#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/30/2213006.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213006_Fobs loop_ _publ_author_name 'Chantrapromma, Suchada' 'Chanawanno, Kullapa' 'Fun, Hoong-Kun' _publ_section_title ; Bis[4-(4-hydroxystyryl)-1-methylpyridinium] triiodide iodide ; _journal_coeditor_code SJ2231 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1554 _journal_page_last o1556 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 121.106 _cell_angle_gamma 90.000 _cell_length_a 14.2337 _cell_length_b 10.5627 _cell_length_c 23.4193 _exptl_crystal_F_000 1752.00 _reflns_d_resolution_high 0.6196 _[local]_cod_data_source_file sj2231Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' zkc2m in P2(1)/c (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 813.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4223.59 15.27 7.33 o 2 0 0 849.43 533.48 37.44 o 3 0 0 40746.34 42521.81 831.45 o 4 0 0 337328.75 325705.63 9639.45 o 5 0 0 54187.41 56752.18 1064.20 o 6 0 0 1563.76 1330.28 99.56 o 7 0 0 33324.51 32014.96 612.28 o 8 0 0 4398.76 3626.61 123.70 o 9 0 0 23329.42 22673.38 407.63 o 10 0 0 54.06 222.36 36.02 o 11 0 0 1906.12 2018.16 105.28 o 12 0 0 351.76 349.81 37.83 o 13 0 0 58.49 109.26 23.69 o 14 0 0 44.77 110.78 26.23 o 15 0 0 548.53 422.64 54.95 o 16 0 0 2283.79 2271.18 102.54 o 17 0 0 1093.90 1035.61 68.59 o 18 0 0 33.35 58.54 32.17 o 19 0 0 24.69 96.05 36.07 o 1 1 0 1132.86 1017.13 55.23 o 2 1 0 3186.45 3259.06 50.83 o 3 1 0 31708.21 32867.18 620.38 o 4 1 0 0.22 242.05 99.82 o 5 1 0 17824.77 17719.56 307.57 o 6 1 0 61504.31 58291.89 832.76 o 7 1 0 19873.70 19010.95 349.43 o 8 1 0 5813.23 5719.06 133.40 o 9 1 0 551.09 542.97 33.77 o 10 1 0 86750.44 82783.73 767.70 o 11 1 0 791.62 902.11 38.75 o 12 1 0 1216.39 1452.58 39.51 o 13 1 0 1623.02 1586.53 42.98 o 14 1 0 25610.73 25873.59 235.26 o 15 1 0 9377.58 9548.96 129.75 o 16 1 0 318.80 444.91 32.18 o 17 1 0 2921.49 3073.46 71.83 o 18 1 0 824.92 891.56 50.81 o 19 1 0 3728.14 3992.54 95.52 o 0 2 0 349602.91 320092.03 5232.76 o 1 2 0 2180.36 2309.73 39.39 o 2 2 0 34.58 34.96 5.98 o 3 2 0 16709.42 17034.80 220.46 o 4 2 0 99838.82 101669.47 1247.74 o 5 2 0 19654.83 18884.41 215.63 o 6 2 0 19.44 44.69 10.83 o 7 2 0 17198.76 16529.83 213.56 o 8 2 0 4108.52 3778.53 73.77 o 9 2 0 7677.94 7404.68 106.38 o 10 2 0 0.02 74.27 17.65 o 11 2 0 3008.00 2860.71 57.12 o 12 2 0 193.00 268.32 22.75 o 13 2 0 41.38 56.03 15.48 o 14 2 0 1.54 55.38 17.46 o 15 2 0 161.89 194.94 26.34 o 16 2 0 987.68 994.87 52.10 o 17 2 0 402.12 272.79 31.72 o 18 2 0 113.55 116.14 24.43 o 19 2 0 13.71 57.11 23.83 o 1 3 0 6356.12 6653.58 101.12 o 2 3 0 3926.59 3958.73 72.56 o 3 3 0 9397.13 9343.74 141.21 o 4 3 0 1517.67 1581.33 49.69 o 5 3 0 293.24 339.83 23.00 o 6 3 0 7850.42 7679.40 118.10 o 7 3 0 2201.67 2271.09 60.72 o 8 3 0 2246.66 2280.34 50.34 o 9 3 0 20.31 75.75 15.71 o 10 3 0 8381.39 8474.38 111.37 o 11 3 0 194.56 196.87 22.15 o 12 3 0 1959.64 1798.77 62.14 o 13 3 0 459.82 466.46 30.42 o 14 3 0 4809.45 4758.86 85.70 o 15 3 0 794.28 843.41 53.85 o 16 3 0 3.23 14.67 18.79 o 17 3 0 879.09 923.68 55.63 o 18 3 0 240.56 187.88 29.80 o 19 3 0 230.23 291.92 33.73 o 0 4 0 6702.64 7529.13 180.03 o 1 4 0 399.60 540.01 28.97 o 2 4 0 5.13 -22.27 11.14 o 3 4 0 3148.85 3414.44 60.54 o 4 4 0 6.60 373.94 70.25 o 5 4 0 7474.64 7575.56 101.21 o 6 4 0 1217.22 1281.94 32.99 o 7 4 0 4781.49 4864.42 71.54 o 8 4 0 397.43 408.73 27.77 o 9 4 0 3671.35 3803.97 68.81 o 10 4 0 238.49 242.70 21.53 o 11 4 0 3827.68 3494.87 66.00 o 12 4 0 91.64 70.99 16.95 o 13 4 0 88.73 105.08 19.99 o 14 4 0 869.24 911.21 44.71 o 15 4 0 431.24 431.44 34.03 o 16 4 0 7.17 6.87 17.97 o 17 4 0 15.05 2.50 19.71 o 18 4 0 253.83 172.68 29.91 o 19 4 0 0.18 43.12 24.64 o 1 5 0 15531.33 16102.83 206.23 o 2 5 0 2567.77 2533.98 49.09 o 3 5 0 1.14 135.41 55.60 o 4 5 0 7847.37 7955.52 109.74 o 5 5 0 14340.48 13656.16 154.15 o 6 5 0 10586.95 10445.52 130.79 o 7 5 0 3300.64 3386.02 61.79 o 8 5 0 1246.44 1360.31 35.37 o 9 5 0 355.49 358.95 20.47 o 10 5 0 21009.51 20022.54 214.49 o 11 5 0 267.94 318.70 24.95 o 12 5 0 1.56 25.78 15.53 o 13 5 0 148.51 107.15 21.40 o 14 5 0 3754.82 3504.54 93.64 o 15 5 0 2362.57 2307.35 83.76 o 16 5 0 46.11 15.01 20.29 o 17 5 0 62.75 77.38 23.38 o 18 5 0 12.40 22.52 21.47 o 0 6 0 124936.47 123542.92 1963.08 o 1 6 0 6778.92 6579.13 96.70 o 2 6 0 76.71 47.46 11.38 o 3 6 0 875.88 943.81 38.35 o 4 6 0 53324.61 54053.82 518.83 o 5 6 0 39322.65 38567.86 424.42 o 6 6 0 242.57 337.17 26.48 o 7 6 0 489.32 536.34 27.36 o 8 6 0 981.79 890.18 31.80 o 9 6 0 16011.38 15362.70 161.05 o 10 6 0 440.37 488.49 29.30 o 11 6 0 264.61 247.73 24.54 o 12 6 0 2353.38 2302.35 58.48 o 13 6 0 221.74 185.97 25.34 o 14 6 0 1030.80 1078.57 58.92 o 15 6 0 1405.56 1396.31 54.24 o 16 6 0 260.58 244.97 29.61 o 17 6 0 281.85 242.41 29.30 o 18 6 0 145.31 85.33 23.14 o 1 7 0 7851.78 8182.64 118.39 o 2 7 0 94.38 120.60 16.05 o 3 7 0 3066.72 3029.57 56.80 o 4 7 0 60.49 87.84 12.55 o 5 7 0 22604.98 21666.26 220.06 o 6 7 0 20786.62 19960.91 199.92 o 7 7 0 3903.14 3931.80 63.18 o 8 7 0 3.39 10.18 12.02 o 9 7 0 2284.79 2373.23 51.68 o 10 7 0 34532.49 33135.93 316.79 o 11 7 0 453.51 505.97 32.64 o 12 7 0 95.17 102.62 20.91 o 13 7 0 559.59 474.28 36.38 o 14 7 0 12715.42 12487.61 181.15 o 15 7 0 4512.74 4491.54 92.55 o 16 7 0 16.27 5.18 21.23 o 17 7 0 936.88 1077.86 51.13 o 0 8 0 102360.59 104371.38 1429.61 o 1 8 0 5160.77 5183.95 71.18 o 2 8 0 339.94 306.99 21.83 o 3 8 0 7825.67 7985.30 93.73 o 4 8 0 37387.04 36694.58 322.35 o 5 8 0 13934.85 13787.51 144.78 o 6 8 0 390.03 560.61 27.30 o 7 8 0 7838.05 7225.85 98.84 o 8 8 0 2734.02 2619.05 53.02 o 9 8 0 5371.25 5329.30 83.18 o 10 8 0 268.84 344.23 26.47 o 11 8 0 875.41 790.60 41.01 o 12 8 0 36.93 25.58 19.25 o 13 8 0 3.90 41.84 21.51 o 14 8 0 0.18 51.20 23.57 o 15 8 0 282.09 287.65 31.80 o 16 8 0 631.43 521.59 42.91 o 17 8 0 212.40 239.06 32.52 o 1 9 0 21.91 58.42 13.60 o 2 9 0 87.89 108.31 14.77 o 3 9 0 2735.76 3027.93 55.46 o 4 9 0 2360.14 2633.30 50.59 o 5 9 0 2503.74 2616.53 51.91 o 6 9 0 10744.52 10530.56 117.75 o 7 9 0 1734.28 1730.78 44.17 o 8 9 0 1435.11 1514.81 44.09 o 9 9 0 1293.07 1347.81 58.38 o 10 9 0 14316.82 13872.86 228.77 o 11 9 0 582.70 546.48 33.19 o 12 9 0 10.66 -5.92 18.21 o 13 9 0 73.85 83.65 24.80 o 14 9 0 6880.80 7165.49 133.26 o 15 9 0 819.01 969.36 58.35 o 16 9 0 0.97 -12.66 21.26 o 0 10 0 11239.55 12236.87 207.32 o 1 10 0 503.31 576.96 28.54 o 2 10 0 376.14 327.87 25.55 o 3 10 0 1128.03 1229.73 39.92 o 4 10 0 4473.93 4527.09 76.85 o 5 10 0 48.95 140.19 18.27 o 6 10 0 1728.63 1703.87 42.59 o 7 10 0 5280.03 4974.96 76.42 o 8 10 0 1374.69 1568.01 46.35 o 9 10 0 376.79 401.95 28.43 o 10 10 0 0.86 56.47 21.67 o 11 10 0 3828.35 4138.86 83.85 o 12 10 0 30.57 20.98 21.85 o 13 10 0 371.49 375.39 38.11 o 14 10 0 1160.14 1028.50 55.39 o 15 10 0 193.44 213.53 32.04 o 1 11 0 8841.26 8982.90 138.78 o 2 11 0 2283.07 2166.72 56.98 o 3 11 0 3090.92 3209.97 66.68 o 4 11 0 4049.92 4200.51 79.19 o 5 11 0 3364.82 3698.35 74.02 o 6 11 0 470.64 519.10 30.38 o 7 11 0 253.48 207.50 21.62 o 8 11 0 3535.11 3125.40 66.62 o 9 11 0 21.84 77.17 25.26 o 10 11 0 10.86 117.39 25.65 o 11 11 0 28.24 48.10 20.82 o 12 11 0 75.76 91.27 25.39 o 13 11 0 2.15 22.80 23.63 o 14 11 0 40.52 119.30 37.48 o 15 11 0 39.04 80.78 31.19 o 0 12 0 2974.13 3272.43 105.42 o 1 12 0 1254.73 1413.42 54.53 o 2 12 0 517.82 433.35 37.09 o 3 12 0 16.40 47.06 19.90 o 4 12 0 557.24 616.95 37.91 o 5 12 0 5563.13 5620.41 102.59 o 6 12 0 441.64 348.02 32.12 o 7 12 0 1414.37 1519.88 53.75 o 8 12 0 398.95 300.09 30.60 o 9 12 0 5465.47 5548.96 98.14 o 10 12 0 192.94 150.80 26.62 o 11 12 0 2440.13 2363.27 65.45 o 12 12 0 591.72 447.09 40.13 o 13 12 0 536.80 433.84 42.54 o 1 13 0 8685.00 8785.98 155.01 o 2 13 0 504.25 374.65 43.11 o 3 13 0 1396.84 1300.66 67.40 o 4 13 0 2004.31 1735.23 77.02 o 5 13 0 7532.49 7917.43 139.74 o 6 13 0 1347.23 1144.15 55.20 o 7 13 0 101.10 57.97 33.68 o 8 13 0 608.11 589.72 43.40 o 9 13 0 1764.64 1742.21 65.47 o 10 13 0 2875.09 2648.56 77.57 o 11 13 0 53.10 111.08 27.52 o 12 13 0 0.22 27.52 27.43 o 0 14 0 5939.52 4939.45 219.72 o 1 14 0 2037.08 1707.96 86.32 o 2 14 0 0.30 55.14 37.45 o 3 14 0 6.71 15.98 31.09 o 4 14 0 2340.28 2408.69 88.45 o 5 14 0 5613.63 5504.86 134.43 o 6 14 0 0.58 45.22 27.78 o 7 14 0 133.33 161.41 34.56 o 8 14 0 3.55 52.20 34.02 o 9 14 0 3639.82 3804.80 105.10 o 10 14 0 109.19 57.33 30.71 o 11 14 0 474.05 393.40 44.20 o 1 15 0 889.01 784.49 75.21 o 2 15 0 135.60 135.68 46.72 o 3 15 0 30.91 -5.64 40.50 o 4 15 0 8.41 99.77 52.10 o 5 15 0 2679.35 3364.25 149.85 o 6 15 0 891.22 634.64 61.76 o 7 15 0 1.72 14.19 32.90 o 8 15 0 11.44 32.17 39.07 o 9 15 0 1716.94 1718.32 88.31 o 0 16 0 2349.06 1824.74 219.85 o 1 16 0 1106.20 780.95 123.67 o 2 16 0 257.02 256.21 66.77 o 3 16 0 47.93 39.02 52.69 o 4 16 0 924.68 869.29 136.67 o 5 16 0 943.94 954.09 97.08 o 6 16 0 645.52 668.15 134.89 o 1 17 0 552.71 777.76 113.22 o -19 1 1 305.43 264.13 34.47 o -18 1 1 90.47 53.24 24.10 o -17 1 1 779.16 796.82 41.43 o -16 1 1 761.12 783.14 40.48 o -15 1 1 141.83 177.52 23.33 o -14 1 1 3082.39 2856.50 56.77 o -13 1 1 408.18 424.08 24.49 o -12 1 1 13.90 13.81 12.39 o -11 1 1 163.67 88.16 15.91 o -10 1 1 11243.22 10993.95 147.69 o -9 1 1 4380.00 4209.81 79.88 o -8 1 1 3354.50 3459.12 80.12 o -7 1 1 139.70 150.80 28.07 o -6 1 1 6478.67 6630.84 108.18 o -5 1 1 19041.05 18860.04 213.08 o -4 1 1 17260.88 19436.88 372.41 o -3 1 1 93.95 52.70 9.87 o -2 1 1 366.93 414.15 12.47 o -1 1 1 809.42 794.12 60.12 o 0 1 1 2852.00 3906.24 73.62 o 1 1 1 17.12 29.62 4.60 o 2 1 1 186.22 226.36 13.01 o 3 1 1 9007.12 9222.79 184.32 o 4 1 1 8801.64 8779.43 240.82 o 5 1 1 1840.85 1873.70 47.42 o 6 1 1 8119.46 8510.06 130.38 o 7 1 1 5661.52 5496.42 106.87 o 8 1 1 1456.15 1464.61 67.02 o 9 1 1 1242.94 1223.16 42.23 o 10 1 1 7126.67 7650.78 115.92 o 11 1 1 5.69 27.27 13.34 o 12 1 1 711.45 703.90 30.30 o 13 1 1 952.20 889.16 36.07 o 14 1 1 1342.58 1513.43 48.75 o 15 1 1 1317.93 1499.02 59.96 o 16 1 1 0.94 28.20 19.17 o 17 1 1 63.87 65.85 21.57 o 18 1 1 60.09 82.07 26.92 o 19 1 1 360.48 343.60 35.51 o -19 2 1 1584.09 1604.35 69.07 o -18 2 1 121.15 79.69 27.30 o -17 2 1 133.80 148.28 28.23 o -16 2 1 49.58 85.84 23.10 o -15 2 1 4540.56 4278.77 88.31 o -14 2 1 5733.85 5682.17 92.49 o -13 2 1 549.02 624.96 30.38 o -12 2 1 157.62 83.62 16.99 o -11 2 1 3.99 31.64 14.27 o -10 2 1 24764.96 23215.24 265.08 o -9 2 1 6026.03 5844.01 90.01 o -8 2 1 193.89 175.32 29.86 o -7 2 1 24139.58 23748.52 271.93 o -6 2 1 21010.77 20932.28 229.00 o -5 2 1 2114.04 2182.76 42.10 o -4 2 1 51757.77 52915.20 635.72 o -3 2 1 28038.33 29131.76 335.65 o -2 2 1 372.31 416.20 15.68 o -1 2 1 252.40 325.02 13.65 o 0 2 1 128016.17 131219.39 1622.15 o 1 2 1 19378.90 20776.59 239.98 o 2 2 1 258.77 313.88 13.81 o 3 2 1 1524.12 1551.00 40.74 o 4 2 1 35031.08 34393.51 484.53 o 5 2 1 71443.78 71540.97 808.62 o 6 2 1 15175.34 14862.22 191.89 o 7 2 1 1239.61 1261.97 54.94 o 8 2 1 4.01 20.47 11.40 o 9 2 1 13696.10 12855.64 164.60 o 10 2 1 28302.75 27056.82 286.35 o 11 2 1 590.13 569.58 29.24 o 12 2 1 137.12 84.06 14.85 o 13 2 1 64.72 47.37 15.35 o 14 2 1 11631.17 11211.77 134.30 o 15 2 1 2246.91 2288.12 60.25 o 16 2 1 539.06 557.37 40.77 o 17 2 1 1087.01 1074.75 56.05 o 18 2 1 378.64 303.88 32.01 o 19 2 1 1066.63 1182.29 57.87 o -19 3 1 1289.01 1264.70 60.26 o -18 3 1 357.41 263.92 29.99 o -17 3 1 3051.23 3163.19 89.69 o -16 3 1 1643.71 1493.42 67.32 o -15 3 1 2017.32 2009.23 64.67 o -14 3 1 11295.76 11313.99 138.61 o -13 3 1 1214.70 1268.72 46.57 o -12 3 1 94.94 142.94 25.00 o -11 3 1 887.82 846.15 33.99 o -10 3 1 49251.16 48265.18 473.28 o -9 3 1 22994.78 22730.84 244.60 o -8 3 1 5439.65 5899.90 91.67 o -7 3 1 36.46 75.19 14.49 o -6 3 1 28699.55 29305.55 345.15 o -5 3 1 93599.55 92311.51 946.54 o -4 3 1 65459.01 66445.23 918.20 o -3 3 1 2431.81 2540.76 59.24 o -2 3 1 112.52 132.15 17.61 o -1 3 1 26570.81 27468.05 383.90 o 0 3 1 284153.75 277824.88 3709.37 o 1 3 1 206.20 291.30 17.02 o 2 3 1 919.45 1034.01 37.72 o 3 3 1 28938.84 29934.43 309.50 o 4 3 1 76921.22 77279.53 797.39 o 5 3 1 3177.43 3175.18 72.44 o 6 3 1 25186.94 24331.36 289.72 o 7 3 1 28614.77 27245.16 287.00 o 8 3 1 301.33 284.74 21.72 o 9 3 1 4071.12 3821.75 72.54 o 10 3 1 31212.87 30130.25 291.50 o 11 3 1 56.99 77.80 17.20 o 12 3 1 6639.59 6182.67 94.15 o 13 3 1 2669.63 2545.48 55.22 o 14 3 1 7833.34 7524.72 113.96 o 15 3 1 6271.53 6227.68 104.24 o 16 3 1 82.79 68.72 21.17 o 17 3 1 239.06 220.05 28.83 o 18 3 1 304.33 234.79 32.43 o 19 3 1 2149.91 2324.60 76.90 o -19 4 1 2291.10 2299.40 81.57 o -18 4 1 817.68 912.05 49.56 o -17 4 1 210.56 178.68 34.68 o -16 4 1 155.63 105.59 22.04 o -15 4 1 5066.88 4992.29 102.85 o -14 4 1 11271.60 11286.82 153.92 o -13 4 1 435.53 466.13 29.59 o -12 4 1 25.67 31.24 14.11 o -11 4 1 2.45 23.81 15.22 o -10 4 1 38005.68 37416.50 346.51 o -9 4 1 2738.99 2850.39 56.48 o -8 4 1 2303.70 2182.98 42.13 o -7 4 1 44849.82 44216.04 404.90 o -6 4 1 35394.57 35776.52 406.47 o -5 4 1 2991.42 3178.79 60.18 o -4 4 1 82746.70 84112.24 895.16 o -3 4 1 49939.42 50535.64 639.25 o -2 4 1 1120.83 1198.34 34.80 o -1 4 1 3.64 32.31 10.01 o 0 4 1 141555.66 142124.41 1905.65 o 1 4 1 3263.70 3097.82 66.45 o 2 4 1 2157.46 2095.82 42.80 o 3 4 1 25.96 45.42 10.70 o 4 4 1 125816.24 127433.90 1225.64 o 5 4 1 57684.50 56962.32 594.77 o 6 4 1 23796.02 23061.66 255.76 o 7 4 1 1583.59 1558.18 39.08 o 8 4 1 9219.30 9140.11 115.25 o 9 4 1 10075.85 9817.24 119.62 o 10 4 1 32360.55 31527.60 292.22 o 11 4 1 4096.38 3836.64 73.06 o 12 4 1 10.57 1.24 13.91 o 13 4 1 676.17 745.84 37.41 o 14 4 1 12694.03 12599.79 169.26 o 15 4 1 2758.09 2746.52 70.90 o 16 4 1 857.53 793.44 50.50 o 17 4 1 2210.49 2092.81 71.16 o 18 4 1 391.03 322.08 34.57 o -19 5 1 630.56 689.75 61.21 o -18 5 1 88.18 67.85 23.48 o -17 5 1 2154.48 2281.48 82.94 o -16 5 1 652.54 587.19 38.19 o -15 5 1 2228.09 2168.13 70.02 o -14 5 1 6104.22 6075.60 111.70 o -13 5 1 966.96 1038.56 43.27 o -12 5 1 1648.10 1630.99 49.72 o -11 5 1 2636.25 2712.41 58.29 o -10 5 1 29724.38 28675.59 269.38 o -9 5 1 10871.79 10400.93 122.17 o -8 5 1 7163.37 7371.54 96.69 o -7 5 1 1526.76 1481.09 37.36 o -6 5 1 23055.96 23440.53 255.82 o -5 5 1 31311.21 31537.06 345.03 o -4 5 1 31722.04 30910.26 386.97 o -3 5 1 352.41 406.36 20.05 o -2 5 1 1008.05 1046.76 29.20 o -1 5 1 3011.33 3493.15 62.82 o 0 5 1 128316.84 134394.66 1502.14 o 1 5 1 1020.10 1040.41 31.74 o 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