#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2213037.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213037_Fobs loop_ _publ_author_name 'Reddy, Pattubala A. N.' 'Md, Nasiruzzaman Sk.' 'Kim, Tae-Jeong' _publ_section_title ; 2,6-Bis({rac-1-[2-(diphenylphosphino)ferrocenyl]ethyl}aminocarbonyl)pyridine ; _journal_coeditor_code TK2134 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m971 _journal_page_last m972 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.503 _cell_angle_gamma 90.000 _cell_length_a 13.0367 _cell_length_b 18.1046 _cell_length_c 19.9474 _exptl_crystal_F_000 1992.00 _reflns_d_resolution_high 0.7494 _[local]_cod_data_source_file tk2134Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' knu1 in P 21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 333.66 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 11423.94 13281.47 208.20 o 4 0 0 458.04 571.79 26.75 o 6 0 0 102.47 261.79 26.69 o 8 0 0 14486.14 14000.81 180.02 o 10 0 0 3173.94 3005.02 93.13 o 12 0 0 68.81 -2.96 90.91 o 14 0 0 863.15 908.96 104.72 o 16 0 0 174.88 130.60 255.73 o 1 1 0 278.29 327.36 6.76 o 2 1 0 33589.03 34585.97 329.81 o 3 1 0 11507.10 12756.08 131.64 o 4 1 0 12695.46 13438.29 128.32 o 5 1 0 420.31 549.07 20.41 o 6 1 0 10006.98 9573.40 89.25 o 7 1 0 1145.76 1023.90 30.02 o 8 1 0 782.82 900.40 31.34 o 9 1 0 2436.23 2646.60 51.50 o 10 1 0 1476.12 1473.88 58.36 o 11 1 0 505.58 535.93 46.81 o 12 1 0 1422.04 1329.23 78.73 o 13 1 0 635.86 585.09 60.74 o 14 1 0 478.46 344.86 62.86 o 15 1 0 1746.16 1893.59 95.10 o 16 1 0 131.23 25.55 85.10 o 17 1 0 3.83 104.41 159.54 o 0 2 0 14094.82 17143.71 215.29 o 1 2 0 10213.35 11965.38 132.11 o 2 2 0 57.47 129.70 9.64 o 3 2 0 36970.80 41965.77 366.25 o 4 2 0 18.04 40.09 14.38 o 5 2 0 29.58 -3.66 11.87 o 6 2 0 37.15 89.21 17.42 o 7 2 0 345.41 385.40 24.58 o 8 2 0 14.78 35.92 22.43 o 9 2 0 7683.12 7257.28 98.04 o 10 2 0 4371.11 4134.83 126.87 o 11 2 0 820.66 905.34 53.55 o 12 2 0 71.75 30.58 45.59 o 13 2 0 2805.79 2607.97 90.29 o 14 2 0 8.07 -11.56 54.22 o 15 2 0 1.44 -28.53 71.02 o 16 2 0 3.95 -68.95 77.44 o 17 2 0 753.85 916.06 133.45 o 1 3 0 2358.43 3000.69 105.92 o 2 3 0 5940.90 6793.99 67.98 o 3 3 0 2594.48 2745.03 37.97 o 4 3 0 9645.20 10673.12 106.93 o 5 3 0 8803.13 9306.62 99.05 o 6 3 0 20307.60 20910.38 185.45 o 7 3 0 2639.94 2600.46 49.90 o 8 3 0 121.93 151.65 28.09 o 9 3 0 2444.65 2252.88 61.11 o 10 3 0 254.77 254.58 35.06 o 11 3 0 345.40 371.73 45.51 o 12 3 0 1.35 -43.69 43.69 o 13 3 0 238.75 210.92 67.12 o 14 3 0 1548.38 1798.51 120.87 o 15 3 0 153.40 137.74 78.94 o 16 3 0 328.92 295.83 89.56 o 17 3 0 5.22 39.89 172.44 o 0 4 0 52062.63 53963.12 712.75 o 1 4 0 33611.79 34635.96 331.81 o 2 4 0 6697.67 7477.83 115.96 o 3 4 0 9119.41 9127.45 91.60 o 4 4 0 1201.36 1049.80 28.16 o 5 4 0 0.94 13.38 17.57 o 6 4 0 4689.33 5167.52 75.92 o 7 4 0 17447.66 16617.68 156.37 o 8 4 0 7292.77 6965.14 84.88 o 9 4 0 1482.58 1366.94 47.78 o 10 4 0 881.43 964.29 44.90 o 11 4 0 1100.09 1004.43 123.87 o 12 4 0 837.10 943.40 66.12 o 13 4 0 524.34 483.66 72.82 o 14 4 0 1.82 89.57 72.16 o 15 4 0 1002.60 1045.75 128.73 o 16 4 0 790.30 885.11 103.94 o 1 5 0 49334.57 50345.96 478.18 o 2 5 0 770.51 709.76 22.51 o 3 5 0 10229.94 10923.50 107.80 o 4 5 0 3702.68 3730.84 50.12 o 5 5 0 18394.79 18886.39 195.42 o 6 5 0 928.71 765.75 30.42 o 7 5 0 5143.10 4594.02 64.30 o 8 5 0 487.53 420.48 32.41 o 9 5 0 59.30 92.82 30.48 o 10 5 0 5.14 22.82 31.77 o 11 5 0 106.47 93.14 39.45 o 12 5 0 336.68 322.56 56.82 o 13 5 0 1.31 -56.72 56.72 o 14 5 0 311.38 217.15 74.24 o 15 5 0 0.11 -42.56 73.28 o 16 5 0 35.59 -17.38 82.91 o 0 6 0 2105.25 2362.77 49.15 o 1 6 0 391.53 291.42 23.87 o 2 6 0 18830.49 19708.46 256.73 o 3 6 0 264.78 330.64 17.50 o 4 6 0 540.65 813.26 26.71 o 5 6 0 14643.95 15131.72 149.91 o 6 6 0 22.84 113.33 22.54 o 7 6 0 1524.20 1373.66 39.47 o 8 6 0 1112.95 1100.20 42.69 o 9 6 0 39.92 44.11 30.83 o 10 6 0 354.85 484.29 52.46 o 11 6 0 354.55 364.86 42.58 o 12 6 0 642.13 697.78 64.12 o 13 6 0 286.49 272.35 57.70 o 14 6 0 49.71 -36.22 66.70 o 15 6 0 1.02 -67.05 74.58 o 16 6 0 297.22 389.22 120.50 o 1 7 0 89.99 60.70 13.95 o 2 7 0 428.33 565.13 20.25 o 3 7 0 3353.14 3670.97 67.96 o 4 7 0 773.65 775.15 26.44 o 5 7 0 3103.89 3376.72 51.35 o 6 7 0 1376.14 1516.46 40.09 o 7 7 0 7.28 -18.89 27.09 o 8 7 0 12.72 12.00 32.57 o 9 7 0 417.87 450.02 41.93 o 10 7 0 2715.76 2505.80 69.97 o 11 7 0 27.37 -19.82 35.96 o 12 7 0 995.77 1022.88 68.82 o 13 7 0 207.36 236.97 55.81 o 14 7 0 2584.71 2404.58 153.24 o 15 7 0 138.99 64.84 80.31 o 16 7 0 196.86 241.66 166.58 o 0 8 0 40.45 45.26 24.72 o 1 8 0 6044.00 6341.95 72.03 o 2 8 0 1070.79 1264.73 30.63 o 3 8 0 1182.57 1025.57 38.68 o 4 8 0 7286.87 8283.28 92.02 o 5 8 0 10737.90 10933.60 117.02 o 6 8 0 1677.12 1408.00 46.77 o 7 8 0 1343.62 1272.45 53.90 o 8 8 0 84.41 21.15 32.96 o 9 8 0 227.76 197.70 44.41 o 10 8 0 137.64 198.32 40.11 o 11 8 0 120.30 167.77 40.61 o 12 8 0 175.16 267.46 54.76 o 13 8 0 374.68 459.11 63.47 o 14 8 0 101.98 -87.28 87.28 o 15 8 0 391.39 314.12 85.56 o 1 9 0 8845.22 8263.01 90.61 o 2 9 0 1664.92 1573.81 45.07 o 3 9 0 38.51 135.65 24.91 o 4 9 0 57.89 71.37 24.65 o 5 9 0 5202.48 4942.48 90.36 o 6 9 0 293.69 281.43 33.89 o 7 9 0 171.38 219.09 38.88 o 8 9 0 1602.57 1581.49 62.66 o 9 9 0 3750.78 3325.70 88.10 o 10 9 0 66.69 28.24 36.57 o 11 9 0 442.33 384.14 45.30 o 12 9 0 2.21 48.48 45.06 o 13 9 0 254.59 118.26 58.82 o 14 9 0 516.60 483.04 82.89 o 15 9 0 35.08 -97.80 97.80 o 0 10 0 6.40 17.08 24.30 o 1 10 0 3647.85 3473.74 51.57 o 2 10 0 1670.69 1797.51 37.46 o 3 10 0 20.69 108.47 24.01 o 4 10 0 2633.74 2439.83 61.70 o 5 10 0 1020.21 1036.22 48.40 o 6 10 0 624.60 693.36 40.57 o 7 10 0 1170.18 1222.64 51.97 o 8 10 0 512.73 624.15 45.94 o 9 10 0 194.68 154.29 39.20 o 10 10 0 237.54 241.98 44.35 o 11 10 0 3577.60 3201.68 82.87 o 12 10 0 504.46 603.05 56.45 o 13 10 0 112.62 60.82 58.25 o 14 10 0 84.14 44.05 62.92 o 1 11 0 234.16 227.58 23.08 o 2 11 0 9021.28 9169.30 116.79 o 3 11 0 9.94 19.96 25.37 o 4 11 0 3289.00 3282.51 85.99 o 5 11 0 1961.70 2033.34 55.44 o 6 11 0 481.80 502.35 39.76 o 7 11 0 142.75 179.35 38.68 o 8 11 0 2848.63 2641.00 70.32 o 9 11 0 10.38 -6.20 35.96 o 10 11 0 460.16 634.33 51.52 o 11 11 0 435.62 467.91 53.32 o 12 11 0 15.12 -37.22 45.83 o 13 11 0 120.24 191.60 65.80 o 14 11 0 27.84 50.58 76.80 o 0 12 0 1702.06 1754.43 59.21 o 1 12 0 2093.27 2157.40 52.18 o 2 12 0 279.89 336.40 31.89 o 3 12 0 374.24 477.13 40.72 o 4 12 0 131.79 102.85 29.13 o 5 12 0 2113.25 1918.13 57.15 o 6 12 0 89.98 119.70 37.47 o 7 12 0 769.88 767.00 49.04 o 8 12 0 0.18 9.64 34.80 o 9 12 0 8.35 5.23 39.34 o 10 12 0 1175.74 1171.61 61.33 o 11 12 0 0.21 6.04 49.69 o 12 12 0 200.60 220.07 57.79 o 13 12 0 1853.49 1902.04 111.00 o 14 12 0 26.57 -14.72 98.18 o 1 13 0 845.87 860.96 41.43 o 2 13 0 4271.01 4113.14 74.93 o 3 13 0 211.01 211.19 31.00 o 4 13 0 217.54 239.47 39.24 o 5 13 0 2532.97 2348.43 72.00 o 6 13 0 3811.11 3682.82 71.79 o 7 13 0 216.10 235.70 72.84 o 8 13 0 1586.96 1424.41 61.15 o 9 13 0 353.06 313.44 50.70 o 10 13 0 101.98 82.31 45.05 o 11 13 0 628.59 882.86 91.01 o 12 13 0 234.73 214.79 71.11 o 13 13 0 12.58 114.30 77.46 o 0 14 0 11059.53 9870.68 210.57 o 1 14 0 184.20 246.27 38.91 o 2 14 0 229.07 317.10 36.18 o 3 14 0 154.11 148.30 35.14 o 4 14 0 10156.30 9572.38 132.51 o 5 14 0 138.81 132.97 34.53 o 6 14 0 1009.85 1153.16 54.39 o 7 14 0 178.33 230.43 40.68 o 8 14 0 141.85 188.99 43.46 o 9 14 0 178.29 121.47 44.03 o 10 14 0 121.80 1.44 43.69 o 11 14 0 216.04 183.32 59.43 o 12 14 0 103.03 -34.27 81.18 o 13 14 0 0.17 -3.11 92.53 o 1 15 0 311.20 338.22 43.00 o 2 15 0 3550.29 3372.67 82.54 o 3 15 0 363.35 335.69 44.22 o 4 15 0 135.87 159.92 41.47 o 5 15 0 1323.20 1208.47 61.85 o 6 15 0 3126.18 2935.42 76.06 o 7 15 0 311.71 237.68 52.25 o 8 15 0 301.59 338.77 48.09 o 9 15 0 93.24 117.30 46.77 o 10 15 0 41.30 20.48 52.65 o 11 15 0 228.46 224.48 72.81 o 12 15 0 355.74 535.29 87.30 o 13 15 0 3.20 111.44 112.62 o 0 16 0 41.88 -4.45 52.18 o 1 16 0 27.67 68.69 38.59 o 2 16 0 544.44 656.73 50.69 o 3 16 0 1.36 -33.85 33.85 o 4 16 0 2178.79 1957.26 57.42 o 5 16 0 1695.03 1834.21 78.27 o 6 16 0 3875.06 3739.79 85.78 o 7 16 0 281.72 328.92 47.54 o 8 16 0 1.97 -40.87 40.87 o 9 16 0 1195.15 1323.59 102.26 o 10 16 0 31.66 101.29 67.90 o 11 16 0 30.80 -36.57 59.31 o 12 16 0 100.74 44.72 80.22 o 1 17 0 515.41 602.08 51.73 o 2 17 0 1378.78 1306.50 62.33 o 3 17 0 574.01 679.58 56.08 o 4 17 0 135.19 53.55 44.36 o 5 17 0 215.05 270.14 56.97 o 6 17 0 74.04 2.49 40.51 o 7 17 0 59.22 78.96 46.42 o 8 17 0 31.42 58.22 46.95 o 9 17 0 588.81 600.62 65.19 o 10 17 0 954.76 1007.89 77.91 o 11 17 0 388.33 349.58 69.64 o 12 17 0 113.86 299.14 126.69 o 0 18 0 1108.39 1175.78 92.06 o 1 18 0 175.23 131.16 44.13 o 2 18 0 415.93 493.61 53.06 o 3 18 0 650.44 576.93 57.26 o 4 18 0 195.84 96.22 57.39 o 5 18 0 49.07 -60.55 60.55 o 6 18 0 905.96 961.67 92.29 o 7 18 0 361.75 500.34 61.41 o 8 18 0 663.17 839.90 70.62 o 9 18 0 198.62 295.41 78.06 o 10 18 0 313.09 313.13 94.12 o 11 18 0 39.05 -53.96 91.25 o 1 19 0 1305.21 1340.31 69.76 o 2 19 0 1287.83 1337.76 71.28 o 3 19 0 1862.60 1897.48 77.05 o 4 19 0 1.21 -19.64 47.06 o 5 19 0 530.99 532.51 66.79 o 6 19 0 157.68 213.69 105.58 o 7 19 0 188.87 115.33 77.56 o 8 19 0 308.60 355.37 90.00 o 9 19 0 8.77 78.56 61.84 o 10 19 0 574.68 893.26 115.26 o 0 20 0 1038.25 1135.98 96.88 o 1 20 0 673.96 863.34 66.55 o 2 20 0 130.24 111.81 51.50 o 3 20 0 128.36 55.14 50.28 o 4 20 0 0.22 -69.66 94.73 o 5 20 0 317.88 341.00 70.70 o 6 20 0 65.44 -79.06 79.06 o 7 20 0 9.14 -83.40 83.40 o 8 20 0 5.39 -81.53 81.53 o 1 21 0 0.04 -51.30 59.09 o 2 21 0 0.45 -42.05 51.07 o 3 21 0 0.00 59.45 54.82 o 4 21 0 33.49 -41.78 64.59 o 5 21 0 3.88 -97.95 97.95 o 6 21 0 189.52 190.71 95.30 o 7 21 0 0.83 -139.60 139.60 o 0 22 0 1.23 64.35 79.58 o 1 22 0 276.33 340.51 60.83 o 2 22 0 390.62 391.24 90.55 o 3 22 0 420.37 425.74 95.81 o 4 22 0 429.42 672.68 109.49 o 5 22 0 51.62 78.60 91.03 o 6 22 0 7.70 268.64 150.16 o 1 23 0 156.73 371.71 77.04 o 2 23 0 53.92 142.41 91.77 o 3 23 0 118.74 57.48 131.39 o 4 23 0 139.04 -133.73 133.73 o 0 24 0 284.12 740.22 141.94 o 1 24 0 23.61 68.61 87.27 o -15 0 1 1.92 -77.59 82.70 o -13 0 1 1653.14 1736.49 111.05 o -11 0 1 1098.00 1257.51 166.58 o -9 0 1 4450.03 4373.52 97.27 o -7 0 1 5147.92 5005.52 81.15 o -5 0 1 4962.47 5669.44 80.85 o -3 0 1 10317.92 10637.03 124.05 o -1 0 1 2.45 114.95 22.29 o 1 0 1 41049.57 45537.11 838.76 o 3 0 1 24708.34 28217.76 453.13 o 5 0 1 1326.83 1328.99 47.49 o 7 0 1 22473.12 22509.70 265.37 o 9 0 1 52.07 54.28 33.42 o 11 0 1 894.18 1004.71 71.75 o 13 0 1 1578.31 1612.23 127.87 o 15 0 1 224.95 293.29 93.48 o -17 1 1 467.43 442.26 160.71 o -16 1 1 22.77 -59.81 80.53 o -15 1 1 299.43 496.38 72.73 o -14 1 1 528.56 525.40 66.09 o -13 1 1 800.25 774.54 67.49 o -12 1 1 1457.74 1380.80 71.65 o -11 1 1 2410.72 2234.25 79.29 o -10 1 1 1520.28 1460.51 81.61 o -9 1 1 12528.10 11836.46 135.36 o -8 1 1 3786.50 3578.85 54.05 o -7 1 1 490.87 715.51 26.59 o -6 1 1 1992.55 1999.51 34.82 o -5 1 1 2577.96 2425.87 36.33 o -4 1 1 161.98 161.69 14.28 o -3 1 1 7.59 23.21 10.90 o -2 1 1 40876.85 45018.75 607.99 o -1 1 1 36106.11 35814.80 380.00 o 1 1 1 3356.07 3238.01 33.15 o 3 1 1 4.39 95.47 15.50 o 4 1 1 2187.69 2552.02 42.49 o 5 1 1 6373.09 7054.97 88.67 o 6 1 1 117.54 162.83 20.08 o 7 1 1 112.58 62.90 19.22 o 8 1 1 3249.05 2857.16 47.88 o 9 1 1 1017.55 1171.36 40.49 o 10 1 1 812.60 829.22 39.93 o 11 1 1 1203.97 1263.80 58.65 o 12 1 1 128.45 160.74 42.74 o 13 1 1 3.55 -14.77 50.41 o 14 1 1 77.92 -16.87 55.95 o 15 1 1 560.28 706.65 88.30 o 16 1 1 270.54 238.73 90.79 o 17 1 1 450.63 602.97 187.69 o -17 2 1 274.73 -138.42 138.42 o -16 2 1 11.66 -106.16 123.73 o -15 2 1 0.79 -67.00 67.00 o -14 2 1 20.79 80.63 57.32 o -13 2 1 216.77 165.88 80.09 o -12 2 1 2450.81 2232.12 81.28 o -11 2 1 443.95 609.78 56.05 o -10 2 1 1288.74 1451.19 77.18 o -9 2 1 280.48 293.13 32.68 o -8 2 1 211.37 206.77 23.76 o -7 2 1 7444.93 7350.86 80.66 o -6 2 1 2017.13 1886.24 35.56 o -5 2 1 27.68 21.42 14.86 o -3 2 1 21408.43 23100.37 207.34 o -2 2 1 111331.22 116559.73 924.01 o -1 2 1 675.72 969.89 13.81 o 0 2 1 19931.57 22848.17 219.81 o 1 2 1 441.82 492.81 16.93 o 2 2 1 35233.67 38132.69 365.19 o 3 2 1 33096.67 37641.68 330.39 o 4 2 1 35.85 82.32 14.72 o 5 2 1 1396.01 1409.51 45.57 o 6 2 1 1216.01 972.45 38.95 o 7 2 1 66.67 111.08 23.54 o 8 2 1 766.98 839.37 31.90 o 9 2 1 1580.32 1528.11 41.07 o 10 2 1 7294.26 6721.59 97.26 o 11 2 1 2661.49 2591.43 73.85 o 12 2 1 269.47 302.12 61.77 o 13 2 1 13.33 -16.47 45.55 o 14 2 1 84.78 97.24 67.32 o 15 2 1 189.00 291.12 81.43 o 16 2 1 1.96 15.25 82.56 o 17 2 1 1.06 -105.10 105.10 o -16 3 1 24.18 -15.83 83.62 o -15 3 1 1158.65 1150.01 98.36 o -14 3 1 53.06 -27.72 65.16 o -13 3 1 8.40 28.03 63.66 o -12 3 1 898.68 852.30 62.78 o -11 3 1 1590.42 1577.08 70.45 o -10 3 1 322.46 316.75 34.95 o -9 3 1 602.15 644.26 37.03 o -8 3 1 228.29 234.70 25.59 o -7 3 1 13984.67 13288.78 354.27 o -6 3 1 788.55 696.41 28.84 o -5 3 1 2203.51 2245.52 36.72 o -4 3 1 2040.27 2634.71 37.11 o -3 3 1 190.99 199.28 14.61 o -2 3 1 16649.61 17972.38 153.77 o -1 3 1 10314.16 11147.49 102.56 o 0 3 1 8351.86 10321.66 94.72 o 1 3 1 43500.64 44787.27 475.04 o 3 3 1 17571.70 18781.66 171.61 o 4 3 1 9267.81 8529.38 82.08 o 5 3 1 6738.02 6483.48 69.53 o 6 3 1 1954.67 2117.69 39.85 o 7 3 1 4107.81 3993.11 57.16 o 8 3 1 6558.63 5997.61 94.50 o 9 3 1 1434.20 1393.48 49.11 o 10 3 1 256.02 271.11 35.11 o 11 3 1 31.73 27.10 38.96 o 12 3 1 1419.06 1350.02 63.51 o 13 3 1 2296.67 2228.27 87.04 o 14 3 1 1.19 -57.63 82.08 o 15 3 1 425.73 397.48 85.40 o 16 3 1 232.36 192.40 86.86 o -16 4 1 161.59 247.64 86.44 o -15 4 1 1768.05 1861.86 137.66 o -14 4 1 197.17 116.94 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