#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/29/2212998.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2212998_Fobs loop_ _publ_author_name 'Patil, P. S.' 'Chantrapromma, Suchada' 'Fun, Hoong-Kun' 'Dharmaprakash, S. M.' _publ_section_title ; 1-(3-Bromophenyl)-3-[4-(dimethylamino)phenyl]prop-2-en-1-one ; _journal_coeditor_code SG2150 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1738 _journal_page_last o1740 _journal_volume 63 _journal_year 2007 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.9586 _cell_length_b 6.0703 _cell_length_c 33.3498 _exptl_crystal_F_000 1344.00 _reflns_d_resolution_high 0.7108 _[local]_cod_data_source_file sg2150Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' patil86m in Pbca (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 658.21 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6495.47 7276.94 178.96 o 4 0 0 433238.34 499325.31 10513.33 o 6 0 0 38663.78 43839.62 871.52 o 8 0 0 760.26 1241.88 72.43 o 10 0 0 19958.76 22890.69 444.33 o 12 0 0 17917.92 20008.15 529.36 o 14 0 0 461.60 536.58 153.46 o 16 0 0 7632.97 8210.83 453.93 o 18 0 0 2294.89 2520.57 286.26 o 2 1 0 21872.78 23027.27 337.72 o 4 1 0 72443.74 80300.38 1150.64 o 6 1 0 995.89 1195.51 36.84 o 8 1 0 60924.26 68706.06 983.33 o 10 1 0 3227.00 3473.73 83.23 o 12 1 0 9733.34 10744.00 200.27 o 14 1 0 2499.45 2713.70 103.51 o 16 1 0 32.89 81.64 96.07 o 18 1 0 38.11 -92.03 118.44 o 0 2 0 48722.52 48107.76 836.35 o 2 2 0 4666.77 4763.95 71.18 o 4 2 0 15576.74 16030.04 218.79 o 6 2 0 14037.45 15001.95 271.48 o 8 2 0 1520.78 1583.05 64.95 o 10 2 0 2864.72 2936.32 89.12 o 12 2 0 10907.35 11669.54 236.10 o 14 2 0 282.14 261.99 55.31 o 16 2 0 5781.40 5350.16 218.25 o 18 2 0 1124.33 1014.98 230.03 o 2 3 0 1634.62 2456.60 47.35 o 4 3 0 5575.43 5009.45 80.95 o 6 3 0 1870.57 2086.17 57.96 o 8 3 0 1964.31 1802.58 80.36 o 10 3 0 2551.41 2371.94 84.80 o 12 3 0 570.47 617.82 67.97 o 14 3 0 1701.64 1855.95 107.75 o 16 3 0 2236.47 2387.41 135.88 o 18 3 0 182.59 245.06 163.53 o 0 4 0 134.96 75.88 28.57 o 2 4 0 441.16 405.82 26.63 o 4 4 0 43.13 80.82 20.88 o 6 4 0 1094.80 1101.80 46.10 o 8 4 0 1132.69 1192.80 62.15 o 10 4 0 123.95 76.05 37.87 o 12 4 0 1118.77 1312.95 96.28 o 14 4 0 244.18 273.74 78.71 o 16 4 0 203.66 160.48 84.42 o 2 5 0 165.89 260.73 30.36 o 4 5 0 527.11 610.45 48.60 o 6 5 0 56.97 105.74 32.72 o 8 5 0 329.26 389.55 48.31 o 10 5 0 2.38 1.07 52.58 o 12 5 0 58.76 7.30 65.62 o 14 5 0 42.40 -16.76 79.69 o 0 6 0 3890.37 4037.24 131.08 o 2 6 0 237.22 306.18 47.24 o 4 6 0 1362.83 1367.14 83.49 o 6 6 0 1024.61 1206.35 68.36 o 8 6 0 119.84 125.67 55.37 o 10 6 0 579.44 367.96 125.27 o 12 6 0 750.08 397.30 174.85 o 2 7 0 567.08 729.64 97.86 o 4 7 0 1310.27 1430.04 102.96 o 6 7 0 15.59 81.44 59.66 o 8 7 0 1167.40 1221.34 137.15 o 10 7 0 246.97 355.14 137.08 o 2 8 0 791.82 741.41 186.32 o 4 8 0 815.07 1059.38 151.78 o 6 8 0 2756.84 3138.42 145.76 o 1 1 1 1110.15 1127.53 18.27 o 2 1 1 28052.35 29084.78 305.49 o 3 1 1 1810.10 2048.23 31.60 o 4 1 1 7871.55 8755.31 99.00 o 5 1 1 3947.81 4494.18 57.89 o 6 1 1 2364.53 2973.08 41.68 o 7 1 1 250.94 389.33 18.03 o 8 1 1 622.60 773.84 25.38 o 9 1 1 4643.11 5018.47 65.52 o 10 1 1 150.84 115.15 20.63 o 11 1 1 222.81 234.77 27.04 o 12 1 1 96.16 91.87 26.31 o 13 1 1 940.23 875.04 41.02 o 14 1 1 258.77 228.34 39.01 o 15 1 1 160.63 141.81 55.28 o 16 1 1 36.83 21.49 63.69 o 17 1 1 75.19 35.45 76.16 o 18 1 1 206.55 168.49 91.38 o 19 1 1 47.14 37.67 91.97 o 0 2 1 3370.07 3501.17 52.29 o 1 2 1 13056.86 12259.52 108.72 o 2 2 1 0.95 5.36 7.49 o 3 2 1 784.86 910.03 21.61 o 4 2 1 630.04 792.14 20.39 o 5 2 1 5876.45 5003.30 60.01 o 6 2 1 36.27 47.25 14.49 o 7 2 1 2516.01 2390.13 44.72 o 8 2 1 8.48 -1.50 17.94 o 9 2 1 245.72 360.65 27.53 o 10 2 1 435.87 503.23 33.28 o 11 2 1 2574.19 2712.25 79.38 o 12 2 1 59.29 88.88 28.43 o 13 2 1 4528.41 4566.00 89.27 o 14 2 1 260.76 250.21 41.56 o 15 2 1 73.03 35.64 41.25 o 16 2 1 167.22 72.85 57.26 o 17 2 1 3298.75 2619.81 158.37 o 18 2 1 15.60 -11.16 101.02 o 19 2 1 263.39 100.86 124.30 o 1 3 1 2851.01 2380.67 31.55 o 2 3 1 1187.93 1337.43 23.39 o 3 3 1 16879.04 15972.49 143.81 o 4 3 1 239.86 309.88 14.40 o 5 3 1 6172.14 6322.30 79.65 o 6 3 1 35.75 34.19 14.34 o 7 3 1 5148.67 4899.17 72.81 o 8 3 1 72.89 113.38 29.76 o 9 3 1 12428.24 11751.29 162.09 o 10 3 1 264.01 217.96 31.90 o 11 3 1 304.17 268.79 36.12 o 12 3 1 4.66 24.13 34.53 o 13 3 1 2992.96 3067.49 82.23 o 14 3 1 338.89 291.01 49.50 o 15 3 1 2066.95 2246.15 87.62 o 16 3 1 26.69 76.43 55.91 o 17 3 1 58.96 31.52 62.92 o 18 3 1 32.80 -63.08 84.98 o 0 4 1 255.39 402.12 24.75 o 1 4 1 13061.11 12601.48 119.13 o 2 4 1 293.02 311.07 17.92 o 3 4 1 146.48 155.48 15.55 o 4 4 1 19.97 17.74 13.87 o 5 4 1 13572.75 13049.17 127.73 o 6 4 1 887.59 997.31 36.70 o 7 4 1 5723.59 5770.98 89.17 o 8 4 1 1.26 6.21 22.96 o 9 4 1 703.10 647.20 39.53 o 10 4 1 139.50 148.04 29.61 o 11 4 1 5238.86 5426.43 121.47 o 12 4 1 37.45 -36.29 42.95 o 13 4 1 1521.95 1646.37 87.36 o 14 4 1 3.76 39.83 47.17 o 15 4 1 530.09 448.80 64.32 o 16 4 1 122.82 65.24 58.24 o 17 4 1 1259.92 1258.76 85.20 o 1 5 1 3070.64 3034.07 48.38 o 2 5 1 673.33 619.17 26.34 o 3 5 1 9342.47 9288.67 100.35 o 4 5 1 188.26 167.84 26.87 o 5 5 1 619.75 612.04 34.47 o 6 5 1 131.04 71.66 26.39 o 7 5 1 2644.67 2783.77 73.28 o 8 5 1 288.87 284.25 34.04 o 9 5 1 3186.97 3293.75 90.22 o 10 5 1 13.97 12.27 36.71 o 11 5 1 153.48 118.56 41.30 o 12 5 1 125.66 77.08 47.68 o 13 5 1 555.71 557.49 65.56 o 14 5 1 61.89 -31.44 56.58 o 15 5 1 1157.38 1347.57 86.78 o 0 6 1 931.55 1031.99 52.19 o 1 6 1 3894.32 4216.56 70.72 o 2 6 1 241.44 168.77 31.21 o 3 6 1 60.24 63.90 34.62 o 4 6 1 470.06 460.14 43.39 o 5 6 1 2765.82 3064.89 77.04 o 6 6 1 912.27 911.44 42.37 o 7 6 1 2191.13 2331.33 72.01 o 8 6 1 27.80 14.56 34.87 o 9 6 1 5.31 48.27 41.87 o 10 6 1 436.42 316.65 53.05 o 11 6 1 2063.79 2270.43 95.39 o 12 6 1 69.17 49.04 44.92 o 13 6 1 780.57 795.55 79.65 o 1 7 1 55.35 108.04 50.55 o 2 7 1 6.42 76.27 59.43 o 3 7 1 1380.38 1792.69 88.32 o 4 7 1 520.22 649.17 64.97 o 5 7 1 790.92 740.57 51.38 o 6 7 1 0.71 24.78 39.61 o 7 7 1 666.16 745.41 62.69 o 8 7 1 490.93 664.99 54.62 o 9 7 1 787.40 909.44 63.56 o 10 7 1 30.22 24.98 57.62 o 11 7 1 48.53 4.56 57.88 o 1 8 1 377.93 274.15 131.36 o 2 8 1 0.08 -160.09 101.99 o 3 8 1 125.47 82.89 77.14 o 4 8 1 11.99 75.60 82.47 o 5 8 1 80.52 197.30 52.12 o 6 8 1 0.13 148.68 63.92 o 0 0 2 16530.36 -4.67 2.34 o 1 0 2 650.12 546.72 97.00 o 2 0 2 10991.45 12615.82 214.50 o 3 0 2 33.54 -21.09 10.55 o 4 0 2 5729.43 6484.84 102.79 o 5 0 2 12318.37 15843.68 225.22 o 6 0 2 24711.62 28215.34 419.25 o 7 0 2 1302.97 1416.67 41.85 o 8 0 2 2638.32 2944.98 70.80 o 9 0 2 5447.26 6510.75 106.87 o 10 0 2 4507.27 4836.14 85.89 o 11 0 2 481.22 495.50 34.38 o 12 0 2 12182.64 13686.09 233.68 o 13 0 2 1773.25 1919.67 98.50 o 14 0 2 295.18 363.79 79.31 o 15 0 2 324.11 266.79 84.37 o 16 0 2 4822.44 5130.56 343.56 o 17 0 2 323.79 376.08 120.18 o 18 0 2 657.14 970.98 142.81 o 19 0 2 1438.54 1427.62 176.76 o 1 1 2 11789.21 11579.04 118.44 o 2 1 2 41087.01 41908.70 428.23 o 3 1 2 12724.98 14489.90 149.98 o 4 1 2 86592.12 94755.24 908.95 o 5 1 2 2540.21 2735.38 40.59 o 6 1 2 2077.48 2243.99 33.69 o 7 1 2 3915.53 5000.32 63.97 o 8 1 2 45394.84 50756.41 519.66 o 9 1 2 362.35 344.91 19.41 o 10 1 2 6601.36 7086.07 93.63 o 11 1 2 1181.29 1444.13 41.93 o 12 1 2 2867.38 3339.91 65.03 o 13 1 2 37.47 27.88 28.40 o 14 1 2 8136.59 8933.31 142.94 o 15 1 2 259.32 180.61 55.47 o 16 1 2 1395.38 1381.47 99.09 o 17 1 2 211.62 248.58 82.14 o 18 1 2 1547.54 1527.04 132.85 o 19 1 2 8.56 -28.06 91.34 o 0 2 2 37347.08 37360.80 437.87 o 1 2 2 434.55 533.02 12.69 o 2 2 2 2069.39 1933.56 25.32 o 3 2 2 567.41 704.57 16.86 o 4 2 2 8422.83 8661.58 90.73 o 5 2 2 1470.89 1750.60 31.55 o 6 2 2 8586.96 8626.69 109.78 o 7 2 2 529.52 645.11 25.21 o 8 2 2 2234.55 2370.31 49.12 o 9 2 2 225.30 240.39 23.43 o 10 2 2 3518.82 3766.53 73.61 o 11 2 2 216.76 164.85 27.97 o 12 2 2 5727.02 5665.76 95.21 o 13 2 2 62.14 101.48 33.86 o 14 2 2 5.10 -13.21 36.72 o 15 2 2 30.73 -3.23 40.45 o 16 2 2 780.13 778.57 79.82 o 17 2 2 140.04 122.16 97.54 o 18 2 2 783.18 801.09 126.56 o 19 2 2 1.08 -20.37 124.74 o 1 3 2 58.96 52.63 10.55 o 2 3 2 22953.36 23927.31 205.71 o 3 3 2 1922.98 2125.78 30.46 o 4 3 2 4371.67 4280.32 49.20 o 5 3 2 562.72 636.99 23.87 o 6 3 2 1292.44 1426.34 35.06 o 7 3 2 1820.54 2013.63 43.10 o 8 3 2 4010.90 3842.25 74.33 o 9 3 2 465.50 604.78 39.23 o 10 3 2 1837.92 1868.47 54.65 o 11 3 2 529.26 530.09 40.60 o 12 3 2 107.08 34.91 35.28 o 13 3 2 291.21 341.08 47.03 o 14 3 2 1769.76 1945.42 79.00 o 15 3 2 224.25 258.48 50.65 o 16 3 2 1135.30 1217.59 73.88 o 17 3 2 123.52 34.53 66.41 o 18 3 2 180.84 197.39 144.16 o 0 4 2 10.40 12.69 18.67 o 1 4 2 3143.84 3802.85 48.28 o 2 4 2 150.34 159.27 15.64 o 3 4 2 914.44 1047.89 25.54 o 4 4 2 89.41 90.89 15.30 o 5 4 2 2226.63 2717.89 43.39 o 6 4 2 402.60 451.00 28.60 o 7 4 2 20.41 110.26 21.60 o 8 4 2 795.34 781.06 39.54 o 9 4 2 407.75 318.73 33.36 o 10 4 2 80.21 49.48 24.07 o 11 4 2 0.69 162.38 42.64 o 12 4 2 710.02 604.21 66.24 o 13 4 2 0.35 17.91 45.35 o 14 4 2 8.63 -33.00 50.22 o 15 4 2 33.70 -45.21 52.20 o 16 4 2 23.64 64.64 56.63 o 17 4 2 113.02 58.46 61.13 o 1 5 2 6.55 126.38 19.72 o 2 5 2 369.19 419.87 24.23 o 3 5 2 125.39 598.87 37.69 o 4 5 2 103.13 100.28 26.37 o 5 5 2 28.19 83.81 23.09 o 6 5 2 115.91 120.94 25.61 o 7 5 2 188.64 332.92 32.23 o 8 5 2 217.29 210.98 32.75 o 9 5 2 4.75 137.33 63.70 o 10 5 2 0.45 -72.58 36.29 o 11 5 2 8.19 -90.52 46.66 o 12 5 2 89.25 114.96 50.86 o 13 5 2 20.39 167.79 59.75 o 14 5 2 81.01 36.60 54.33 o 15 5 2 49.62 117.62 60.90 o 0 6 2 220.62 380.94 45.84 o 1 6 2 743.35 1007.94 38.87 o 2 6 2 334.38 388.42 32.87 o 3 6 2 475.89 344.70 40.99 o 4 6 2 12.09 82.86 36.50 o 5 6 2 155.21 484.40 38.78 o 6 6 2 1389.58 1565.02 54.02 o 7 6 2 1.41 201.58 37.20 o 8 6 2 388.48 358.19 42.46 o 9 6 2 4.00 67.94 41.22 o 10 6 2 698.17 640.18 60.19 o 11 6 2 201.19 273.83 56.33 o 12 6 2 602.70 504.30 70.53 o 13 6 2 5.58 90.15 60.95 o 1 7 2 102.17 149.25 53.33 o 2 7 2 3063.30 3312.51 112.09 o 3 7 2 2.27 125.16 57.70 o 4 7 2 1032.23 1223.77 85.63 o 5 7 2 184.56 203.86 43.82 o 6 7 2 126.01 135.28 50.04 o 7 7 2 48.36 94.38 44.95 o 8 7 2 1062.54 1182.07 63.15 o 9 7 2 73.01 195.84 49.18 o 10 7 2 726.66 973.75 100.49 o 11 7 2 45.05 69.71 75.49 o 1 8 2 108.11 67.79 138.48 o 2 8 2 123.71 78.21 102.86 o 3 8 2 62.00 96.56 76.00 o 4 8 2 650.80 608.62 98.50 o 5 8 2 80.18 58.12 58.26 o 6 8 2 548.74 526.18 58.66 o 1 1 3 86.30 127.61 6.60 o 2 1 3 20.61 18.61 6.58 o 3 1 3 17352.92 17985.86 176.75 o 4 1 3 55.12 68.58 8.99 o 5 1 3 4903.84 5425.49 63.24 o 6 1 3 57.73 77.00 12.14 o 7 1 3 6978.86 7908.65 86.65 o 8 1 3 82.03 117.89 15.56 o 9 1 3 1911.36 2029.96 37.13 o 10 1 3 9.22 17.50 18.31 o 11 1 3 2.82 -6.55 23.22 o 12 1 3 16.82 -23.18 24.66 o 13 1 3 349.81 315.94 32.46 o 14 1 3 233.78 245.93 39.45 o 15 1 3 894.31 976.34 74.77 o 16 1 3 111.49 277.42 69.30 o 17 1 3 19.00 13.26 73.01 o 18 1 3 203.35 374.54 95.63 o 19 1 3 187.81 89.15 95.54 o 0 2 3 1092.31 1152.96 24.76 o 1 2 3 9116.08 8812.10 81.22 o 2 2 3 4580.65 4445.57 48.06 o 3 2 3 497.85 528.73 16.37 o 4 2 3 25.03 41.15 9.41 o 5 2 3 9157.77 9353.66 100.22 o 6 2 3 9385.96 10187.14 115.66 o 7 2 3 1157.95 1068.55 30.57 o 8 2 3 33.51 41.48 16.99 o 9 2 3 188.44 146.38 23.16 o 10 2 3 2902.39 3361.32 64.08 o 11 2 3 1179.37 1282.93 43.91 o 12 2 3 64.53 89.02 30.08 o 13 2 3 1723.25 1845.52 60.46 o 14 2 3 100.51 70.72 38.48 o 15 2 3 24.28 -31.58 39.45 o 16 2 3 258.25 281.26 64.03 o 17 2 3 1492.30 1411.88 147.28 o 18 2 3 1.80 93.84 152.37 o 19 2 3 203.65 185.88 108.51 o 1 3 3 4277.40 3972.00 43.86 o 2 3 3 9693.89 10345.02 97.85 o 3 3 3 11854.93 10988.99 104.64 o 4 3 3 666.20 687.06 18.59 o 5 3 3 1710.84 1686.91 29.83 o 6 3 3 651.09 762.36 24.27 o 7 3 3 3189.61 3076.42 52.26 o 8 3 3 721.61 830.82 36.56 o 9 3 3 7641.11 7478.86 114.99 o 10 3 3 699.48 711.26 39.22 o 11 3 3 246.39 244.11 34.58 o 12 3 3 101.70 105.97 34.93 o 13 3 3 2031.25 2043.48 71.11 o 14 3 3 940.31 929.74 60.78 o 15 3 3 1844.57 1945.89 80.87 o 16 3 3 15.34 41.26 51.30 o 17 3 3 53.75 20.69 61.67 o 18 3 3 141.26 18.07 101.66 o 0 4 3 3421.72 3651.93 64.51 o 1 4 3 13029.28 12538.36 120.12 o 2 4 3 740.67 760.67 22.59 o 3 4 3 157.67 136.50 16.25 o 4 4 3 1403.99 1534.50 30.19 o 5 4 3 9411.35 8949.55 102.98 o 6 4 3 3048.92 3080.00 53.34 o 7 4 3 7482.64 7157.49 103.10 o 8 4 3 1.73 -4.78 22.71 o 9 4 3 244.27 247.90 33.76 o 10 4 3 835.59 895.45 50.74 o 11 4 3 7026.51 7009.09 137.97 o 12 4 3 438.74 368.50 51.62 o 13 4 3 1306.38 1247.79 70.78 o 14 4 3 82.14 26.70 49.92 o 15 4 3 464.21 399.12 57.46 o 16 4 3 377.52 387.99 64.59 o 17 4 3 1032.30 892.27 78.11 o 1 5 3 5745.63 5474.92 68.54 o 2 5 3 659.96 802.76 28.35 o 3 5 3 19578.12 18953.42 197.45 o 4 5 3 403.04 388.91 33.28 o 5 5 3 1546.87 1475.84 47.31 o 6 5 3 165.54 103.34 25.20 o 7 5 3 8127.80 7980.96 132.53 o 8 5 3 770.06 778.28 46.57 o 9 5 3 7476.73 7343.10 158.72 o 10 5 3 1479.45 1351.68 66.30 o 11 5 3 8.91 -64.10 32.05 o 12 5 3 482.37 432.54 57.81 o 13 5 3 3246.51 3341.21 111.83 o 14 5 3 740.59 596.72 79.99 o 15 5 3 1764.13 1940.26 98.12 o 0 6 3 3260.32 3098.13 93.93 o 1 6 3 6417.79 6512.02 101.18 o 2 6 3 203.38 202.10 29.58 o 3 6 3 271.40 250.02 38.58 o 4 6 3 1261.24 1357.55 64.66 o 5 6 3 6332.61 6698.69 114.61 o 6 6 3 798.01 910.79 42.90 o 7 6 3 2092.41 2202.75 70.29 o 8 6 3 1.62 25.23 44.27 o 9 6 3 687.27 699.03 54.09 o 10 6 3 263.95 336.11 52.32 o 11 6 3 2777.43 3047.46 108.18 o 12 6 3 283.58 290.15 60.62 o 13 6 3 211.41 214.39 75.49 o 1 7 3 745.93 858.82 66.62 o 2 7 3 1463.77 1648.13 85.24 o 3 7 3 2104.84 2289.72 101.48 o 4 7 3 317.38 441.63 57.98 o 5 7 3 387.15 325.59 56.75 o 6 7 3 163.99 124.82 39.53 o 7 7 3 678.82 666.99 64.06 o 8 7 3 415.11 432.45 59.10 o 9 7 3 2034.83 2341.11 85.77 o 10 7 3 58.34 188.36 59.93 o 11 7 3 7.99 -43.56 55.43 o 1 8 3 158.39 303.49 125.81 o 2 8 3 29.69 88.25 99.74 o 3 8 3 9.70 12.25 75.07 o 4 8 3 182.23 257.35 66.10 o 5 8 3 26.21 54.19 58.16 o 6 8 3 113.80 144.78 71.25 o 0 0 4 15245.11 13508.63 292.15 o 1 0 4 2361.61 2274.17 47.46 o 2 0 4 8730.17 8648.85 150.98 o 3 0 4 18307.80 20194.19 288.91 o 4 0 4 4535.69 4935.72 81.25 o 5 0 4 8232.19 9381.41 134.74 o 6 0 4 22986.49 25359.96 352.70 o 7 0 4 5279.41 6039.71 101.10 o 8 0 4 2948.17 3307.08 66.58 o 9 0 4 2357.94 2886.37 60.38 o 10 0 4 5046.78 5333.83 89.85 o 11 0 4 974.51 1002.55 39.97 o 12 0 4 6576.25 6999.77 139.62 o 13 0 4 38.14 56.95 51.31 o 14 0 4 591.01 657.22 83.33 o 15 0 4 17.65 -27.02 70.56 o 16 0 4 1383.54 1450.11 135.86 o 17 0 4 72.49 127.02 104.25 o 18 0 4 3098.07 3408.55 225.50 o 19 0 4 45.15 180.56 136.90 o 1 1 4 14015.56 13767.46 151.80 o 2 1 4 35624.09 35202.23 383.36 o 3 1 4 21188.36 22587.25 223.98 o 4 1 4 1075.22 958.81 19.90 o 5 1 4 1941.49 2379.68 33.47 o 6 1 4 353.35 382.59 15.43 o 7 1 4 3533.39 3657.73 49.31 o 8 1 4 1809.70 1766.56 33.63 o 9 1 4 77.42 70.78 16.45 o 10 1 4 5799.85 6135.93 82.16 o 11 1 4 523.48 605.40 31.89 o 12 1 4 169.30 164.92 28.18 o 13 1 4 111.32 108.52 29.44 o 14 1 4 3559.11 3855.41 86.85 o 15 1 4 2345.51 2375.88 99.14 o 16 1 4 2454.14 2669.12 133.11 o 17 1 4 0.12 19.55 74.86 o 18 1 4 28.61 12.00 93.61 o 19 1 4 900.69 913.14 134.35 o 0 2 4 22976.29 22676.51 265.47 o 1 2 4 26.55 40.45 8.34 o 2 2 4 12457.91 12474.03 121.37 o 3 2 4 193.15 239.13 13.75 o 4 2 4 2807.87 2565.13 35.73 o 5 2 4 185.72 296.71 15.51 o 6 2 4 36608.43 38372.87 387.63 o 7 2 4 1795.10 1972.89 37.17 o 8 2 4 3399.95 3551.26 57.16 o 9 2 4 111.89 122.56 20.79 o 10 2 4 12136.13 12761.71 162.33 o 11 2 4 913.45 1010.94 40.52 o 12 2 4 7283.69 7622.62 117.23 o 13 2 4 6.26 45.06 33.15 o 14 2 4 176.81 161.05 39.72 o 15 2 4 40.78 46.51 41.72 o 16 2 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13 5 10 49.92 105.97 56.36 o 14 5 10 3.05 27.44 56.73 o 15 5 10 18.87 102.12 72.71 o 0 6 10 149.49 285.72 65.16 o 1 6 10 1079.68 1139.77 47.68 o 2 6 10 10.82 29.01 27.72 o 3 6 10 0.88 0.08 29.10 o 4 6 10 4.14 66.01 34.72 o 5 6 10 1780.82 1825.15 68.44 o 6 6 10 47.33 79.22 32.59 o 7 6 10 250.98 209.92 43.39 o 8 6 10 376.31 317.93 44.96 o 9 6 10 166.37 165.63 45.29 o 10 6 10 28.02 55.08 37.19 o 11 6 10 165.83 299.82 57.67 o 12 6 10 551.06 472.40 67.14 o 13 6 10 309.94 350.29 79.50 o 1 7 10 325.05 319.87 50.29 o 2 7 10 347.42 316.70 47.24 o 3 7 10 2276.07 2391.86 88.17 o 4 7 10 820.19 840.48 66.83 o 5 7 10 126.74 142.99 75.21 o 6 7 10 17.93 -2.58 41.63 o 7 7 10 1733.33 1613.53 75.25 o 8 7 10 728.49 692.80 61.14 o 9 7 10 304.06 335.32 59.10 o 10 7 10 127.19 187.86 62.19 o 0 8 10 516.45 526.01 115.24 o 1 8 10 1530.20 1518.91 187.84 o 2 8 10 218.48 225.46 64.77 o 3 8 10 44.47 -45.93 54.95 o 4 8 10 220.39 303.59 64.32 o 5 8 10 1712.29 2122.07 160.94 o 1 1 11 547.58 545.02 16.72 o 2 1 11 5646.58 5209.47 61.11 o 3 1 11 10.15 -9.49 10.17 o 4 1 11 208.23 157.42 12.10 o 5 1 11 30.62 27.04 10.95 o 6 1 11 621.78 629.56 20.86 o 7 1 11 412.91 446.67 20.66 o 8 1 11 651.81 668.84 25.55 o 9 1 11 360.09 317.94 23.18 o 10 1 11 208.57 225.84 24.65 o 11 1 11 425.99 441.84 35.29 o 12 1 11 207.46 171.08 32.80 o 13 1 11 43.14 81.80 39.37 o 14 1 11 207.00 223.60 50.44 o 15 1 11 174.03 214.11 80.54 o 16 1 11 8.02 5.92 83.05 o 17 1 11 161.97 196.69 100.84 o 18 1 11 5.57 -140.29 155.39 o 0 2 11 30327.77 29222.20 390.21 o 1 2 11 293.99 299.09 13.04 o 2 2 11 4828.00 4761.23 53.41 o 3 2 11 781.36 908.60 21.82 o 4 2 11 11366.45 11636.68 119.10 o 5 2 11 2077.66 2132.44 34.31 o 6 2 11 13331.79 12870.25 133.81 o 7 2 11 1207.70 1249.04 30.05 o 8 2 11 36.91 35.76 17.93 o 9 2 11 279.47 261.43 23.21 o 10 2 11 5732.32 5624.01 90.77 o 11 2 11 191.37 211.94 32.70 o 12 2 11 1880.27 1789.55 61.01 o 13 2 11 255.91 197.20 42.40 o 14 2 11 284.90 211.21 47.92 o 15 2 11 20.57 -7.78 53.35 o 16 2 11 475.98 547.78 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206.05 39.66 o 2 3 28 6724.87 6283.97 123.79 o 3 3 28 425.78 403.71 44.57 o 4 3 28 1466.01 1495.16 62.27 o 5 3 28 47.58 40.53 37.38 o 6 3 28 708.57 534.29 49.65 o 7 3 28 56.97 26.44 41.29 o 8 3 28 1612.31 1700.19 75.07 o 9 3 28 1.38 61.51 47.58 o 10 3 28 262.00 267.00 58.04 o 11 3 28 208.99 242.13 66.82 o 12 3 28 217.34 166.44 77.71 o 13 3 28 2.21 40.08 71.13 o 14 3 28 212.82 365.12 87.07 o 0 4 28 1220.66 1165.88 86.60 o 1 4 28 497.96 498.85 48.69 o 2 4 28 214.37 90.25 40.86 o 3 4 28 332.78 292.01 45.95 o 4 4 28 396.98 215.90 47.24 o 5 4 28 379.25 302.28 57.39 o 6 4 28 739.95 595.13 57.79 o 7 4 28 166.32 79.86 50.19 o 8 4 28 42.25 -0.62 45.38 o 9 4 28 81.71 100.83 53.34 o 10 4 28 310.31 186.09 57.33 o 11 4 28 62.17 80.22 59.89 o 12 4 28 247.97 289.90 67.43 o 1 5 28 72.23 54.83 46.68 o 2 5 28 112.39 100.88 48.42 o 3 5 28 57.54 112.28 52.50 o 4 5 28 14.10 -25.73 50.88 o 5 5 28 1.19 -46.05 58.32 o 6 5 28 0.29 2.98 55.43 o 7 5 28 1.30 40.92 53.42 o 8 5 28 40.56 41.98 53.28 o 9 5 28 60.41 23.22 58.85 o 10 5 28 62.23 82.65 60.62 o 0 6 28 192.45 258.80 89.87 o 1 6 28 21.72 82.31 59.82 o 2 6 28 252.98 260.56 60.08 o 3 6 28 230.08 178.97 61.00 o 4 6 28 60.01 -0.31 59.19 o 5 6 28 39.94 42.48 56.25 o 6 6 28 949.35 987.41 96.14 o 7 6 28 229.67 205.80 72.31 o 1 1 29 453.22 410.28 34.52 o 2 1 29 406.01 357.93 34.80 o 3 1 29 2580.03 2639.23 73.82 o 4 1 29 8.27 31.01 33.14 o 5 1 29 173.61 147.83 36.44 o 6 1 29 34.61 55.48 34.96 o 7 1 29 1850.79 1949.52 68.39 o 8 1 29 124.23 157.53 41.15 o 9 1 29 587.08 402.73 58.29 o 10 1 29 155.38 88.84 53.14 o 11 1 29 167.08 160.03 68.08 o 12 1 29 124.70 102.10 85.95 o 13 1 29 277.26 209.84 107.69 o 14 1 29 9.44 -4.25 115.01 o 15 1 29 33.88 179.01 157.56 o 0 2 29 1412.61 1184.79 70.64 o 1 2 29 6601.90 6214.97 107.62 o 2 2 29 214.81 191.69 34.13 o 3 2 29 735.07 670.18 42.85 o 4 2 29 446.50 357.00 39.06 o 5 2 29 5488.42 5407.75 104.36 o 6 2 29 702.88 713.01 49.29 o 7 2 29 1146.86 1061.00 60.15 o 8 2 29 44.04 34.55 48.87 o 9 2 29 631.05 364.71 58.46 o 10 2 29 302.33 218.72 63.47 o 11 2 29 2062.60 2086.02 99.24 o 12 2 29 134.92 89.42 68.35 o 13 2 29 151.46 71.64 77.14 o 14 2 29 103.50 -36.67 99.27 o 1 3 29 2309.10 2343.91 77.15 o 2 3 29 195.97 182.40 43.03 o 3 3 29 7911.30 7883.93 153.45 o 4 3 29 333.53 304.03 45.38 o 5 3 29 750.91 623.78 59.23 o 6 3 29 19.80 50.23 43.54 o 7 3 29 3190.05 3109.08 91.51 o 8 3 29 278.09 253.28 49.32 o 9 3 29 3527.99 3457.18 102.66 o 10 3 29 2.15 -8.26 55.99 o 11 3 29 4.88 55.72 63.15 o 12 3 29 16.26 -33.17 66.60 o 13 3 29 1179.51 1187.96 96.62 o 0 4 29 177.84 110.57 62.28 o 1 4 29 5647.67 5303.78 126.80 o 2 4 29 76.99 24.29 38.74 o 3 4 29 151.78 140.95 52.00 o 4 4 29 50.91 18.06 40.17 o 5 4 29 4676.53 4463.39 167.26 o 6 4 29 263.56 291.05 50.96 o 7 4 29 2741.34 2986.06 98.89 o 8 4 29 17.81 82.11 48.96 o 9 4 29 111.62 144.75 57.01 o 10 4 29 120.35 18.01 65.10 o 11 4 29 3314.90 3421.55 125.31 o 12 4 29 115.99 10.83 70.93 o 1 5 29 841.02 709.06 63.00 o 2 5 29 1665.48 1735.60 88.43 o 3 5 29 4884.08 4962.90 132.67 o 4 5 29 435.66 448.11 63.88 o 5 5 29 1158.35 1102.78 80.39 o 6 5 29 613.78 670.65 70.96 o 7 5 29 2098.28 2214.74 117.27 o 8 5 29 510.23 463.85 64.69 o 9 5 29 3101.46 2881.21 124.76 o 10 5 29 44.48 58.17 65.62 o 0 6 29 33.22 18.46 84.74 o 1 6 29 2883.10 2833.15 122.98 o 2 6 29 27.41 -10.97 59.29 o 3 6 29 46.82 3.10 61.23 o 4 6 29 21.18 6.17 59.60 o 5 6 29 2833.80 3155.42 118.82 o 6 6 29 175.83 112.89 69.87 o 0 0 30 8186.16 8619.88 248.87 o 1 0 30 229.21 237.85 39.29 o 2 0 30 1507.67 1599.27 73.35 o 3 0 30 1348.50 1452.06 68.67 o 4 0 30 1762.29 1879.35 77.45 o 5 0 30 279.02 281.20 52.57 o 6 0 30 6506.24 6562.46 194.65 o 7 0 30 533.21 555.68 81.30 o 8 0 30 1316.05 1396.86 132.94 o 9 0 30 759.53 635.58 101.95 o 10 0 30 2626.15 3028.27 223.90 o 11 0 30 19.71 -31.96 120.18 o 12 0 30 2558.19 2446.13 225.13 o 13 0 30 456.23 329.43 149.26 o 14 0 30 33.72 81.03 171.61 o 15 0 30 7.91 -6.57 215.87 o 1 1 30 1851.15 1810.52 65.67 o 2 1 30 14435.76 15240.52 209.92 o 3 1 30 1233.13 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