#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2213316.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213316_Fobs loop_ _publ_author_name 'Che, Xi-Quan' 'Wang, Li-Bin' _publ_section_title ; The Schiff base 11-thiosemicarbazonoindeno[1,2-b]quinoxaline-8-carboxylic acid dimethyl sulfoxide solvate ; _journal_coeditor_code FL2127 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2681 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.775 _cell_angle_gamma 90.000 _cell_length_a 14.8758 _cell_length_b 25.2055 _cell_length_c 11.0201 _exptl_crystal_F_000 1776.00 _reflns_d_resolution_high 0.8380 _[local]_cod_data_source_file fl2127Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' qa215 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 772.47 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 866.55 -11.59 11.59 o 3 0 0 692.54 737.45 37.21 o 4 0 0 127507.69 135943.80 1859.78 o 5 0 0 398.01 428.19 40.26 o 6 0 0 8.07 51.24 17.08 o 7 0 0 113.75 141.51 32.33 o 8 0 0 459.40 383.67 50.02 o 9 0 0 303.29 298.88 46.36 o 11 0 0 72.70 77.47 33.55 o 12 0 0 40.61 65.27 34.16 o 13 0 0 12.57 34.16 28.67 o 14 0 0 1085.34 1094.88 111.62 o 15 0 0 92.34 137.24 48.19 o 16 0 0 6.25 17.69 35.38 o 17 0 0 0.19 30.50 39.65 o 1 1 0 225.69 178.72 12.20 o 2 1 0 3432.35 3624.16 45.60 o 3 1 0 90.48 99.68 12.75 o 4 1 0 44135.05 47043.44 699.63 o 5 1 0 23.29 14.17 9.76 o 6 1 0 233.17 215.93 35.99 o 7 1 0 716.82 735.01 56.12 o 8 1 0 877.04 891.74 46.35 o 9 1 0 481.60 436.53 63.13 o 10 1 0 141.92 117.92 23.01 o 11 1 0 104.11 94.98 23.62 o 12 1 0 38.75 69.54 31.72 o 13 1 0 0.12 -38.90 46.36 o 14 1 0 19.27 40.87 32.33 o 15 1 0 4.82 6.10 33.55 o 16 1 0 0.31 -43.31 43.31 o 17 1 0 54.88 103.80 38.43 o 0 2 0 80186.80 61613.64 871.03 o 1 2 0 331.21 197.42 16.87 o 2 2 0 3690.07 7361.80 67.29 o 3 2 0 273.03 233.47 13.80 o 4 2 0 2831.33 2968.38 64.92 o 5 2 0 52.73 79.29 18.60 o 6 2 0 1443.88 1390.70 51.19 o 7 2 0 59.82 78.53 17.46 o 8 2 0 627.26 634.64 44.20 o 9 2 0 250.13 257.35 31.93 o 10 2 0 551.67 530.09 53.07 o 11 2 0 10.75 25.02 16.16 o 12 2 0 72.75 99.83 45.75 o 13 2 0 729.97 744.17 77.16 o 14 2 0 2.51 28.96 22.57 o 15 2 0 0.00 -29.89 29.89 o 16 2 0 184.67 183.05 44.08 o 17 2 0 23.77 54.90 50.02 o 1 3 0 2946.00 2623.64 33.22 o 2 3 0 5915.42 6115.82 61.62 o 3 3 0 12.15 18.45 5.63 o 4 3 0 1761.82 1771.98 38.72 o 5 3 0 91.24 115.43 18.02 o 6 3 0 446.72 436.75 30.33 o 7 3 0 274.03 261.20 29.58 o 8 3 0 812.64 785.70 43.77 o 9 3 0 3.81 -1.49 11.43 o 10 3 0 108.52 87.20 21.75 o 11 3 0 139.95 175.66 29.86 o 12 3 0 55.52 35.16 21.04 o 13 3 0 35.84 53.91 20.76 o 14 3 0 107.37 117.21 33.40 o 15 3 0 43.79 18.91 37.21 o 16 3 0 2.06 31.72 37.82 o 17 3 0 0.10 37.21 51.85 o 0 4 0 8992.19 14673.95 171.09 o 1 4 0 3983.99 4075.26 40.42 o 2 4 0 58661.55 68007.41 425.98 o 3 4 0 1172.34 1125.24 24.33 o 4 4 0 719.12 711.41 24.12 o 5 4 0 1.02 -8.06 9.09 o 6 4 0 1240.46 1259.57 48.59 o 7 4 0 189.03 172.96 26.53 o 8 4 0 2183.62 2087.12 72.76 o 9 4 0 280.15 320.37 36.35 o 10 4 0 333.62 326.34 39.19 o 11 4 0 74.81 73.63 22.66 o 12 4 0 2517.79 2320.47 92.43 o 13 4 0 1.80 12.75 16.42 o 14 4 0 618.21 533.44 81.43 o 15 4 0 9.78 32.84 23.27 o 16 4 0 123.02 157.98 56.73 o 17 4 0 48.82 74.42 53.68 o 1 5 0 305.63 367.26 11.87 o 2 5 0 1495.46 1237.46 22.44 o 3 5 0 5646.47 5888.31 60.59 o 4 5 0 134.89 74.59 9.34 o 5 5 0 284.08 240.21 16.36 o 6 5 0 1854.38 1678.52 47.94 o 7 5 0 660.07 610.71 32.81 o 8 5 0 54.47 36.05 12.39 o 9 5 0 373.30 378.09 39.94 o 10 5 0 1430.28 1396.82 65.83 o 11 5 0 5.42 6.21 13.30 o 12 5 0 220.51 220.94 32.17 o 13 5 0 0.04 -17.29 17.29 o 14 5 0 111.42 156.43 30.15 o 15 5 0 3.91 12.84 21.19 o 16 5 0 3.86 54.90 45.14 o 17 5 0 18.76 -6.71 43.92 o 0 6 0 4051.97 4726.58 121.08 o 1 6 0 1349.34 1382.17 26.62 o 2 6 0 10313.30 11677.90 97.48 o 3 6 0 68.14 72.05 7.95 o 4 6 0 133.85 127.40 10.99 o 5 6 0 413.22 381.52 18.04 o 6 6 0 475.57 505.90 23.29 o 7 6 0 18.04 13.65 9.01 o 8 6 0 182.98 179.96 23.87 o 9 6 0 91.68 106.90 19.13 o 10 6 0 0.20 4.01 9.95 o 11 6 0 2.42 -1.61 10.08 o 12 6 0 589.97 595.83 44.99 o 13 6 0 201.12 187.24 32.50 o 14 6 0 0.76 61.35 22.61 o 15 6 0 82.37 44.46 45.44 o 16 6 0 2.74 20.13 37.82 o 17 6 0 2.91 -40.26 40.87 o 1 7 0 57.74 59.13 8.24 o 2 7 0 724.68 559.01 17.25 o 3 7 0 9795.17 10460.71 94.98 o 4 7 0 1042.73 1165.80 26.90 o 5 7 0 16.13 7.38 7.08 o 6 7 0 22.13 39.96 8.95 o 7 7 0 1332.12 1300.80 44.12 o 8 7 0 247.38 252.12 23.14 o 9 7 0 1214.58 1121.43 48.07 o 10 7 0 151.96 185.76 22.72 o 11 7 0 39.71 43.48 13.79 o 12 7 0 18.81 22.76 14.14 o 13 7 0 1038.58 998.94 66.15 o 14 7 0 90.76 109.03 32.98 o 15 7 0 105.62 80.67 30.91 o 16 7 0 75.18 40.87 46.97 o 17 7 0 0.99 56.73 51.24 o 0 8 0 13810.49 15210.74 229.96 o 1 8 0 188.22 151.18 12.42 o 2 8 0 155.24 137.94 10.90 o 3 8 0 136.03 170.00 16.24 o 4 8 0 2866.59 2835.73 44.50 o 5 8 0 43.49 48.58 7.99 o 6 8 0 930.29 922.51 34.37 o 7 8 0 689.66 618.66 32.68 o 8 8 0 326.82 310.54 25.80 o 9 8 0 258.46 283.58 30.80 o 10 8 0 421.22 418.46 36.37 o 11 8 0 46.95 51.98 15.63 o 12 8 0 115.33 97.24 22.84 o 13 8 0 401.44 383.74 45.45 o 14 8 0 228.20 223.29 42.90 o 15 8 0 5.12 4.39 27.14 o 16 8 0 39.91 41.32 54.90 o 17 8 0 1.31 124.43 62.22 o 1 9 0 5408.98 5913.52 73.37 o 2 9 0 4456.20 5240.08 116.13 o 3 9 0 4006.12 4658.32 59.35 o 4 9 0 7039.56 7463.11 82.16 o 5 9 0 231.42 293.22 17.01 o 6 9 0 882.36 833.50 39.74 o 7 9 0 1965.68 2012.11 44.49 o 8 9 0 972.10 932.97 39.15 o 9 9 0 1480.48 1464.63 50.14 o 10 9 0 295.97 316.83 35.22 o 11 9 0 370.70 350.52 39.53 o 12 9 0 165.31 188.20 38.75 o 13 9 0 159.56 160.96 37.49 o 14 9 0 22.33 28.90 22.93 o 15 9 0 4.07 16.83 24.05 o 16 9 0 0.83 12.81 27.08 o 0 10 0 567.47 629.61 52.15 o 1 10 0 3061.95 3069.37 82.41 o 2 10 0 421.88 382.12 19.44 o 3 10 0 119.58 176.69 13.76 o 4 10 0 385.02 445.06 22.61 o 5 10 0 17.07 15.91 7.26 o 6 10 0 56.68 67.05 10.86 o 7 10 0 1384.32 1253.74 35.08 o 8 10 0 1939.39 1914.81 72.28 o 9 10 0 88.44 118.84 18.91 o 10 10 0 318.79 347.94 31.47 o 11 10 0 2.12 5.84 15.94 o 12 10 0 1.00 -7.68 20.04 o 13 10 0 4.17 -10.97 19.62 o 14 10 0 24.51 27.70 24.97 o 15 10 0 17.23 47.13 28.96 o 16 10 0 26.29 49.80 40.87 o 1 11 0 3564.37 3944.14 67.79 o 2 11 0 1998.85 1881.80 43.32 o 3 11 0 1624.14 1592.21 35.26 o 4 11 0 1692.16 1786.55 46.79 o 5 11 0 13584.46 14613.48 137.73 o 6 11 0 67.47 78.44 11.37 o 7 11 0 16.60 11.78 9.07 o 8 11 0 1452.72 1490.47 50.51 o 9 11 0 461.85 456.59 34.03 o 10 11 0 288.55 232.25 26.73 o 11 11 0 1473.13 1441.48 55.88 o 12 11 0 75.69 75.20 30.50 o 13 11 0 33.31 30.67 21.25 o 14 11 0 0.23 -0.87 22.27 o 15 11 0 535.41 572.34 74.95 o 16 11 0 1.77 74.66 32.75 o 0 12 0 2371.93 2561.48 71.67 o 1 12 0 11143.36 12435.65 132.45 o 2 12 0 1261.50 1379.27 36.61 o 3 12 0 1236.98 1061.50 32.14 o 4 12 0 1150.67 1148.69 31.21 o 5 12 0 211.37 211.34 16.45 o 6 12 0 291.43 352.23 24.12 o 7 12 0 115.78 106.78 17.87 o 8 12 0 156.32 153.19 20.89 o 9 12 0 231.19 282.51 29.41 o 10 12 0 3.68 -9.06 10.95 o 11 12 0 118.92 136.77 27.33 o 12 12 0 28.18 41.08 23.91 o 13 12 0 9.82 31.65 23.71 o 14 12 0 18.37 26.98 25.00 o 15 12 0 23.45 9.71 23.70 o 16 12 0 0.55 -12.49 28.72 o 1 13 0 4692.15 4728.36 73.87 o 2 13 0 2945.27 2838.20 55.43 o 3 13 0 1110.71 1468.77 46.84 o 4 13 0 817.56 834.78 37.54 o 5 13 0 1620.09 1549.36 38.03 o 6 13 0 19.32 34.67 12.34 o 7 13 0 85.08 100.94 17.98 o 8 13 0 271.23 289.53 28.82 o 9 13 0 1334.91 1215.75 76.24 o 10 13 0 28.14 44.13 15.72 o 11 13 0 133.58 227.24 89.36 o 12 13 0 1.38 9.57 21.45 o 13 13 0 405.61 318.31 55.41 o 14 13 0 331.40 354.75 59.29 o 15 13 0 43.41 6.74 105.22 o 0 14 0 2770.90 2589.39 81.13 o 1 14 0 1331.44 1208.90 36.99 o 2 14 0 693.29 598.37 27.30 o 3 14 0 1383.21 1206.79 36.73 o 4 14 0 128.87 125.03 14.59 o 5 14 0 152.84 161.04 21.25 o 6 14 0 379.09 364.65 35.27 o 7 14 0 46.84 33.65 14.09 o 8 14 0 38.93 20.88 13.14 o 9 14 0 0.42 -8.30 12.31 o 10 14 0 50.49 58.23 18.62 o 11 14 0 127.03 82.83 48.19 o 12 14 0 312.72 282.50 51.93 o 13 14 0 4.79 18.78 25.17 o 14 14 0 31.58 53.23 32.08 o 15 14 0 39.32 21.51 36.29 o 1 15 0 1316.83 1377.29 58.11 o 2 15 0 608.70 665.79 33.36 o 3 15 0 0.04 12.06 8.20 o 4 15 0 374.64 376.40 36.24 o 5 15 0 3696.14 3490.16 78.98 o 6 15 0 7.58 2.14 16.38 o 7 15 0 662.92 779.58 44.66 o 8 15 0 79.31 67.99 17.37 o 9 15 0 39.65 50.11 16.12 o 10 15 0 17.14 31.54 25.44 o 11 15 0 48.59 27.30 20.78 o 12 15 0 32.41 -11.77 24.73 o 13 15 0 43.50 19.70 25.27 o 14 15 0 54.64 70.52 36.12 o 15 15 0 111.07 170.59 46.24 o 0 16 0 36.50 47.11 17.12 o 1 16 0 1001.56 937.16 34.91 o 2 16 0 927.99 829.21 33.53 o 3 16 0 132.46 110.12 29.40 o 4 16 0 114.20 162.83 24.21 o 5 16 0 113.76 127.86 21.90 o 6 16 0 884.79 949.90 52.21 o 7 16 0 429.60 406.26 36.14 o 8 16 0 596.04 625.74 43.54 o 9 16 0 353.07 441.26 45.06 o 10 16 0 32.53 68.05 26.35 o 11 16 0 31.02 23.47 23.91 o 12 16 0 25.27 16.59 22.98 o 13 16 0 141.60 242.39 52.92 o 14 16 0 12.65 7.32 30.19 o 1 17 0 556.86 601.39 31.34 o 2 17 0 468.75 464.44 28.84 o 3 17 0 9.95 30.51 17.26 o 4 17 0 0.27 1.69 10.10 o 5 17 0 835.12 832.81 76.97 o 6 17 0 5.71 14.66 14.26 o 7 17 0 236.32 210.27 27.30 o 8 17 0 32.69 10.18 15.67 o 9 17 0 1117.39 1144.26 91.45 o 10 17 0 210.02 299.77 52.37 o 11 17 0 162.07 138.16 42.03 o 12 17 0 49.10 15.10 27.76 o 13 17 0 7.61 15.86 25.01 o 14 17 0 1.68 46.89 31.16 o 0 18 0 155.17 169.02 29.18 o 1 18 0 555.17 614.21 34.95 o 2 18 0 2025.68 1865.69 65.86 o 3 18 0 8.60 -10.24 12.33 o 4 18 0 3.73 15.15 12.35 o 5 18 0 30.11 29.62 14.22 o 6 18 0 207.32 188.78 35.01 o 7 18 0 66.24 79.97 21.08 o 8 18 0 88.70 89.83 22.76 o 9 18 0 109.33 119.93 33.83 o 10 18 0 25.81 60.39 48.80 o 11 18 0 299.06 310.72 61.91 o 12 18 0 65.05 20.36 29.02 o 13 18 0 44.43 44.19 30.40 o 14 18 0 1.14 -22.30 39.65 o 1 19 0 11.05 11.76 17.36 o 2 19 0 357.10 346.98 34.90 o 3 19 0 84.99 105.36 21.32 o 4 19 0 133.38 135.75 23.74 o 5 19 0 721.84 746.21 52.87 o 6 19 0 1019.11 908.76 59.31 o 7 19 0 191.05 208.12 32.63 o 8 19 0 287.71 300.33 37.76 o 9 19 0 3.35 -0.66 22.13 o 10 19 0 55.85 53.61 28.62 o 11 19 0 56.09 -22.41 24.14 o 12 19 0 58.69 70.01 37.95 o 13 19 0 43.21 37.52 41.17 o 0 20 0 167.42 229.35 54.90 o 1 20 0 714.31 644.78 45.98 o 2 20 0 2308.34 2274.58 76.05 o 3 20 0 229.94 308.74 35.16 o 4 20 0 518.32 540.05 46.38 o 5 20 0 1330.19 1240.75 63.57 o 6 20 0 1583.62 1506.29 67.49 o 7 20 0 29.70 35.75 18.52 o 8 20 0 203.94 254.34 36.50 o 9 20 0 18.05 9.42 23.53 o 10 20 0 207.15 127.77 39.99 o 11 20 0 1.36 -9.32 25.23 o 12 20 0 23.36 3.96 25.93 o 13 20 0 27.94 -18.77 29.35 o 1 21 0 223.88 380.07 51.67 o 2 21 0 10.18 43.84 16.84 o 3 21 0 894.16 885.59 54.31 o 4 21 0 1308.88 1276.06 62.99 o 5 21 0 1375.64 1259.53 63.89 o 6 21 0 26.32 23.63 25.41 o 7 21 0 56.48 72.98 23.04 o 8 21 0 186.64 156.49 29.88 o 9 21 0 2.28 -9.35 51.24 o 10 21 0 20.46 -18.43 29.28 o 11 21 0 3.90 9.69 44.53 o 12 21 0 0.41 41.14 32.70 o 0 22 0 1255.38 1084.52 115.89 o 1 22 0 124.72 135.83 32.21 o 2 22 0 349.19 433.74 68.32 o 3 22 0 121.23 184.71 29.87 o 4 22 0 178.22 248.21 33.44 o 5 22 0 184.89 166.30 43.37 o 6 22 0 213.56 162.58 30.25 o 7 22 0 10.96 55.44 29.74 o 8 22 0 270.83 309.21 53.23 o 9 22 0 114.27 157.60 46.97 o 10 22 0 73.50 87.10 59.47 o 11 22 0 7.06 11.74 33.55 o 12 22 0 29.60 30.72 59.78 o 1 23 0 36.76 38.22 20.05 o 2 23 0 193.63 151.22 35.68 o 3 23 0 9.59 6.98 17.11 o 4 23 0 63.47 64.67 19.06 o 5 23 0 202.99 207.60 32.39 o 6 23 0 30.13 40.63 19.90 o 7 23 0 58.18 81.71 41.83 o 8 23 0 5.15 10.74 23.48 o 9 23 0 38.83 23.78 29.97 o 10 23 0 9.23 34.31 31.21 o 11 23 0 7.40 34.02 68.01 o 0 24 0 349.78 269.60 62.22 o 1 24 0 38.49 55.36 21.51 o 2 24 0 957.51 832.05 77.84 o 3 24 0 88.74 129.00 36.60 o 4 24 0 390.88 416.59 96.37 o 5 24 0 13.93 17.18 17.62 o 6 24 0 317.29 295.16 37.33 o 7 24 0 16.76 46.99 20.24 o 8 24 0 42.32 79.47 74.42 o 9 24 0 0.61 2.82 25.33 o 10 24 0 75.01 107.40 54.59 o 1 25 0 1.14 -12.59 12.59 o 2 25 0 127.75 149.65 32.80 o 3 25 0 221.80 244.42 45.90 o 4 25 0 391.26 300.80 47.73 o 5 25 0 11.15 7.22 20.48 o 6 25 0 3.53 -16.94 18.01 o 7 25 0 2.59 17.54 23.10 o 8 25 0 37.13 63.08 32.13 o 9 25 0 99.63 52.54 30.18 o 0 26 0 811.29 674.62 105.52 o 1 26 0 0.09 -6.38 24.40 o 2 26 0 23.39 19.40 20.22 o 3 26 0 2.28 -4.85 19.52 o 4 26 0 76.72 69.48 32.94 o 5 26 0 0.80 -7.83 22.26 o 6 26 0 259.21 280.73 49.59 o 7 26 0 70.68 82.83 48.49 o 8 26 0 4.83 -11.30 23.86 o 1 27 0 65.64 60.48 24.84 o 2 27 0 154.60 239.47 90.27 o 3 27 0 3.23 -14.41 14.41 o 4 27 0 209.09 162.86 53.68 o 5 27 0 41.22 28.97 32.33 o 6 27 0 289.18 293.39 79.30 o 7 27 0 148.72 162.25 56.73 o 0 28 0 399.77 395.87 81.74 o 1 28 0 7.05 -6.47 19.45 o 2 28 0 64.99 104.14 31.81 o 3 28 0 1.05 -18.78 28.06 o 4 28 0 94.24 71.29 43.31 o 5 28 0 66.48 102.25 32.24 o 6 28 0 32.10 28.06 32.94 o 1 29 0 22.10 9.35 37.82 o 2 29 0 6.27 15.56 62.83 o 3 29 0 135.30 143.22 38.59 o 4 29 0 122.73 150.62 93.63 o 0 30 0 207.55 228.13 62.83 o 1 30 0 0.34 14.87 20.52 o -17 1 1 72.60 54.29 45.75 o -16 1 1 119.14 49.06 30.62 o -15 1 1 68.62 123.89 34.16 o -14 1 1 269.00 222.15 41.61 o -13 1 1 132.99 98.87 27.99 o -12 1 1 309.18 274.61 27.57 o -11 1 1 22.19 27.67 11.45 o -10 1 1 323.47 383.37 32.92 o -9 1 1 57.31 36.67 16.85 o -8 1 1 0.01 -7.54 7.54 o -7 1 1 429.82 452.70 26.25 o -6 1 1 3656.99 3649.21 66.14 o -5 1 1 617.04 585.41 23.38 o -4 1 1 95279.21 108502.11 740.44 o -3 1 1 312.20 295.67 11.15 o -2 1 1 108.78 11.74 11.42 o -1 1 1 1661.00 1492.17 20.84 o 0 1 1 7415.11 8930.48 67.95 o 1 1 1 672.72 550.97 17.78 o 2 1 1 7575.21 7174.87 72.17 o 3 1 1 3610.35 3888.27 53.18 o 4 1 1 92.62 71.96 10.63 o 5 1 1 34.22 49.93 11.20 o 6 1 1 2815.09 2677.43 121.38 o 7 1 1 32.68 18.11 13.15 o 8 1 1 1527.33 1392.73 79.91 o 9 1 1 522.26 491.33 45.72 o 10 1 1 2294.73 2246.05 87.48 o 11 1 1 306.07 337.92 63.44 o 12 1 1 81.19 85.48 25.35 o 13 1 1 221.05 231.88 43.61 o 14 1 1 161.32 326.72 49.80 o 15 1 1 26.60 27.47 21.27 o -17 2 1 32.45 45.14 42.09 o -16 2 1 73.72 40.94 26.96 o -15 2 1 6.34 -6.15 22.27 o -14 2 1 6.56 -15.25 21.04 o -13 2 1 89.96 79.82 20.81 o -12 2 1 26.59 33.06 21.83 o -11 2 1 104.30 113.00 24.19 o -10 2 1 615.95 645.05 39.98 o -9 2 1 62.61 88.35 15.78 o -8 2 1 1037.31 1085.52 41.09 o -7 2 1 783.72 763.71 31.98 o -6 2 1 939.50 896.84 69.97 o -5 2 1 170.29 226.21 17.29 o -4 2 1 36271.74 39937.48 416.33 o -3 2 1 5571.34 6183.18 56.80 o -2 2 1 12511.45 11908.50 108.64 o -1 2 1 74.09 156.25 11.19 o 0 2 1 824.56 497.99 10.97 o 1 2 1 1028.21 1172.80 24.63 o 2 2 1 2754.16 2551.71 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