#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2213448.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213448_Fobs loop_ _publ_author_name 'Best, Daniel' 'Jenkinson, Sarah F.' 'Booth, Kathrine V.' 'Fleet, George W. J.' 'Watkin, David J.' _publ_section_title ; 1-Deoxy-4-C-hydroxymethyl-3,4-O-isopropylidene-\b-L-ribulofuranose [(2R,3S,4S)-4-(hydroxymethyl)-3,4-O-isopropylidene-2-methyltetrahydrofuran-2,3,4-triol] ; _journal_coeditor_code LH2347 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2165 _journal_page_last o2167 _journal_volume 63 _journal_year 2007 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _audit_creation_date 07-01-10 _audit_creation_method CRYSTALS _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 6.2405(2) _cell_length_b 10.8088(3) _cell_length_c 14.9369(6) _[local]_cod_data_source_file lh23473sup2.hkl _[local]_cod_data_source_block 3 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma _refln_observed_status 2 0 0 91.30 175.21 10.10 o 4 0 0 553.90 521.67 18.30 o 6 0 0 58.30 60.70 3.90 o 2 1 0 1772.60 2140.12 40.20 o 3 1 0 13.60 14.21 0.90 o 4 1 0 0.50 0.41 1.27 o 5 1 0 6.80 9.44 1.30 o 6 1 0 4.10 3.01 1.30 o 7 1 0 178.60 166.35 5.60 o 8 1 0 17.30 20.04 2.50 o 2 2 0 207.40 225.20 5.10 o 3 2 0 612.20 659.74 14.90 o 4 2 0 510.70 539.54 12.40 o 5 2 0 58.40 55.05 2.40 o 6 2 0 382.60 388.49 9.70 o 7 2 0 14.70 18.86 2.60 o 8 2 0 49.60 42.55 5.30 o 1 3 0 36.20 32.08 0.70 o 2 3 0 1265.30 1346.30 21.00 o 3 3 0 1140.90 1104.91 18.50 o 4 3 0 388.70 411.39 7.80 o 5 3 0 81.20 90.52 2.40 o 6 3 0 185.80 188.15 5.40 o 7 3 0 5.90 7.11 2.60 o 0 4 0 475.60 456.73 16.70 o 1 4 0 3899.80 3931.35 70.00 o 2 4 0 53.20 57.09 1.10 o 3 4 0 44.30 36.83 1.30 o 4 4 0 345.30 341.03 6.70 o 5 4 0 464.70 520.48 10.30 o 6 4 0 125.50 127.97 3.70 o 7 4 0 39.10 43.31 3.50 o 1 5 0 160.50 164.53 3.10 o 2 5 0 250.20 271.10 4.50 o 3 5 0 396.80 410.06 8.80 o 4 5 0 13.70 18.98 0.90 o 5 5 0 169.90 169.13 3.90 o 6 5 0 13.20 12.38 1.60 o 7 5 0 223.40 200.39 7.80 o 0 6 0 2038.70 1918.04 63.70 o 1 6 0 295.70 279.27 5.30 o 2 6 0 80.90 82.19 1.80 o 3 6 0 152.30 156.63 3.40 o 4 6 0 183.80 201.76 4.30 o 5 6 0 46.50 49.42 1.90 o 6 6 0 69.30 65.25 2.70 o 7 6 0 18.00 9.07 3.60 o 1 7 0 623.20 609.23 14.20 o 2 7 0 111.90 104.90 2.30 o 3 7 0 240.70 231.24 5.00 o 4 7 0 511.30 526.70 10.80 o 5 7 0 41.10 43.44 2.20 o 6 7 0 2.00 0.06 2.10 o 0 8 0 19.40 21.35 0.80 o 1 8 0 2.50 2.56 0.30 o 2 8 0 128.80 130.04 3.30 o 3 8 0 149.30 141.51 3.80 o 4 8 0 4.50 5.28 0.90 o 5 8 0 54.20 63.45 2.00 o 6 8 0 21.50 18.88 2.30 o 1 9 0 563.30 522.73 11.70 o 2 9 0 496.90 456.96 11.60 o 3 9 0 80.10 82.63 2.20 o 4 9 0 64.90 65.01 2.70 o 5 9 0 11.50 9.42 2.10 o 6 9 0 0.50 0.00 2.69 o 0 10 0 867.40 785.53 50.70 o 1 10 0 1.70 2.31 2.00 o 2 10 0 48.80 54.23 1.50 o 3 10 0 1.10 0.29 1.00 o 4 10 0 31.00 23.42 2.70 o 5 10 0 6.50 8.89 2.20 o 1 11 0 152.90 142.85 10.60 o 2 11 0 402.70 385.60 16.70 o 4 11 0 58.70 55.48 7.70 o 5 11 0 63.60 67.38 4.00 o 0 12 0 9.80 10.16 3.20 o 1 12 0 2.20 5.83 2.70 o 2 12 0 41.30 45.41 5.20 o 3 12 0 40.30 49.20 5.10 o 4 12 0 11.60 14.90 2.00 o 1 13 0 2.90 0.23 3.30 o 2 13 0 7.00 13.25 4.40 o 3 13 0 15.80 30.34 5.00 o 2 0 1 1249.70 1371.32 26.80 o 3 0 1 1014.90 1022.71 22.10 o 4 0 1 3.70 7.78 0.80 o 5 0 1 43.90 40.86 2.20 o 6 0 1 3.80 2.26 1.40 o 7 0 1 143.60 136.67 5.00 o 8 0 1 -0.20 2.12 1.97 o 2 1 1 90.60 103.42 2.32 o 3 1 1 413.15 426.53 8.30 o 4 1 1 216.40 209.25 6.63 o 5 1 1 206.65 211.40 5.70 o 6 1 1 5.75 6.85 1.45 o 7 1 1 1.85 1.09 1.80 o 8 1 1 27.15 31.81 4.45 o 1 2 1 2317.55 3770.52 168.46 o 2 2 1 115.90 136.40 2.65 o 3 2 1 477.25 470.01 9.85 o 4 2 1 152.70 160.42 3.87 o 5 2 1 39.45 43.81 1.97 o 6 2 1 144.50 142.75 5.04 o 7 2 1 40.10 36.63 2.91 o 8 2 1 12.80 9.47 4.61 o 0 3 1 681.40 774.58 16.70 o 1 3 1 475.50 551.15 8.08 o 2 3 1 95.80 97.51 1.95 o 3 3 1 79.60 83.07 2.11 o 4 3 1 45.45 46.66 1.57 o 5 3 1 49.05 48.51 2.06 o 6 3 1 91.45 94.35 3.76 o 7 3 1 76.20 77.15 3.66 o 0 4 1 310.50 310.98 6.00 o 1 4 1 65.70 72.76 1.32 o 2 4 1 1077.35 1096.72 19.34 o 3 4 1 951.05 893.34 19.26 o 4 4 1 26.50 26.41 1.26 o 5 4 1 3.20 2.59 0.80 o 6 4 1 122.20 126.87 3.81 o 7 4 1 53.80 57.41 3.35 o 0 5 1 930.50 920.67 20.10 o 1 5 1 898.20 838.71 21.70 o 2 5 1 945.35 916.14 17.21 o 3 5 1 329.40 321.01 6.27 o 4 5 1 11.70 14.21 0.91 o 5 5 1 54.95 58.30 1.95 o 6 5 1 9.25 8.57 1.30 o 7 5 1 17.40 13.23 2.87 o 0 6 1 254.70 277.65 5.80 o 1 6 1 208.20 188.22 4.60 o 2 6 1 445.65 418.63 9.36 o 3 6 1 187.50 172.26 4.00 o 4 6 1 127.05 138.13 3.10 o 5 6 1 112.65 105.98 3.50 o 6 6 1 91.25 92.33 3.57 o 7 6 1 73.45 67.59 4.65 o 0 7 1 25.80 21.53 1.20 o 1 7 1 128.30 128.69 2.98 o 2 7 1 76.90 67.97 1.70 o 3 7 1 8.35 6.22 0.70 o 4 7 1 36.80 35.08 1.40 o 5 7 1 186.60 177.48 5.36 o 6 7 1 88.35 78.61 3.35 o 0 8 1 3.40 4.02 0.50 o 1 8 1 183.10 177.58 4.86 o 2 8 1 22.90 20.24 0.95 o 3 8 1 180.65 197.70 4.55 o 4 8 1 45.05 39.59 1.75 o 5 8 1 4.40 3.57 1.30 o 6 8 1 30.50 29.72 3.30 o 0 9 1 294.60 308.43 6.80 o 1 9 1 361.25 350.65 11.22 o 2 9 1 213.65 226.02 5.10 o 3 9 1 192.50 175.93 5.40 o 4 9 1 14.10 14.78 1.05 o 5 9 1 8.15 9.21 1.77 o 6 9 1 17.10 17.91 3.70 o 0 10 1 81.90 68.69 2.30 o 1 10 1 142.35 143.84 5.00 o 2 10 1 14.20 16.65 0.81 o 3 10 1 11.85 10.42 1.22 o 4 10 1 8.10 8.50 1.70 o 5 10 1 15.50 14.68 2.45 o 0 11 1 26.40 30.52 4.00 o 1 11 1 54.20 56.67 3.83 o 2 11 1 105.90 110.22 6.75 o 3 11 1 159.00 154.89 9.09 o 4 11 1 2.25 2.51 2.58 o 5 11 1 60.70 62.52 5.40 o 0 12 1 9.90 5.15 4.30 o 1 12 1 20.10 21.19 4.80 o 2 12 1 3.85 1.15 2.95 o 3 12 1 41.55 42.34 5.71 o 4 12 1 23.50 25.35 3.01 o 0 13 1 13.00 10.71 5.10 o 1 13 1 7.80 5.00 3.50 o 2 13 1 12.45 12.03 5.86 o 3 13 1 11.60 9.49 4.30 o 2 0 2 410.60 424.62 8.20 o 3 0 2 566.00 627.03 11.90 o 4 0 2 10.50 8.90 0.90 o 5 0 2 198.00 208.28 4.70 o 6 0 2 29.70 28.64 1.80 o 7 0 2 3.50 0.28 2.20 o 8 0 2 2.80 1.39 2.80 o 2 1 2 699.20 693.32 12.90 o 3 1 2 447.85 447.06 8.52 o 4 1 2 50.65 53.06 1.60 o 5 1 2 90.95 81.99 2.65 o 6 1 2 75.05 89.61 3.13 o 7 1 2 102.30 85.66 5.58 o 8 1 2 -1.25 0.13 2.77 o 1 2 2 937.85 1016.42 16.54 o 2 2 2 2197.95 2091.90 40.09 o 3 2 2 648.85 683.29 12.03 o 4 2 2 290.75 287.45 6.37 o 5 2 2 72.00 84.81 2.69 o 6 2 2 36.15 30.89 1.55 o 7 2 2 54.95 60.67 3.62 o 1 3 2 64.40 82.07 1.26 o 2 3 2 71.60 58.80 1.61 o 3 3 2 205.00 204.44 3.95 o 4 3 2 474.90 498.86 10.71 o 5 3 2 44.50 53.32 1.60 o 6 3 2 29.80 25.52 1.70 o 7 3 2 0.85 1.32 1.63 o 0 4 2 175.10 194.17 4.90 o 1 4 2 89.50 87.76 1.60 o 2 4 2 451.40 416.32 8.34 o 3 4 2 1.25 1.46 0.55 o 4 4 2 61.60 64.29 1.80 o 5 4 2 233.25 228.49 5.25 o 6 4 2 29.35 33.64 1.70 o 7 4 2 27.55 25.18 2.92 o 0 5 2 64.40 57.32 1.50 o 1 5 2 1127.50 1101.86 19.56 o 2 5 2 691.70 661.56 13.17 o 3 5 2 6.60 6.81 0.65 o 4 5 2 86.70 87.64 2.40 o 5 5 2 2.50 3.59 0.81 o 6 5 2 43.65 44.40 2.29 o 7 5 2 60.90 54.53 3.67 o 0 6 2 342.60 365.75 7.00 o 1 6 2 1812.55 1770.59 33.68 o 2 6 2 144.60 130.74 2.66 o 3 6 2 254.10 254.41 5.63 o 4 6 2 102.30 105.43 2.57 o 5 6 2 126.50 133.79 4.20 o 6 6 2 5.45 6.12 1.49 o 7 6 2 82.35 80.10 8.31 o 0 7 2 0.40 0.02 0.38 o 1 7 2 62.05 55.58 1.61 o 2 7 2 94.95 99.88 2.08 o 3 7 2 173.70 182.73 3.87 o 4 7 2 34.40 43.11 1.41 o 5 7 2 45.95 46.20 2.11 o 6 7 2 23.65 23.86 2.24 o 0 8 2 260.40 242.76 6.20 o 1 8 2 344.05 360.35 9.41 o 2 8 2 247.90 255.40 5.50 o 3 8 2 232.95 211.20 5.51 o 4 8 2 41.30 43.21 1.84 o 5 8 2 41.25 42.06 2.60 o 6 8 2 10.25 11.42 2.24 o 0 9 2 38.30 38.68 1.60 o 1 9 2 83.25 85.15 2.45 o 2 9 2 245.75 242.67 6.01 o 3 9 2 25.60 28.46 1.20 o 4 9 2 44.00 44.44 1.95 o 5 9 2 41.15 40.78 3.28 o 6 9 2 37.65 38.73 3.21 o 0 10 2 255.50 247.75 8.30 o 1 10 2 64.95 64.51 2.60 o 2 10 2 192.60 189.29 6.27 o 3 10 2 20.30 23.33 1.71 o 4 10 2 7.95 9.11 1.75 o 5 10 2 19.35 23.50 2.75 o 0 11 2 88.80 80.80 3.80 o 1 11 2 5.00 5.96 0.85 o 2 11 2 160.55 149.18 10.47 o 3 11 2 49.50 48.99 4.31 o 4 11 2 11.00 12.58 1.96 o 0 12 2 6.50 0.78 3.20 o 1 12 2 64.75 56.83 5.91 o 2 12 2 30.10 33.72 4.60 o 3 12 2 11.30 13.50 4.21 o 4 12 2 4.80 5.21 4.81 o 0 13 2 1.90 2.60 3.10 o 1 13 2 10.80 14.53 5.20 o 2 13 2 16.60 21.71 4.40 o 1 0 3 487.60 503.72 9.00 o 2 0 3 25.00 26.99 0.70 o 3 0 3 92.60 119.34 2.20 o 4 0 3 622.20 645.06 12.10 o 5 0 3 347.90 369.19 9.00 o 6 0 3 -0.50 0.00 2.26 o 7 0 3 7.90 10.79 1.90 o 8 0 3 41.30 36.76 4.90 o 1 1 3 750.20 845.02 18.46 o 2 1 3 1274.15 1366.13 21.16 o 3 1 3 586.70 604.21 12.65 o 4 1 3 275.25 291.34 5.86 o 5 1 3 89.25 93.68 2.95 o 6 1 3 42.60 42.49 2.40 o 7 1 3 75.50 78.13 4.00 o 0 2 3 50.00 48.39 1.40 o 1 2 3 560.55 575.51 10.55 o 2 2 3 180.20 185.71 3.21 o 3 2 3 764.75 796.31 16.91 o 4 2 3 341.30 366.87 7.40 o 5 2 3 257.60 264.90 5.81 o 6 2 3 25.80 28.38 1.75 o 7 2 3 40.65 39.62 3.10 o 0 3 3 1.60 1.18 0.30 o 1 3 3 1945.25 1863.49 42.06 o 2 3 3 572.60 547.67 14.23 o 3 3 3 182.95 187.83 3.65 o 4 3 3 31.70 32.68 1.30 o 5 3 3 218.30 214.17 5.50 o 6 3 3 -0.55 0.11 1.42 o 7 3 3 49.45 51.52 3.40 o 0 4 3 1084.60 1081.19 26.20 o 1 4 3 62.55 60.54 1.35 o 2 4 3 762.30 740.83 18.10 o 3 4 3 25.05 23.66 0.95 o 4 4 3 206.30 201.08 4.47 o 5 4 3 0.60 0.65 0.67 o 6 4 3 44.45 43.64 2.22 o 7 4 3 0.80 1.76 2.65 o 0 5 3 62.20 49.50 2.50 o 1 5 3 544.80 495.94 11.64 o 2 5 3 43.45 45.70 1.02 o 3 5 3 99.35 77.49 2.25 o 4 5 3 42.25 39.51 1.81 o 5 5 3 4.10 4.56 1.06 o 6 5 3 40.65 39.82 2.10 o 7 5 3 1.75 2.45 2.36 o 0 6 3 1403.50 1266.34 28.10 o 1 6 3 202.70 198.20 3.78 o 2 6 3 53.90 46.90 1.27 o 3 6 3 250.50 229.95 5.18 o 4 6 3 653.00 600.52 15.85 o 5 6 3 19.90 19.64 1.63 o 6 6 3 42.85 48.30 2.55 o 7 6 3 20.05 16.98 3.18 o 0 7 3 1395.30 1405.73 28.30 o 1 7 3 218.30 196.18 5.69 o 2 7 3 211.00 196.25 4.22 o 3 7 3 72.70 70.50 1.88 o 4 7 3 94.10 106.73 2.73 o 5 7 3 13.55 15.80 1.36 o 6 7 3 20.60 19.08 2.56 o 0 8 3 17.10 19.89 0.90 o 1 8 3 89.85 85.08 2.41 o 2 8 3 38.00 42.40 1.25 o 3 8 3 123.35 121.56 3.35 o 4 8 3 131.15 132.08 4.00 o 5 8 3 17.65 20.40 1.82 o 6 8 3 24.70 20.41 3.36 o 0 9 3 2.70 1.88 0.60 o 1 9 3 258.40 261.54 7.16 o 2 9 3 266.95 249.34 6.94 o 3 9 3 63.45 69.27 2.10 o 4 9 3 67.30 70.53 2.83 o 5 9 3 128.25 121.61 8.38 o 6 9 3 4.80 4.60 2.14 o 0 10 3 56.20 60.18 2.20 o 1 10 3 260.35 249.62 8.10 o 2 10 3 8.50 11.26 1.14 o 3 10 3 4.50 4.63 1.18 o 4 10 3 22.45 21.10 2.45 o 5 10 3 74.15 73.24 6.64 o 0 11 3 0.80 1.42 1.43 o 1 11 3 11.90 11.18 1.53 o 2 11 3 26.65 25.41 3.36 o 3 11 3 7.95 5.30 3.34 o 4 11 3 -0.15 0.38 2.64 o 0 12 3 141.00 130.98 10.90 o 1 12 3 5.45 6.47 3.20 o 3 12 3 5.10 6.75 5.40 o 4 12 3 32.90 30.39 5.80 o 0 13 3 97.60 88.76 9.30 o 1 13 3 59.35 54.43 6.75 o 2 13 3 75.30 61.02 8.20 o 1 0 4 4713.70 5407.70 164.00 o 2 0 4 3394.90 5927.67 184.70 o 3 0 4 71.80 74.92 2.00 o 4 0 4 23.90 27.05 1.20 o 5 0 4 55.20 68.34 2.20 o 6 0 4 125.10 124.56 4.40 o 7 0 4 -3.80 0.05 2.70 o 0 1 4 1213.00 1342.74 37.80 o 1 1 4 513.20 529.03 11.82 o 2 1 4 342.10 324.47 6.29 o 3 1 4 536.15 513.31 9.75 o 4 1 4 112.95 113.75 2.85 o 5 1 4 57.75 52.60 2.10 o 6 1 4 16.75 17.97 1.97 o 7 1 4 21.30 20.73 2.40 o 0 2 4 1305.30 1257.50 34.80 o 1 2 4 668.65 632.40 11.91 o 2 2 4 610.75 600.50 10.60 o 3 2 4 12.15 9.90 0.80 o 4 2 4 85.05 70.13 2.40 o 5 2 4 215.15 235.60 5.05 o 6 2 4 166.30 175.25 5.40 o 7 2 4 24.70 23.96 3.49 o 0 3 4 3.30 5.40 0.30 o 1 3 4 94.00 89.31 1.87 o 2 3 4 737.90 682.74 12.96 o 3 3 4 253.40 273.22 5.50 o 4 3 4 89.80 99.60 2.60 o 5 3 4 433.20 439.87 11.06 o 6 3 4 225.60 215.89 8.09 o 7 3 4 23.25 23.46 2.80 o 0 4 4 150.90 140.26 3.60 o 1 4 4 858.05 837.81 16.01 o 2 4 4 427.85 406.65 7.76 o 3 4 4 794.60 751.33 15.62 o 4 4 4 68.95 67.74 2.01 o 5 4 4 200.90 201.60 5.15 o 6 4 4 12.95 13.96 1.90 o 7 4 4 26.45 29.63 3.16 o 0 5 4 135.70 113.39 2.50 o 1 5 4 126.45 122.20 3.41 o 2 5 4 61.65 51.71 1.51 o 3 5 4 0.55 0.40 0.99 o 4 5 4 202.65 200.49 4.66 o 5 5 4 43.70 45.54 2.07 o 6 5 4 135.25 119.50 4.90 o 7 5 4 -0.30 0.78 1.91 o 0 6 4 3.20 4.68 0.50 o 1 6 4 72.35 74.60 1.75 o 2 6 4 184.60 167.32 4.19 o 3 6 4 43.45 49.06 1.30 o 4 6 4 372.90 392.12 8.83 o 5 6 4 11.10 12.16 1.22 o 6 6 4 30.85 30.33 2.40 o 7 6 4 19.70 15.98 4.35 o 0 7 4 187.30 176.41 5.00 o 1 7 4 685.20 604.33 16.90 o 2 7 4 95.45 90.30 2.16 o 3 7 4 563.65 574.00 12.08 o 4 7 4 48.10 46.73 1.76 o 5 7 4 86.35 90.83 3.10 o 6 7 4 85.40 78.45 5.06 o 0 8 4 313.30 306.95 7.00 o 1 8 4 58.10 56.29 1.91 o 2 8 4 52.30 55.86 1.60 o 3 8 4 132.80 135.61 3.60 o 4 8 4 125.60 122.92 3.93 o 5 8 4 175.30 165.79 6.41 o 6 8 4 12.35 16.26 3.80 o 0 9 4 18.80 20.04 1.20 o 1 9 4 280.85 273.55 8.35 o 2 9 4 335.10 317.24 12.24 o 3 9 4 19.75 21.42 1.05 o 4 9 4 28.40 30.33 1.80 o 5 9 4 60.40 61.64 5.80 o 0 10 4 1.90 2.46 0.70 o 1 10 4 116.25 120.79 4.15 o 2 10 4 36.20 40.92 2.18 o 3 10 4 14.05 13.29 1.20 o 4 10 4 3.05 3.21 1.56 o 5 10 4 39.80 37.25 3.40 o 0 11 4 6.90 12.64 1.00 o 1 11 4 39.05 46.35 2.45 o 2 11 4 50.85 53.10 4.55 o 3 11 4 24.00 19.12 5.00 o 4 11 4 24.10 24.89 2.70 o 0 12 4 87.80 83.24 6.90 o 1 12 4 5.25 6.30 4.04 o 2 12 4 14.95 16.18 3.66 o 3 12 4 15.20 13.24 5.00 o 0 13 4 -0.70 2.64 5.19 o 1 13 4 85.85 80.45 9.11 o 2 13 4 0.80 0.43 6.44 o 1 0 5 1109.50 1011.25 22.90 o 2 0 5 1396.50 1299.24 30.80 o 3 0 5 105.10 90.81 2.50 o 4 0 5 2.30 3.92 0.70 o 5 0 5 411.00 400.87 9.10 o 6 0 5 46.70 43.50 2.80 o 7 0 5 9.70 14.34 2.20 o 0 1 5 323.40 347.77 9.30 o 1 1 5 2707.60 2636.40 57.05 o 2 1 5 1150.80 1113.92 21.49 o 3 1 5 272.25 271.80 5.49 o 4 1 5 248.30 238.33 6.25 o 5 1 5 31.50 30.29 1.65 o 6 1 5 5.50 4.41 1.85 o 7 1 5 26.15 23.53 2.81 o 0 2 5 588.80 589.69 14.60 o 1 2 5 1173.40 1031.88 24.02 o 2 2 5 1718.70 1680.55 28.55 o 3 2 5 57.70 59.68 1.55 o 4 2 5 246.40 263.00 6.06 o 5 2 5 47.00 47.64 1.96 o 6 2 5 33.25 35.89 2.35 o 7 2 5 12.25 9.39 2.80 o 0 3 5 37.70 43.90 1.20 o 1 3 5 596.45 573.24 11.70 o 2 3 5 834.15 783.02 13.68 o 3 3 5 11.20 11.68 0.76 o 4 3 5 156.40 171.78 3.80 o 5 3 5 237.55 232.52 6.15 o 6 3 5 70.25 69.32 3.42 o 7 3 5 4.40 1.00 2.45 o 0 4 5 2048.00 2090.81 51.70 o 1 4 5 13.30 18.45 0.55 o 2 4 5 831.40 804.94 15.10 o 3 4 5 166.20 163.04 3.60 o 4 4 5 307.80 298.87 9.15 o 5 4 5 187.55 174.01 5.00 o 6 4 5 99.50 91.43 4.86 o 7 4 5 1.05 1.82 2.75 o 0 5 5 253.80 284.75 5.00 o 1 5 5 143.60 158.28 3.32 o 2 5 5 496.10 488.33 10.88 o 3 5 5 748.75 721.59 15.12 o 4 5 5 194.40 188.84 5.10 o 5 5 5 128.90 119.61 4.65 o 6 5 5 11.50 11.33 1.96 o 7 5 5 32.30 30.65 4.07 o 0 6 5 66.00 63.97 1.60 o 1 6 5 63.15 68.74 1.70 o 2 6 5 138.45 140.96 3.08 o 3 6 5 378.35 383.06 8.13 o 4 6 5 192.65 219.17 6.26 o 5 6 5 101.35 89.26 3.65 o 6 6 5 29.10 28.15 2.81 o 7 6 5 7.10 7.79 4.48 o 0 7 5 59.70 62.37 2.60 o 1 7 5 140.25 139.24 3.47 o 2 7 5 89.95 85.15 2.45 o 3 7 5 146.00 149.86 4.17 o 4 7 5 175.05 173.78 5.30 o 5 7 5 52.50 50.61 2.60 o 6 7 5 65.35 53.50 4.94 o 0 8 5 72.10 80.47 3.50 o 1 8 5 179.75 185.23 5.00 o 2 8 5 569.80 548.48 15.45 o 3 8 5 407.30 426.02 10.49 o 4 8 5 62.25 65.47 2.45 o 5 8 5 24.70 24.83 2.50 o 6 8 5 37.60 32.43 4.52 o 0 9 5 1454.00 1325.26 42.40 o 1 9 5 33.60 36.25 1.60 o 2 9 5 60.80 69.37 2.22 o 3 9 5 67.45 64.87 2.65 o 4 9 5 167.50 170.22 7.46 o 5 9 5 0.65 2.42 3.11 o 0 10 5 2.20 0.89 0.70 o 1 10 5 170.35 164.61 6.10 o 2 10 5 58.60 65.36 2.85 o 3 10 5 53.60 47.66 3.69 o 4 10 5 3.75 3.39 1.90 o 5 10 5 4.90 4.92 2.01 o 0 11 5 295.10 301.89 13.70 o 1 11 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64.09 5.06 o 5 6 12 39.90 36.87 3.90 o 0 7 12 7.40 6.39 0.90 o 1 7 12 86.70 81.16 3.35 o 2 7 12 26.00 33.95 1.92 o 3 7 12 62.25 58.94 3.85 o 4 7 12 46.50 43.27 3.85 o 0 8 12 46.30 43.38 2.30 o 1 8 12 43.95 47.10 2.35 o 2 8 12 88.45 88.86 4.86 o 3 8 12 9.70 9.84 2.09 o 4 8 12 66.50 68.98 6.11 o 0 9 12 44.00 42.41 2.90 o 1 9 12 13.05 15.20 2.97 o 2 9 12 45.75 48.27 3.10 o 3 9 12 18.30 16.02 2.53 o 1 10 12 103.80 105.44 10.90 o 2 10 12 0.90 5.25 5.69 o 1 0 13 956.20 917.32 22.40 o 2 0 13 102.00 112.40 2.90 o 3 0 13 2.50 4.23 2.00 o 4 0 13 7.90 8.80 2.00 o 5 0 13 74.40 68.23 5.10 o 0 1 13 0.90 0.81 1.33 o 1 1 13 367.70 339.12 11.44 o 2 1 13 628.45 596.34 19.71 o 3 1 13 60.50 72.94 3.45 o 4 1 13 32.30 31.99 2.97 o 5 1 13 39.25 37.71 4.00 o 0 2 13 283.80 383.29 9.30 o 1 2 13 66.50 70.53 2.25 o 2 2 13 34.65 33.51 1.56 o 3 2 13 75.80 78.49 3.70 o 4 2 13 41.20 32.41 3.10 o 5 2 13 27.10 32.15 4.51 o 0 3 13 506.80 448.23 17.10 o 1 3 13 238.05 229.59 7.67 o 2 3 13 101.50 121.40 3.50 o 3 3 13 58.50 68.72 3.77 o 4 3 13 78.60 76.18 4.16 o 5 3 13 7.05 5.48 2.35 o 0 4 13 282.60 257.52 7.60 o 1 4 13 254.65 245.61 7.71 o 2 4 13 111.80 111.84 4.16 o 3 4 13 74.25 77.62 3.75 o 4 4 13 14.65 15.70 3.02 o 5 4 13 119.80 102.83 7.75 o 0 5 13 10.20 12.70 1.00 o 1 5 13 340.70 335.24 11.06 o 2 5 13 381.65 365.77 12.55 o 3 5 13 5.35 5.80 1.51 o 4 5 13 81.65 82.22 5.61 o 5 5 13 9.95 11.29 3.05 o 0 6 13 25.40 24.55 1.80 o 1 6 13 410.30 403.62 15.50 o 2 6 13 25.05 27.47 1.86 o 3 6 13 41.85 37.26 3.26 o 4 6 13 9.55 7.54 2.82 o 0 7 13 14.90 15.57 1.40 o 1 7 13 6.05 6.39 1.32 o 2 7 13 1.75 0.91 2.73 o 3 7 13 60.25 56.59 3.72 o 4 7 13 44.80 52.59 5.02 o 0 8 13 166.50 159.59 9.40 o 1 8 13 24.50 24.69 2.79 o 2 8 13 46.65 43.23 3.45 o 3 8 13 2.70 3.13 2.16 o 0 9 13 83.90 88.78 8.30 o 1 9 13 171.45 161.38 15.78 o 2 9 13 -0.20 0.22 2.55 o 3 9 13 7.15 9.10 2.73 o 0 0 14 1262.90 1134.61 48.00 o 1 0 14 3.30 3.44 1.20 o 2 0 14 520.70 531.94 17.00 o 3 0 14 150.00 159.84 6.20 o 4 0 14 -0.10 0.58 1.14 o 5 0 14 12.00 13.16 2.90 o 0 1 14 16.20 16.67 1.40 o 1 1 14 39.40 38.40 2.00 o 2 1 14 125.05 112.12 4.77 o 3 1 14 38.70 41.85 2.80 o 4 1 14 28.15 40.48 4.30 o 5 1 14 91.25 81.57 6.11 o 0 2 14 2.00 1.52 0.90 o 1 2 14 118.35 109.74 5.24 o 2 2 14 110.00 113.84 4.68 o 3 2 14 39.65 36.41 3.08 o 4 2 14 3.70 3.12 2.06 o 5 2 14 11.90 15.69 2.85 o 0 3 14 139.40 140.25 5.90 o 1 3 14 64.45 52.62 3.81 o 2 3 14 8.05 4.97 1.67 o 3 3 14 1.80 2.97 1.50 o 4 3 14 6.00 8.42 2.21 o 5 3 14 68.40 62.35 5.84 o 0 4 14 75.90 80.57 2.90 o 1 4 14 137.00 136.39 5.60 o 2 4 14 16.70 15.02 1.97 o 3 4 14 11.80 13.71 1.76 o 4 4 14 16.45 18.96 2.65 o 5 4 14 28.50 24.40 6.35 o 0 5 14 83.60 79.81 3.90 o 1 5 14 11.55 10.79 1.77 o 2 5 14 22.20 20.18 1.96 o 3 5 14 23.30 22.62 2.95 o 4 5 14 39.65 37.79 3.65 o 0 6 14 39.50 43.62 3.20 o 1 6 14 7.45 7.39 2.26 o 2 6 14 19.90 34.36 3.49 o 3 6 14 0.95 1.82 1.76 o 4 6 14 63.80 53.18 5.40 o 0 7 14 26.80 26.82 2.80 o 1 7 14 11.75 8.61 2.63 o 2 7 14 35.65 34.14 3.30 o 3 7 14 6.90 6.26 2.08 o 0 8 14 17.30 20.72 2.20 o 1 8 14 26.65 31.29 3.41 o 2 8 14 5.65 5.92 1.90 o 3 8 14 0.80 0.72 2.33 o 0 9 14 20.30 20.83 2.50 o 1 9 14 25.05 28.30 2.81 o 2 9 14 57.85 62.73 6.30 o 1 0 15 402.80 372.07 13.80 o 2 0 15 73.20 61.85 4.50 o 3 0 15 13.30 10.30 2.10 o 4 0 15 5.90 9.71 2.70 o 0 1 15 16.00 15.18 1.90 o 1 1 15 43.15 51.90 2.60 o 2 1 15 3.65 4.30 1.35 o 3 1 15 122.05 109.90 5.81 o 4 1 15 2.90 3.13 1.90 o 0 2 15 67.30 70.84 3.80 o 1 2 15 209.95 199.54 8.17 o 2 2 15 26.95 20.92 2.16 o 3 2 15 4.05 4.90 1.75 o 4 2 15 45.60 49.37 3.85 o 0 3 15 26.90 24.78 1.90 o 1 3 15 5.20 6.27 1.40 o 2 3 15 174.20 165.88 7.32 o 3 3 15 16.60 19.00 2.42 o 4 3 15 17.45 20.65 3.05 o 0 4 15 1.60 5.00 1.10 o 1 4 15 8.10 6.41 1.77 o 2 4 15 37.40 35.37 2.75 o 3 4 15 65.75 72.34 4.55 o 4 4 15 31.85 30.10 3.60 o 0 5 15 79.60 102.18 7.90 o 1 5 15 30.30 31.86 2.70 o 2 5 15 21.95 23.50 2.60 o 3 5 15 33.30 38.70 4.51 o 4 5 15 42.70 50.43 4.35 o 0 6 15 59.10 52.93 3.80 o 1 6 15 40.90 45.90 2.95 o 2 6 15 -1.50 1.28 1.70 o 3 6 15 5.45 3.45 2.21 o 0 7 15 11.90 12.48 2.20 o 1 7 15 92.20 95.60 6.17 o 2 7 15 37.75 38.66 3.45 o 3 7 15 82.55 99.77 7.06 o 0 8 15 45.80 41.15 3.90 o 1 8 15 3.75 3.55 1.96 o 2 8 15 39.15 43.40 4.35 o 0 0 16 10.90 18.09 3.00 o 1 0 16 -0.60 1.87 1.86 o 2 0 16 29.00 30.22 2.60 o 3 0 16 5.40 2.43 2.00 o 4 0 16 4.50 6.21 3.00 o 0 1 16 34.10 30.83 2.50 o 1 1 16 1.35 0.67 1.35 o 2 1 16 9.55 10.46 2.25 o 3 1 16 13.35 15.40 2.16 o 4 1 16 8.00 7.79 2.45 o 0 2 16 22.90 20.54 1.90 o 1 2 16 101.65 97.43 5.53 o 2 2 16 103.25 106.40 5.81 o 3 2 16 8.60 11.33 2.65 o 4 2 16 9.50 10.38 2.50 o 0 3 16 33.60 41.26 2.50 o 1 3 16 7.90 7.93 1.88 o 2 3 16 40.50 36.42 3.00 o 3 3 16 10.25 9.96 2.30 o 4 3 16 24.30 26.11 3.61 o 0 4 16 73.10 60.42 4.40 o 1 4 16 64.05 59.35 4.15 o 2 4 16 16.95 24.12 2.61 o 3 4 16 6.30 4.52 1.96 o 0 5 16 17.00 16.47 2.40 o 1 5 16 24.20 24.07 2.80 o 2 5 16 43.30 42.25 3.80 o 3 5 16 34.70 33.69 3.91 o 0 6 16 4.10 6.38 1.60 o 1 6 16 32.00 31.19 3.16 o 2 6 16 1.30 2.31 4.26 o 0 7 16 9.20 11.68 2.80 o 1 7 16 30.45 31.43 3.55 o 2 7 16 29.30 28.01 3.46 o 1 0 17 0.00 0.15 0.01 o 2 0 17 199.00 167.82 10.20 o 3 0 17 37.50 35.62 3.80 o 0 1 17 473.30 424.98 18.50 o 1 1 17 60.55 53.36 4.75 o 2 1 17 63.45 61.50 4.85 o 3 1 17 72.55 70.55 5.66 o 0 2 17 2.10 1.79 1.60 o 1 2 17 94.70 84.79 5.81 o 2 2 17 18.05 14.34 2.67 o 3 2 17 10.60 7.38 2.50 o 0 3 17 1.00 0.02 3.60 o 1 3 17 103.60 107.58 6.30 o 2 3 17 20.75 22.22 2.81 o 3 3 17 54.55 64.47 5.20 o 0 4 17 119.10 140.20 6.80 o 1 4 17 9.90 8.79 2.00 o 2 4 17 32.55 35.47 3.89 o 3 4 17 42.65 53.78 4.96 o 0 5 17 22.00 18.35 2.60 o 1 5 17 14.85 14.33 3.20 o 2 5 17 66.75 61.31 6.88 o 0 6 17 13.30 13.18 2.40 o 1 6 17 39.20 41.99 3.67 o 0 0 18 16.70 16.80 3.30 o 1 0 18 123.50 115.06 7.40 o 2 0 18 -0.60 0.08 2.79 o 0 1 18 54.60 63.79 4.40 o 1 1 18 86.95 80.38 6.45 o 2 1 18 28.05 26.21 3.15 o 0 2 18 10.90 11.22 2.10 o 1 2 18 13.00 13.15 2.45 o 2 2 18 37.95 40.04 3.60 o 0 3 18 3.50 0.97 1.80 o 1 3 18 33.20 34.59 3.25 o 2 3 18 29.45 31.99 3.61 o 0 4 18 73.70 77.74 6.40 o 1 4 18 22.65 23.70 3.49 o 0 5 18 65.00 86.86 5.60 o