#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/33/2213305.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213305_Fobs loop_ _publ_author_name 'Mac\'ias, Francisco A.' 'Fronczek, Frank R.' _publ_section_title ; The absolute configuration of heliespirone B, from sunflower Helianthus annuus ; _journal_coeditor_code FJ2010 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2104 _journal_page_last o2105 _journal_volume 63 _journal_year 2007 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.223 _cell_angle_gamma 90.000 _cell_length_a 10.3142 _cell_length_b 11.9229 _cell_length_c 12.2124 _exptl_crystal_F_000 584.00 _reflns_d_resolution_high 0.8427 _[local]_cod_data_source_file fj2010Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' LSU05Cu in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 105.38 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -14 0 95.48 107.94 2.26 o 1 -13 0 8.17 11.92 0.48 o 2 -13 0 39.99 43.19 0.85 o 3 -13 0 26.87 32.33 0.66 o 0 -12 0 52.14 40.25 1.39 o 1 -12 0 39.12 42.53 1.05 o 2 -12 0 55.19 54.48 0.97 o 3 -12 0 57.44 57.49 0.93 o 4 -12 0 104.51 106.37 1.64 o 5 -12 0 3.47 5.69 0.35 o 1 -11 0 44.95 38.66 0.66 o 2 -11 0 25.51 20.87 0.56 o 3 -11 0 50.32 41.85 0.79 o 4 -11 0 21.31 20.97 0.54 o 5 -11 0 84.32 83.28 1.47 o 6 -11 0 30.02 32.83 0.78 o 7 -11 0 8.73 11.61 0.61 o 0 -10 0 677.20 611.49 6.78 o 1 -10 0 4.15 5.25 0.27 o 2 -10 0 160.47 131.64 1.31 o 3 -10 0 504.79 487.06 4.72 o 4 -10 0 2.64 3.61 0.27 o 5 -10 0 4.47 3.74 0.36 o 6 -10 0 16.17 12.21 0.52 o 7 -10 0 60.38 66.08 1.22 o 8 -10 0 0.88 1.05 0.41 o 1 -9 0 217.26 207.38 3.75 o 2 -9 0 327.28 316.91 3.34 o 3 -9 0 83.70 81.57 1.01 o 4 -9 0 62.98 61.99 0.97 o 5 -9 0 166.52 150.30 2.04 o 6 -9 0 71.03 64.44 1.27 o 7 -9 0 79.50 78.13 2.03 o 8 -9 0 40.45 47.50 0.97 o 0 -8 0 820.58 811.02 12.30 o 1 -8 0 58.73 60.37 1.16 o 2 -8 0 531.42 504.15 10.63 o 3 -8 0 1144.21 1062.24 13.84 o 4 -8 0 36.54 35.82 0.64 o 5 -8 0 476.52 451.86 5.43 o 6 -8 0 198.71 195.08 2.50 o 7 -8 0 27.75 34.19 0.87 o 8 -8 0 29.88 32.36 0.81 o 9 -8 0 39.09 39.71 1.18 o 1 -7 0 199.65 176.10 2.23 o 2 -7 0 333.75 311.31 4.31 o 3 -7 0 250.84 230.05 3.35 o 4 -7 0 35.53 35.65 0.89 o 5 -7 0 495.23 480.33 4.17 o 6 -7 0 352.86 341.49 3.57 o 7 -7 0 41.71 43.87 1.00 o 8 -7 0 63.25 58.93 1.20 o 9 -7 0 37.15 37.05 1.21 o 0 -6 0 1100.70 1229.45 15.45 o 1 -6 0 82.73 89.18 1.24 o 2 -6 0 976.38 991.22 12.69 o 3 -6 0 722.40 753.76 8.48 o 4 -6 0 146.37 154.21 2.38 o 5 -6 0 186.79 178.22 2.74 o 6 -6 0 278.89 283.95 2.82 o 7 -6 0 130.53 139.92 1.86 o 8 -6 0 64.13 65.75 1.10 o 9 -6 0 52.98 47.53 1.08 o 10 -6 0 14.95 18.15 0.76 o 1 -5 0 2441.42 2329.60 41.58 o 2 -5 0 203.43 174.08 2.24 o 3 -5 0 869.45 900.51 10.00 o 4 -5 0 537.42 515.89 5.94 o 5 -5 0 300.60 300.02 5.40 o 6 -5 0 323.59 305.21 3.64 o 7 -5 0 69.94 63.24 0.95 o 8 -5 0 23.19 21.57 0.59 o 9 -5 0 116.37 131.70 2.22 o 10 -5 0 54.77 58.52 2.21 o 0 -4 0 677.98 693.36 16.44 o 1 -4 0 2333.06 2594.94 34.15 o 2 -4 0 2265.90 2310.53 26.40 o 3 -4 0 282.76 279.60 3.68 o 4 -4 0 849.24 875.72 9.23 o 5 -4 0 307.16 281.35 3.94 o 6 -4 0 502.92 501.28 8.68 o 7 -4 0 233.63 219.77 2.24 o 8 -4 0 38.02 28.25 1.83 o 9 -4 0 88.94 84.59 1.60 o 10 -4 0 27.26 29.59 1.21 o 1 -3 0 7773.80 7019.00 94.93 o 2 -3 0 2816.84 2801.03 38.53 o 3 -3 0 2342.55 2525.87 29.01 o 4 -3 0 577.25 660.17 11.23 o 5 -3 0 1536.14 1595.84 18.64 o 6 -3 0 114.75 123.22 1.86 o 7 -3 0 232.30 231.77 3.32 o 8 -3 0 20.86 22.57 0.76 o 9 -3 0 63.46 53.73 2.21 o 10 -3 0 183.09 183.09 4.26 o 1 -2 0 3443.28 3159.18 54.58 o 2 -2 0 2294.74 2152.16 30.75 o 3 -2 0 442.75 483.12 6.88 o 4 -2 0 2256.60 2379.83 29.23 o 5 -2 0 664.48 766.57 10.95 o 6 -2 0 98.65 108.46 1.97 o 7 -2 0 81.90 69.95 1.62 o 8 -2 0 77.45 70.65 1.01 o 9 -2 0 42.16 50.28 1.74 o 10 -2 0 59.30 56.75 1.85 o 11 -2 0 60.72 72.99 2.02 o 1 -1 0 2521.26 2909.96 72.96 o 2 -1 0 417.88 450.17 6.49 o 3 -1 0 289.26 250.49 4.85 o 4 -1 0 511.96 567.61 10.11 o 5 -1 0 41.05 43.05 0.91 o 6 -1 0 188.50 179.89 3.78 o 7 -1 0 133.94 151.57 2.84 o 8 -1 0 314.58 333.62 4.81 o 9 -1 0 23.05 25.96 0.53 o 10 -1 0 63.51 58.79 1.91 o 11 -1 0 209.51 220.98 4.86 o 1 0 0 0.45 0.64 0.20 o 2 0 0 4599.58 4592.27 83.39 o 3 0 0 318.52 322.42 5.17 o 4 0 0 1814.60 1866.25 29.30 o 5 0 0 3650.75 3903.58 69.27 o 6 0 0 26.56 28.68 1.37 o 7 0 0 840.20 764.52 11.86 o 8 0 0 22.35 14.66 0.46 o 9 0 0 14.30 9.87 0.36 o 10 0 0 100.90 92.10 2.58 o 11 0 0 157.18 139.20 3.31 o 1 1 0 2520.49 2927.91 72.95 o 2 1 0 418.74 441.19 7.98 o 3 1 0 288.96 238.86 3.61 o 4 1 0 511.87 571.48 10.99 o 5 1 0 39.43 42.01 1.23 o 6 1 0 189.98 186.16 3.75 o 7 1 0 134.36 149.16 4.05 o 8 1 0 315.20 325.22 3.30 o 9 1 0 22.93 25.56 0.52 o 10 1 0 63.44 59.43 0.84 o 1 2 0 3441.99 3089.84 65.72 o 2 2 0 2297.84 2125.10 53.67 o 3 2 0 446.05 469.63 12.12 o 4 2 0 2258.92 2344.51 37.39 o 5 2 0 663.43 767.32 10.93 o 6 2 0 99.10 105.66 2.38 o 7 2 0 82.35 71.06 1.20 o 8 2 0 77.68 71.70 1.00 o 9 2 0 41.78 46.21 0.77 o 10 2 0 59.16 56.96 0.84 o 11 2 0 60.34 70.99 1.68 o 1 3 0 7778.78 6746.76 115.33 o 2 3 0 2810.72 2737.85 46.50 o 4 3 0 574.36 649.15 12.12 o 5 3 0 1538.17 1587.59 21.77 o 6 3 0 112.86 124.31 3.13 o 7 3 0 229.22 226.75 2.98 o 8 3 0 20.58 21.92 0.51 o 9 3 0 62.06 51.85 0.82 o 10 3 0 183.51 182.93 2.57 o 0 4 0 689.85 718.94 16.07 o 1 4 0 2332.02 2558.79 43.22 o 2 4 0 2265.73 2292.35 38.38 o 3 4 0 283.94 276.63 4.40 o 4 4 0 844.93 887.08 38.15 o 5 4 0 307.49 277.74 4.23 o 6 4 0 498.27 512.75 13.35 o 7 4 0 234.72 225.61 4.78 o 8 4 0 37.19 26.07 1.02 o 9 4 0 89.46 83.02 1.40 o 10 4 0 27.44 28.16 1.46 o 1 5 0 2440.01 2310.59 34.71 o 2 5 0 202.80 187.64 6.90 o 3 5 0 871.79 891.53 13.64 o 4 5 0 534.98 526.40 10.91 o 5 5 0 298.54 301.39 8.95 o 6 5 0 324.06 305.90 4.04 o 7 5 0 70.94 64.24 1.74 o 8 5 0 22.74 20.61 0.64 o 9 5 0 116.62 140.00 2.23 o 10 5 0 55.18 58.50 1.00 o 0 6 0 1099.63 1220.50 18.51 o 1 6 0 82.60 87.55 1.35 o 2 6 0 972.31 1001.85 15.32 o 3 6 0 721.13 752.43 11.55 o 4 6 0 145.33 151.21 3.76 o 5 6 0 185.65 177.78 3.44 o 6 6 0 274.71 286.46 3.83 o 7 6 0 131.17 142.15 3.06 o 8 6 0 63.73 64.23 1.77 o 9 6 0 54.49 50.53 0.97 o 10 6 0 14.83 19.61 0.66 o 1 7 0 197.06 171.37 2.43 o 2 7 0 333.14 308.99 5.06 o 3 7 0 250.40 229.09 5.52 o 4 7 0 34.73 35.63 1.13 o 5 7 0 492.35 486.96 6.73 o 6 7 0 351.84 340.81 4.54 o 7 7 0 41.67 42.85 2.25 o 8 7 0 63.33 59.76 1.64 o 9 7 0 38.34 39.91 1.76 o 10 7 0 5.51 7.17 0.38 o 0 8 0 823.95 788.77 8.08 o 1 8 0 58.91 58.35 0.61 o 2 8 0 532.93 501.41 4.70 o 3 8 0 1145.72 1082.33 10.79 o 4 8 0 36.01 35.27 0.76 o 5 8 0 476.84 439.82 5.37 o 6 8 0 201.05 199.56 3.19 o 7 8 0 27.89 33.36 1.18 o 8 8 0 29.13 31.32 1.07 o 9 8 0 39.94 38.68 1.08 o 1 9 0 218.55 206.82 1.51 o 2 9 0 325.74 323.13 2.50 o 3 9 0 83.18 81.09 1.09 o 4 9 0 62.36 59.72 0.90 o 5 9 0 165.67 150.98 1.95 o 6 9 0 71.50 64.43 1.77 o 7 9 0 79.51 76.73 1.94 o 0 10 0 681.13 623.88 5.54 o 1 10 0 4.07 4.92 0.22 o 2 10 0 162.25 134.17 1.29 o 3 10 0 506.45 483.90 4.43 o 4 10 0 2.54 3.64 0.44 o 5 10 0 4.74 3.32 0.52 o 6 10 0 15.79 11.70 0.71 o 7 10 0 60.52 68.88 1.70 o 1 11 0 45.60 37.58 0.52 o 2 11 0 24.82 20.63 0.39 o 3 11 0 50.34 42.32 0.93 o 4 11 0 21.35 21.12 0.46 o 5 11 0 85.57 86.80 1.39 o 6 11 0 30.01 34.30 0.71 o 7 11 0 8.93 11.05 0.56 o 0 12 0 53.74 43.64 0.93 o 1 12 0 39.80 43.91 0.83 o 2 12 0 55.43 55.91 0.82 o 3 12 0 57.00 59.47 1.49 o 4 12 0 105.92 106.60 1.61 o 5 12 0 3.28 5.50 0.29 o 6 12 0 15.55 25.21 0.83 o 1 13 0 8.34 12.65 0.51 o 2 13 0 39.48 42.74 0.67 o 3 13 0 26.93 32.12 0.66 o 4 13 0 16.90 13.81 0.62 o 0 14 0 96.41 100.77 2.22 o 0 -14 1 25.01 31.49 0.98 o 1 -14 1 29.04 39.58 1.12 o -4 -13 1 1.33 1.63 0.33 o -3 -13 1 10.25 10.08 0.61 o -2 -13 1 80.61 86.13 1.46 o -1 -13 1 39.13 34.84 0.83 o 0 -13 1 33.12 35.32 0.67 o 1 -13 1 27.37 22.48 0.44 o 2 -13 1 23.92 31.70 0.60 o 3 -13 1 24.11 22.34 0.48 o -6 -12 1 109.36 126.24 1.82 o -5 -12 1 84.42 88.95 1.44 o -4 -12 1 98.48 95.62 1.27 o -3 -12 1 22.43 26.96 0.59 o -2 -12 1 17.06 20.31 0.66 o -1 -12 1 6.69 4.15 0.44 o 0 -12 1 154.45 152.85 2.11 o 1 -12 1 127.41 113.52 1.32 o 2 -12 1 39.14 33.42 0.59 o 3 -12 1 168.24 151.43 1.84 o 4 -12 1 44.52 43.29 0.74 o 5 -12 1 105.70 110.28 2.34 o -7 -11 1 25.92 29.80 0.69 o -6 -11 1 36.55 38.30 0.85 o -5 -11 1 73.11 76.07 1.35 o -4 -11 1 50.81 47.09 0.84 o -3 -11 1 147.44 144.20 1.82 o -2 -11 1 237.64 221.47 2.23 o -1 -11 1 14.08 15.83 0.61 o 0 -11 1 195.05 186.36 1.83 o 1 -11 1 256.66 245.60 2.28 o 2 -11 1 95.16 98.02 1.27 o 3 -11 1 41.61 42.30 0.79 o 4 -11 1 13.91 16.92 0.48 o 5 -11 1 99.78 96.76 1.59 o 6 -11 1 155.52 160.37 2.30 o -8 -10 1 86.15 98.88 2.15 o -7 -10 1 37.42 33.57 0.97 o -6 -10 1 23.06 22.06 0.68 o -5 -10 1 54.54 57.59 1.18 o -4 -10 1 416.93 415.53 4.16 o -3 -10 1 314.97 298.37 2.98 o -2 -10 1 227.25 214.81 1.70 o -1 -10 1 9.20 10.07 0.35 o 0 -10 1 65.56 62.61 0.83 o 1 -10 1 166.34 156.42 1.58 o 2 -10 1 32.24 27.12 0.69 o 3 -10 1 412.49 399.67 3.60 o 4 -10 1 37.42 36.49 0.80 o 5 -10 1 33.53 40.24 1.32 o 6 -10 1 27.56 30.65 0.78 o 7 -10 1 47.28 48.66 0.96 o -9 -9 1 13.82 18.06 0.73 o -8 -9 1 39.35 42.89 0.94 o -7 -9 1 45.35 50.33 1.31 o -6 -9 1 152.13 143.27 2.24 o -5 -9 1 95.49 93.48 1.43 o -4 -9 1 35.11 34.57 0.69 o -3 -9 1 112.48 96.72 1.03 o -2 -9 1 299.75 293.12 5.22 o -1 -9 1 39.33 36.74 1.11 o 0 -9 1 101.39 97.76 1.70 o 1 -9 1 41.80 37.84 0.85 o 2 -9 1 161.19 157.37 1.81 o 3 -9 1 190.62 186.23 1.88 o 4 -9 1 247.76 234.83 2.61 o 5 -9 1 334.18 332.97 3.88 o 6 -9 1 76.61 79.03 1.45 o 7 -9 1 222.62 217.57 4.33 o 8 -9 1 26.02 28.54 0.98 o -8 -8 1 94.68 89.38 1.56 o -7 -8 1 75.91 75.91 1.43 o -6 -8 1 13.91 16.12 0.85 o -5 -8 1 471.82 456.10 5.11 o -4 -8 1 201.32 171.15 1.87 o -3 -8 1 183.81 176.86 2.73 o -2 -8 1 52.31 50.92 1.10 o -1 -8 1 535.81 547.40 7.00 o 0 -8 1 153.61 147.79 2.29 o 1 -8 1 411.76 415.25 9.91 o 2 -8 1 318.45 306.42 4.43 o 3 -8 1 14.11 16.87 0.61 o 4 -8 1 29.90 29.98 0.64 o 5 -8 1 104.25 104.66 1.39 o 6 -8 1 44.26 47.55 2.61 o 7 -8 1 138.31 143.63 2.21 o 8 -8 1 24.90 25.31 0.70 o 9 -8 1 13.19 17.32 0.72 o -9 -7 1 103.23 105.58 2.40 o -8 -7 1 26.38 32.49 0.73 o -7 -7 1 155.58 158.32 2.42 o -6 -7 1 333.80 315.19 4.18 o -5 -7 1 153.97 149.13 2.45 o -4 -7 1 151.80 138.53 2.25 o -3 -7 1 259.69 251.54 3.63 o -2 -7 1 932.76 884.83 11.52 o -1 -7 1 273.17 262.27 2.81 o 0 -7 1 828.68 855.53 15.69 o 1 -7 1 522.04 519.05 5.89 o 2 -7 1 120.39 141.14 2.21 o 3 -7 1 53.16 51.39 0.90 o 4 -7 1 163.62 157.75 2.15 o 5 -7 1 540.28 540.72 5.39 o 6 -7 1 254.14 255.79 3.09 o 7 -7 1 128.55 122.33 1.98 o 8 -7 1 38.76 41.88 0.95 o -9 -6 1 1.69 2.23 1.01 o -8 -6 1 56.89 53.31 0.96 o -7 -6 1 30.36 30.61 0.71 o -6 -6 1 89.72 96.95 1.31 o -5 -6 1 213.59 191.25 2.49 o -4 -6 1 165.43 188.41 2.76 o -3 -6 1 611.90 595.76 7.76 o -2 -6 1 177.18 205.91 2.94 o -1 -6 1 197.16 206.88 2.22 o 0 -6 1 56.88 58.03 1.15 o 1 -6 1 2238.63 2304.61 27.04 o 2 -6 1 1466.36 1596.70 20.15 o 3 -6 1 10.82 14.39 0.53 o 4 -6 1 185.09 185.68 2.57 o 5 -6 1 521.73 506.99 6.88 o 6 -6 1 203.43 190.77 4.14 o 7 -6 1 48.74 51.51 1.11 o 8 -6 1 4.37 4.45 0.40 o 9 -6 1 4.22 6.00 0.55 o -10 -5 1 12.03 11.44 0.52 o -9 -5 1 164.76 152.39 2.47 o -8 -5 1 284.40 260.66 3.07 o -7 -5 1 356.52 351.07 3.56 o -6 -5 1 52.72 50.15 0.89 o -5 -5 1 79.88 97.24 1.65 o -4 -5 1 321.43 286.51 3.43 o -3 -5 1 246.09 241.91 2.90 o -2 -5 1 618.74 707.81 10.70 o -1 -5 1 104.10 106.34 2.61 o 0 -5 1 422.89 428.11 4.85 o 1 -5 1 9404.78 9474.92 127.10 o 2 -5 1 355.11 355.45 4.44 o 3 -5 1 1624.93 1662.80 18.98 o 4 -5 1 213.90 225.62 2.79 o 5 -5 1 551.36 536.61 12.49 o 6 -5 1 326.81 310.96 8.26 o 7 -5 1 316.85 289.04 3.33 o 8 -5 1 229.41 218.80 3.26 o 9 -5 1 17.21 23.63 1.12 o -10 -4 1 2.16 1.67 0.30 o -9 -4 1 63.01 62.45 1.33 o -8 -4 1 81.15 75.05 1.04 o -7 -4 1 64.58 47.15 1.18 o -6 -4 1 89.56 74.07 1.71 o -5 -4 1 161.49 161.07 2.42 o -4 -4 1 1374.30 1511.16 16.67 o -3 -4 1 782.62 818.00 20.11 o -2 -4 1 1414.87 1416.50 18.06 o -1 -4 1 755.07 734.58 17.29 o 0 -4 1 2611.20 2254.86 36.75 o 1 -4 1 962.83 910.03 10.57 o 2 -4 1 2295.05 2482.21 28.54 o 3 -4 1 732.05 782.90 9.18 o 4 -4 1 529.94 558.85 6.68 o 5 -4 1 215.72 208.64 3.48 o 6 -4 1 0.09 0.61 0.21 o 7 -4 1 6.88 8.00 0.42 o 8 -4 1 239.23 237.03 5.24 o 9 -4 1 128.30 110.47 2.92 o 10 -4 1 1.70 3.42 0.52 o -11 -3 1 76.44 80.44 2.16 o -10 -3 1 130.98 135.94 2.22 o -9 -3 1 494.86 445.73 13.74 o -8 -3 1 608.20 573.40 5.48 o -7 -3 1 10.05 9.30 0.44 o -6 -3 1 63.73 66.80 1.14 o -5 -3 1 51.81 60.38 0.88 o -4 -3 1 2256.89 2299.27 26.42 o -3 -3 1 173.56 172.82 1.99 o -2 -3 1 1159.54 1078.37 13.00 o -1 -3 1 642.43 663.85 11.61 o 0 -3 1 312.62 262.33 3.20 o 1 -3 1 11102.90 11113.38 189.27 o 2 -3 1 109.62 104.29 1.64 o 3 -3 1 815.20 929.71 10.80 o 4 -3 1 1002.56 1045.14 14.00 o 5 -3 1 259.24 244.43 3.87 o 6 -3 1 36.59 41.85 2.30 o 7 -3 1 217.87 208.44 4.94 o 8 -3 1 33.35 36.14 1.45 o 9 -3 1 28.39 24.17 1.16 o 10 -3 1 14.90 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260.65 2.45 o 1 -7 9 321.44 346.30 3.38 o 2 -7 9 198.52 206.46 2.50 o 3 -7 9 31.08 32.09 0.82 o 4 -7 9 11.57 13.11 0.75 o -9 -6 9 150.01 147.13 1.52 o -8 -6 9 67.97 74.55 0.96 o -7 -6 9 59.37 53.96 0.82 o -6 -6 9 69.67 65.03 0.91 o -5 -6 9 670.63 633.79 8.12 o -4 -6 9 2.92 5.36 0.35 o -3 -6 9 157.25 156.03 1.45 o -2 -6 9 36.71 38.82 0.52 o -1 -6 9 84.84 70.19 0.99 o 0 -6 9 115.25 120.81 1.34 o 1 -6 9 71.61 58.92 0.81 o 2 -6 9 24.03 17.59 0.44 o 3 -6 9 57.48 56.01 0.94 o 4 -6 9 7.25 7.06 0.63 o -10 -5 9 228.50 244.46 4.45 o -9 -5 9 48.45 60.13 0.81 o -8 -5 9 55.69 44.19 0.70 o -7 -5 9 48.39 47.51 0.74 o -6 -5 9 72.00 84.60 1.82 o -5 -5 9 363.10 367.10 3.68 o -4 -5 9 147.40 138.73 1.31 o -3 -5 9 91.44 79.62 0.93 o -2 -5 9 95.36 84.79 1.07 o -1 -5 9 30.56 26.47 0.46 o 0 -5 9 133.68 110.83 1.63 o 1 -5 9 244.60 207.56 2.20 o 2 -5 9 83.00 72.71 1.22 o 3 -5 9 117.43 124.81 2.37 o 4 -5 9 79.33 65.77 2.02 o 5 -5 9 59.46 67.23 1.95 o -10 -4 9 136.38 143.27 2.24 o -9 -4 9 229.46 223.29 2.20 o -8 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428.94 429.91 4.73 o -4 -2 9 84.46 73.34 0.98 o -3 -2 9 162.09 166.15 2.14 o -2 -2 9 3.27 4.48 0.51 o -1 -2 9 62.03 61.39 1.04 o 0 -2 9 22.77 24.15 0.43 o 1 -2 9 173.26 159.89 1.81 o 2 -2 9 24.43 24.33 0.58 o 3 -2 9 104.23 102.15 1.46 o 4 -2 9 39.03 35.56 0.98 o 5 -2 9 248.64 246.34 3.55 o -11 -1 9 93.08 101.74 1.24 o -10 -1 9 71.87 75.48 1.07 o -9 -1 9 188.97 180.43 2.11 o -8 -1 9 352.49 350.18 4.53 o -7 -1 9 23.44 20.85 0.57 o -6 -1 9 38.00 37.11 0.98 o -5 -1 9 593.82 578.06 11.80 o -4 -1 9 67.97 54.72 2.18 o -3 -1 9 20.61 16.61 0.62 o -2 -1 9 903.66 883.06 12.37 o -1 -1 9 111.74 105.60 1.81 o 0 -1 9 921.31 875.44 9.06 o 1 -1 9 30.83 30.53 0.57 o 2 -1 9 19.05 22.01 0.46 o 3 -1 9 292.76 275.79 2.99 o 4 -1 9 152.60 155.80 2.34 o 5 -1 9 218.65 215.49 2.94 o 6 -1 9 51.48 51.16 1.33 o -11 0 9 33.71 35.88 0.75 o -10 0 9 16.53 22.27 0.51 o -9 0 9 230.47 222.15 3.07 o -8 0 9 1.78 1.69 0.40 o -7 0 9 4.18 3.79 0.40 o -6 0 9 11.74 12.81 0.58 o -5 0 9 1033.26 1057.33 10.90 o -4 0 9 274.41 249.79 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