#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2213183.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213183_Fobs loop_ _publ_author_name 'Spencer, Lara C.' 'Bjelosevic, Haris' _publ_section_title ; [2-(1-Acetoxyethyl)-1,1'-bis(diphenylphosphino)ferrocene-\k^2^P,P']dichloridoplatinum(II) dichloromethane solvate ; _journal_coeditor_code BT2342 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1536 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.953 _cell_angle_gamma 90.000 _cell_length_a 10.5116 _cell_length_b 22.3275 _cell_length_c 15.7340 _exptl_crystal_F_000 1952.00 _reflns_d_resolution_high 0.7210 _[local]_cod_data_source_file bt2342Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' darkwa55 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 614.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10226.75 9872.19 206.49 o 4 0 0 14665.66 15080.64 340.17 o 6 0 0 36111.63 39097.87 685.29 o 8 0 0 12908.06 12749.48 320.13 o 10 0 0 19726.70 20239.13 559.27 o 12 0 0 5174.78 4669.62 200.99 o 14 0 0 7200.13 7286.15 319.09 o 1 1 0 2204.72 2216.41 74.30 o 2 1 0 27164.64 30605.42 373.92 o 3 1 0 39826.37 42844.70 521.95 o 4 1 0 2071.79 2454.64 41.98 o 5 1 0 1257.06 1017.21 27.59 o 6 1 0 29068.03 28925.83 375.42 o 7 1 0 36684.73 36332.02 500.12 o 8 1 0 11597.35 11220.70 204.20 o 9 1 0 212.98 166.38 39.55 o 10 1 0 3931.59 4091.71 119.06 o 11 1 0 4418.99 4237.08 129.96 o 12 1 0 8771.97 9006.08 201.10 o 13 1 0 3413.57 3353.60 122.51 o 14 1 0 248.20 318.68 77.06 o 1 2 0 125550.99 132314.52 1670.45 o 2 2 0 202.76 229.25 10.30 o 3 2 0 32641.41 37352.71 476.44 o 4 2 0 5209.44 5785.55 85.99 o 5 2 0 62073.17 60179.63 792.38 o 6 2 0 19.01 44.85 15.93 o 7 2 0 6510.89 6061.69 107.98 o 8 2 0 240.34 222.98 36.63 o 9 2 0 15008.53 14165.39 252.69 o 10 2 0 135.88 143.88 45.05 o 11 2 0 2637.88 2722.93 98.06 o 12 2 0 1.72 -42.12 54.99 o 13 2 0 8630.56 8729.84 216.49 o 14 2 0 290.42 357.54 78.97 o 1 3 0 3161.16 3240.53 45.57 o 2 3 0 75269.43 81021.84 1009.80 o 3 3 0 29988.81 31578.25 376.41 o 4 3 0 8387.06 9486.31 147.71 o 5 3 0 2150.71 1788.25 35.53 o 6 3 0 4448.01 4554.42 76.96 o 7 3 0 23816.75 22179.79 344.64 o 8 3 0 9386.12 9014.67 172.68 o 9 3 0 16.26 -18.24 38.04 o 10 3 0 2592.99 2374.10 86.98 o 11 3 0 12345.31 10906.02 218.05 o 12 3 0 7004.61 6600.82 208.71 o 13 3 0 2050.39 1973.58 112.76 o 14 3 0 80.48 78.33 66.97 o 0 4 0 202722.78 212904.67 6897.67 o 1 4 0 3031.44 3299.61 64.38 o 2 4 0 3226.40 3454.20 55.41 o 3 4 0 203.68 227.37 18.09 o 4 4 0 2630.46 2338.22 43.55 o 5 4 0 83.32 114.16 14.62 o 6 4 0 7417.41 7210.20 110.96 o 7 4 0 1122.88 1221.83 50.58 o 8 4 0 10588.23 10923.73 283.71 o 9 4 0 970.21 789.53 53.38 o 10 4 0 33414.05 34249.93 550.02 o 11 4 0 3.89 -2.27 48.36 o 12 4 0 6367.08 6373.81 161.15 o 13 4 0 221.31 155.30 59.01 o 14 4 0 5450.44 5728.50 169.81 o 1 5 0 8133.53 8544.74 135.25 o 2 5 0 83226.79 88281.15 1212.10 o 3 5 0 1590.06 1566.41 29.41 o 4 5 0 4851.08 5580.04 77.54 o 5 5 0 869.17 826.26 27.13 o 6 5 0 37243.60 36412.85 428.08 o 7 5 0 17752.82 17798.98 356.27 o 8 5 0 22217.28 22877.51 333.80 o 9 5 0 5262.92 5305.69 150.42 o 10 5 0 6215.55 6440.97 148.25 o 11 5 0 1537.23 1394.75 86.93 o 12 5 0 13060.96 13528.05 251.97 o 13 5 0 3784.83 3696.90 129.02 o 14 5 0 411.29 227.11 85.56 o 0 6 0 5331.86 5639.60 114.61 o 1 6 0 55652.54 59452.36 1228.85 o 2 6 0 12276.85 12137.09 210.98 o 3 6 0 921.75 919.22 28.42 o 4 6 0 16878.09 17514.15 219.15 o 5 6 0 66503.57 67364.31 771.02 o 6 6 0 173.39 157.87 20.31 o 7 6 0 21119.60 20899.41 412.90 o 8 6 0 1617.08 1568.92 64.51 o 9 6 0 9490.78 8751.66 166.08 o 10 6 0 3526.51 3337.96 108.80 o 11 6 0 1711.34 1501.91 94.70 o 12 6 0 13.05 27.17 56.74 o 13 6 0 7361.80 6843.18 187.11 o 14 6 0 575.78 750.49 105.02 o 1 7 0 54674.83 56749.95 894.48 o 2 7 0 22789.03 24013.59 314.56 o 3 7 0 17400.14 17973.11 238.04 o 4 7 0 42.04 65.66 16.18 o 5 7 0 4536.15 4192.86 72.90 o 6 7 0 1276.71 1295.14 53.83 o 7 7 0 61409.63 62401.57 885.65 o 8 7 0 4027.88 4445.55 95.44 o 9 7 0 315.80 288.18 48.31 o 10 7 0 3762.21 3093.60 111.57 o 11 7 0 13792.61 13512.80 288.86 o 12 7 0 3710.45 3489.21 118.80 o 13 7 0 3846.38 3845.54 160.55 o 14 7 0 434.31 655.07 111.69 o 0 8 0 212498.81 216574.59 4019.79 o 1 8 0 1512.40 1381.16 36.07 o 2 8 0 39.98 27.53 16.81 o 3 8 0 130.65 112.60 14.49 o 4 8 0 17629.45 17946.48 211.10 o 5 8 0 2064.51 1967.84 43.68 o 6 8 0 14280.70 14250.80 189.58 o 7 8 0 387.36 334.65 32.64 o 8 8 0 9815.98 9396.52 160.65 o 9 8 0 6168.77 5686.21 140.17 o 10 8 0 18364.26 17452.13 669.57 o 11 8 0 1219.92 1225.65 74.45 o 12 8 0 7428.67 6722.84 481.25 o 13 8 0 1066.68 1270.60 133.17 o 14 8 0 6933.08 7153.27 334.21 o 1 9 0 82.23 74.00 16.92 o 2 9 0 31151.85 31222.15 477.91 o 3 9 0 9717.94 9990.19 129.24 o 4 9 0 4058.77 4126.53 66.22 o 5 9 0 37.44 34.58 18.05 o 6 9 0 29219.91 29000.42 359.19 o 7 9 0 4200.43 4363.29 114.37 o 8 9 0 13364.08 13540.93 243.51 o 9 9 0 283.71 191.17 40.90 o 10 9 0 3956.96 3939.25 127.12 o 11 9 0 91.39 127.15 68.79 o 12 9 0 15237.26 15826.28 364.07 o 13 9 0 938.16 1283.24 283.93 o 0 10 0 10520.28 11135.01 215.99 o 1 10 0 31546.60 33391.45 433.39 o 2 10 0 18729.12 19347.22 343.26 o 3 10 0 119.17 146.70 15.90 o 4 10 0 33267.05 33537.89 406.35 o 5 10 0 58156.98 58862.69 726.50 o 6 10 0 351.15 327.05 31.43 o 7 10 0 2151.60 2186.10 66.85 o 8 10 0 1601.27 1456.65 56.24 o 9 10 0 10928.69 10217.92 242.33 o 10 10 0 1411.13 1403.97 111.44 o 11 10 0 2816.64 2985.76 179.17 o 12 10 0 17.77 121.12 72.69 o 13 10 0 7258.39 7623.52 259.60 o 1 11 0 13790.42 13659.19 193.53 o 2 11 0 8396.58 8659.93 132.61 o 3 11 0 40773.13 41360.16 559.57 o 4 11 0 245.38 206.88 21.20 o 5 11 0 5238.49 4859.62 125.51 o 6 11 0 34.62 63.42 24.88 o 7 11 0 29727.39 30170.37 472.15 o 8 11 0 1258.54 1335.88 91.56 o 9 11 0 2308.45 2375.88 89.41 o 10 11 0 131.10 164.00 67.11 o 11 11 0 20065.31 19819.14 393.66 o 12 11 0 723.17 451.45 109.26 o 13 11 0 646.54 707.14 97.92 o 0 12 0 78282.38 80590.55 2113.60 o 1 12 0 45542.06 44852.59 647.44 o 2 12 0 9776.08 10292.42 175.55 o 3 12 0 2752.95 2678.92 66.75 o 4 12 0 8335.37 7884.71 124.94 o 5 12 0 2829.82 2547.52 63.00 o 6 12 0 9172.40 9215.12 246.33 o 7 12 0 88.13 94.10 36.08 o 8 12 0 4122.02 4274.99 110.08 o 9 12 0 7501.53 6990.30 185.06 o 10 12 0 10522.79 9859.99 277.21 o 11 12 0 180.96 177.56 71.09 o 12 12 0 5836.06 5841.86 194.09 o 13 12 0 2586.50 2624.99 143.70 o 1 13 0 301.33 392.42 32.32 o 2 13 0 31967.05 31584.05 438.38 o 3 13 0 3866.04 3987.71 105.53 o 4 13 0 3988.16 3854.43 75.80 o 5 13 0 259.40 332.73 32.43 o 6 13 0 44866.51 43335.64 661.31 o 7 13 0 5070.48 4954.36 119.32 o 8 13 0 9441.88 9278.11 194.87 o 9 13 0 561.15 419.93 55.45 o 10 13 0 2222.21 2247.09 134.74 o 11 13 0 378.84 358.00 110.05 o 12 13 0 11767.15 11794.06 301.38 o 13 13 0 1807.96 1810.48 145.64 o 0 14 0 7823.14 7110.55 222.29 o 1 14 0 10317.20 10275.49 156.35 o 2 14 0 21953.84 21572.98 297.95 o 3 14 0 817.56 819.88 44.09 o 4 14 0 8327.39 7691.58 143.29 o 5 14 0 47959.07 48132.21 630.86 o 6 14 0 4142.73 4077.77 125.27 o 7 14 0 601.79 591.55 79.79 o 8 14 0 2299.26 2333.71 90.40 o 9 14 0 4267.51 4475.44 160.13 o 10 14 0 2865.05 2831.95 141.96 o 11 14 0 589.97 829.63 94.69 o 12 14 0 549.56 274.92 96.72 o 1 15 0 14170.32 13387.58 205.62 o 2 15 0 2694.48 2582.82 74.36 o 3 15 0 8972.40 8476.49 145.24 o 4 15 0 1537.30 1639.80 92.73 o 5 15 0 11786.02 11916.64 203.31 o 6 15 0 7.36 -12.05 37.31 o 7 15 0 26019.53 25059.49 432.89 o 8 15 0 39.25 23.38 44.73 o 9 15 0 2042.50 1976.84 91.16 o 10 15 0 26.95 47.23 68.75 o 11 15 0 18630.96 18423.81 413.95 o 12 15 0 56.91 -45.57 77.38 o 0 16 0 10830.60 10618.27 270.94 o 1 16 0 26675.69 26675.44 395.41 o 2 16 0 2036.36 2154.03 66.81 o 3 16 0 5606.60 5290.75 105.16 o 4 16 0 18233.55 17264.83 262.66 o 5 16 0 10544.60 9988.79 178.47 o 6 16 0 3511.06 3526.25 106.93 o 7 16 0 16.87 13.58 42.16 o 8 16 0 1704.21 1622.30 78.17 o 9 16 0 7484.37 7276.77 177.72 o 10 16 0 12408.33 13530.59 357.86 o 11 16 0 25.98 -84.14 84.14 o 12 16 0 4800.64 5022.87 189.26 o 1 17 0 1388.33 1365.35 62.73 o 2 17 0 22303.70 21502.78 371.13 o 3 17 0 258.20 301.10 36.29 o 4 17 0 3649.81 3539.50 114.54 o 5 17 0 4909.81 4358.90 104.68 o 6 17 0 22515.12 21835.19 387.13 o 7 17 0 103.43 81.28 45.79 o 8 17 0 5530.35 5615.05 149.35 o 9 17 0 210.07 172.12 62.84 o 10 17 0 3424.40 3369.66 145.35 o 11 17 0 677.54 761.72 99.25 o 12 17 0 10540.20 10801.27 469.24 o 0 18 0 5084.93 5165.14 169.42 o 1 18 0 215.02 324.91 40.41 o 2 18 0 5976.29 6166.98 142.91 o 3 18 0 4500.86 4512.59 117.56 o 4 18 0 28827.04 28038.61 535.60 o 5 18 0 26927.96 26262.63 606.14 o 6 18 0 1502.55 1410.38 75.32 o 7 18 0 2200.94 2390.30 95.26 o 8 18 0 2269.57 2246.93 99.34 o 9 18 0 4233.43 4028.58 133.91 o 10 18 0 2527.23 2563.14 135.91 o 11 18 0 1495.86 1468.36 117.96 o 1 19 0 18682.89 17860.17 321.04 o 2 19 0 109.83 44.50 39.53 o 3 19 0 19050.18 19223.83 323.17 o 4 19 0 383.00 238.75 46.90 o 5 19 0 316.60 279.77 64.77 o 6 19 0 3076.24 2977.49 107.36 o 7 19 0 11934.88 11875.58 247.11 o 8 19 0 462.62 527.03 66.09 o 9 19 0 1115.46 1062.40 85.05 o 10 19 0 18.14 -1.14 74.08 o 11 19 0 18411.51 18469.46 472.88 o 0 20 0 4752.72 4721.33 168.40 o 1 20 0 4673.87 5019.97 130.87 o 2 20 0 6.90 17.18 37.89 o 3 20 0 5578.19 5440.19 130.48 o 4 20 0 9045.94 8324.18 197.79 o 5 20 0 8241.29 8098.66 234.19 o 6 20 0 3251.38 3101.40 166.96 o 7 20 0 373.70 395.07 69.34 o 8 20 0 1541.58 1421.49 91.18 o 9 20 0 8537.69 8568.27 226.20 o 10 20 0 5405.41 5886.96 203.08 o 11 20 0 38.80 -32.39 111.18 o 1 21 0 402.46 470.71 48.89 o 2 21 0 20807.14 18420.53 413.64 o 3 21 0 53.13 -12.08 43.27 o 4 21 0 2987.59 2864.89 111.64 o 5 21 0 33.95 -31.89 56.89 o 6 21 0 14603.20 14332.92 327.81 o 7 21 0 1101.42 1101.74 93.50 o 8 21 0 2383.32 2459.05 126.19 o 9 21 0 7.10 -44.73 74.97 o 10 21 0 1135.01 1163.66 96.46 o 0 22 0 6948.37 6769.01 215.07 o 1 22 0 898.95 835.58 61.67 o 2 22 0 2308.70 2145.01 146.91 o 3 22 0 30.90 -10.43 46.35 o 4 22 0 18885.11 18611.35 434.92 o 5 22 0 6287.16 6280.88 211.82 o 6 22 0 4918.35 4989.55 168.38 o 7 22 0 198.89 142.06 72.59 o 8 22 0 3928.42 4066.64 161.24 o 9 22 0 1293.31 1497.89 154.39 o 10 22 0 2231.26 2163.55 180.05 o 1 23 0 7831.62 7499.54 178.60 o 2 23 0 1635.42 1718.92 82.43 o 3 23 0 10264.61 10650.45 226.63 o 4 23 0 143.22 197.05 59.42 o 5 23 0 1163.81 1071.33 136.99 o 6 23 0 2083.87 2148.10 130.81 o 7 23 0 7002.14 7446.37 238.13 o 8 23 0 50.63 3.11 76.78 o 9 23 0 1593.46 1606.62 117.93 o 0 24 0 1470.05 1489.22 181.79 o 1 24 0 9039.39 8972.64 191.13 o 2 24 0 15.04 -24.04 47.75 o 3 24 0 7833.36 7837.71 175.69 o 4 24 0 4594.17 4135.57 178.71 o 5 24 0 11181.93 10530.95 332.79 o 6 24 0 54.45 11.49 73.17 o 7 24 0 524.84 511.22 90.94 o 8 24 0 780.52 729.19 101.91 o 9 24 0 8500.16 8641.69 359.94 o 1 25 0 1280.99 1352.85 100.08 o 2 25 0 13126.68 12978.69 252.52 o 3 25 0 892.14 740.81 77.52 o 4 25 0 4415.62 4593.72 166.18 o 5 25 0 839.18 843.26 88.63 o 6 25 0 10603.54 10960.91 284.70 o 7 25 0 2035.60 1985.91 144.04 o 8 25 0 1542.97 1586.86 122.72 o 0 26 0 3972.86 3826.60 195.42 o 1 26 0 55.13 160.00 58.51 o 2 26 0 998.20 1069.64 79.41 o 3 26 0 266.98 355.66 70.36 o 4 26 0 12602.94 12681.01 287.39 o 5 26 0 1751.81 1655.66 117.06 o 6 26 0 4468.33 5506.63 551.35 o 7 26 0 459.12 429.22 97.50 o 1 27 0 7192.46 7327.27 168.36 o 2 27 0 1106.32 1134.55 84.62 o 3 27 0 5669.41 5885.34 167.89 o 4 27 0 48.05 82.81 74.78 o 5 27 0 143.35 112.37 96.16 o 6 27 0 2637.12 2450.38 141.71 o 0 28 0 18.48 50.16 91.46 o 1 28 0 3043.84 3253.77 125.53 o 2 28 0 43.23 8.49 63.64 o 3 28 0 4747.31 4745.81 153.13 o 4 28 0 329.60 384.41 87.43 o 5 28 0 5398.34 5128.20 286.81 o 6 28 0 40.21 -57.91 194.06 o 1 29 0 2094.13 2481.48 191.65 o 2 29 0 4420.16 4600.47 143.69 o 3 29 0 1419.59 1128.13 108.62 o 4 29 0 2642.15 2731.93 135.22 o 0 30 0 3485.94 3433.88 235.87 o 1 30 0 73.31 156.42 72.61 o 2 30 0 40.31 33.99 74.00 o 3 30 0 73.04 69.42 228.96 o -13 0 1 7701.56 8125.90 247.69 o -11 0 1 1237.29 1075.37 192.45 o -9 0 1 21364.16 20437.97 483.73 o -7 0 1 2587.78 2157.18 100.13 o -5 0 1 84694.62 87587.53 1750.12 o -3 0 1 69235.37 72979.27 1363.48 o -1 0 1 94515.76 96269.52 1798.92 o 1 0 1 104079.67 110340.09 2013.02 o 3 0 1 7809.58 8880.88 166.85 o 5 0 1 98235.16 97055.71 1669.04 o 7 0 1 30284.26 31301.46 564.08 o 9 0 1 6261.72 5710.55 192.79 o 11 0 1 6019.46 5409.17 160.84 o 13 0 1 9856.46 9950.46 278.55 o -14 1 1 43.74 178.17 72.70 o -13 1 1 5025.76 5509.16 146.06 o -12 1 1 4762.09 4489.30 131.36 o -11 1 1 12255.14 12294.87 254.29 o -10 1 1 10972.97 10364.12 248.58 o -9 1 1 1335.07 1218.59 59.72 o -8 1 1 9580.50 9187.82 184.91 o -7 1 1 20333.90 19468.74 315.71 o -6 1 1 19420.14 20115.47 282.11 o -5 1 1 920.47 832.27 23.13 o -4 1 1 234.48 321.03 13.79 o -3 1 1 26152.64 27543.71 355.05 o -2 1 1 32787.69 35537.04 497.68 o -1 1 1 12101.31 12858.78 173.34 o 0 1 1 2413.35 43.29 6.24 o 1 1 1 1507.96 1488.92 21.01 o 2 1 1 72175.53 77590.66 904.42 o 3 1 1 487.26 592.70 18.91 o 4 1 1 49.09 75.24 11.51 o 5 1 1 1881.05 2039.86 46.39 o 6 1 1 30397.76 31679.38 446.79 o 7 1 1 62796.59 61254.24 841.74 o 8 1 1 14557.04 14055.40 244.93 o 9 1 1 1396.91 1573.44 80.90 o 10 1 1 188.10 243.83 49.63 o 11 1 1 5605.32 5078.64 134.11 o 12 1 1 8799.17 9373.56 183.19 o 13 1 1 2957.68 3100.13 119.26 o 14 1 1 658.96 589.52 86.68 o -14 2 1 4713.00 4941.81 168.40 o -13 2 1 11.49 80.81 60.33 o -12 2 1 9188.90 9271.18 191.77 o -11 2 1 687.28 682.63 67.08 o -10 2 1 22592.74 21764.43 392.82 o -9 2 1 49.94 8.02 34.55 o -8 2 1 9917.81 9649.51 181.01 o -7 2 1 226.94 241.88 24.68 o -6 2 1 21069.09 21035.88 324.85 o -5 2 1 2781.13 2981.86 56.86 o -4 2 1 40750.67 42750.62 563.03 o -3 2 1 3512.37 3957.46 78.36 o -2 2 1 22523.55 25756.42 417.37 o -1 2 1 117.42 107.53 7.52 o 0 2 1 288955.91 268221.31 6814.76 o 1 2 1 20.73 49.69 6.09 o 2 2 1 4115.97 4439.39 59.96 o 3 2 1 2378.21 2602.84 44.78 o 4 2 1 1677.76 1458.23 31.10 o 5 2 1 5481.67 5889.20 89.20 o 6 2 1 13294.38 13689.03 199.65 o 7 2 1 1517.49 1733.41 46.49 o 8 2 1 15964.25 16025.38 246.27 o 9 2 1 60.37 56.53 36.31 o 10 2 1 39957.55 40438.52 638.66 o 11 2 1 469.36 393.90 67.03 o 12 2 1 5022.45 4690.25 150.15 o 13 2 1 90.18 116.12 64.55 o 14 2 1 8900.31 9833.19 292.52 o -14 3 1 23.75 -17.88 64.76 o -13 3 1 3438.29 3609.74 126.23 o -12 3 1 10301.20 10299.90 231.66 o -11 3 1 5036.64 4502.81 124.74 o -10 3 1 15369.20 15163.83 272.75 o -9 3 1 0.73 18.02 33.27 o -8 3 1 8626.79 8460.59 163.72 o -7 3 1 14412.06 14524.87 236.56 o -6 3 1 5189.79 4999.74 78.64 o -5 3 1 4667.08 4414.98 72.43 o -4 3 1 12400.16 13360.58 190.78 o -3 3 1 19774.49 19926.96 273.85 o -2 3 1 25098.45 26271.98 300.17 o -1 3 1 3339.32 3774.93 66.36 o 0 3 1 1941.45 2094.68 30.62 o 1 3 1 323.86 386.93 15.94 o 2 3 1 97163.29 106758.80 1198.40 o 3 3 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