 329.38 75.04 o -1 5 0 1155.16 1068.78 85.64 o 0 5 0 5134.43 5150.93 256.87 o 1 5 0 8.84 14.97 29.08 o 2 5 0 2385.71 2266.94 174.26 o 3 5 0 38.11 60.82 26.39 o 4 5 0 1852.02 1727.03 191.26 o 5 5 0 2.85 34.65 27.20 o 6 5 0 441.92 459.60 30.63 o 7 5 0 30.65 42.44 27.74 o 8 5 0 136.88 153.43 26.47 o 9 5 0 1.46 4.76 23.37 o 10 5 0 0.01 -23.56 28.80 o 11 5 0 22.43 11.45 29.50 o -14 6 0 14.87 2.22 34.63 o -13 6 0 13.89 37.14 32.46 o -12 6 0 21.86 -16.95 44.50 o -11 6 0 2.68 24.07 41.48 o -10 6 0 37.21 68.69 42.06 o -9 6 0 625.55 555.82 41.55 o -8 6 0 0.13 21.90 35.36 o -7 6 0 111.38 121.15 35.80 o -6 6 0 156.04 134.19 30.23 o -5 6 0 2842.46 2332.22 365.14 o -4 6 0 992.25 1050.05 76.10 o -3 6 0 56.49 142.48 65.26 o -1 6 0 135.00 92.77 65.15 o 0 6 0 306.96 398.57 89.06 o 1 6 0 285.18 245.55 41.45 o 2 6 0 2202.19 1955.28 239.18 o 3 6 0 549.51 613.79 57.97 o 4 6 0 48.12 98.25 26.54 o 5 6 0 17.14 76.50 30.61 o 6 6 0 38.31 51.47 21.89 o 7 6 0 1.52 -24.47 24.47 o 8 6 0 11.63 35.82 23.56 o 9 6 0 271.79 330.66 31.07 o 10 6 0 123.26 108.49 28.08 o 11 6 0 36.94 20.21 31.53 o -14 7 0 7.65 -2.78 40.32 o -13 7 0 16.51 4.23 32.75 o -12 7 0 79.69 122.94 47.54 o -11 7 0 125.05 109.94 43.00 o -10 7 0 120.94 139.63 39.55 o -9 7 0 2.17 31.25 35.50 o -8 7 0 121.74 150.71 38.20 o -7 7 0 138.41 128.58 27.19 o -6 7 0 270.71 292.50 69.83 o -5 7 0 0.18 100.43 53.01 o -4 7 0 136.64 287.86 59.31 o -3 7 0 23.73 60.79 41.76 o -2 7 0 239.56 199.27 47.00 o -1 7 0 13.62 57.43 45.00 o 0 7 0 1760.55 1919.43 59.01 o 1 7 0 149.80 214.47 45.49 o 2 7 0 149.56 155.58 38.80 o 3 7 0 381.20 394.22 34.85 o 4 7 0 1067.82 1112.57 85.30 o 5 7 0 167.62 178.92 27.00 o 6 7 0 221.12 256.91 23.30 o 7 7 0 49.90 63.42 28.93 o 8 7 0 21.95 40.36 23.23 o 9 7 0 123.74 139.31 24.79 o 10 7 0 64.80 53.28 25.06 o -13 8 0 0.00 41.49 43.07 o -12 8 0 11.43 24.26 42.55 o -11 8 0 145.30 142.82 40.25 o -10 8 0 1.15 47.14 41.41 o -9 8 0 86.00 132.38 35.86 o -8 8 0 65.61 107.10 33.01 o -7 8 0 18.44 18.06 33.87 o -6 8 0 354.72 206.26 34.81 o -5 8 0 8.67 27.27 34.58 o -4 8 0 5.97 31.28 52.13 o -3 8 0 1764.07 1797.64 77.10 o -2 8 0 2026.33 1331.61 61.08 o -1 8 0 209.42 73.19 36.81 o 0 8 0 682.94 607.02 99.54 o 1 8 0 33.22 32.62 63.88 o 2 8 0 6.06 18.14 43.23 o 3 8 0 43.41 41.58 38.13 o 4 8 0 622.07 631.14 50.69 o 5 8 0 180.26 240.60 41.49 o 6 8 0 10.97 9.45 29.45 o 7 8 0 35.11 44.59 25.79 o 8 8 0 5.12 30.08 24.60 o 9 8 0 28.46 9.59 26.11 o -13 9 0 92.15 155.21 46.32 o -12 9 0 10.48 20.36 41.81 o -11 9 0 28.36 59.26 40.39 o -10 9 0 92.83 118.86 57.19 o -9 9 0 13.26 32.75 49.24 o -8 9 0 78.83 141.47 38.82 o -7 9 0 32.79 25.21 30.60 o -6 9 0 413.24 481.53 44.43 o -5 9 0 8.61 48.48 49.42 o -4 9 0 846.43 853.44 63.32 o -3 9 0 149.16 77.23 41.52 o -2 9 0 4.92 15.08 58.02 o -1 9 0 0.16 63.35 38.84 o 0 9 0 67.14 62.41 36.19 o 1 9 0 12.30 -17.70 63.59 o 2 9 0 21.50 69.79 44.03 o 3 9 0 281.55 282.60 95.36 o 4 9 0 170.68 199.65 60.64 o 5 9 0 0.03 21.83 26.63 o 6 9 0 148.58 128.38 29.42 o 7 9 0 141.55 137.66 27.87 o 8 9 0 17.79 -3.18 40.48 o 9 9 0 37.28 13.62 29.20 o -13 10 0 3.74 3.89 71.39 o -12 10 0 11.46 40.58 67.03 o -11 10 0 8.99 22.80 64.38 o -10 10 0 33.99 55.49 55.37 o -9 10 0 252.68 243.91 45.54 o -8 10 0 12.78 37.51 36.79 o -7 10 0 4.07 26.16 34.30 o -6 10 0 0.02 28.32 39.67 o -5 10 0 37.51 133.65 53.54 o -4 10 0 382.74 478.07 52.22 o -3 10 0 445.21 572.37 92.36 o -2 10 0 1.48 36.17 58.31 o -1 10 0 1.46 25.91 38.83 o 0 10 0 1.19 32.62 46.62 o 1 10 0 149.73 79.07 37.71 o 2 10 0 163.95 268.62 44.74 o 3 10 0 361.92 528.34 71.18 o 4 10 0 54.45 93.39 31.23 o 5 10 0 9.81 13.68 26.73 o 6 10 0 26.21 34.23 26.52 o 7 10 0 37.92 36.61 46.23 o 8 10 0 18.13 -23.06 26.69 o -12 11 0 70.02 17.32 70.39 o -11 11 0 0.53 -37.52 63.91 o -10 11 0 2.49 -27.86 60.73 o -9 11 0 23.98 20.18 38.19 o -8 11 0 1655.30 1448.18 246.24 o -7 11 0 62.53 89.30 33.26 o -6 11 0 381.61 387.44 42.24 o -5 11 0 519.15 464.61 117.49 o -4 11 0 145.35 159.66 33.48 o -3 11 0 93.47 69.36 44.56 o -2 11 0 243.46 213.99 49.10 o -1 11 0 392.72 535.07 50.38 o 0 11 0 71.31 42.14 37.46 o 1 11 0 1004.44 1079.07 310.12 o 2 11 0 11.51 -27.52 29.04 o 3 11 0 129.51 138.36 31.42 o 4 11 0 13.23 -8.33 28.79 o 5 11 0 0.32 -17.19 30.43 o 6 11 0 5.65 37.78 25.82 o 7 11 0 2.56 19.49 39.65 o -12 12 0 3.23 25.39 68.97 o -11 12 0 105.48 72.39 65.62 o -10 12 0 36.22 78.50 46.44 o -9 12 0 0.55 -17.33 38.27 o -8 12 0 226.01 218.77 45.18 o -7 12 0 351.17 490.98 45.62 o -6 12 0 107.45 138.66 32.90 o -5 12 0 494.44 627.57 79.65 o -4 12 0 230.95 270.05 72.85 o -3 12 0 0.11 59.76 41.13 o -2 12 0 15.70 9.26 31.86 o -1 12 0 210.05 269.52 46.77 o 0 12 0 151.29 169.48 56.87 o 1 12 0 19.85 -1.21 53.37 o 2 12 0 96.96 159.17 29.12 o 3 12 0 240.50 166.52 34.78 o 4 12 0 365.58 344.98 48.72 o 5 12 0 39.81 99.27 37.95 o 6 12 0 59.86 51.63 47.46 o -11 13 0 34.48 -39.64 67.27 o -10 13 0 0.68 -12.35 42.60 o -9 13 0 98.51 83.12 39.49 o -8 13 0 221.49 234.35 40.92 o -7 13 0 247.09 180.55 36.40 o -6 13 0 0.68 -12.75 32.61 o -5 13 0 6.23 17.65 26.18 o -4 13 0 18.11 6.81 24.32 o -3 13 0 29.81 24.25 27.01 o -2 13 0 5.65 20.33 24.94 o -1 13 0 203.40 217.20 45.31 o 0 13 0 91.90 103.51 40.74 o 1 13 0 352.56 278.05 43.74 o 2 13 0 127.01 130.89 27.79 o 3 13 0 29.83 63.15 29.15 o 4 13 0 142.07 155.99 35.24 o 5 13 0 81.15 36.69 31.55 o -10 14 0 28.42 56.97 36.33 o -9 14 0 14.15 45.33 24.97 o -8 14 0 32.09 7.54 35.68 o -7 14 0 17.27 31.72 33.07 o -6 14 0 16.22 9.65 33.29 o -5 14 0 48.75 53.66 27.52 o -4 14 0 16.85 26.51 33.70 o -3 14 0 3.10 -20.19 30.82 o -2 14 0 21.22 13.59 25.03 o -1 14 0 0.60 -16.01 52.17 o 0 14 0 1.41 8.42 30.05 o 1 14 0 37.70 32.95 37.54 o 2 14 0 125.77 124.06 38.07 o 3 14 0 45.71 26.94 32.94 o -9 15 0 7.24 21.70 32.65 o -8 15 0 0.12 56.01 31.20 o -7 15 0 42.58 91.96 37.53 o -6 15 0 94.43 107.02 30.74 o -5 15 0 0.93 -34.74 35.81 o -4 15 0 0.31 18.80 24.26 o -3 15 0 12.66 -15.59 26.07 o -2 15 0 19.10 21.80 32.17 o -1 15 0 132.33 87.98 26.86 o 0 15 0 5.90 1.69 27.95 o 1 15 0 66.83 82.01 32.60 o -7 16 0 112.97 154.02 56.54 o -6 16 0 0.76 7.72 37.44 o -5 16 0 69.91 81.24 32.10 o -4 16 0 57.44 62.56 32.77 o -3 16 0 0.33 1.68 28.34 o -2 16 0 6.07 37.96 28.15 o -1 16 0 48.52 16.82 38.22 o 0 -16 1 32.36 -0.38 36.94 o 1 -16 1 22.58 -0.10 26.16 o 2 -16 1 7.20 34.54 27.81 o 3 -16 1 13.79 6.36 28.43 o 4 -16 1 5.12 35.57 28.29 o 5 -16 1 0.43 -6.42 31.53 o 6 -16 1 0.22 46.22 31.69 o 7 -16 1 12.78 -0.65 32.53 o -2 -15 1 13.08 62.29 33.44 o -1 -15 1 3.42 44.62 30.44 o 0 -15 1 95.13 93.12 23.62 o 1 -15 1 3.73 -8.12 46.11 o 2 -15 1 18.35 66.28 31.01 o 3 -15 1 46.32 81.88 38.28 o 4 -15 1 145.39 127.37 29.20 o 5 -15 1 23.19 54.91 31.83 o 6 -15 1 23.88 54.69 28.47 o 7 -15 1 68.30 88.58 34.51 o 8 -15 1 10.41 26.08 26.57 o 9 -15 1 6.73 31.61 34.22 o -4 -14 1 2.40 59.46 29.98 o -3 -14 1 5.44 2.47 31.51 o -2 -14 1 91.93 170.02 45.76 o -1 -14 1 123.47 121.95 76.51 o 0 -14 1 23.66 56.42 33.50 o 1 -14 1 5.95 67.82 31.47 o 2 -14 1 2.31 -28.06 28.06 o 3 -14 1 16.99 34.82 31.66 o 4 -14 1 166.56 184.44 46.33 o 5 -14 1 515.28 555.62 83.99 o 6 -14 1 387.24 266.84 40.63 o 7 -14 1 108.14 113.42 35.27 o 8 -14 1 236.19 304.67 59.59 o 9 -14 1 51.64 7.96 41.23 o 10 -14 1 7.67 -10.90 36.57 o -5 -13 1 6.26 -31.06 31.06 o -4 -13 1 0.00 2.77 31.79 o -3 -13 1 33.20 56.88 46.30 o -2 -13 1 1.80 31.73 36.28 o -1 -13 1 182.13 209.73 79.31 o 0 -13 1 9.69 43.06 45.97 o 1 -13 1 69.21 62.39 35.03 o 2 -13 1 95.98 75.09 28.91 o 3 -13 1 44.26 23.06 29.21 o 4 -13 1 39.29 90.78 34.87 o 5 -13 1 102.82 90.46 27.00 o 6 -13 1 14.73 19.65 41.15 o 7 -13 1 0.96 29.43 52.19 o 8 -13 1 776.23 904.23 90.97 o 9 -13 1 34.47 22.80 38.25 o 10 -13 1 8.43 55.38 44.33 o 11 -13 1 1.57 -31.57 63.67 o -6 -12 1 0.69 -19.03 31.26 o -5 -12 1 0.03 0.82 32.01 o -4 -12 1 72.15 64.31 37.97 o -3 -12 1 8.16 66.65 45.35 o -2 -12 1 108.54 67.05 77.66 o -1 -12 1 185.76 226.34 45.89 o 0 -12 1 103.58 47.54 32.83 o 1 -12 1 27.49 59.15 42.94 o 2 -12 1 192.54 190.10 34.96 o 3 -12 1 26.91 38.84 33.16 o 4 -12 1 32.63 42.44 28.82 o 5 -12 1 462.52 356.83 45.41 o 6 -12 1 9.14 -11.13 50.07 o 7 -12 1 864.15 616.10 171.29 o 8 -12 1 1.97 6.87 31.76 o 9 -12 1 27.40 38.24 37.83 o 10 -12 1 32.46 14.71 47.28 o 11 -12 1 12.44 -1.47 63.32 o 12 -12 1 32.74 11.66 70.86 o -7 -11 1 31.62 45.44 28.47 o -6 -11 1 8.79 7.53 37.89 o -5 -11 1 20.31 36.24 49.83 o -4 -11 1 369.55 420.74 73.75 o -3 -11 1 214.81 237.23 50.54 o -2 -11 1 413.93 314.99 123.28 o -1 -11 1 6.90 -19.61 44.18 o 0 -11 1 788.48 856.71 225.33 o 1 -11 1 1.57 -37.62 37.62 o 2 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