#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:28:35 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181052 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/32/2213251.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213251_Fobs loop_ _publ_author_name 'Zhang, Zhu-Yan' 'Gao, Shan' 'Huo, Li-Hua' 'Zhao, Jing-Gui' _publ_section_title ; Tetraaquabis[(4-oxo-4H-pyridin-1-yl)acetato]manganese(II) ; _journal_coeditor_code CI2374 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1514 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 108.158 _cell_angle_beta 99.325 _cell_angle_gamma 103.375 _cell_length_a 5.4191 _cell_length_b 9.0498 _cell_length_c 10.0442 _exptl_crystal_F_000 223.00 _reflns_d_resolution_high 0.7707 _cod_data_source_file ci2374Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' z in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 73.73 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4289.74 4479.23 66.27 o 2 0 0 1104.69 1287.50 9.72 o 3 0 0 0.43 4.04 0.35 o 4 0 0 168.23 159.09 1.24 o 5 0 0 0.42 0.16 0.30 o 6 0 0 0.78 0.83 0.73 o -6 1 0 106.94 109.37 2.39 o -5 1 0 175.15 168.24 2.30 o -4 1 0 30.17 27.99 1.27 o -3 1 0 19.38 18.51 0.31 o -2 1 0 177.72 173.90 1.34 o -1 1 0 1175.89 1198.17 17.60 o 1 1 0 5.58 9.84 0.30 o 2 1 0 93.56 81.87 0.66 o 3 1 0 351.29 359.15 2.54 o 4 1 0 291.38 287.47 2.15 o 5 1 0 109.22 102.68 0.94 o 6 1 0 56.83 52.13 2.00 o -6 2 0 54.65 53.75 0.88 o -5 2 0 17.07 19.68 0.73 o -4 2 0 13.01 14.78 0.39 o -3 2 0 188.75 186.28 1.69 o -2 2 0 403.89 377.16 3.52 o -1 2 0 204.35 189.21 1.91 o 0 2 0 179.07 184.10 1.72 o 1 2 0 3321.68 3462.66 38.22 o 2 2 0 1731.39 1946.43 19.25 o 3 2 0 195.03 199.16 1.68 o 4 2 0 12.69 7.90 0.54 o 5 2 0 38.57 32.10 0.52 o 6 2 0 36.06 36.92 1.90 o -6 3 0 137.60 130.84 2.71 o -5 3 0 82.57 82.73 0.78 o -4 3 0 342.49 349.05 3.47 o -3 3 0 1107.33 1174.88 10.54 o -2 3 0 129.67 157.08 2.12 o -1 3 0 4148.53 4596.30 69.63 o 0 3 0 226.91 220.87 2.99 o 1 3 0 2217.08 2404.22 24.38 o 2 3 0 83.98 85.31 0.92 o 3 3 0 7.15 7.65 0.44 o 4 3 0 253.26 254.92 3.16 o 5 3 0 101.56 105.40 1.36 o -6 4 0 18.28 20.08 1.12 o -5 4 0 49.44 48.26 0.79 o -4 4 0 7.78 9.25 0.78 o -3 4 0 30.27 30.53 0.89 o -2 4 0 520.97 515.37 5.03 o -1 4 0 684.43 671.37 6.72 o 0 4 0 546.05 526.82 5.20 o 1 4 0 669.60 675.56 5.65 o 2 4 0 159.79 148.30 1.47 o 3 4 0 2.94 1.56 0.44 o 4 4 0 7.48 6.74 0.51 o 5 4 0 21.50 25.96 0.69 o -6 5 0 55.37 53.77 1.71 o -5 5 0 311.61 311.45 2.76 o -4 5 0 312.97 309.26 2.55 o -3 5 0 129.64 124.02 2.04 o -2 5 0 293.56 295.24 3.23 o -1 5 0 83.81 81.75 1.12 o 0 5 0 11.97 14.29 1.29 o 1 5 0 4.40 5.57 0.55 o 2 5 0 47.66 46.33 1.00 o 3 5 0 55.26 62.92 1.55 o 4 5 0 34.68 38.52 1.38 o -6 6 0 112.14 106.01 1.98 o -5 6 0 61.85 61.78 0.77 o -4 6 0 6.95 7.41 0.71 o -3 6 0 54.00 55.66 1.39 o -2 6 0 610.28 608.15 6.50 o -1 6 0 116.42 112.61 1.72 o 0 6 0 20.59 21.07 0.75 o 1 6 0 381.25 388.33 3.48 o 2 6 0 284.86 279.00 2.96 o 3 6 0 26.05 24.39 0.87 o 4 6 0 2.84 1.62 0.48 o -6 7 0 25.32 25.91 1.14 o -5 7 0 104.23 101.56 1.11 o -4 7 0 148.48 142.41 3.11 o -3 7 0 67.19 66.75 1.69 o -2 7 0 96.19 91.48 1.45 o -1 7 0 24.76 27.87 3.15 o 0 7 0 2.57 1.86 0.77 o 1 7 0 53.83 50.84 1.03 o 2 7 0 257.44 251.42 3.56 o 3 7 0 90.79 89.51 1.81 o -6 8 0 24.58 25.87 0.99 o -5 8 0 9.41 8.76 0.73 o -4 8 0 126.16 128.98 2.63 o -3 8 0 37.03 39.72 1.51 o -2 8 0 20.19 19.93 0.90 o -1 8 0 177.80 178.55 2.42 o 0 8 0 232.05 223.02 2.90 o 1 8 0 62.24 61.72 1.07 o 2 8 0 14.60 14.20 1.02 o 3 8 0 12.23 11.84 1.31 o -5 9 0 109.90 117.57 2.74 o -4 9 0 71.24 76.51 2.15 o -3 9 0 12.04 10.94 1.25 o -2 9 0 50.27 49.07 2.09 o -1 9 0 48.59 48.00 2.57 o 0 9 0 1.36 1.33 0.75 o 1 9 0 1.22 1.47 0.67 o 2 9 0 23.41 22.80 0.91 o -4 10 0 4.41 4.39 1.21 o -3 10 0 5.14 4.13 2.19 o -2 10 0 9.98 13.73 1.31 o -1 10 0 60.32 61.41 1.63 o 0 10 0 48.74 51.34 1.29 o 1 10 0 11.35 10.43 0.83 o -3 11 0 24.35 27.25 1.96 o -2 11 0 0.17 -0.29 0.85 o -1 11 0 0.52 0.97 0.93 o 1 -11 1 1.81 1.43 0.93 o 2 -11 1 16.07 20.38 1.95 o 3 -11 1 54.75 54.88 2.32 o -1 -10 1 9.17 12.95 1.34 o 0 -10 1 36.98 34.44 1.36 o 1 -10 1 76.56 75.76 1.74 o 2 -10 1 20.07 21.95 1.12 o 3 -10 1 7.08 11.15 1.20 o 4 -10 1 18.94 22.05 1.47 o -2 -9 1 91.99 90.02 2.06 o -1 -9 1 33.47 34.22 0.98 o 0 -9 1 38.36 36.60 1.98 o 1 -9 1 61.47 64.51 2.13 o 2 -9 1 23.60 24.40 1.23 o 3 -9 1 25.30 26.76 1.17 o 4 -9 1 63.52 59.55 1.80 o 5 -9 1 37.59 34.31 1.42 o -3 -8 1 26.64 27.22 1.10 o -2 -8 1 3.07 3.51 0.69 o -1 -8 1 20.89 20.29 1.26 o 0 -8 1 103.37 102.78 1.72 o 1 -8 1 24.11 24.20 0.95 o 2 -8 1 0.28 -0.04 0.66 o 3 -8 1 117.75 112.61 1.67 o 4 -8 1 142.45 146.29 2.77 o 5 -8 1 8.75 10.12 0.55 o 6 -8 1 2.96 2.53 0.83 o -4 -7 1 1.90 0.00 0.70 o -3 -7 1 1.77 1.65 0.53 o -2 -7 1 106.34 100.92 1.74 o -1 -7 1 30.51 31.17 1.15 o 0 -7 1 7.32 8.51 0.74 o 1 -7 1 60.17 58.29 1.39 o 2 -7 1 288.27 280.77 3.18 o 3 -7 1 148.27 147.86 1.85 o 4 -7 1 135.15 136.22 3.26 o 5 -7 1 92.44 92.50 1.42 o 6 -7 1 14.79 14.69 0.54 o -4 -6 1 0.17 0.14 0.43 o -3 -6 1 9.29 9.97 1.09 o -2 -6 1 188.05 185.22 2.74 o -1 -6 1 169.64 160.05 2.26 o 0 -6 1 34.23 29.72 1.04 o 1 -6 1 163.03 159.78 3.28 o 2 -6 1 56.64 52.79 0.95 o 3 -6 1 16.33 16.55 0.87 o 4 -6 1 4.83 7.39 1.41 o 5 -6 1 85.77 81.73 1.06 o 6 -6 1 44.90 41.42 0.78 o -5 -5 1 7.73 7.85 0.64 o -4 -5 1 67.41 64.84 0.96 o -3 -5 1 136.01 135.24 1.57 o -2 -5 1 147.09 151.88 1.79 o -1 -5 1 292.40 299.30 3.40 o 0 -5 1 719.79 699.43 7.26 o 1 -5 1 69.72 61.86 1.91 o 2 -5 1 375.68 395.18 4.16 o 3 -5 1 2.93 4.83 0.57 o 4 -5 1 503.36 508.03 4.22 o 5 -5 1 345.71 347.82 3.00 o 6 -5 1 18.35 18.06 0.87 o -5 -4 1 191.87 180.94 3.14 o -4 -4 1 105.35 93.53 1.15 o -3 -4 1 1.17 0.76 0.52 o -2 -4 1 505.52 511.47 4.43 o -1 -4 1 1631.88 1805.53 21.79 o 0 -4 1 172.38 154.59 1.63 o 1 -4 1 0.71 0.79 0.45 o 2 -4 1 307.27 288.78 2.89 o 3 -4 1 9.52 10.51 0.60 o 4 -4 1 2.62 2.87 0.29 o 5 -4 1 35.84 34.06 0.67 o 6 -4 1 27.88 29.55 2.20 o -5 -3 1 75.06 73.08 1.39 o -4 -3 1 76.98 72.03 0.86 o -3 -3 1 5.89 6.79 0.44 o -2 -3 1 2.26 0.94 0.29 o -1 -3 1 720.04 736.50 7.64 o 0 -3 1 1204.91 1296.26 16.19 o 1 -3 1 2292.95 2418.74 29.67 o 2 -3 1 1533.86 1714.84 19.64 o 3 -3 1 116.94 120.69 1.06 o 4 -3 1 4.10 6.14 0.62 o 5 -3 1 48.65 47.17 0.54 o 6 -3 1 81.29 76.62 2.05 o -6 -2 1 41.92 43.73 1.16 o -5 -2 1 31.75 32.81 0.65 o -4 -2 1 65.42 68.20 0.93 o -3 -2 1 53.37 43.62 0.87 o -2 -2 1 28.47 21.00 0.51 o -1 -2 1 335.64 324.04 3.00 o 0 -2 1 5001.41 5124.72 75.19 o 1 -2 1 5436.80 5620.35 84.59 o 2 -2 1 493.26 503.41 4.71 o 3 -2 1 106.83 128.10 0.96 o 4 -2 1 15.37 19.48 0.70 o 5 -2 1 64.04 63.33 1.31 o 6 -2 1 60.05 59.57 1.95 o -6 -1 1 1.17 0.91 0.29 o -5 -1 1 57.23 57.69 0.83 o -4 -1 1 278.95 273.84 3.11 o -3 -1 1 9.88 10.46 0.31 o -2 -1 1 11.20 15.42 0.41 o -1 -1 1 673.42 698.21 6.61 o 1 -1 1 0.50 2.65 0.54 o 2 -1 1 1626.52 1739.06 15.98 o 3 -1 1 1033.53 1159.51 10.14 o 4 -1 1 95.70 104.72 1.00 o 5 -1 1 166.60 152.09 1.42 o 6 -1 1 232.66 223.12 3.02 o -6 0 1 23.10 22.74 0.69 o -5 0 1 70.57 68.95 0.81 o -4 0 1 667.91 681.42 5.25 o -3 0 1 476.58 500.46 3.37 o -2 0 1 137.21 149.72 1.32 o -1 0 1 36.22 37.58 0.56 o 1 0 1 421.47 427.26 3.06 o 2 0 1 272.60 274.28 1.70 o 3 0 1 549.95 599.92 4.12 o 4 0 1 103.47 98.14 0.81 o 5 0 1 7.85 7.11 0.43 o 6 0 1 26.20 26.83 1.44 o -6 1 1 102.70 103.12 1.23 o -5 1 1 55.57 49.75 0.99 o -4 1 1 28.03 25.25 0.38 o -3 1 1 114.97 110.31 0.82 o -2 1 1 132.77 124.33 0.81 o -1 1 1 1.22 0.65 0.20 o 0 1 1 19.08 16.56 0.34 o 1 1 1 215.42 245.92 1.95 o 2 1 1 799.02 833.08 6.27 o 3 1 1 474.72 472.41 3.24 o 4 1 1 74.95 81.12 0.87 o 5 1 1 2.39 3.61 0.32 o 6 1 1 57.60 61.20 2.27 o -6 2 1 45.01 45.12 1.72 o -5 2 1 22.54 24.33 0.88 o -4 2 1 255.33 252.16 2.01 o -3 2 1 645.86 660.04 6.40 o -2 2 1 415.30 426.67 3.92 o -1 2 1 782.55 853.06 12.12 o 0 2 1 821.15 848.08 6.85 o 1 2 1 198.43 181.24 1.53 o 2 2 1 130.32 104.80 0.88 o 3 2 1 94.24 91.42 0.76 o 4 2 1 40.82 31.74 0.51 o 5 2 1 29.78 23.66 0.93 o -6 3 1 73.46 69.55 0.95 o -5 3 1 73.44 74.93 0.78 o -4 3 1 301.43 292.20 2.32 o -3 3 1 855.88 863.43 7.32 o -2 3 1 8.18 6.48 1.01 o -1 3 1 470.45 527.22 5.09 o 0 3 1 466.38 479.87 4.58 o 1 3 1 822.20 847.48 7.20 o 2 3 1 13.97 9.12 0.77 o 3 3 1 46.44 46.63 0.82 o 4 3 1 266.79 264.51 2.35 o 5 3 1 81.08 80.68 1.41 o -6 4 1 159.65 158.48 1.45 o -5 4 1 321.02 317.29 2.78 o -4 4 1 118.39 113.48 1.22 o -3 4 1 101.40 105.39 1.12 o -2 4 1 314.72 302.75 4.20 o -1 4 1 364.80 348.26 3.40 o 0 4 1 294.44 285.74 2.81 o 1 4 1 213.76 218.59 2.06 o 2 4 1 144.68 151.97 1.49 o 3 4 1 153.94 148.23 1.51 o 4 4 1 104.08 95.03 1.04 o 5 4 1 4.64 5.88 1.42 o -6 5 1 9.32 9.70 0.41 o -5 5 1 13.01 14.65 1.07 o -4 5 1 104.79 107.18 1.11 o -3 5 1 288.20 278.95 4.16 o -2 5 1 180.86 181.98 2.86 o -1 5 1 61.07 61.48 1.50 o 0 5 1 73.67 72.74 1.30 o 1 5 1 72.94 71.43 0.89 o 2 5 1 102.32 96.63 1.33 o 3 5 1 242.86 233.59 2.46 o 4 5 1 105.89 97.46 3.05 o -6 6 1 0.45 0.64 0.43 o -5 6 1 23.71 23.48 0.94 o -4 6 1 58.19 61.35 1.26 o -3 6 1 406.81 404.80 6.22 o -2 6 1 729.81 729.62 8.00 o -1 6 1 57.90 56.21 1.69 o 0 6 1 19.71 21.47 0.92 o 1 6 1 284.75 284.40 3.20 o 2 6 1 97.00 91.73 1.15 o 3 6 1 2.66 1.87 0.50 o 4 6 1 9.15 10.62 1.11 o -6 7 1 2.25 1.86 0.93 o -5 7 1 45.96 48.60 0.85 o -4 7 1 36.60 39.08 0.86 o -3 7 1 39.36 39.13 1.42 o -2 7 1 95.96 91.56 2.20 o -1 7 1 16.21 17.04 0.99 o 0 7 1 0.65 1.29 0.45 o 1 7 1 62.77 63.47 1.12 o 2 7 1 84.81 79.91 1.26 o 3 7 1 22.88 23.13 1.05 o -6 8 1 7.06 7.77 1.32 o -5 8 1 0.20 -0.04 0.32 o -4 8 1 12.41 11.96 2.01 o -3 8 1 28.44 27.24 1.43 o -2 8 1 9.95 11.42 0.84 o -1 8 1 38.45 36.80 1.11 o 0 8 1 157.45 161.22 1.80 o 1 8 1 123.23 125.08 1.92 o 2 8 1 17.12 18.48 1.27 o -5 9 1 27.32 30.46 1.10 o -4 9 1 3.83 4.84 2.02 o -3 9 1 1.54 1.54 1.08 o -2 9 1 61.23 59.39 1.48 o -1 9 1 83.74 82.49 1.72 o 0 9 1 3.34 5.33 1.70 o 1 9 1 1.93 1.87 0.61 o -4 10 1 18.77 17.29 1.61 o -3 10 1 34.61 35.27 1.92 o -2 10 1 83.38 84.44 2.69 o -1 10 1 29.38 30.87 1.04 o 0 10 1 5.53 7.44 2.15 o 0 -11 2 28.83 32.61 1.44 o 1 -11 2 2.75 3.47 1.18 o 2 -11 2 12.51 14.29 1.38 o 3 -11 2 33.78 31.01 1.56 o -1 -10 2 4.22 4.07 0.97 o 0 -10 2 2.29 3.39 1.07 o 1 -10 2 4.39 4.32 1.08 o 2 -10 2 3.83 4.43 1.02 o 3 -10 2 70.92 68.10 1.79 o 4 -10 2 114.13 114.34 3.92 o -2 -9 2 2.00 2.13 0.77 o -1 -9 2 57.72 56.00 1.68 o 0 -9 2 83.31 86.31 2.00 o 1 -9 2 18.49 21.13 1.22 o 2 -9 2 11.09 11.17 0.83 o 3 -9 2 35.87 34.15 1.22 o 4 -9 2 15.94 14.26 1.10 o 5 -9 2 4.91 2.84 0.81 o -3 -8 2 34.06 37.50 1.01 o -2 -8 2 2.83 3.08 0.61 o -1 -8 2 17.06 16.87 2.44 o 0 -8 2 183.77 180.41 2.93 o 1 -8 2 58.02 56.21 1.22 o 2 -8 2 54.40 53.51 1.33 o 3 -8 2 0.96 0.63 0.51 o 4 -8 2 92.93 92.96 2.78 o 5 -8 2 51.66 53.10 1.50 o 6 -8 2 26.42 25.70 0.78 o -4 -7 2 0.95 0.96 0.59 o -3 -7 2 53.97 50.66 1.00 o -2 -7 2 199.80 196.32 2.11 o -1 -7 2 287.05 289.39 3.40 o 0 -7 2 409.76 407.39 4.59 o 1 -7 2 215.44 197.44 2.41 o 2 -7 2 20.57 17.92 1.02 o 3 -7 2 23.46 21.84 1.15 o 4 -7 2 32.01 31.07 1.00 o 5 -7 2 42.08 41.92 0.75 o -4 -6 2 46.80 47.58 1.70 o -3 -6 2 62.97 61.46 1.50 o -2 -6 2 63.95 66.64 1.12 o -1 -6 2 21.60 21.06 0.78 o 0 -6 2 10.14 11.80 0.82 o 1 -6 2 212.68 214.73 2.39 o 2 -6 2 419.16 405.32 6.03 o 3 -6 2 115.78 111.76 1.32 o 4 -6 2 17.77 19.11 0.98 o 5 -6 2 12.78 12.44 0.44 o -5 -5 2 0.52 0.91 0.46 o -4 -5 2 7.36 7.78 0.69 o -3 -5 2 134.95 131.98 1.54 o -2 -5 2 46.43 45.50 1.09 o -1 -5 2 4.51 6.90 0.67 o 0 -5 2 861.07 886.86 10.79 o 1 -5 2 4529.83 4844.27 72.94 o 2 -5 2 636.77 650.96 6.85 o 3 -5 2 71.61 66.82 1.66 o 4 -5 2 2.94 2.90 0.35 o 5 -5 2 41.36 43.63 1.14 o -5 -4 2 173.84 174.50 1.90 o -4 -4 2 80.52 80.81 1.14 o -3 -4 2 1.97 2.05 0.58 o -2 -4 2 35.22 29.60 0.70 o -1 -4 2 65.77 63.12 1.07 o 0 -4 2 47.33 44.85 0.76 o 1 -4 2 490.49 486.43 4.68 o 2 -4 2 489.29 500.26 4.70 o 3 -4 2 103.79 105.58 1.14 o 4 -4 2 107.20 106.10 1.13 o 5 -4 2 126.29 125.03 1.03 o 6 -4 2 48.75 49.10 1.77 o -6 -3 2 8.88 9.16 0.60 o -5 -3 2 45.18 42.30 0.84 o -4 -3 2 31.73 26.94 0.66 o -3 -3 2 25.28 25.30 0.73 o -2 -3 2 457.93 483.46 4.96 o -1 -3 2 1497.52 1558.12 17.65 o 0 -3 2 15.81 16.44 0.55 o 1 -3 2 0.45 0.66 0.71 o 2 -3 2 1157.98 1211.79 12.72 o 3 -3 2 555.54 603.73 4.70 o 4 -3 2 27.82 34.78 0.49 o 5 -3 2 26.86 28.59 1.39 o 6 -3 2 125.41 122.85 2.86 o -6 -2 2 108.28 108.82 1.29 o -5 -2 2 172.16 173.80 1.75 o -4 -2 2 74.70 75.70 1.11 o -3 -2 2 177.56 186.71 3.70 o -2 -2 2 349.69 362.53 2.91 o -1 -2 2 194.40 222.02 2.35 o 0 -2 2 1991.49 2181.51 28.83 o 1 -2 2 676.89 690.38 9.33 o 2 -2 2 1969.49 2127.38 25.13 o 3 -2 2 79.50 85.18 0.60 o 4 -2 2 37.32 30.88 0.26 o 5 -2 2 221.18 218.30 5.12 o 6 -2 2 50.30 53.77 2.00 o -6 -1 2 1.28 1.43 0.41 o -5 -1 2 36.92 39.64 0.70 o -4 -1 2 102.29 92.50 1.02 o -3 -1 2 0.73 0.37 0.25 o -2 -1 2 116.31 104.74 1.07 o -1 -1 2 2977.40 3158.03 48.15 o 0 -1 2 1914.87 1997.69 23.18 o 1 -1 2 253.13 269.78 4.77 o 2 -1 2 703.29 735.51 7.41 o 3 -1 2 216.89 211.69 2.51 o 4 -1 2 0.43 0.10 0.51 o 5 -1 2 2.68 1.01 0.67 o 6 -1 2 10.42 9.07 1.43 o -6 0 2 13.75 13.72 0.61 o -5 0 2 201.23 202.25 1.99 o -4 0 2 1084.63 1114.99 10.37 o -3 0 2 454.31 448.69 5.99 o -2 0 2 234.44 257.68 1.89 o -1 0 2 91.69 81.95 0.91 o 0 0 2 590.63 585.67 5.13 o 1 0 2 120.95 116.56 0.97 o 2 0 2 59.39 49.29 0.43 o 3 0 2 558.70 543.69 4.89 o 4 0 2 84.84 91.05 0.86 o 5 0 2 1.57 1.48 0.72 o 6 0 2 28.32 29.60 1.34 o -6 1 2 10.89 10.56 0.61 o -5 1 2 295.67 286.76 2.59 o -4 1 2 364.42 356.54 2.55 o -3 1 2 134.18 115.18 0.84 o -2 1 2 284.91 301.39 2.17 o -1 1 2 1430.46 1519.72 23.64 o 0 1 2 242.34 240.63 3.24 o 1 1 2 108.50 108.75 1.13 o 2 1 2 880.72 931.95 6.81 o 3 1 2 310.67 318.87 2.14 o 4 1 2 17.97 17.09 0.79 o 5 1 2 35.69 31.42 1.48 o 6 1 2 18.79 19.79 1.75 o -6 2 2 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740.08 780.52 8.08 o 3 -4 3 461.20 485.46 5.15 o 4 -4 3 174.73 175.88 1.32 o 5 -4 3 71.37 68.22 1.92 o 6 -4 3 2.97 4.03 1.17 o -6 -3 3 59.04 61.81 1.36 o -5 -3 3 42.05 41.04 0.77 o -4 -3 3 4.32 4.32 0.51 o -3 -3 3 185.98 170.05 1.57 o -2 -3 3 763.48 782.73 8.13 o -1 -3 3 439.55 420.23 4.06 o 0 -3 3 115.97 122.58 1.29 o 1 -3 3 596.26 588.57 5.66 o 2 -3 3 270.41 253.06 2.35 o 3 -3 3 11.38 8.79 0.80 o 4 -3 3 2.54 6.38 0.93 o 5 -3 3 0.80 -0.57 0.93 o 6 -3 3 0.72 1.01 1.10 o -6 -2 3 8.29 9.23 2.12 o -5 -2 3 66.69 66.74 1.10 o -4 -2 3 398.02 398.10 3.43 o -3 -2 3 1048.90 1059.20 9.65 o -2 -2 3 444.51 441.17 4.50 o -1 -2 3 1129.01 1282.92 16.57 o 0 -2 3 839.71 892.71 8.94 o 1 -2 3 1355.05 1417.19 15.10 o 2 -2 3 980.27 1142.75 53.12 o 3 -2 3 49.61 55.83 1.41 o 4 -2 3 146.41 144.28 2.74 o 5 -2 3 232.89 227.20 4.25 o 6 -2 3 23.09 25.06 1.72 o -6 -1 3 25.04 27.36 0.72 o -5 -1 3 324.22 321.78 2.97 o -4 -1 3 1042.52 1039.62 9.62 o -3 -1 3 162.14 147.59 1.60 o -2 -1 3 129.36 109.96 1.36 o -1 -1 3 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