#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:28:51 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181053 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/33/2213363.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213363_Fobs loop_ _publ_author_name 'Ali, Hapipah M.' 'Nazzatush Shimar, Jamaludin' 'Ng, Seik Weng' _publ_section_title ; 2'-[(5-Bromo-1H-indol-3-yl)methylene]-2-(1H-indol-3-yl)acetohydrazide ethyl acetate solvate ; _journal_coeditor_code HB2384 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2731 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 110.665 _cell_angle_gamma 90.000 _cell_length_a 11.9285 _cell_length_b 12.8010 _cell_length_c 15.5177 _exptl_crystal_F_000 992.00 _reflns_d_resolution_high 0.7696 _cod_data_source_file hb2384Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 264.56 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 10069.29 -1.03 0.69 o 2 0 0 3871.51 4081.60 72.59 o 3 0 0 30907.00 31610.71 515.12 o 4 0 0 2396.91 2335.16 40.07 o 5 0 0 1597.54 1706.19 35.13 o 6 0 0 2794.82 2844.48 65.03 o 7 0 0 713.44 802.68 41.17 o 8 0 0 134.28 154.70 12.37 o 9 0 0 4.12 5.95 10.27 o 10 0 0 359.74 342.25 21.44 o 11 0 0 1124.22 1211.16 44.93 o 12 0 0 57.47 71.79 21.01 o 13 0 0 212.46 198.31 38.09 o 14 0 0 715.89 824.42 57.57 o 2 1 0 1059.24 1180.21 14.86 o 3 1 0 24966.96 25878.31 297.88 o 4 1 0 10147.62 10046.88 133.09 o 5 1 0 512.61 439.22 12.14 o 6 1 0 5808.01 5865.31 84.03 o 7 1 0 8376.70 8022.25 124.49 o 8 1 0 2354.42 2300.65 38.93 o 9 1 0 1166.82 1183.68 23.82 o 10 1 0 1840.61 1788.58 35.69 o 11 1 0 9.55 21.98 16.65 o 12 1 0 5.11 -17.90 16.06 o 13 1 0 937.33 881.25 40.23 o 14 1 0 59.33 59.84 28.48 o 0 2 0 7123.75 6702.28 565.57 o 1 2 0 114.62 112.13 2.49 o 2 2 0 68.97 82.28 2.97 o 3 2 0 40477.30 42158.78 518.68 o 4 2 0 1438.16 1299.46 21.62 o 5 2 0 629.78 644.98 13.53 o 6 2 0 1311.88 1214.02 21.53 o 7 2 0 176.13 193.71 8.63 o 8 2 0 2484.52 2456.09 41.38 o 9 2 0 74.94 57.56 11.28 o 10 2 0 193.33 195.17 11.47 o 11 2 0 2556.57 2563.20 62.02 o 12 2 0 574.50 582.10 25.46 o 13 2 0 414.55 402.02 23.87 o 14 2 0 259.70 295.73 29.43 o 1 3 0 7.52 18.16 3.51 o 2 3 0 581.66 635.91 11.60 o 3 3 0 3604.53 3696.73 47.57 o 4 3 0 11493.86 12001.40 162.35 o 5 3 0 2936.41 2904.31 41.35 o 6 3 0 3162.45 3070.56 48.16 o 7 3 0 4477.09 4463.80 65.10 o 8 3 0 1927.07 1983.24 31.96 o 9 3 0 600.73 579.13 17.02 o 10 3 0 3434.17 3513.96 66.25 o 11 3 0 623.62 656.93 22.30 o 12 3 0 182.52 182.01 20.81 o 13 3 0 187.90 208.55 21.03 o 14 3 0 32.98 48.63 24.50 o 0 4 0 10608.48 11740.34 255.90 o 1 4 0 6010.65 6152.08 101.00 o 2 4 0 4098.60 3969.67 65.77 o 3 4 0 8757.76 9179.97 117.27 o 4 4 0 2207.40 2195.83 33.30 o 5 4 0 468.00 455.90 10.14 o 6 4 0 1211.40 1255.03 24.05 o 7 4 0 199.71 199.69 9.53 o 8 4 0 2.91 -3.59 6.37 o 9 4 0 3.57 0.67 9.49 o 10 4 0 45.64 54.44 12.09 o 11 4 0 121.96 140.87 13.93 o 12 4 0 118.92 126.49 18.84 o 13 4 0 117.61 123.27 23.28 o 14 4 0 513.56 487.15 28.13 o 1 5 0 653.28 647.08 11.58 o 2 5 0 1558.88 1518.05 30.02 o 3 5 0 762.69 646.42 12.47 o 4 5 0 5928.65 6250.61 86.52 o 5 5 0 331.19 318.96 8.29 o 6 5 0 2409.87 2392.01 38.54 o 7 5 0 3205.20 3292.06 52.19 o 8 5 0 992.03 951.46 20.82 o 9 5 0 1236.52 1251.23 31.18 o 10 5 0 103.85 118.05 13.35 o 11 5 0 727.80 697.79 23.59 o 12 5 0 8.10 -12.31 16.92 o 13 5 0 0.55 12.35 19.16 o 0 6 0 2839.39 2835.26 69.90 o 1 6 0 4801.44 4967.75 97.91 o 2 6 0 612.51 553.81 14.30 o 3 6 0 270.01 215.73 6.33 o 4 6 0 1841.83 1841.80 29.80 o 5 6 0 157.12 164.51 7.42 o 6 6 0 24.60 32.44 5.88 o 7 6 0 22.07 32.41 7.77 o 8 6 0 10.62 11.64 11.12 o 9 6 0 379.39 360.13 16.23 o 10 6 0 1491.43 1454.58 35.78 o 11 6 0 362.36 386.05 22.58 o 12 6 0 253.58 270.51 26.10 o 13 6 0 34.96 45.25 24.14 o 1 7 0 2532.92 2680.38 54.45 o 2 7 0 447.86 460.26 11.59 o 3 7 0 1323.01 1260.66 20.89 o 4 7 0 1696.42 1761.41 31.95 o 5 7 0 3458.49 3528.66 55.07 o 6 7 0 2824.58 2810.03 47.51 o 7 7 0 2894.91 2865.12 54.47 o 8 7 0 1773.51 1693.92 38.18 o 9 7 0 2027.30 1994.57 44.32 o 10 7 0 9.31 4.04 14.79 o 11 7 0 159.00 158.46 18.35 o 12 7 0 46.48 75.14 23.21 o 13 7 0 65.92 49.13 24.22 o 0 8 0 4903.17 5226.48 114.76 o 1 8 0 4981.00 5195.83 102.96 o 2 8 0 4425.44 4834.10 91.10 o 3 8 0 1461.35 1390.64 25.58 o 4 8 0 17.74 23.81 5.51 o 5 8 0 322.20 357.14 10.89 o 6 8 0 343.97 356.45 11.04 o 7 8 0 92.46 86.39 10.00 o 8 8 0 27.68 18.54 12.43 o 9 8 0 146.60 180.96 16.60 o 10 8 0 15.74 7.06 14.92 o 11 8 0 88.61 78.86 21.08 o 12 8 0 308.92 299.60 26.96 o 1 9 0 1.08 -10.31 8.18 o 2 9 0 27.82 22.78 11.81 o 3 9 0 1712.14 1727.90 38.86 o 4 9 0 1112.24 1152.30 20.72 o 5 9 0 9.25 5.54 6.87 o 6 9 0 500.71 488.24 22.78 o 7 9 0 80.05 88.48 13.21 o 8 9 0 319.76 310.14 18.08 o 9 9 0 9.19 9.57 14.71 o 10 9 0 132.69 133.39 17.62 o 11 9 0 162.98 157.44 19.74 o 12 9 0 47.35 34.49 19.52 o 0 10 0 160.36 158.01 9.10 o 1 10 0 52.44 46.64 8.85 o 2 10 0 465.96 487.33 29.47 o 3 10 0 913.90 938.09 33.76 o 4 10 0 902.32 857.59 20.22 o 5 10 0 1354.12 1343.20 29.36 o 6 10 0 297.58 310.87 13.76 o 7 10 0 5.47 -6.31 12.46 o 8 10 0 156.31 159.92 15.93 o 9 10 0 15.63 7.42 14.69 o 10 10 0 7.56 15.17 16.50 o 11 10 0 538.71 565.62 26.73 o 1 11 0 0.37 -7.63 8.96 o 2 11 0 53.72 47.58 11.72 o 3 11 0 91.33 99.58 15.94 o 4 11 0 7.03 0.90 17.75 o 5 11 0 341.56 365.44 12.98 o 6 11 0 2.86 14.45 11.44 o 7 11 0 364.09 336.80 17.75 o 8 11 0 443.79 414.33 20.41 o 9 11 0 23.49 36.85 17.41 o 10 11 0 7.89 9.12 16.85 o 0 12 0 593.00 652.51 32.97 o 1 12 0 50.43 47.48 9.90 o 2 12 0 31.26 11.86 14.37 o 3 12 0 404.29 379.22 23.68 o 4 12 0 47.58 62.55 17.96 o 5 12 0 20.60 27.33 7.08 o 6 12 0 29.59 2.53 11.31 o 7 12 0 113.71 119.86 14.29 o 8 12 0 47.91 48.87 15.31 o 9 12 0 27.48 0.03 16.38 o 10 12 0 19.01 8.81 17.94 o 1 13 0 299.36 338.81 22.68 o 2 13 0 1.16 11.88 27.18 o 3 13 0 50.99 12.13 16.31 o 4 13 0 45.92 68.63 18.80 o 5 13 0 126.65 140.26 20.87 o 6 13 0 27.58 12.77 10.92 o 7 13 0 25.61 17.22 12.88 o 8 13 0 55.29 71.12 21.24 o 9 13 0 5.99 8.98 16.28 o 0 14 0 1.31 -13.27 13.60 o 1 14 0 53.08 61.28 16.45 o 2 14 0 70.78 79.76 17.06 o 3 14 0 5.00 -3.92 17.23 o 4 14 0 7.62 9.21 19.48 o 5 14 0 1.20 -6.09 19.33 o 6 14 0 4.26 11.95 22.12 o 7 14 0 26.30 30.80 12.62 o 1 15 0 111.63 104.82 17.54 o 2 15 0 86.46 107.02 20.69 o 3 15 0 1.44 22.62 21.69 o 4 15 0 104.27 142.50 24.71 o 5 15 0 0.47 -30.05 20.03 o 6 15 0 32.50 57.57 31.81 o 0 16 0 205.53 170.82 23.65 o 1 16 0 39.32 15.40 16.60 o 2 16 0 86.87 132.45 21.54 o 3 16 0 4.86 7.44 22.41 o -14 1 1 14.64 9.37 24.56 o -13 1 1 25.63 10.68 22.03 o -12 1 1 46.23 19.23 16.39 o -11 1 1 0.22 -11.69 12.27 o -10 1 1 79.30 88.17 9.68 o -9 1 1 37.96 43.06 9.66 o -8 1 1 16.63 11.07 7.45 o -7 1 1 404.19 418.40 11.98 o -6 1 1 1938.39 2000.62 32.75 o -5 1 1 172.07 178.99 6.35 o -4 1 1 3482.21 3727.00 46.65 o -3 1 1 102.39 108.55 4.09 o -2 1 1 907.43 1012.35 12.42 o 0 1 1 167.87 -0.78 0.52 o 1 1 1 851.67 784.65 14.53 o 2 1 1 23731.29 25019.96 308.04 o 3 1 1 13806.94 14234.38 170.48 o 4 1 1 6.44 12.36 4.14 o 5 1 1 152.47 138.20 6.73 o 6 1 1 728.58 732.88 15.44 o 7 1 1 7.52 10.24 6.76 o 8 1 1 325.68 358.07 11.40 o 9 1 1 0.17 2.13 7.82 o 10 1 1 249.82 249.69 12.59 o 11 1 1 9.54 -5.88 12.91 o 12 1 1 272.33 290.83 21.43 o 13 1 1 72.23 42.47 22.43 o 14 1 1 11.42 31.83 25.52 o -14 2 1 76.96 97.16 26.58 o -13 2 1 232.19 244.85 21.48 o -12 2 1 1.52 -22.77 15.18 o -11 2 1 0.88 -18.69 12.46 o -10 2 1 820.69 805.87 21.12 o -9 2 1 9.42 1.54 8.96 o -8 2 1 646.12 596.91 15.78 o -7 2 1 305.73 302.02 9.32 o -6 2 1 1020.89 1175.94 21.19 o -5 2 1 583.56 636.28 13.20 o -4 2 1 3309.28 3346.14 42.17 o -3 2 1 4642.57 4783.40 57.00 o -2 2 1 1160.41 1167.73 13.83 o -1 2 1 144.50 171.31 3.00 o 0 2 1 8532.05 8741.39 141.92 o 1 2 1 1457.10 1489.94 17.85 o 2 2 1 6897.56 7082.84 101.45 o 3 2 1 574.33 603.86 10.16 o 4 2 1 766.30 849.72 14.37 o 5 2 1 3.28 14.32 5.53 o 6 2 1 64.61 62.40 6.35 o 7 2 1 328.78 331.48 13.35 o 8 2 1 15.83 16.46 9.00 o 9 2 1 115.91 137.68 9.12 o 10 2 1 384.83 393.47 14.57 o 11 2 1 65.57 53.12 16.60 o 12 2 1 270.50 292.18 24.75 o 13 2 1 146.46 124.21 25.23 o 14 2 1 11.44 -21.67 25.87 o -14 3 1 2.15 -10.50 23.93 o -13 3 1 167.92 153.90 19.69 o -12 3 1 63.07 50.22 16.83 o -11 3 1 20.43 16.59 11.48 o -10 3 1 244.16 286.00 15.27 o -9 3 1 93.82 104.32 11.25 o -8 3 1 377.31 432.69 12.46 o -7 3 1 3.50 12.07 6.56 o -6 3 1 931.75 983.46 17.07 o -5 3 1 60.99 58.06 4.82 o -4 3 1 27.80 30.84 3.53 o -3 3 1 1980.43 1968.75 24.29 o -2 3 1 10.54 22.95 2.67 o -1 3 1 692.48 659.80 9.63 o 0 3 1 11359.02 11679.66 166.44 o 2 3 1 201.24 209.17 4.38 o 3 3 1 975.12 921.72 14.74 o 4 3 1 13.24 32.43 5.27 o 5 3 1 140.32 167.78 8.07 o 6 3 1 1207.57 1283.67 22.97 o 7 3 1 113.08 125.17 9.14 o 8 3 1 14.29 14.10 8.71 o 9 3 1 1.16 -14.24 9.50 o 10 3 1 109.44 99.51 12.99 o 11 3 1 101.86 72.24 13.55 o 12 3 1 0.89 10.28 16.79 o 13 3 1 3.65 1.64 19.23 o -14 4 1 89.95 88.63 21.15 o -13 4 1 152.88 157.80 20.60 o -12 4 1 1.47 -20.98 15.77 o -11 4 1 5.00 0.03 11.84 o -10 4 1 1566.28 1518.93 35.97 o -9 4 1 861.76 847.60 21.50 o -8 4 1 47.50 55.54 8.13 o -7 4 1 2637.05 2727.70 42.96 o -6 4 1 428.83 385.22 9.61 o -5 4 1 59.80 54.18 4.96 o -4 4 1 1203.50 1171.48 19.07 o -3 4 1 1571.97 1569.59 20.34 o -2 4 1 1.53 2.69 2.20 o -1 4 1 112.04 105.81 2.72 o 0 4 1 1961.43 1991.08 31.37 o 1 4 1 122.55 121.46 4.36 o 2 4 1 144.21 138.56 4.48 o 3 4 1 156.24 167.65 5.01 o 4 4 1 1862.08 1829.96 28.48 o 5 4 1 2641.10 2731.71 41.25 o 6 4 1 1300.79 1384.05 25.65 o 7 4 1 304.76 287.66 10.11 o 8 4 1 537.51 537.36 14.37 o 9 4 1 115.52 116.28 13.45 o 10 4 1 113.64 138.73 13.29 o 11 4 1 265.46 265.87 16.45 o 12 4 1 18.89 19.61 17.91 o 13 4 1 55.66 24.08 19.37 o -14 5 1 37.41 41.73 26.25 o -13 5 1 98.55 124.44 20.50 o -12 5 1 38.19 33.11 17.34 o -11 5 1 14.07 13.11 12.71 o -10 5 1 4.16 -14.21 11.69 o -9 5 1 499.76 500.29 17.92 o -8 5 1 233.81 223.51 9.26 o -7 5 1 20.61 18.81 7.04 o -6 5 1 1018.05 1109.75 21.40 o -5 5 1 108.65 92.21 5.14 o -4 5 1 148.34 167.10 5.86 o -3 5 1 2254.70 2515.03 40.23 o -2 5 1 2807.19 2772.94 45.95 o -1 5 1 2084.68 2142.15 32.26 o 0 5 1 7055.18 7282.53 119.45 o 1 5 1 532.45 433.08 11.03 o 2 5 1 6467.49 6584.51 102.86 o 3 5 1 7055.20 7426.00 110.95 o 4 5 1 279.44 271.16 6.84 o 5 5 1 31.39 30.17 5.39 o 6 5 1 58.65 55.37 6.91 o 7 5 1 7.83 0.14 7.19 o 8 5 1 102.09 93.56 9.68 o 9 5 1 67.25 82.39 12.38 o 10 5 1 47.19 31.85 12.72 o 11 5 1 316.50 323.78 17.32 o 12 5 1 782.07 731.98 32.59 o 13 5 1 81.11 110.27 24.87 o -13 6 1 237.82 239.31 32.62 o -12 6 1 70.53 73.96 21.95 o -11 6 1 115.06 141.57 15.07 o -10 6 1 212.51 245.39 18.81 o -9 6 1 168.48 195.37 13.87 o -8 6 1 530.35 568.20 16.54 o -7 6 1 3075.85 3041.85 50.78 o -6 6 1 1144.05 1105.75 19.57 o -5 6 1 12.64 11.04 6.23 o -4 6 1 1186.31 1183.92 20.44 o -3 6 1 1397.43 1453.60 22.50 o -2 6 1 1263.71 1503.85 28.05 o -1 6 1 405.82 432.41 10.17 o 0 6 1 17.11 9.46 3.53 o 1 6 1 8.11 22.37 5.91 o 2 6 1 2531.94 2508.16 52.40 o 3 6 1 1521.88 1529.81 25.96 o 4 6 1 568.85 505.40 11.62 o 5 6 1 2079.38 2119.91 31.77 o 6 6 1 1736.07 1737.07 30.90 o 7 6 1 2127.07 2167.78 36.48 o 8 6 1 1348.56 1339.65 32.54 o 9 6 1 858.47 842.45 24.98 o 10 6 1 336.05 355.20 17.33 o 11 6 1 238.76 224.10 17.15 o 12 6 1 7.73 -32.46 21.64 o 13 6 1 4.74 33.55 25.31 o -13 7 1 109.16 95.16 25.85 o -12 7 1 2.58 -13.81 20.76 o -11 7 1 20.05 35.23 16.59 o -10 7 1 850.60 846.37 25.72 o -9 7 1 56.12 50.76 12.02 o -8 7 1 61.72 44.35 11.17 o -7 7 1 93.35 104.26 10.47 o -6 7 1 1443.95 1447.54 26.10 o -5 7 1 2037.43 2002.58 32.99 o -4 7 1 3368.60 3347.22 54.03 o -3 7 1 3791.46 3940.05 65.11 o -2 7 1 247.15 212.40 7.21 o -1 7 1 4818.19 4940.96 76.63 o 0 7 1 8879.58 9339.40 143.45 o 1 7 1 3652.90 3448.81 87.92 o 2 7 1 2292.83 2323.46 49.02 o 3 7 1 777.26 717.65 13.72 o 4 7 1 727.60 764.42 15.45 o 5 7 1 1310.07 1318.46 23.88 o 6 7 1 52.89 39.86 8.53 o 7 7 1 446.76 405.76 14.57 o 8 7 1 126.59 131.65 16.03 o 9 7 1 615.93 582.46 20.29 o 10 7 1 69.22 80.11 18.20 o 11 7 1 145.90 165.39 23.11 o 12 7 1 86.59 108.98 24.13 o -12 8 1 114.23 97.33 18.87 o -11 8 1 333.72 327.26 21.00 o -10 8 1 487.61 512.12 23.21 o -9 8 1 781.73 748.31 30.89 o -8 8 1 481.02 477.75 18.44 o -7 8 1 280.24 299.04 11.89 o -6 8 1 1754.12 1667.64 29.25 o -5 8 1 109.75 131.24 8.43 o -4 8 1 2391.13 2538.06 40.06 o -3 8 1 31.23 13.57 5.35 o -2 8 1 613.30 585.27 17.09 o -1 8 1 339.76 365.60 9.52 o 0 8 1 27.49 30.95 4.05 o 1 8 1 2253.11 2247.28 51.98 o 2 8 1 837.65 838.70 19.69 o 3 8 1 592.26 592.24 12.34 o 4 8 1 365.86 360.60 9.65 o 5 8 1 1545.96 1529.39 27.39 o 6 8 1 486.02 498.79 15.25 o 7 8 1 65.63 54.92 11.10 o 8 8 1 644.11 669.20 24.76 o 9 8 1 220.42 238.03 17.49 o 10 8 1 253.77 270.68 19.91 o 11 8 1 14.77 -3.16 17.66 o 12 8 1 26.64 10.72 22.46 o -12 9 1 359.57 374.58 24.19 o -11 9 1 354.14 414.73 23.10 o -10 9 1 2.36 -1.95 15.49 o -9 9 1 204.60 210.38 22.91 o -8 9 1 34.09 8.93 13.27 o -7 9 1 0.71 -6.19 11.99 o -6 9 1 39.15 22.36 8.92 o -5 9 1 408.86 407.31 11.05 o -4 9 1 453.95 473.50 14.70 o -3 9 1 4498.94 4430.59 78.09 o -2 9 1 3761.82 3682.87 74.98 o -1 9 1 1717.62 1690.18 28.25 o 0 9 1 715.52 639.30 13.01 o 1 9 1 2382.91 2417.65 56.14 o 2 9 1 2201.75 2214.80 52.67 o 3 9 1 1823.89 1698.63 32.19 o 4 9 1 1432.23 1441.93 24.87 o 5 9 1 552.25 591.87 16.07 o 6 9 1 146.93 139.99 13.91 o 7 9 1 15.77 16.58 12.46 o 8 9 1 360.09 383.88 19.57 o 9 9 1 15.01 26.79 15.26 o 10 9 1 2.04 -15.61 15.69 o 11 9 1 23.69 27.62 18.68 o -11 10 1 340.91 348.28 26.23 o -10 10 1 58.96 60.92 17.03 o -9 10 1 416.46 425.93 21.21 o -8 10 1 416.96 480.98 21.18 o -7 10 1 1045.89 1067.69 32.17 o -6 10 1 1491.81 1461.02 40.04 o -5 10 1 1192.22 1160.22 26.22 o -4 10 1 642.28 686.07 16.34 o -3 10 1 2357.01 2305.18 78.27 o -2 10 1 4.17 12.84 9.21 o -1 10 1 6.21 6.75 4.97 o 0 10 1 135.59 133.05 7.09 o 1 10 1 29.83 32.37 9.53 o 2 10 1 65.40 51.42 10.72 o 3 10 1 124.21 88.21 18.19 o 4 10 1 602.58 648.48 16.78 o 5 10 1 1053.00 1048.54 31.32 o 6 10 1 1492.02 1443.08 38.90 o 7 10 1 1438.83 1417.18 39.52 o 8 10 1 431.58 448.56 23.76 o 9 10 1 438.06 467.55 24.48 o 10 10 1 138.68 114.57 18.35 o 11 10 1 179.74 206.13 21.08 o -11 11 1 41.15 57.17 19.40 o -10 11 1 70.61 60.21 17.27 o -9 11 1 8.39 -6.12 15.24 o -8 11 1 5.37 12.58 13.91 o -7 11 1 13.55 13.78 12.85 o -6 11 1 323.16 319.87 15.79 o -5 11 1 227.80 258.05 12.33 o -4 11 1 390.82 433.58 24.38 o -3 11 1 349.81 336.02 21.31 o -2 11 1 1249.48 1268.39 31.25 o -1 11 1 1728.05 1768.18 31.51 o 0 11 1 2340.85 2326.86 65.94 o 1 11 1 606.88 678.71 46.69 o 2 11 1 735.94 736.40 24.37 o 3 11 1 682.05 631.42 28.54 o 4 11 1 273.88 282.86 9.98 o 5 11 1 5.14 -2.79 7.56 o 6 11 1 123.75 128.88 13.40 o 7 11 1 103.27 123.98 17.47 o 8 11 1 4.24 1.76 14.12 o 9 11 1 268.30 283.69 20.05 o 10 11 1 12.85 -1.84 17.58 o -10 12 1 328.63 336.83 22.13 o -9 12 1 720.78 753.09 29.57 o -8 12 1 737.21 734.05 27.37 o -7 12 1 818.90 823.06 27.47 o -6 12 1 1127.04 1085.13 31.78 o -5 12 1 153.26 154.21 8.16 o -4 12 1 1133.91 1171.32 44.78 o -3 12 1 374.06 352.98 22.34 o -2 12 1 33.57 48.12 18.18 o -1 12 1 858.45 826.81 26.54 o 0 12 1 70.49 77.67 6.30 o 1 12 1 1.59 25.63 11.95 o 2 12 1 142.10 145.19 30.76 o 3 12 1 1843.13 1799.60 59.76 o 4 12 1 487.81 518.81 34.64 o 5 12 1 716.81 758.10 24.23 o 6 12 1 735.71 807.18 26.26 o 7 12 1 584.72 595.64 24.20 o 8 12 1 552.55 543.66 36.70 o 9 12 1 140.07 115.97 18.24 o -9 13 1 4.06 -5.47 16.26 o -8 13 1 13.01 5.43 14.42 o -7 13 1 5.12 11.10 12.57 o -6 13 1 364.59 370.34 16.61 o -5 13 1 274.88 260.97 24.37 o -4 13 1 60.36 60.76 19.10 o -3 13 1 833.46 847.12 43.59 o -2 13 1 354.28 375.40 25.64 o -1 13 1 688.78 683.04 17.38 o 0 13 1 1943.76 1993.62 52.19 o 1 13 1 1482.22 1500.55 50.20 o 2 13 1 1170.79 1215.53 54.90 o 3 13 1 927.71 951.33 45.83 o 4 13 1 307.07 308.32 23.18 o 5 13 1 74.65 55.04 20.27 o 6 13 1 36.53 18.45 13.92 o 7 13 1 17.92 16.56 13.78 o 8 13 1 11.02 9.39 15.33 o -8 14 1 201.54 211.85 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