#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/33/2213362.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213362_Fobs loop_ _publ_author_name 'Ali, Hapipah M.' 'Puvaneswary, Subramaniam' 'Wan Jefrey, Basirun' 'Ng, Seik Weng' _publ_section_title ; Bis[1,3-dihydroxy-2-hydroxymethyl-2-(5-nitro-2-oxidobenzylideneamino)propane-\k^3^N,O,O']zinc(II) trihydrate ; _journal_coeditor_code HB2383 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1532 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.227 _cell_angle_gamma 90.000 _cell_length_a 10.7231 _cell_length_b 11.7429 _cell_length_c 21.7538 _exptl_crystal_F_000 1368.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file hb2383Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 228.59 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 34026.25 33469.76 368.96 o 4 0 0 33.58 16.18 2.50 o 6 0 0 1151.60 1028.64 16.02 o 8 0 0 12377.96 12383.06 156.96 o 10 0 0 158.70 142.69 7.96 o 12 0 0 186.92 203.71 14.13 o 1 1 0 22282.91 13161.07 420.51 o 2 1 0 493.02 503.43 7.07 o 3 1 0 63.07 73.28 3.67 o 4 1 0 407.61 394.67 4.55 o 5 1 0 327.46 233.40 3.79 o 6 1 0 25.17 39.56 2.16 o 7 1 0 3581.57 3446.85 31.51 o 8 1 0 262.58 280.76 5.47 o 9 1 0 587.39 621.16 8.71 o 10 1 0 3.19 9.87 3.89 o 11 1 0 170.90 180.53 8.67 o 12 1 0 2071.12 2089.67 35.09 o 13 1 0 476.85 522.34 20.42 o 0 2 0 52254.99 39035.33 1202.31 o 1 2 0 917.17 1023.28 7.10 o 2 2 0 1675.07 1546.85 12.31 o 3 2 0 2895.11 2650.49 19.91 o 4 2 0 4866.42 4710.48 40.37 o 5 2 0 959.78 1088.01 11.30 o 6 2 0 3153.72 2948.22 27.32 o 7 2 0 1850.88 1810.00 19.61 o 8 2 0 9058.91 8729.16 83.19 o 9 2 0 8.84 8.15 3.86 o 10 2 0 89.94 96.58 5.30 o 11 2 0 736.34 756.24 16.21 o 12 2 0 1244.39 1303.25 37.69 o 13 2 0 1555.36 1598.53 37.77 o 1 3 0 16427.17 17016.97 118.32 o 2 3 0 749.19 780.54 6.65 o 3 3 0 26.43 41.02 2.12 o 4 3 0 607.62 632.43 7.14 o 5 3 0 5526.57 5668.09 48.65 o 6 3 0 4520.87 4646.84 42.07 o 7 3 0 1103.48 1091.65 11.95 o 8 3 0 2425.10 2380.08 24.61 o 9 3 0 960.13 887.48 12.04 o 10 3 0 3516.89 3382.07 39.65 o 11 3 0 1349.59 1311.18 26.53 o 12 3 0 1532.23 1618.59 30.00 o 13 3 0 324.39 367.16 19.36 o 0 4 0 2590.06 2804.98 29.50 o 1 4 0 7507.13 7849.09 57.31 o 2 4 0 65.32 120.16 3.43 o 3 4 0 18.93 10.45 1.46 o 4 4 0 12027.22 12355.47 100.21 o 5 4 0 3445.81 3329.08 30.58 o 6 4 0 296.23 262.37 5.07 o 7 4 0 1397.89 1267.72 13.45 o 8 4 0 199.94 194.88 5.88 o 9 4 0 26.51 21.67 4.41 o 10 4 0 30.31 28.94 5.00 o 11 4 0 187.02 181.77 8.89 o 12 4 0 345.20 385.00 14.05 o 13 4 0 1128.35 1179.59 30.68 o 1 5 0 1513.90 1631.19 14.51 o 2 5 0 1017.73 1130.79 10.36 o 3 5 0 294.95 335.27 7.71 o 4 5 0 6932.69 6860.13 56.07 o 5 5 0 133.39 147.55 4.10 o 6 5 0 3318.58 3258.26 29.39 o 7 5 0 31.47 26.25 3.40 o 8 5 0 2240.82 2153.86 24.72 o 9 5 0 266.62 242.93 7.34 o 10 5 0 1707.44 1631.47 22.06 o 11 5 0 92.87 107.61 7.08 o 12 5 0 533.40 548.15 16.87 o 0 6 0 87.98 95.96 3.51 o 1 6 0 421.25 461.08 5.16 o 2 6 0 2496.58 2671.61 22.57 o 3 6 0 1045.78 1157.19 10.40 o 4 6 0 2370.89 2434.11 20.58 o 5 6 0 4434.57 4644.72 41.51 o 6 6 0 1068.73 1084.10 13.83 o 7 6 0 1813.77 1699.11 18.57 o 8 6 0 177.10 207.17 8.02 o 9 6 0 119.80 148.49 6.40 o 10 6 0 111.14 111.43 6.28 o 11 6 0 36.86 31.84 7.47 o 12 6 0 73.44 94.19 9.66 o 1 7 0 1155.96 1209.31 13.42 o 2 7 0 701.87 756.99 7.62 o 3 7 0 349.14 333.98 4.72 o 4 7 0 15.20 29.67 2.35 o 5 7 0 134.67 141.44 4.79 o 6 7 0 2498.80 2522.40 24.34 o 7 7 0 417.46 384.54 9.35 o 8 7 0 1069.15 1039.46 16.29 o 9 7 0 1591.31 1541.07 21.03 o 10 7 0 671.12 672.82 15.96 o 11 7 0 89.02 105.68 9.84 o 12 7 0 1764.91 1825.50 35.40 o 0 8 0 518.84 541.13 9.68 o 1 8 0 33.12 41.43 2.21 o 2 8 0 1277.54 1249.70 12.32 o 3 8 0 933.46 985.51 12.44 o 4 8 0 1573.06 1555.95 15.84 o 5 8 0 51.06 71.38 3.67 o 6 8 0 161.81 157.65 5.41 o 7 8 0 201.88 160.33 5.80 o 8 8 0 1105.09 1098.88 26.02 o 9 8 0 1126.42 1270.80 23.31 o 10 8 0 668.79 659.72 16.18 o 11 8 0 715.21 743.91 19.99 o 1 9 0 2803.99 2771.04 25.43 o 2 9 0 677.02 653.63 7.65 o 3 9 0 956.62 939.38 11.83 o 4 9 0 281.27 291.83 6.18 o 5 9 0 15.70 25.98 3.92 o 6 9 0 216.91 212.55 7.20 o 7 9 0 2709.52 2633.84 37.24 o 8 9 0 1884.14 1774.65 29.27 o 9 9 0 1397.00 1376.31 24.96 o 10 9 0 15.35 19.41 6.76 o 11 9 0 17.28 32.72 7.96 o 0 10 0 4797.93 4574.54 70.08 o 1 10 0 220.81 225.52 5.61 o 2 10 0 4253.04 4227.18 41.61 o 3 10 0 0.08 4.70 3.56 o 4 10 0 4763.95 4703.11 50.13 o 5 10 0 1591.68 1558.63 20.25 o 6 10 0 1196.80 1234.08 18.17 o 7 10 0 1.10 8.49 5.98 o 8 10 0 430.18 413.12 12.94 o 9 10 0 660.36 670.03 16.37 o 10 10 0 574.41 553.63 15.98 o 1 11 0 3163.52 3129.74 35.40 o 2 11 0 2.28 -3.70 3.74 o 3 11 0 3797.13 3680.54 43.67 o 4 11 0 342.97 369.20 8.97 o 5 11 0 3931.45 3808.72 45.48 o 6 11 0 1206.72 1151.87 21.12 o 7 11 0 55.97 49.02 7.08 o 8 11 0 107.40 94.46 8.10 o 9 11 0 297.82 334.79 12.35 o 0 12 0 17.08 10.92 6.80 o 1 12 0 360.42 338.91 9.19 o 2 12 0 2796.15 2742.95 35.47 o 3 12 0 47.96 34.10 5.22 o 4 12 0 4660.27 4594.57 53.98 o 5 12 0 271.22 298.85 9.11 o 6 12 0 1518.98 1436.14 25.29 o 7 12 0 316.43 343.29 13.04 o 8 12 0 11.38 10.58 7.16 o 1 13 0 17.31 21.08 5.31 o 2 13 0 75.24 64.05 6.18 o 3 13 0 1362.16 1381.06 22.00 o 4 13 0 217.52 249.03 8.78 o 5 13 0 382.48 373.74 10.96 o 6 13 0 674.93 670.71 16.11 o 7 13 0 392.12 425.56 13.61 o 0 14 0 280.47 258.38 12.30 o 1 14 0 94.70 86.41 7.03 o 2 14 0 123.67 126.88 7.49 o 3 14 0 56.90 61.72 6.79 o 4 14 0 86.02 100.14 7.44 o 5 14 0 7.94 7.35 7.03 o 1 15 0 425.29 444.20 15.18 o 2 15 0 416.55 433.75 12.38 o -13 0 1 1736.42 1723.57 56.67 o -11 0 1 1502.30 1494.27 28.99 o -9 0 1 315.80 317.25 11.06 o -7 0 1 7327.64 7366.59 94.81 o -5 0 1 64.32 35.74 3.20 o -3 0 1 6813.76 6999.45 77.65 o 3 0 1 3400.55 3024.55 34.28 o 5 0 1 363.41 385.19 6.94 o 7 0 1 1591.86 1606.24 23.70 o 9 0 1 2.40 3.03 4.14 o 11 0 1 7.76 11.39 6.98 o 13 0 1 1583.59 1644.50 93.79 o -13 1 1 360.83 358.14 18.34 o -12 1 1 1478.94 1593.85 26.76 o -11 1 1 211.83 228.58 10.19 o -10 1 1 1032.04 1013.72 15.29 o -9 1 1 128.05 134.53 4.44 o -8 1 1 15229.79 15123.17 130.57 o -7 1 1 949.45 940.54 10.62 o -6 1 1 1457.78 1330.30 14.11 o -5 1 1 953.26 915.91 9.41 o -4 1 1 8369.66 8303.70 63.50 o -3 1 1 1628.88 1525.59 12.18 o -2 1 1 3644.88 3639.97 26.82 o -1 1 1 5955.44 4240.75 196.94 o 1 1 1 8935.00 8925.51 111.55 o 2 1 1 6958.44 7237.05 52.11 o 3 1 1 1044.58 1024.83 8.63 o 4 1 1 6607.11 7119.08 56.16 o 5 1 1 345.49 279.16 4.15 o 6 1 1 22.62 8.04 1.89 o 7 1 1 1610.58 1481.13 15.05 o 8 1 1 340.57 336.10 6.04 o 9 1 1 197.53 180.05 5.40 o 10 1 1 402.41 431.58 8.69 o 11 1 1 247.54 257.40 11.23 o 12 1 1 1569.02 1493.61 27.58 o 13 1 1 613.08 636.98 22.81 o -13 2 1 548.12 557.03 21.74 o -12 2 1 5.89 3.73 7.65 o -11 2 1 384.02 383.15 11.48 o -10 2 1 139.65 143.47 5.95 o -9 2 1 4809.71 4608.75 46.11 o -8 2 1 359.61 390.96 7.71 o -7 2 1 7844.12 7794.77 70.88 o -6 2 1 128.27 121.25 3.45 o -5 2 1 100.34 78.11 2.60 o -4 2 1 1102.36 1366.89 12.31 o -3 2 1 14083.27 14069.45 101.49 o -2 2 1 42139.61 42584.22 294.30 o -1 2 1 842.32 807.61 7.01 o 0 2 1 2269.52 2289.39 64.30 o 1 2 1 338.67 368.69 3.13 o 2 2 1 10678.24 11321.84 78.13 o 3 2 1 3827.05 4213.00 35.84 o 4 2 1 8095.72 7610.17 63.98 o 5 2 1 0.62 9.75 2.64 o 6 2 1 791.55 756.48 8.69 o 7 2 1 1073.19 1091.33 11.82 o 8 2 1 262.76 279.83 9.57 o 9 2 1 847.24 774.75 11.42 o 10 2 1 46.45 40.80 4.94 o 11 2 1 6.25 6.68 6.28 o 12 2 1 702.99 748.31 19.57 o 13 2 1 75.17 77.12 12.38 o -13 3 1 210.34 203.54 14.59 o -12 3 1 313.89 318.31 17.28 o -11 3 1 251.62 245.51 9.91 o -10 3 1 441.71 448.26 10.00 o -9 3 1 756.15 756.49 10.80 o -8 3 1 5212.78 5168.07 49.28 o -7 3 1 701.45 723.24 8.97 o -6 3 1 3190.28 3097.56 27.82 o -5 3 1 224.69 180.53 3.46 o -4 3 1 12014.92 12875.67 98.13 o -3 3 1 31914.39 31841.79 272.60 o -2 3 1 23505.93 24054.52 171.98 o -1 3 1 24549.60 24830.71 190.18 o 0 3 1 38916.51 39383.80 268.81 o 1 3 1 6308.96 6384.94 47.15 o 2 3 1 1449.02 1575.45 11.68 o 3 3 1 1177.90 1049.40 9.41 o 4 3 1 3301.23 3605.05 30.36 o 5 3 1 21835.80 22328.76 198.00 o 6 3 1 466.65 546.51 7.16 o 7 3 1 4936.65 4804.66 43.90 o 8 3 1 870.38 810.54 11.05 o 9 3 1 1086.15 1110.40 13.88 o 10 3 1 281.37 276.74 8.32 o 11 3 1 126.37 129.91 7.04 o 12 3 1 351.49 358.57 14.48 o 13 3 1 1565.32 1642.39 38.90 o -13 4 1 122.18 150.82 12.18 o -12 4 1 101.47 133.20 9.82 o -11 4 1 257.68 268.83 9.45 o -10 4 1 300.08 311.81 10.85 o -9 4 1 1380.82 1392.82 17.70 o -8 4 1 436.79 409.18 7.67 o -7 4 1 29.22 26.48 3.09 o -6 4 1 711.21 747.81 8.34 o -5 4 1 3246.56 3519.38 30.85 o -4 4 1 3307.70 3545.40 29.18 o -3 4 1 10900.79 11634.17 99.87 o -2 4 1 13335.55 13943.22 114.58 o -1 4 1 19896.03 20130.53 149.13 o 0 4 1 7590.99 7613.63 54.22 o 1 4 1 1214.68 1187.70 10.81 o 2 4 1 1548.93 1416.13 11.10 o 3 4 1 611.56 614.35 6.47 o 4 4 1 3094.60 2873.37 28.59 o 5 4 1 461.88 515.11 7.77 o 6 4 1 7102.79 7019.56 62.48 o 7 4 1 427.44 398.84 6.59 o 8 4 1 224.79 230.77 7.35 o 9 4 1 192.27 175.47 6.36 o 10 4 1 1144.23 1152.57 17.22 o 11 4 1 71.94 66.21 6.29 o 12 4 1 1937.91 1989.49 35.00 o 13 4 1 22.88 20.36 11.25 o -13 5 1 85.76 106.03 19.10 o -12 5 1 60.89 83.48 8.22 o -11 5 1 187.88 219.69 10.30 o -10 5 1 24.10 24.71 5.16 o -9 5 1 0.39 0.88 4.22 o -8 5 1 38.76 52.90 5.24 o -7 5 1 713.90 739.36 9.73 o -6 5 1 217.48 187.24 5.83 o -5 5 1 468.82 458.29 6.85 o -4 5 1 1302.13 1412.15 15.55 o -3 5 1 20900.42 22138.68 171.19 o -2 5 1 3778.14 4143.12 38.55 o -1 5 1 89.36 93.47 2.97 o 0 5 1 1094.91 1132.21 10.23 o 1 5 1 433.83 320.75 5.53 o 2 5 1 6.87 5.77 1.86 o 3 5 1 3119.02 3003.58 23.94 o 4 5 1 601.99 699.79 7.30 o 5 5 1 9182.48 9115.10 83.42 o 6 5 1 254.70 241.02 5.47 o 7 5 1 2660.11 2580.73 24.28 o 8 5 1 175.54 175.51 5.96 o 9 5 1 1727.15 1836.98 23.75 o 10 5 1 0.66 -6.83 4.70 o 11 5 1 3130.61 3249.95 42.95 o 12 5 1 114.39 121.92 10.20 o -12 6 1 2.79 11.24 8.01 o -11 6 1 2.96 8.22 6.93 o -10 6 1 334.05 355.25 12.40 o -9 6 1 114.39 129.47 6.13 o -8 6 1 85.21 74.92 4.78 o -7 6 1 186.37 203.53 5.97 o -6 6 1 151.24 136.78 4.14 o -5 6 1 4656.06 4955.73 44.93 o -4 6 1 918.19 985.05 9.65 o -3 6 1 3945.51 4108.64 35.83 o -2 6 1 13.75 14.80 1.83 o -1 6 1 4196.83 4270.69 34.73 o 0 6 1 2352.72 2277.20 18.93 o 1 6 1 2365.04 2464.91 21.53 o 2 6 1 5152.66 5329.54 43.44 o 3 6 1 665.03 748.78 7.27 o 4 6 1 1884.23 1777.86 15.58 o 5 6 1 652.76 756.38 10.24 o 6 6 1 5530.67 5626.25 48.97 o 7 6 1 1054.48 1117.07 14.75 o 8 6 1 4897.55 4888.56 50.91 o 9 6 1 8.42 8.89 4.68 o 10 6 1 2750.45 2795.86 35.66 o 11 6 1 87.84 105.92 7.56 o 12 6 1 649.11 647.40 22.09 o -12 7 1 8.82 6.49 8.37 o -11 7 1 150.90 169.11 10.78 o -10 7 1 158.99 170.56 8.35 o -9 7 1 4.10 7.75 4.95 o -8 7 1 1831.80 1770.40 23.00 o -7 7 1 67.74 90.99 5.16 o -6 7 1 691.38 716.59 15.57 o -5 7 1 948.81 887.51 9.70 o -4 7 1 254.77 258.24 6.26 o -3 7 1 641.93 623.22 7.27 o -2 7 1 1552.26 1660.04 14.79 o -1 7 1 1783.28 1734.12 15.17 o 0 7 1 3287.54 3512.09 28.92 o 1 7 1 7725.81 7568.51 61.11 o 2 7 1 130.31 136.85 3.16 o 3 7 1 1416.51 1268.00 12.54 o 4 7 1 1088.57 1174.13 12.04 o 5 7 1 3882.77 3822.22 33.47 o 6 7 1 243.32 248.58 6.59 o 7 7 1 2321.69 2204.44 26.09 o 8 7 1 1181.49 1161.53 16.77 o 9 7 1 2211.97 2263.61 28.51 o 10 7 1 128.96 125.46 8.45 o 11 7 1 2225.60 2269.39 37.03 o 12 7 1 234.17 249.88 14.05 o -11 8 1 797.54 833.77 21.33 o -10 8 1 74.54 86.05 8.05 o -9 8 1 1813.15 1815.17 28.33 o -8 8 1 51.15 57.64 5.75 o -7 8 1 3054.49 2942.31 34.85 o -6 8 1 244.87 245.42 7.19 o -5 8 1 9021.40 8955.00 83.59 o -4 8 1 148.32 155.43 4.35 o -3 8 1 10315.73 10233.99 87.63 o -2 8 1 429.44 386.78 5.49 o -1 8 1 4706.16 4720.14 39.76 o 0 8 1 2272.09 2249.67 20.79 o 1 8 1 719.03 732.35 8.31 o 2 8 1 732.32 708.99 14.65 o 3 8 1 1137.73 1178.06 14.99 o 4 8 1 2501.88 2476.61 30.62 o 5 8 1 165.77 167.42 4.42 o 6 8 1 199.13 217.71 6.08 o 7 8 1 343.82 353.12 8.06 o 8 8 1 2636.78 2502.79 52.39 o 9 8 1 1.78 9.41 6.20 o 10 8 1 127.59 119.44 9.29 o 11 8 1 390.87 388.11 14.54 o -11 9 1 171.22 210.10 11.10 o -10 9 1 636.85 597.80 18.10 o -9 9 1 18.55 28.03 6.84 o -8 9 1 3002.88 2897.72 43.60 o -7 9 1 459.88 479.51 10.89 o -6 9 1 1904.00 1920.03 25.77 o -5 9 1 8.46 12.30 3.88 o -4 9 1 3603.34 3495.17 39.45 o -3 9 1 37.34 31.77 2.99 o -2 9 1 52.41 41.97 3.22 o -1 9 1 666.06 663.56 7.89 o 0 9 1 1378.50 1422.28 14.30 o 1 9 1 1545.57 1582.69 17.71 o 2 9 1 554.44 555.37 7.44 o 3 9 1 2060.57 2054.41 20.86 o 4 9 1 1452.46 1446.48 15.60 o 5 9 1 8.10 17.26 3.84 o 6 9 1 241.26 250.77 6.87 o 7 9 1 328.28 296.01 9.41 o 8 9 1 23.92 21.75 5.86 o 9 9 1 2.41 7.99 6.10 o 10 9 1 333.99 355.24 11.38 o -10 10 1 3.51 4.68 7.32 o -9 10 1 857.38 851.96 18.97 o -8 10 1 2.96 7.73 6.46 o -7 10 1 1854.37 1877.93 30.48 o -6 10 1 767.12 724.41 14.03 o -5 10 1 4302.89 4317.56 48.41 o -4 10 1 1021.09 967.22 19.62 o -3 10 1 1705.54 1708.34 20.43 o -2 10 1 74.40 78.25 4.47 o -1 10 1 893.34 870.76 12.38 o 0 10 1 179.91 182.40 5.04 o 1 10 1 1017.07 1034.21 13.01 o 2 10 1 197.40 195.30 6.37 o 3 10 1 1206.65 1184.00 14.45 o 4 10 1 370.43 351.61 11.13 o 5 10 1 8.65 3.11 4.12 o 6 10 1 160.67 139.86 6.25 o 7 10 1 1.13 0.63 5.94 o 8 10 1 190.63 194.83 9.22 o 9 10 1 6.95 13.85 7.15 o 10 10 1 494.47 526.46 15.35 o -9 11 1 14.87 16.48 7.31 o -8 11 1 20.10 24.93 6.94 o -7 11 1 7.34 5.23 6.16 o -6 11 1 387.77 382.15 10.38 o -5 11 1 99.33 87.49 5.73 o -4 11 1 90.32 111.59 5.83 o -3 11 1 62.39 88.30 4.78 o -2 11 1 604.47 582.35 10.16 o -1 11 1 349.68 338.59 7.83 o 0 11 1 373.74 368.64 8.02 o 1 11 1 11.43 16.57 3.92 o 2 11 1 238.15 230.25 6.30 o 3 11 1 55.59 63.20 5.05 o 4 11 1 818.48 814.36 13.52 o 5 11 1 431.63 448.58 11.92 o 6 11 1 0.87 2.04 5.61 o 7 11 1 71.91 86.94 7.62 o 8 11 1 291.32 310.59 11.31 o 9 11 1 26.11 14.12 8.87 o -8 12 1 16.09 21.42 7.40 o -7 12 1 322.59 366.57 12.26 o -6 12 1 83.74 69.37 7.42 o -5 12 1 396.79 410.73 10.47 o -4 12 1 580.42 624.44 13.27 o -3 12 1 494.62 468.07 11.22 o -2 12 1 1825.23 1756.42 25.88 o -1 12 1 115.30 119.11 6.06 o 0 12 1 32.45 34.13 5.09 o 1 12 1 1071.33 1019.11 20.41 o 2 12 1 1444.67 1373.25 20.34 o 3 12 1 354.40 348.36 9.31 o 4 12 1 95.60 112.57 8.32 o 5 12 1 44.95 35.68 5.65 o 6 12 1 202.09 238.08 13.16 o 7 12 1 19.03 24.94 7.09 o 8 12 1 8.17 13.52 7.25 o -7 13 1 7.45 1.06 7.15 o -6 13 1 91.09 83.21 8.10 o -5 13 1 47.88 58.87 6.55 o -4 13 1 69.03 73.30 6.56 o -3 13 1 2294.21 2258.62 32.31 o -2 13 1 224.14 211.15 11.07 o -1 13 1 1272.85 1268.65 20.63 o 0 13 1 142.02 155.29 7.06 o 1 13 1 474.67 480.58 10.94 o 2 13 1 42.16 28.52 5.78 o 3 13 1 1258.98 1229.19 20.26 o 4 13 1 0.91 6.54 5.37 o 5 13 1 486.84 472.39 13.23 o 6 13 1 6.07 0.90 6.63 o 7 13 1 755.74 754.49 17.70 o -5 14 1 18.94 10.48 7.27 o -4 14 1 1156.92 1116.57 20.38 o -3 14 1 98.31 93.92 7.32 o -2 14 1 1099.97 1094.75 19.17 o -1 14 1 123.91 138.44 7.72 o 0 14 1 593.65 589.51 12.63 o 1 14 1 475.76 445.07 11.80 o 2 14 1 1329.65 1350.31 22.12 o 3 14 1 4.48 -0.27 5.86 o 4 14 1 2198.84 2198.15 32.18 o 5 14 1 8.64 7.51 6.90 o -2 15 1 8.57 5.85 6.43 o -1 15 1 105.31 120.22 7.92 o 0 15 1 205.01 194.16 8.45 o 1 15 1 2272.18 2344.71 34.11 o 2 15 1 1448.90 1438.60 23.70 o -12 0 2 1514.01 1529.84 50.02 o -10 0 2 134.52 128.46 6.29 o -8 0 2 2746.45 2714.48 37.98 o -6 0 2 26.46 42.86 4.89 o -4 0 2 272.76 285.39 6.93 o -2 0 2 3416.57 3540.21 39.59 o 0 0 2 231.38 -0.44 0.29 o 2 0 2 2951.17 2750.89 26.58 o 4 0 2 93.21 53.32 2.66 o 6 0 2 157.41 98.96 4.75 o 8 0 2 1506.62 1442.02 28.20 o 10 0 2 2057.95 2080.65 36.92 o 12 0 2 3417.19 3326.35 72.83 o -13 1 2 23.45 33.62 11.46 o -12 1 2 104.67 98.47 10.29 o -11 1 2 3110.78 3053.34 40.64 o -10 1 2 208.32 236.56 11.19 o -9 1 2 3939.18 3890.29 38.60 o -8 1 2 1602.12 1531.96 16.02 o -7 1 2 3177.83 3196.08 30.85 o -6 1 2 1677.59 1847.71 19.48 o -5 1 2 3017.57 3027.25 29.43 o -4 1 2 199.76 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