#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/32/2213282.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213282_Fobs loop_ _publ_author_name 'Herrera-Alvarez, Cesar' 'Hern\'andez-Ortega, Sim\'on' 'Morales-Morales, David' _publ_section_title ; C---H···F, C---F···\p and C---F···F---C interactions in a palladium(II) benzenethiolate complex ; _journal_coeditor_code DN2163 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1490 _journal_page_last m1491 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.665 _cell_angle_gamma 90.000 _cell_length_a 19.7191 _cell_length_b 22.0781 _cell_length_c 19.7875 _exptl_crystal_F_000 4224.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file dn2163Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 074MMD07 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 773.08 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 55523.38 61226.54 1351.59 o 4 0 0 241403.14 269076.47 5485.15 o 6 0 0 391.40 412.51 220.07 o 8 0 0 3858.81 3677.46 254.01 o 10 0 0 8548.62 7858.82 797.58 o 12 0 0 4477.09 4197.46 676.19 o 14 0 0 42.93 52.28 347.02 o 16 0 0 3706.63 3147.68 845.89 o 18 0 0 8799.14 9107.63 1195.42 o 20 0 0 11337.62 12191.20 1476.13 o 22 0 0 637.03 1069.06 727.11 o 2 1 0 16494.97 18946.47 435.44 o 3 1 0 12840.04 12485.36 492.45 o 4 1 0 21411.10 21210.75 558.42 o 5 1 0 13347.11 13627.06 505.02 o 6 1 0 6951.49 6451.66 230.15 o 7 1 0 3777.48 3356.60 181.75 o 8 1 0 109.77 198.08 94.87 o 9 1 0 3834.46 4004.71 272.51 o 10 1 0 12410.46 12756.51 544.68 o 11 1 0 3630.42 4053.32 465.48 o 12 1 0 13675.74 13366.46 800.39 o 13 1 0 1138.60 1081.18 344.40 o 14 1 0 2984.23 2590.17 517.85 o 15 1 0 3812.69 4341.42 640.60 o 16 1 0 5757.15 5691.65 700.92 o 17 1 0 791.33 996.84 408.52 o 18 1 0 2117.18 2178.23 533.43 o 19 1 0 1204.99 719.59 401.48 o 20 1 0 203.09 553.13 427.49 o 21 1 0 189.60 434.17 402.89 o 22 1 0 20.98 201.89 386.62 o 0 2 0 1970.63 2017.59 157.66 o 1 2 0 196124.70 219215.55 2325.85 o 2 2 0 36797.88 39583.05 598.14 o 3 2 0 18608.69 18518.30 345.22 o 4 2 0 251753.50 276506.22 2434.21 o 5 2 0 11794.71 12080.15 334.85 o 6 2 0 52105.99 55499.79 722.83 o 7 2 0 7867.33 7422.88 282.56 o 8 2 0 131.33 241.08 102.63 o 9 2 0 1307.46 1477.60 170.45 o 10 2 0 3085.47 3178.22 228.12 o 11 2 0 45.94 231.92 132.09 o 12 2 0 682.59 828.20 183.31 o 13 2 0 10781.86 9912.77 730.82 o 14 2 0 10730.37 10509.71 794.56 o 15 2 0 1724.45 1570.35 441.95 o 16 2 0 540.09 609.28 336.33 o 17 2 0 444.80 342.91 325.10 o 18 2 0 1816.83 2107.42 569.71 o 19 2 0 4138.99 4152.60 755.02 o 20 2 0 3.94 5.26 337.75 o 21 2 0 8764.87 9074.71 948.07 o 22 2 0 807.02 1126.99 509.87 o 1 3 0 34960.85 36767.28 475.11 o 2 3 0 6756.65 6263.55 202.79 o 3 3 0 76210.48 81578.38 1004.54 o 4 3 0 23251.96 22934.85 456.78 o 5 3 0 8224.12 7702.53 287.98 o 6 3 0 36671.91 36048.14 745.90 o 7 3 0 247.55 471.26 122.93 o 8 3 0 214.54 325.98 118.74 o 9 3 0 138.29 183.39 107.79 o 10 3 0 3081.19 3425.35 244.18 o 11 3 0 3609.54 3736.94 259.58 o 12 3 0 6809.47 6632.66 368.72 o 13 3 0 14601.82 13831.27 856.98 o 14 3 0 20410.54 19575.42 1062.54 o 15 3 0 137.73 179.44 278.90 o 16 3 0 1692.29 1759.63 478.92 o 17 3 0 11.29 279.85 327.94 o 18 3 0 191.39 455.73 341.94 o 19 3 0 59.20 164.14 344.29 o 20 3 0 32.93 42.76 349.38 o 21 3 0 8.14 -22.75 330.63 o 22 3 0 550.99 739.49 488.53 o 0 4 0 2493.50 2840.43 200.23 o 1 4 0 4705.37 4714.73 177.69 o 2 4 0 17.29 56.13 66.78 o 3 4 0 39950.66 41258.34 607.69 o 4 4 0 1215.41 1237.57 163.81 o 5 4 0 17548.14 17436.07 454.59 o 6 4 0 2720.62 2491.66 200.86 o 7 4 0 5785.48 5544.11 291.75 o 8 4 0 8452.64 7820.26 351.98 o 9 4 0 2958.64 2905.10 257.07 o 10 4 0 1536.96 1808.49 224.09 o 11 4 0 3774.83 3848.51 303.60 o 12 4 0 8616.19 8453.68 398.48 o 13 4 0 773.49 877.89 325.16 o 14 4 0 531.70 568.61 295.09 o 15 4 0 164.87 315.63 281.27 o 16 4 0 2703.66 3603.60 790.67 o 17 4 0 83.94 118.55 303.80 o 18 4 0 1020.12 1292.82 473.26 o 19 4 0 637.65 704.03 438.58 o 20 4 0 6245.29 8271.80 892.34 o 21 4 0 15.10 -101.27 400.04 o 22 4 0 3370.35 4334.73 856.01 o 1 5 0 88650.46 93496.45 851.15 o 2 5 0 172356.00 187596.41 1409.82 o 3 5 0 7668.32 7371.09 285.88 o 4 5 0 182.40 108.77 94.25 o 5 5 0 39473.94 39628.95 714.02 o 6 5 0 119.45 61.50 98.10 o 7 5 0 37937.43 38694.66 772.47 o 8 5 0 5487.65 4992.32 306.15 o 9 5 0 458.84 496.78 159.89 o 10 5 0 40107.18 39157.23 903.46 o 11 5 0 4950.95 4671.72 326.66 o 12 5 0 28338.04 27845.36 749.71 o 13 5 0 10726.30 10340.08 760.12 o 14 5 0 10971.12 10449.57 793.90 o 15 5 0 19504.26 18031.76 1062.79 o 16 5 0 4988.51 5010.92 669.15 o 17 5 0 68.33 157.51 317.19 o 18 5 0 21.43 122.58 343.38 o 19 5 0 293.65 69.94 372.03 o 20 5 0 869.44 1411.86 505.41 o 21 5 0 299.34 732.04 460.00 o 22 5 0 1134.66 1176.94 543.36 o 0 6 0 102989.59 105070.08 1354.22 o 1 6 0 47382.10 49094.98 665.29 o 2 6 0 695.38 809.08 132.98 o 3 6 0 33882.03 34354.72 623.37 o 4 6 0 1233.99 1238.57 179.69 o 5 6 0 13031.80 13378.21 443.09 o 6 6 0 141.77 144.95 109.77 o 7 6 0 59545.84 57965.68 986.02 o 8 6 0 7793.86 7619.17 389.37 o 9 6 0 1740.39 1735.07 252.95 o 10 6 0 1270.04 1738.85 265.40 o 11 6 0 16563.72 16380.88 599.82 o 12 6 0 71.59 349.77 173.98 o 13 6 0 8812.83 8963.79 475.32 o 14 6 0 1610.97 1622.25 427.12 o 15 6 0 82.21 203.53 312.89 o 16 6 0 221.83 445.59 338.54 o 17 6 0 2055.37 2030.16 538.80 o 18 6 0 1138.44 1536.67 502.82 o 19 6 0 513.13 676.20 430.18 o 20 6 0 0.58 34.41 366.28 o 21 6 0 3329.64 3304.38 729.91 o 1 7 0 3687.95 3741.23 211.01 o 2 7 0 62987.52 67072.04 868.09 o 3 7 0 6799.14 6730.63 302.90 o 4 7 0 1020.71 1175.37 184.56 o 5 7 0 717.23 1035.77 184.34 o 6 7 0 6598.39 6622.55 349.60 o 7 7 0 5266.88 4396.50 304.88 o 8 7 0 2597.86 2707.83 289.90 o 9 7 0 27046.88 25929.29 740.64 o 10 7 0 2886.35 3144.15 327.75 o 11 7 0 30711.09 30074.11 898.16 o 12 7 0 282.49 326.87 185.82 o 13 7 0 14482.63 14060.93 606.66 o 14 7 0 8003.10 7637.28 697.43 o 15 7 0 3884.60 4310.14 641.28 o 16 7 0 9.30 48.23 276.49 o 17 7 0 456.36 391.44 314.69 o 18 7 0 680.79 1329.24 482.58 o 19 7 0 1306.58 1328.85 499.04 o 20 7 0 627.28 859.46 452.64 o 21 7 0 645.19 1233.17 506.84 o 0 8 0 56240.69 54986.63 1125.41 o 1 8 0 20235.06 20810.18 499.63 o 2 8 0 81460.70 83324.84 1023.13 o 3 8 0 34713.98 35051.56 695.88 o 4 8 0 47318.64 47186.31 843.41 o 5 8 0 2733.03 2587.72 246.85 o 6 8 0 18156.33 17269.48 626.12 o 7 8 0 5400.07 5155.06 339.41 o 8 8 0 53636.81 52151.11 1046.06 o 9 8 0 6164.59 6345.01 397.78 o 10 8 0 365.53 427.00 189.57 o 11 8 0 50.69 233.26 164.19 o 12 8 0 1399.01 1634.88 292.73 o 13 8 0 280.93 560.93 213.45 o 14 8 0 14.61 188.77 273.62 o 15 8 0 114.34 146.44 304.97 o 16 8 0 1190.94 1243.74 436.47 o 17 8 0 2754.39 2870.09 600.42 o 18 8 0 288.78 756.02 419.07 o 19 8 0 538.18 721.20 420.33 o 20 8 0 2230.99 3530.93 759.77 o 21 8 0 712.78 1045.04 487.33 o 1 9 0 22469.01 23124.42 558.92 o 2 9 0 627.34 714.77 158.02 o 3 9 0 50992.26 51579.50 880.88 o 4 9 0 4923.64 4082.55 283.33 o 5 9 0 3514.08 3924.66 292.64 o 6 9 0 20019.91 19713.26 625.72 o 7 9 0 1927.18 2414.87 309.86 o 8 9 0 16481.16 15514.54 599.91 o 9 9 0 58.02 76.10 144.59 o 10 9 0 4624.31 4448.37 369.37 o 11 9 0 343.49 391.66 200.36 o 12 9 0 17161.38 16902.69 754.22 o 13 9 0 1689.63 1441.55 306.88 o 14 9 0 874.88 671.99 341.89 o 15 9 0 2443.09 2686.19 556.31 o 16 9 0 620.96 513.59 367.04 o 17 9 0 1776.86 1618.76 478.74 o 18 9 0 2484.40 2490.64 594.50 o 19 9 0 1476.45 1604.95 539.19 o 20 9 0 125.57 331.50 387.89 o 21 9 0 923.31 870.23 509.19 o 0 10 0 13815.38 15694.35 691.07 o 1 10 0 146559.44 151117.00 1610.86 o 2 10 0 34082.03 32815.86 749.03 o 3 10 0 21432.71 22333.77 611.65 o 4 10 0 22496.86 21603.51 624.98 o 5 10 0 1017.07 1036.79 208.54 o 6 10 0 4498.52 4596.63 336.83 o 7 10 0 10695.27 11544.80 520.19 o 8 10 0 2456.92 2447.84 331.24 o 9 10 0 2030.07 2403.38 339.78 o 10 10 0 112.05 374.71 195.87 o 11 10 0 2651.63 2919.93 378.97 o 12 10 0 3006.45 3015.04 408.04 o 13 10 0 51.75 2.00 199.80 o 14 10 0 699.22 519.00 334.55 o 15 10 0 323.36 573.22 356.21 o 16 10 0 1115.18 1357.18 454.36 o 17 10 0 1109.93 1197.15 458.39 o 18 10 0 77.69 373.33 362.43 o 19 10 0 3031.69 3439.15 692.46 o 20 10 0 12.65 167.22 384.75 o 1 11 0 2161.63 2243.93 249.05 o 2 11 0 91835.95 92310.13 1244.88 o 3 11 0 30.75 228.03 139.64 o 4 11 0 10298.11 10679.10 462.21 o 5 11 0 36651.61 37083.22 875.29 o 6 11 0 7026.80 5982.69 386.22 o 7 11 0 6001.49 5648.38 393.12 o 8 11 0 4205.96 4311.74 371.28 o 9 11 0 15.42 -25.98 174.15 o 10 11 0 4006.05 3889.45 404.00 o 11 11 0 4863.04 4869.03 428.05 o 12 11 0 15.05 73.52 197.27 o 13 11 0 813.13 1003.18 284.11 o 14 11 0 2976.07 3114.79 593.23 o 15 11 0 2463.37 2705.87 583.63 o 16 11 0 417.42 340.75 350.65 o 17 11 0 581.91 292.93 358.55 o 18 11 0 2039.93 1917.37 537.38 o 19 11 0 15.21 182.72 375.54 o 20 11 0 49.06 627.97 449.75 o 0 12 0 166640.19 170259.27 3586.71 o 1 12 0 17652.74 17075.37 563.46 o 2 12 0 8049.87 7320.58 384.40 o 3 12 0 2514.48 2294.56 268.02 o 4 12 0 1871.27 2150.07 292.66 o 5 12 0 3267.85 3156.10 317.26 o 6 12 0 1113.42 1181.74 248.46 o 7 12 0 5087.48 4987.97 388.37 o 8 12 0 265.32 274.52 192.06 o 9 12 0 2616.20 2650.91 381.97 o 10 12 0 1374.90 1676.69 325.19 o 11 12 0 2491.30 2599.71 394.70 o 12 12 0 2836.12 2595.19 399.41 o 13 12 0 332.22 407.14 258.94 o 14 12 0 382.28 298.00 308.47 o 15 12 0 195.98 79.52 305.16 o 16 12 0 2714.66 3283.12 646.96 o 17 12 0 1057.56 1184.38 479.09 o 18 12 0 21.94 254.32 357.00 o 19 12 0 1.17 214.77 389.45 o 1 13 0 9563.26 9936.86 454.82 o 2 13 0 14027.95 13543.81 531.27 o 3 13 0 925.23 872.44 212.01 o 4 13 0 1816.68 2258.10 310.76 o 5 13 0 22980.58 22848.22 799.28 o 6 13 0 8087.08 8010.58 468.91 o 7 13 0 518.89 550.24 204.19 o 8 13 0 5042.29 5526.09 428.19 o 9 13 0 4591.97 4814.79 424.52 o 10 13 0 7693.17 7438.49 513.41 o 11 13 0 3105.89 3392.98 457.85 o 12 13 0 3118.01 3471.95 472.23 o 13 13 0 1175.14 1289.32 354.35 o 14 13 0 522.68 780.82 390.68 o 15 13 0 4175.48 4989.53 724.94 o 16 13 0 973.83 1322.56 469.84 o 17 13 0 14.84 99.70 345.29 o 18 13 0 312.13 147.23 377.91 o 19 13 0 164.18 298.53 396.94 o 0 14 0 1853.96 2116.85 381.94 o 1 14 0 31094.36 30195.24 797.62 o 2 14 0 1501.83 1356.46 249.18 o 3 14 0 6301.20 6789.38 409.62 o 4 14 0 17195.45 17087.98 645.20 o 5 14 0 2940.51 2773.98 347.84 o 6 14 0 10304.32 9582.95 563.88 o 7 14 0 2694.15 2852.66 376.98 o 8 14 0 2870.57 2942.77 402.23 o 9 14 0 26.11 203.42 212.32 o 10 14 0 1486.83 1624.23 338.76 o 11 14 0 5936.82 5626.14 492.34 o 12 14 0 389.75 654.06 266.76 o 13 14 0 548.13 677.25 313.30 o 14 14 0 70.99 170.06 330.48 o 15 14 0 405.30 460.82 373.13 o 16 14 0 1403.25 1873.98 534.49 o 17 14 0 422.54 201.18 400.80 o 18 14 0 398.53 308.91 392.94 o 19 14 0 1126.09 707.66 462.77 o 1 15 0 3.04 -33.26 152.04 o 2 15 0 49.33 114.79 158.68 o 3 15 0 1850.26 2128.93 318.51 o 4 15 0 2754.92 2550.44 336.61 o 5 15 0 8671.53 8015.37 480.98 o 6 15 0 674.94 649.10 230.65 o 7 15 0 4.78 40.50 185.69 o 8 15 0 1344.35 1313.50 307.77 o 9 15 0 11898.02 11650.92 637.82 o 10 15 0 4641.91 4812.45 463.26 o 11 15 0 18252.76 18917.97 843.97 o 12 15 0 2064.72 1925.21 391.43 o 13 15 0 1652.96 2315.50 469.26 o 14 15 0 4357.69 4448.89 725.66 o 15 15 0 505.50 785.93 405.33 o 16 15 0 1478.58 2484.71 598.51 o 17 15 0 745.03 689.01 410.83 o 18 15 0 847.82 1059.46 495.68 o 0 16 0 8915.86 8202.16 654.58 o 1 16 0 229.92 353.26 181.07 o 2 16 0 1033.27 1331.34 274.47 o 3 16 0 14608.11 14450.49 623.72 o 4 16 0 644.98 577.64 223.61 o 5 16 0 10393.07 9887.74 549.47 o 6 16 0 5124.77 4848.82 410.54 o 7 16 0 3979.48 3904.12 429.14 o 8 16 0 852.03 1171.84 302.32 o 9 16 0 13.72 -26.71 201.03 o 10 16 0 1099.67 1008.54 306.20 o 11 16 0 1318.51 1796.00 391.94 o 12 16 0 6719.05 6540.23 557.63 o 13 16 0 2.63 -10.60 273.29 o 14 16 0 692.89 681.11 468.99 o 15 16 0 1089.20 1345.37 612.48 o 16 16 0 103.68 299.99 463.11 o 17 16 0 885.28 1404.30 644.25 o 1 17 0 2604.69 2883.28 364.04 o 2 17 0 4087.27 4256.58 393.66 o 3 17 0 4102.21 4203.51 394.76 o 4 17 0 356.96 520.45 251.88 o 5 17 0 4164.19 4617.04 537.06 o 6 17 0 2494.60 2686.05 458.89 o 7 17 0 428.23 541.79 275.15 o 8 17 0 4474.05 5110.32 560.37 o 9 17 0 2189.81 2619.55 480.83 o 10 17 0 31148.50 30045.98 1343.69 o 11 17 0 3250.10 3421.85 560.18 o 12 17 0 5593.93 5944.91 617.22 o 13 17 0 966.57 1074.93 436.89 o 14 17 0 370.98 594.08 476.94 o 15 17 0 814.97 875.76 578.91 o 16 17 0 19.27 440.17 526.89 o 17 17 0 32.73 75.40 512.22 o 0 18 0 3747.32 3364.02 839.87 o 1 18 0 6.38 188.85 250.91 o 2 18 0 3700.45 3372.35 598.62 o 3 18 0 7488.15 6937.57 567.77 o 4 18 0 11879.54 11137.30 702.94 o 5 18 0 1052.56 1454.27 355.00 o 6 18 0 154.81 353.97 246.13 o 7 18 0 5653.88 5580.64 577.64 o 8 18 0 4818.95 4991.10 585.12 o 9 18 0 1557.83 2195.00 449.92 o 10 18 0 0.90 422.62 290.63 o 11 18 0 11.96 169.55 279.96 o 12 18 0 408.91 776.50 333.22 o 13 18 0 12.77 379.37 370.10 o 14 18 0 150.13 207.13 433.35 o 15 18 0 447.91 969.65 571.56 o 16 18 0 1744.66 1363.78 629.09 o 1 19 0 889.46 825.84 384.63 o 2 19 0 24999.71 25138.66 1260.21 o 3 19 0 248.91 464.11 314.00 o 4 19 0 6156.66 6201.77 695.31 o 5 19 0 218.24 327.62 312.87 o 6 19 0 1376.41 1325.70 436.23 o 7 19 0 2232.02 2347.05 461.21 o 8 19 0 213.41 185.70 272.61 o 9 19 0 12228.83 13053.88 844.19 o 10 19 0 1625.63 1957.48 458.13 o 11 19 0 5923.38 6788.15 733.50 o 12 19 0 167.71 262.19 311.74 o 13 19 0 3093.08 3254.54 670.26 o 14 19 0 37.60 61.43 449.84 o 15 19 0 0.44 75.30 524.68 o 0 20 0 2734.41 2578.41 787.43 o 1 20 0 7103.98 7407.38 744.92 o 2 20 0 2529.15 2889.22 601.59 o 3 20 0 5175.94 5377.00 696.27 o 4 20 0 222.08 387.19 350.41 o 5 20 0 365.61 370.20 316.56 o 6 20 0 526.54 690.98 367.53 o 7 20 0 342.93 198.89 349.07 o 8 20 0 1587.13 2085.81 552.25 o 9 20 0 288.92 387.79 360.79 o 10 20 0 226.57 383.79 334.24 o 11 20 0 338.03 283.27 356.39 o 12 20 0 11.52 321.09 417.80 o 13 20 0 1412.79 1564.72 520.04 o 14 20 0 23.29 -17.01 483.00 o 1 21 0 3370.40 3492.15 683.17 o 2 21 0 15090.13 14492.44 1027.37 o 3 21 0 3154.24 3897.05 680.52 o 4 21 0 1008.07 1406.12 462.96 o 5 21 0 319.16 650.12 347.75 o 6 21 0 140.23 626.91 388.88 o 7 21 0 0.64 10.23 316.42 o 8 21 0 292.06 457.35 394.52 o 9 21 0 1677.31 1933.65 556.15 o 10 21 0 1194.16 2589.01 622.32 o 11 21 0 1711.01 2143.40 558.54 o 12 21 0 2635.63 2976.09 676.28 o 13 21 0 219.75 407.11 419.48 o 0 22 0 7.62 196.81 473.77 o 1 22 0 2131.17 2437.67 580.53 o 2 22 0 6756.23 7491.88 841.92 o 3 22 0 37.85 137.77 347.33 o 4 22 0 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