#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:28:35 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181052 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/32/2213252.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213252_Fobs loop_ _publ_author_name 'Fun, Hoong-Kun' 'Chantrapromma, Suchada' 'Patil, P. S.' 'Dharmaprakash, S. M.' _publ_section_title ; 1-(4-Bromophenyl)-3-(3-methyl-2-thienyl)prop-2-en-1-one ; _journal_coeditor_code CI2377 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2724 _journal_page_last o2725 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 90.736 _cell_angle_beta 90.731 _cell_angle_gamma 93.942 _cell_length_a 7.4329 _cell_length_b 17.3541 _cell_length_c 19.2551 _exptl_crystal_F_000 1232.00 _reflns_d_resolution_high 0.7107 _cod_data_source_file ci2377Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' patil98m in P-1 (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 788.85 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 769.47 753.22 35.00 o 2 0 0 22358.69 22624.13 474.17 o 3 0 0 2703.28 2526.05 53.52 o 4 0 0 5500.84 5327.50 126.42 o 5 0 0 1141.05 1172.79 33.98 o 6 0 0 3390.47 3118.67 62.71 o 7 0 0 2.37 23.68 45.69 o 8 0 0 186.14 291.69 56.30 o 9 0 0 398.31 460.32 67.44 o 10 0 0 107.22 159.85 104.16 o -10 1 0 93.42 215.46 81.11 o -9 1 0 356.95 467.44 67.42 o -8 1 0 1556.14 1518.60 89.36 o -7 1 0 107.20 81.35 32.98 o -6 1 0 934.74 934.87 33.05 o -5 1 0 539.39 486.30 20.13 o -4 1 0 1936.19 1822.79 36.32 o -3 1 0 39479.10 38232.97 588.61 o -2 1 0 1.85 -18.16 13.38 o -1 1 0 24326.22 23693.75 468.18 o 0 1 0 10.09 -1.14 0.57 o 2 1 0 1011.98 986.96 35.94 o 3 1 0 3784.26 3778.81 107.46 o 4 1 0 199.30 136.36 17.68 o 5 1 0 11968.95 11539.88 179.00 o 6 1 0 1115.69 1097.22 39.48 o 7 1 0 568.83 582.49 49.43 o 8 1 0 285.09 476.83 62.28 o 9 1 0 47.03 106.55 61.66 o 10 1 0 367.23 405.90 73.10 o -10 2 0 777.65 711.87 196.65 o -9 2 0 218.50 229.27 61.26 o -8 2 0 8.63 17.20 35.63 o -7 2 0 1392.59 1306.38 59.42 o -6 2 0 2335.11 2179.17 49.21 o -5 2 0 77.98 69.89 15.53 o -4 2 0 24030.64 22023.63 318.00 o -3 2 0 1610.36 1601.23 33.58 o -2 2 0 15802.17 16077.43 279.88 o -1 2 0 230.57 246.74 26.04 o 0 2 0 7598.30 4873.80 184.41 o 1 2 0 1027.50 1060.93 46.67 o 2 2 0 622285.00 569014.38 19924.93 o 3 2 0 5226.67 4875.83 135.63 o 4 2 0 17341.01 17639.31 288.48 o 5 2 0 3866.78 3720.09 67.55 o 6 2 0 350.05 352.90 27.11 o 7 2 0 215.30 210.05 43.37 o 8 2 0 124.64 99.17 48.31 o 9 2 0 0.74 -2.92 60.04 o 10 2 0 17.62 75.53 86.80 o -10 3 0 197.56 391.35 69.76 o -9 3 0 1.17 -84.84 56.64 o -8 3 0 169.21 208.93 39.68 o -7 3 0 3120.62 3036.00 78.56 o -6 3 0 3554.61 3307.56 64.49 o -5 3 0 1346.63 1355.03 32.30 o -4 3 0 1257.36 1153.46 28.61 o -3 3 0 43.40 41.54 10.39 o -2 3 0 574.59 596.38 39.94 o -1 3 0 45720.68 46407.03 1202.96 o 0 3 0 2.09 -12.52 15.37 o 1 3 0 31375.24 31169.58 650.71 o 2 3 0 4822.91 5518.10 207.18 o 3 3 0 766.13 730.57 72.85 o 4 3 0 299.19 335.94 19.11 o 5 3 0 136.01 192.84 19.56 o 6 3 0 145.74 116.69 42.14 o 7 3 0 1076.23 1105.37 60.22 o 8 3 0 183.19 215.54 51.07 o 9 3 0 105.30 89.89 63.53 o 10 3 0 21.38 125.63 71.15 o -10 4 0 27.30 66.85 63.35 o -9 4 0 710.40 834.70 73.79 o -8 4 0 3198.47 2915.36 90.03 o -7 4 0 853.24 807.69 41.53 o -6 4 0 661.44 680.75 29.04 o -5 4 0 1834.81 1653.69 40.16 o -4 4 0 5513.44 5163.29 77.21 o -3 4 0 169.24 197.57 12.67 o -2 4 0 82617.21 79989.78 1185.05 o -1 4 0 28.45 34.86 8.46 o 0 4 0 13309.73 13427.45 352.96 o 1 4 0 863.42 804.94 25.50 o 2 4 0 727.40 733.10 27.49 o 3 4 0 1818.22 1742.35 68.98 o 4 4 0 93507.17 97038.88 1552.93 o 5 4 0 3547.93 3490.64 60.99 o 6 4 0 5212.83 5431.27 105.66 o 7 4 0 2539.20 2526.85 90.17 o 8 4 0 140.28 112.56 51.52 o 9 4 0 3.75 -9.35 54.70 o 10 4 0 23.51 -15.36 71.30 o -10 5 0 59.79 98.04 117.25 o -9 5 0 326.08 377.25 63.37 o -8 5 0 753.89 819.45 50.22 o -7 5 0 40.41 -6.54 28.85 o -6 5 0 46.09 25.38 20.58 o -5 5 0 10255.64 9629.06 152.37 o -4 5 0 3082.28 2821.05 47.55 o -3 5 0 3874.82 3830.16 67.85 o -2 5 0 392.77 382.26 17.18 o -1 5 0 85.36 91.98 13.33 o 0 5 0 20.14 37.95 10.20 o 1 5 0 9121.65 9020.86 166.03 o 2 5 0 23.95 21.42 13.09 o 3 5 0 8986.17 8742.04 166.57 o 4 5 0 6840.47 7383.16 129.69 o 5 5 0 1266.25 1191.00 45.48 o 6 5 0 31.34 23.12 25.56 o 7 5 0 1288.50 1356.74 72.17 o 8 5 0 2.86 4.14 51.20 o 9 5 0 3.66 56.73 55.98 o 10 5 0 2.81 125.67 65.65 o -10 6 0 130.37 23.79 54.36 o -9 6 0 35.24 30.54 43.30 o -8 6 0 37.36 15.97 36.82 o -7 6 0 1760.91 1776.20 59.26 o -6 6 0 6432.20 6059.40 103.50 o -5 6 0 1346.67 1224.02 38.91 o -4 6 0 3388.67 3121.92 63.86 o -3 6 0 605.54 589.47 19.33 o -2 6 0 2821.74 2733.18 57.36 o -1 6 0 14.33 4.55 12.82 o 0 6 0 89049.55 89143.34 1839.51 o 1 6 0 2067.32 1877.65 85.37 o 2 6 0 7437.12 7566.67 144.54 o 3 6 0 2291.99 2151.58 60.51 o 4 6 0 185.12 182.91 20.22 o 5 6 0 491.53 582.03 25.01 o 6 6 0 8347.46 8657.02 132.59 o 7 6 0 1209.27 1184.46 78.48 o 8 6 0 434.96 410.06 92.49 o 9 6 0 736.59 914.82 89.70 o -10 7 0 424.44 533.31 105.30 o -9 7 0 516.30 592.66 57.72 o -8 7 0 483.81 553.84 55.29 o -7 7 0 882.49 932.50 50.19 o -6 7 0 1027.21 978.39 38.17 o -5 7 0 9.82 -24.71 17.57 o -4 7 0 2.65 -3.15 15.18 o -3 7 0 14104.01 13545.11 205.54 o -2 7 0 132.75 179.74 11.42 o -1 7 0 4186.84 4197.50 118.74 o 0 7 0 816.11 861.22 31.95 o 1 7 0 344.36 376.15 28.10 o 2 7 0 63.21 70.44 14.47 o 3 7 0 17.23 1.04 15.90 o 4 7 0 32.88 15.09 18.85 o 5 7 0 106.57 78.36 23.05 o 6 7 0 3768.07 4012.64 89.36 o 7 7 0 589.85 627.94 149.12 o 8 7 0 27.42 52.63 67.38 o 9 7 0 1109.27 1246.86 297.11 o -10 8 0 96.16 150.83 95.62 o -9 8 0 166.61 252.35 57.10 o -8 8 0 420.27 448.70 52.63 o -7 8 0 13.59 42.82 30.97 o -6 8 0 27.98 -6.53 23.85 o -5 8 0 1464.15 1396.46 39.47 o -4 8 0 7528.91 7172.81 116.65 o -3 8 0 523.35 534.50 20.15 o -2 8 0 4207.50 3909.09 73.91 o -1 8 0 4.80 -3.83 10.09 o 0 8 0 66.43 67.23 17.21 o 1 8 0 311.04 374.88 19.29 o 2 8 0 21987.19 21870.42 355.23 o 3 8 0 4177.22 4065.97 78.44 o 4 8 0 2792.27 2889.98 63.58 o 5 8 0 2571.39 2553.22 79.29 o 6 8 0 702.53 811.08 38.83 o 7 8 0 17.51 56.43 53.11 o 8 8 0 265.18 159.34 72.93 o 9 8 0 351.50 411.86 136.89 o -9 9 0 63.80 122.09 54.35 o -8 9 0 810.77 898.04 66.18 o -7 9 0 814.88 853.46 79.77 o -6 9 0 1059.90 1065.13 40.55 o -5 9 0 245.15 211.56 22.32 o -4 9 0 465.92 458.45 22.28 o -3 9 0 32.31 18.88 8.68 o -2 9 0 1.82 0.97 13.65 o -1 9 0 5074.87 4862.24 97.75 o 0 9 0 1279.39 1277.69 33.88 o 1 9 0 1908.39 2025.57 45.04 o 2 9 0 3957.00 4054.50 76.16 o 3 9 0 759.69 730.26 29.35 o 4 9 0 47.78 42.11 22.02 o 5 9 0 1827.56 1789.85 52.83 o 6 9 0 25.09 25.82 35.65 o 7 9 0 861.84 896.35 73.63 o 8 9 0 831.67 936.01 155.38 o 9 9 0 46.58 72.61 84.15 o -9 10 0 756.14 929.21 72.85 o -8 10 0 11.73 66.11 75.98 o -7 10 0 257.33 230.79 40.74 o -6 10 0 1061.78 1048.21 55.00 o -5 10 0 53.24 52.33 32.86 o -4 10 0 126.71 145.73 22.43 o -3 10 0 131.95 132.76 15.17 o -2 10 0 4544.65 4616.77 86.87 o -1 10 0 472.23 517.07 28.10 o 0 10 0 1191.79 1140.98 35.86 o 1 10 0 170.56 179.96 16.66 o 2 10 0 1884.33 1719.02 39.88 o 3 10 0 351.32 311.99 29.93 o 4 10 0 710.49 791.53 48.99 o 5 10 0 2249.59 2203.50 69.11 o 6 10 0 378.47 439.72 43.21 o 7 10 0 1379.67 1514.40 78.11 o 8 10 0 614.42 644.34 88.70 o 9 10 0 4.58 -8.24 86.54 o -9 11 0 643.57 809.07 69.42 o -8 11 0 499.01 512.78 59.53 o -7 11 0 1.59 2.37 37.22 o -6 11 0 516.42 550.51 75.96 o -5 11 0 1076.41 1037.98 45.43 o -4 11 0 454.64 500.74 31.01 o -3 11 0 731.26 676.37 59.40 o -2 11 0 13.63 51.49 22.10 o -1 11 0 8.40 -8.75 13.86 o 0 11 0 1.25 15.94 12.76 o 1 11 0 117.40 85.34 14.89 o 2 11 0 3390.51 3204.06 61.07 o 3 11 0 10.40 1.19 20.83 o 4 11 0 4654.77 4562.46 91.95 o 5 11 0 796.02 781.65 46.63 o 6 11 0 199.25 161.90 41.36 o 7 11 0 1506.83 1773.25 87.06 o 8 11 0 24.34 53.66 80.29 o -9 12 0 300.08 323.27 60.92 o -8 12 0 100.70 115.55 51.30 o -7 12 0 1354.03 1308.57 65.08 o -6 12 0 824.19 797.09 64.60 o -5 12 0 192.85 186.67 32.75 o -4 12 0 1123.67 931.90 61.29 o -3 12 0 0.09 -21.01 29.89 o -2 12 0 833.77 803.04 49.65 o -1 12 0 163.65 144.57 25.63 o 0 12 0 1241.46 1323.76 37.70 o 1 12 0 3584.81 3539.89 94.17 o 2 12 0 16.85 7.47 19.98 o 3 12 0 178.22 177.47 25.47 o 4 12 0 1913.49 1835.62 69.65 o 5 12 0 71.44 23.80 35.74 o 6 12 0 589.19 555.56 48.95 o 7 12 0 410.92 537.34 64.80 o 8 12 0 1.45 -35.15 79.80 o -9 13 0 10.53 88.63 54.91 o -8 13 0 438.96 504.21 57.71 o -7 13 0 799.75 848.25 71.46 o -6 13 0 283.43 331.19 38.18 o -5 13 0 18.59 108.01 47.54 o -4 13 0 57.12 10.57 54.07 o -3 13 0 1194.74 1206.81 56.25 o -2 13 0 172.98 166.68 39.29 o -1 13 0 3521.84 3260.95 196.23 o 0 13 0 116.81 82.13 28.21 o 1 13 0 464.10 438.52 24.62 o 2 13 0 20.64 24.19 24.34 o 3 13 0 2918.12 2793.95 74.06 o 4 13 0 2494.07 2357.16 72.62 o 5 13 0 681.34 693.58 52.19 o 6 13 0 2288.03 2424.47 81.21 o 7 13 0 505.91 590.11 98.44 o 8 13 0 132.06 223.76 88.19 o -8 14 0 73.54 186.69 80.25 o -7 14 0 173.27 262.26 59.88 o -6 14 0 179.17 147.36 54.17 o -5 14 0 636.68 684.51 62.56 o -4 14 0 5014.30 4913.07 229.38 o -3 14 0 23.72 51.41 44.46 o -2 14 0 221.92 136.07 43.23 o -1 14 0 32.02 -22.41 44.11 o 0 14 0 1872.76 1313.27 279.18 o 1 14 0 392.24 407.05 49.12 o 2 14 0 21.05 0.28 27.03 o 3 14 0 4388.70 4178.75 97.07 o 4 14 0 91.38 88.16 34.90 o 5 14 0 91.73 108.34 40.39 o 6 14 0 868.50 1042.43 75.19 o 7 14 0 1.38 -62.34 57.84 o 8 14 0 681.34 773.23 100.49 o -8 15 0 401.11 498.02 94.48 o -7 15 0 195.85 202.10 60.04 o -6 15 0 460.28 446.65 62.63 o -5 15 0 36.59 0.27 50.07 o -4 15 0 16.33 107.00 70.01 o -3 15 0 18.61 70.58 48.06 o -2 15 0 3.61 1.99 41.65 o -1 15 0 686.95 705.77 55.94 o 1 15 0 2924.66 2851.49 81.85 o 2 15 0 308.69 348.03 43.81 o 3 15 0 837.87 728.47 50.61 o 4 15 0 225.43 184.04 50.99 o 5 15 0 2674.87 2668.88 82.38 o 6 15 0 1020.69 1118.57 113.53 o 7 15 0 913.11 973.25 107.29 o -8 16 0 69.02 121.23 89.93 o -7 16 0 3.13 10.33 60.92 o -6 16 0 0.79 -36.31 55.32 o -5 16 0 51.48 95.64 67.45 o -4 16 0 206.80 116.11 77.41 o -3 16 0 23.20 58.48 51.11 o -2 16 0 8154.11 7359.50 214.19 o -1 16 0 114.38 134.92 47.81 o 0 16 0 82.49 47.23 26.18 o 1 16 0 12.82 16.90 43.26 o 2 16 0 1407.28 1333.39 63.68 o 3 16 0 175.36 262.22 44.12 o 4 16 0 203.37 265.57 49.73 o 5 16 0 2146.17 2243.55 122.62 o 6 16 0 137.95 17.96 46.41 o 7 16 0 15.94 -51.64 76.43 o -7 17 0 41.25 17.31 62.16 o -6 17 0 211.44 209.96 110.99 o -5 17 0 668.44 676.80 85.38 o -4 17 0 58.43 125.79 82.53 o -3 17 0 1207.25 1361.89 155.10 o -2 17 0 7.11 21.21 46.66 o -1 17 0 79.32 68.54 48.47 o 0 17 0 8.80 35.86 67.16 o 1 17 0 45.25 24.79 48.69 o 2 17 0 2139.80 2139.50 75.00 o 3 17 0 857.63 920.52 59.74 o 4 17 0 235.71 297.43 51.49 o 5 17 0 409.52 438.84 70.30 o 6 17 0 286.59 206.37 75.07 o -7 18 0 349.95 447.96 74.06 o -6 18 0 1307.61 1511.60 93.86 o -5 18 0 0.20 -37.43 60.27 o -4 18 0 234.50 241.33 91.07 o -3 18 0 2.52 1.65 64.89 o -2 18 0 304.04 340.02 57.80 o -1 18 0 755.85 665.04 159.08 o 0 18 0 5350.78 5152.12 239.62 o 1 18 0 458.62 424.12 59.56 o 2 18 0 170.92 197.59 63.18 o 3 18 0 3.38 54.88 42.85 o 4 18 0 460.41 546.59 55.50 o 5 18 0 38.40 0.94 73.83 o 6 18 0 172.51 156.29 59.94 o -7 19 0 281.67 264.90 74.25 o -6 19 0 1.77 -43.42 66.02 o -5 19 0 18.91 -7.51 63.39 o -4 19 0 13.69 -35.64 17.82 o -3 19 0 401.40 387.50 109.85 o -2 19 0 338.07 373.84 61.75 o -1 19 0 3302.11 1961.93 121.23 o 0 19 0 3.45 121.69 38.08 o 1 19 0 344.18 380.56 75.41 o 2 19 0 8.89 -16.34 141.44 o 3 19 0 104.20 72.19 59.35 o 4 19 0 857.82 986.61 62.32 o 5 19 0 88.40 50.62 53.95 o -6 20 0 34.58 88.93 81.39 o -5 20 0 29.79 21.95 67.77 o -3 20 0 0.03 -64.67 68.30 o -2 20 0 1074.83 927.75 188.40 o -1 20 0 38.46 190.10 87.65 o 0 20 0 339.10 416.66 59.84 o 1 20 0 782.12 804.11 73.35 o 2 20 0 1912.21 1899.44 102.50 o 3 20 0 392.77 357.38 68.51 o 4 20 0 10.64 -88.21 65.47 o 5 20 0 5.56 -45.37 53.20 o -5 21 0 58.83 34.25 71.21 o -4 21 0 14.47 -34.86 39.27 o -3 21 0 145.07 71.91 112.98 o -2 21 0 5.04 -34.55 71.43 o -1 21 0 29.50 -4.10 38.99 o 0 21 0 1314.72 1433.91 88.67 o 1 21 0 2009.01 2300.53 116.65 o 2 21 0 1.44 -56.79 62.28 o 3 21 0 478.56 599.05 77.30 o 4 21 0 14.69 0.86 68.64 o -5 22 0 21.30 -53.49 72.03 o -4 22 0 45.82 126.92 105.30 o -3 22 0 212.24 46.11 66.59 o -1 22 0 6.82 -30.56 21.05 o 0 22 0 1369.91 1395.51 90.61 o 1 22 0 227.83 440.28 73.67 o 2 22 0 140.21 147.47 68.29 o 3 22 0 240.47 287.22 74.02 o -4 23 0 4.70 -6.31 75.41 o -3 23 0 98.06 -60.81 30.40 o -2 23 0 135.51 233.36 107.57 o -1 23 0 230.91 340.36 109.85 o 0 23 0 6.82 94.14 64.70 o 1 23 0 30.00 47.59 94.48 o 2 23 0 1125.89 1148.01 91.09 o -2 24 0 180.69 167.34 111.56 o -1 24 0 683.57 543.78 205.19 o 0 24 0 593.92 619.72 79.78 o 1 24 0 57.65 92.71 87.94 o -1 -24 1 3.35 -37.89 66.35 o 0 -24 1 156.04 123.51 110.42 o 1 -24 1 29.49 63.21 65.87 o 2 -24 1 1045.92 1229.70 94.15 o -2 -23 1 4.13 27.25 67.96 o -1 -23 1 28.80 -19.89 64.73 o 0 -23 1 93.42 64.87 21.16 o 1 -23 1 179.84 281.94 69.68 o 2 -23 1 0.99 35.37 65.95 o 3 -23 1 124.76 -4.43 69.14 o 4 -23 1 272.26 286.67 112.13 o -3 -22 1 32.24 40.78 69.85 o -2 -22 1 577.53 640.31 76.61 o -1 -22 1 456.82 571.50 148.55 o 0 -22 1 232.34 308.49 100.17 o 1 -22 1 13.65 76.79 62.64 o 2 -22 1 694.50 852.17 80.52 o 3 -22 1 5.73 -126.22 63.11 o 4 -22 1 462.63 502.18 77.66 o 5 -22 1 102.44 66.66 54.81 o -4 -21 1 68.65 32.62 69.77 o -3 -21 1 304.24 292.41 69.86 o -2 -21 1 1067.20 1111.79 84.92 o -1 -21 1 978.12 959.01 152.25 o 0 -21 1 104.24 59.79 50.30 o 1 -21 1 891.67 873.48 76.21 o 2 -21 1 10.07 17.76 60.11 o 3 -21 1 741.43 943.61 81.89 o 4 -21 1 2.57 24.57 101.31 o 5 -21 1 27.35 -17.07 49.35 o -5 -20 1 69.13 32.47 69.40 o -4 -20 1 493.67 570.30 75.68 o -3 -20 1 183.21 83.55 63.09 o -2 -20 1 56.66 32.94 62.89 o -1 -20 1 56.54 56.01 53.59 o 0 -20 1 156.07 151.12 113.55 o 1 -20 1 157.85 211.91 59.16 o 2 -20 1 117.03 118.65 83.10 o 3 -20 1 11.11 23.93 59.74 o 4 -20 1 655.11 684.99 76.20 o 5 -20 1 13.26 -2.74 48.09 o 6 -20 1 29.60 -0.23 66.16 o -5 -19 1 514.82 607.01 59.51 o -4 -19 1 30.03 64.24 63.58 o -3 -19 1 73.16 122.57 62.32 o -2 -19 1 107.30 92.14 57.22 o -1 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86.97 57.79 o -6 -7 2 1788.00 1791.24 74.10 o -5 -7 2 9466.44 9532.34 167.52 o -4 -7 2 4856.30 4900.32 92.59 o -3 -7 2 8503.57 7894.95 183.61 o -2 -7 2 5949.86 5754.23 108.15 o -1 -7 2 4758.06 4793.50 76.75 o 0 -7 2 1828.30 1897.31 46.93 o 1 -7 2 3401.65 3633.21 63.20 o 2 -7 2 19908.32 20678.74 288.70 o 3 -7 2 318.27 393.52 18.28 o 4 -7 2 3305.90 3037.86 54.36 o 5 -7 2 7.00 -17.68 17.50 o 6 -7 2 727.43 793.78 32.63 o 7 -7 2 2190.14 2080.14 77.85 o 8 -7 2 657.06 838.16 63.67 o 9 -7 2 1650.97 1800.78 95.00 o 10 -7 2 52.57 94.80 49.83 o -9 -6 2 70.39 174.93 94.77 o -8 -6 2 6019.91 5920.50 293.69 o -7 -6 2 9.66 24.08 53.75 o -6 -6 2 30.90 32.51 31.61 o -5 -6 2 476.39 414.13 34.75 o -4 -6 2 206.82 181.19 24.86 o -3 -6 2 922.40 876.26 29.74 o -2 -6 2 668.99 654.06 35.35 o -1 -6 2 10494.66 10500.15 192.55 o 0 -6 2 181.18 195.01 11.92 o 1 -6 2 8763.00 8641.86 138.98 o 2 -6 2 1289.49 1205.52 24.84 o 3 -6 2 1974.25 1837.84 36.69 o 4 -6 2 1297.89 1090.87 34.50 o 5 -6 2 148.55 151.86 18.74 o 6 -6 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1201.98 36.50 o -3 -4 2 5518.53 4691.92 93.86 o -2 -4 2 452.65 414.00 23.01 o -1 -4 2 592.97 687.59 21.73 o 0 -4 2 3737.89 3590.52 415.78 o 1 -4 2 19204.89 19962.40 341.23 o 2 -4 2 7687.84 7609.02 121.00 o 3 -4 2 11864.13 10980.01 207.30 o 4 -4 2 1939.47 1778.00 62.73 o 5 -4 2 158.09 128.06 17.02 o 6 -4 2 1276.77 1195.00 36.07 o 7 -4 2 27.30 5.86 31.86 o 8 -4 2 1816.05 1784.32 71.39 o 9 -4 2 18.34 16.64 40.95 o 10 -4 2 272.31 269.45 65.60 o -10 -3 2 5.20 39.99 60.97 o -9 -3 2 23.57 67.38 54.64 o -8 -3 2 737.66 685.46 76.83 o -7 -3 2 131.98 130.17 42.10 o -6 -3 2 10333.76 9843.68 174.30 o -5 -3 2 4.69 -10.59 16.75 o -4 -3 2 28.65 64.95 16.58 o -3 -3 2 4132.76 4218.21 126.21 o -2 -3 2 11509.87 12144.64 396.71 o -1 -3 2 20106.14 20889.67 738.21 o 0 -3 2 34702.70 38709.97 1002.13 o 1 -3 2 4.97 7.66 7.56 o 2 -3 2 29416.15 28907.89 443.94 o 3 -3 2 10675.81 10175.22 188.61 o 4 -3 2 1276.42 1080.22 27.38 o 5 -3 2 5217.00 4809.62 89.32 o 6 -3 2 4463.60 4292.85 84.07 o 7 -3 2 884.05 928.03 48.53 o 8 -3 2 871.52 1030.02 55.09 o 9 -3 2 0.36 -51.65 56.16 o 10 -3 2 207.79 261.34 70.50 o -10 -2 2 469.37 483.84 182.13 o -9 -2 2 399.59 468.98 59.76 o -8 -2 2 9.41 -2.32 46.08 o -7 -2 2 1122.70 1142.06 59.24 o -6 -2 2 1254.46 1220.29 43.48 o -5 -2 2 269.99 289.36 24.94 o -4 -2 2 29804.71 30752.74 558.83 o -3 -2 2 4009.78 3690.96 85.67 o -2 -2 2 7382.17 7306.94 193.46 o -1 -2 2 13042.37 12626.46 449.64 o 0 -2 2 4263.19 4925.60 186.12 o 1 -2 2 8866.44 9426.79 187.49 o 2 -2 2 16653.79 16507.93 293.78 o 3 -2 2 5147.72 4970.70 76.04 o 4 -2 2 12928.75 12491.89 183.54 o 5 -2 2 5840.99 5471.37 87.73 o 6 -2 2 846.57 792.78 37.02 o 7 -2 2 142.00 171.88 34.52 o 8 -2 2 352.87 393.45 44.03 o 9 -2 2 5.50 84.31 92.49 o 10 -2 2 181.29 225.22 87.94 o -10 -1 2 147.85 108.18 104.16 o -9 -1 2 65.10 38.26 59.23 o -8 -1 2 23.26 47.55 73.44 o -7 -1 2 5.19 -4.15 32.65 o -6 -1 2 2730.48 2493.99 53.04 o -5 -1 2 31.69 19.87 16.04 o -4 -1 2 31754.65 31036.32 499.78 o -3 -1 2 4.28 34.85 13.22 o -2 -1 2 3259.82 3006.88 84.85 o -1 -1 2 25906.57 25977.48 953.93 o 1 -1 2 4710.48 4979.62 208.32 o 2 -1 2 38475.79 38856.39 742.67 o 3 -1 2 2859.36 2676.24 55.40 o 4 -1 2 13106.27 12228.37 204.03 o 5 -1 2 3196.24 3038.89 70.41 o 6 -1 2 407.15 404.74 30.39 o 7 -1 2 3557.47 3320.92 95.48 o 8 -1 2 391.81 405.91 44.03 o 9 -1 2 279.18 303.86 64.66 o 10 -1 2 60.23 89.93 67.91 o -10 0 2 42.85 96.07 66.05 o -9 0 2 35.23 53.11 57.91 o -8 0 2 748.92 865.72 68.80 o -7 0 2 2590.19 2455.04 74.18 o -6 0 2 73.17 74.89 19.27 o -5 0 2 12589.21 11960.68 166.63 o -4 0 2 45.67 24.53 11.87 o -3 0 2 519.87 504.23 38.65 o -2 0 2 43183.36 44321.75 924.40 o -1 0 2 6314.65 6145.86 146.69 o 0 0 2 7121.90 7760.67 459.60 o 2 0 2 15454.05 15621.30 683.86 o 3 0 2 6902.71 6822.10 147.35 o 4 0 2 12433.78 11841.02 221.28 o 5 0 2 28.07 29.32 19.09 o 6 0 2 8689.10 8408.34 166.54 o 7 0 2 733.12 763.21 46.34 o 8 0 2 215.17 84.73 54.86 o 9 0 2 239.59 231.40 63.37 o 10 0 2 18.07 38.81 88.51 o -10 1 2 23.73 106.88 66.58 o -9 1 2 3.14 15.82 57.40 o -8 1 2 2918.50 2977.06 117.92 o -7 1 2 280.96 313.39 31.47 o -6 1 2 447.57 450.59 31.31 o -5 1 2 456.25 392.84 17.54 o -4 1 2 5080.67 4568.84 68.64 o -3 1 2 863.47 881.70 24.07 o -2 1 2 50280.43 48729.82 841.57 o -1 1 2 157.43 180.97 14.51 o 0 1 2 8452.53 9182.06 340.70 o 1 1 2 38492.25 41646.88 1091.88 o 2 1 2 11982.34 12066.34 311.41 o 3 1 2 1375.65 1190.12 35.71 o 4 1 2 9929.33 9844.50 186.09 o 5 1 2 2127.57 2032.78 49.45 o 6 1 2 3617.50 3447.43 74.01 o 7 1 2 563.46 546.96 43.37 o 8 1 2 18.58 129.59 55.51 o 9 1 2 722.23 775.56 100.17 o 10 1 2 0.53 38.61 143.15 o -10 2 2 418.76 440.60 71.48 o -9 2 2 9.71 -34.15 55.88 o -8 2 2 637.55 733.20 64.90 o -7 2 2 62.87 3.09 25.98 o -6 2 2 1078.87 1016.51 38.74 o -5 2 2 6238.71 5815.34 82.41 o -4 2 2 1352.29 1309.31 29.43 o -3 2 2 39054.52 36672.22 565.53 o -2 2 2 1842.42 1866.97 39.50 o -1 2 2 6566.06 6289.51 153.43 o 0 2 2 9017.42 9195.94 260.96 o 1 2 2 2425.70 2385.32 54.00 o 2 2 2 4074.78 4014.47 109.67 o 3 2 2 7719.97 7565.48 163.14 o 4 2 2 6263.30 6605.55 129.45 o 5 2 2 961.54 933.20 30.39 o 6 2 2 3238.63 3255.81 80.68 o 7 2 2 467.94 440.27 56.30 o 8 2 2 2476.93 2400.94 110.86 o 9 2 2 42.34 195.64 85.66 o 10 2 2 48.80 33.43 70.41 o -10 3 2 9.16 23.86 72.00 o -9 3 2 22.04 98.05 84.24 o -8 3 2 243.54 269.31 55.83 o -7 3 2 100.90 112.21 27.00 o -6 3 2 13585.86 12867.44 201.56 o -5 3 2 436.34 393.79 20.21 o -4 3 2 3207.56 3003.89 55.14 o -3 3 2 4537.14 4156.86 72.23 o -2 3 2 3075.10 2869.05 56.96 o -1 3 2 3748.16 3837.34 158.23 o 0 3 2 30224.32 32846.05 853.02 o 1 3 2 70.54 125.86 16.65 o 2 3 2 2927.43 2918.91 83.69 o 3 3 2 20387.76 20253.24 521.63 o 4 3 2 13334.52 13580.31 207.23 o 5 3 2 3298.30 3097.50 59.81 o 6 3 2 128.43 161.04 29.93 o 7 3 2 725.58 738.32 55.34 o 8 3 2 480.41 580.40 81.96 o 9 3 2 77.64 117.69 66.63 o 10 3 2 0.59 45.83 131.76 o -10 4 2 95.10 218.07 92.77 o -9 4 2 1440.96 1585.61 151.68 o -8 4 2 793.49 805.97 51.24 o -7 4 2 446.08 430.62 31.89 o -6 4 2 1783.66 1792.11 45.88 o -5 4 2 2.48 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745.26 810.73 63.98 o 9 5 2 186.99 189.76 61.65 o 10 5 2 7.21 61.83 76.72 o -10 6 2 3.06 58.34 62.79 o -9 6 2 24.23 35.80 57.21 o -8 6 2 12.22 -4.68 33.84 o -7 6 2 2958.36 2838.27 76.75 o -6 6 2 882.64 866.64 35.92 o -5 6 2 2857.52 2541.88 53.58 o -4 6 2 1528.06 1675.36 35.76 o -3 6 2 879.51 876.40 26.36 o -2 6 2 3126.81 2898.73 143.52 o -1 6 2 3069.92 2984.57 75.61 o 0 6 2 1313.34 1320.27 39.42 o 1 6 2 17135.84 17527.89 468.27 o 2 6 2 605.66 629.50 22.76 o 3 6 2 2557.59 2615.67 54.84 o 4 6 2 3718.92 3532.88 65.59 o 5 6 2 3140.51 3113.97 57.52 o 6 6 2 1191.45 1294.79 64.90 o 7 6 2 24.29 48.20 47.40 o 8 6 2 136.32 118.00 59.74 o 9 6 2 151.43 191.35 64.36 o -10 7 2 78.34 270.36 100.74 o -9 7 2 895.13 1044.54 76.04 o -8 7 2 997.57 1042.13 49.96 o -7 7 2 1441.65 1445.91 55.81 o -6 7 2 12.81 37.61 24.53 o -5 7 2 37.28 24.25 19.40 o -4 7 2 294.31 274.51 19.71 o -3 7 2 173.77 81.68 14.13 o -2 7 2 20498.01 20317.95 321.68 o -1 7 2 25.49 6.96 11.94 o 0 7 2 3032.67 2951.44 73.64 o 1 7 2 13761.12 13468.90 223.77 o 2 7 2 4946.94 4900.25 81.13 o 3 7 2 3407.11 3369.11 66.99 o 4 7 2 185.05 160.08 20.05 o 5 7 2 10.06 17.97 20.71 o 6 7 2 446.93 470.70 42.66 o 7 7 2 921.37 998.88 75.53 o 8 7 2 1541.99 1736.58 89.11 o 9 7 2 43.41 61.50 63.27 o -10 8 2 287.98 194.09 88.79 o -9 8 2 72.16 -42.51 32.79 o -8 8 2 144.05 147.42 43.22 o -7 8 2 7.07 16.38 31.30 o -6 8 2 5.53 -32.89 24.13 o -5 8 2 1779.37 1623.14 51.56 o -4 8 2 656.82 657.25 29.83 o -3 8 2 3342.37 2848.42 84.00 o -2 8 2 133.71 249.84 21.00 o -1 8 2 3797.51 3769.08 72.46 o 0 8 2 924.93 940.40 37.13 o 1 8 2 150.31 151.63 14.41 o 2 8 2 6.67 1.74 13.85 o 3 8 2 1739.33 1955.85 47.73 o 4 8 2 136.29 142.05 20.78 o 5 8 2 87.11 102.46 31.27 o 6 8 2 681.64 738.36 45.72 o 7 8 2 2541.12 2602.77 122.36 o 8 8 2 250.68 201.37 73.93 o 9 8 2 371.18 387.79 88.38 o -9 9 2 33.35 50.70 53.64 o -8 9 2 41.12 9.95 42.41 o -7 9 2 1492.10 1413.19 147.45 o -6 9 2 1871.39 1550.52 67.86 o -5 9 2 895.47 879.89 34.97 o -4 9 2 58.20 54.63 18.13 o -3 9 2 220.64 238.54 24.14 o -2 9 2 2.95 0.52 16.28 o -1 9 2 42.76 104.83 16.67 o 0 9 2 3829.57 3978.97 76.16 o 1 9 2 152.16 138.21 20.62 o 2 9 2 27.21 47.27 15.64 o 3 9 2 6735.75 6801.56 122.43 o 4 9 2 5718.12 5527.21 104.89 o 5 9 2 612.76 625.83 33.74 o 6 9 2 2627.02 2554.35 99.73 o 7 9 2 19.58 2.85 66.54 o 8 9 2 651.50 712.42 131.48 o 9 9 2 108.91 72.84 85.00 o -9 10 2 860.83 924.74 72.79 o -8 10 2 249.85 221.49 47.35 o -7 10 2 29.26 59.19 39.46 o -6 10 2 566.59 591.25 49.74 o -5 10 2 30.40 -1.09 27.36 o -4 10 2 269.28 270.99 29.23 o -3 10 2 31.90 29.01 20.18 o -2 10 2 200.95 196.57 32.29 o -1 10 2 217.53 217.25 22.69 o 0 10 2 373.87 288.17 24.68 o 1 10 2 3706.43 3642.66 89.24 o 2 10 2 24.47 26.44 16.48 o 3 10 2 1093.34 1103.37 39.37 o 4 10 2 253.19 268.75 27.53 o 5 10 2 12.43 17.79 26.70 o 6 10 2 68.65 96.51 38.42 o 7 10 2 160.12 79.20 95.05 o 8 10 2 1.17 42.86 76.11 o 9 10 2 725.25 1026.04 170.18 o -9 11 2 962.89 1148.47 79.29 o -8 11 2 9.20 -11.72 44.40 o -7 11 2 461.34 473.60 47.62 o -6 11 2 1.06 -14.64 35.31 o -5 11 2 983.59 1035.08 86.61 o -4 11 2 578.49 595.89 36.46 o -3 11 2 117.74 108.75 25.35 o -2 11 2 367.11 456.14 28.59 o -1 11 2 1243.55 1175.52 37.59 o 0 11 2 248.80 215.72 21.36 o 1 11 2 60.93 88.75 16.34 o 2 11 2 19.53 -6.25 16.56 o 3 11 2 548.89 578.23 30.80 o 4 11 2 1656.65 1687.74 51.55 o 5 11 2 1675.93 1708.63 62.76 o 6 11 2 2381.72 2566.01 81.07 o 7 11 2 4.78 -2.95 110.70 o 8 11 2 2436.78 2476.88 136.88 o -9 12 2 64.61 -4.03 58.91 o -8 12 2 466.97 625.66 55.25 o -7 12 2 847.89 888.39 56.06 o -6 12 2 17.23 76.49 46.50 o -5 12 2 4.26 1.55 34.00 o -4 12 2 446.49 444.95 38.24 o -3 12 2 77.29 114.25 26.23 o -2 12 2 1897.11 1863.01 63.75 o -1 12 2 618.32 639.69 33.98 o 0 12 2 78.63 58.95 23.13 o 1 12 2 1462.86 1445.09 44.61 o 2 12 2 639.53 612.82 31.88 o 3 12 2 989.52 1054.76 40.96 o 4 12 2 47.08 13.36 31.86 o 5 12 2 2157.44 2122.69 71.40 o 6 12 2 240.66 235.19 44.50 o 7 12 2 224.98 164.86 78.17 o 8 12 2 70.65 71.05 83.90 o -9 13 2 412.25 656.85 74.85 o -8 13 2 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