#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/31/2213114.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213114_Fobs loop_ _publ_author_name 'Du, Zhi-Yun' 'Zhang, Kun' 'Ng, Seik Weng' _publ_section_title ; (2E,5E)-2,5-Bis(2,3,4-trimethoxybenzylidene)cyclopentanone ; _journal_coeditor_code BG2039 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2595 _journal_page_last o2596 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 108.089 _cell_angle_beta 95.412 _cell_angle_gamma 111.242 _cell_length_a 12.6636 _cell_length_b 15.4927 _cell_length_c 19.2967 _exptl_crystal_F_000 1404.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file bg2039Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 458.85 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 11526.35 11937.07 211.37 o 3 0 0 38883.34 39422.37 509.05 o 4 0 0 1643.56 1728.79 35.98 o 5 0 0 46.83 23.09 11.01 o 6 0 0 5707.03 5961.68 115.39 o 7 0 0 431.23 436.64 25.13 o 8 0 0 350.29 312.48 66.13 o 9 0 0 25.07 14.41 21.00 o 10 0 0 254.75 186.06 41.68 o 11 0 0 281.28 354.32 114.30 o 12 0 0 30.67 -5.10 63.16 o 13 0 0 22.25 70.81 75.28 o -13 1 0 281.01 236.68 74.00 o -12 1 0 187.51 217.72 49.87 o -11 1 0 16.40 -23.92 30.81 o -10 1 0 58.92 24.67 23.84 o -9 1 0 114.51 54.96 22.05 o -8 1 0 45.01 -4.51 16.50 o -7 1 0 21.63 14.21 19.66 o -6 1 0 781.92 726.61 51.46 o -5 1 0 1696.18 1591.87 58.27 o -4 1 0 378.33 291.83 25.24 o -3 1 0 272.31 271.39 14.70 o -2 1 0 26235.82 24736.41 920.54 o -1 1 0 940.08 741.07 92.29 o 0 1 0 25.98 9.09 6.80 o 1 1 0 5521.72 5294.26 131.95 o 2 1 0 66039.60 66919.28 854.47 o 3 1 0 12239.96 12546.66 175.35 o 4 1 0 5919.05 6147.93 94.82 o 5 1 0 504.08 573.70 22.85 o 6 1 0 1222.81 1282.45 35.71 o 7 1 0 468.63 522.72 27.93 o 8 1 0 537.12 458.78 28.31 o 9 1 0 99.10 123.86 33.60 o 10 1 0 64.62 53.98 32.70 o 11 1 0 98.94 61.24 60.82 o 12 1 0 106.59 18.29 68.47 o 13 1 0 41.34 67.62 80.38 o -14 2 0 0.17 -56.56 72.94 o -13 2 0 209.42 200.53 69.54 o -12 2 0 0.99 -14.42 33.30 o -11 2 0 87.97 105.74 33.87 o -10 2 0 212.98 198.89 40.31 o -9 2 0 225.92 233.90 46.36 o -8 2 0 57.18 31.17 18.04 o -7 2 0 350.69 293.29 24.50 o -6 2 0 277.51 344.38 21.16 o -5 2 0 230.43 200.73 25.30 o -4 2 0 7.07 3.37 8.34 o -3 2 0 1109.62 1040.82 37.53 o -2 2 0 6210.18 5833.66 106.07 o -1 2 0 28.47 23.74 9.17 o 0 2 0 3526.31 3560.05 51.91 o 1 2 0 35411.05 34648.53 561.79 o 2 2 0 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52.09 41.47 o -12 8 0 13.23 -29.05 33.50 o -11 8 0 584.26 609.24 41.92 o -10 8 0 15.15 10.14 28.76 o -9 8 0 655.35 753.15 43.37 o -8 8 0 2.55 8.36 24.86 o -7 8 0 162.44 112.13 24.57 o -6 8 0 18.96 35.67 22.97 o -5 8 0 269.84 247.29 26.81 o -4 8 0 715.35 801.53 22.43 o -3 8 0 9739.53 9585.91 139.95 o -2 8 0 20946.94 22171.31 299.77 o -1 8 0 803.10 735.12 27.42 o 0 8 0 1170.36 1127.02 32.13 o 1 8 0 364.86 363.22 31.83 o 2 8 0 882.11 829.65 30.74 o 3 8 0 953.06 913.22 33.76 o 4 8 0 13.09 -7.21 18.78 o 6 8 0 49.14 23.84 36.88 o 7 8 0 14.06 -80.38 53.59 o 8 8 0 153.89 149.70 73.15 o -14 9 0 63.25 73.58 79.10 o -13 9 0 20.24 15.90 40.32 o -12 9 0 51.56 87.77 38.41 o -11 9 0 196.26 192.19 41.02 o -10 9 0 124.24 180.19 36.43 o -9 9 0 312.84 357.10 59.22 o -8 9 0 315.89 313.31 36.27 o -7 9 0 13.85 14.70 22.04 o -6 9 0 93.20 38.17 21.41 o -5 9 0 2.54 24.07 20.14 o -4 9 0 215.28 128.15 35.83 o -3 9 0 572.02 608.64 22.74 o -2 9 0 244.11 240.73 19.22 o -1 9 0 218.63 173.55 18.95 o 0 9 0 2805.31 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