#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:29:10 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/34/2213456.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213456_Fobs loop_ _publ_author_name 'Gryz, Micha\/l' 'Starosta, Wojciech' 'Leciejewicz, Janusz' _publ_section_title ; trans-Diaquabis(5-methylpyrazine-2-carboxylato-\k^2^O,N)zinc(II) ; _journal_coeditor_code LH2355 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1402 _journal_page_last m1403 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 104.671 _cell_angle_beta 90.609 _cell_angle_gamma 109.436 _cell_length_a 5.1405 _cell_length_b 6.4312 _cell_length_c 12.2343 _exptl_crystal_F_000 192.00 _reflns_d_resolution_high 0.7096 _cod_data_source_file lh2355Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' zimpyrs2 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 90.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2795.65 3089.38 10.21 o 2 0 0 26.25 18.88 0.62 o 3 0 0 132.65 147.48 1.53 o 4 0 0 125.91 156.44 1.93 o 5 0 0 199.53 214.39 2.67 o 6 0 0 25.43 23.19 1.08 o -7 1 0 12.85 11.91 0.57 o -6 1 0 51.57 47.52 1.81 o -5 1 0 72.19 77.34 1.70 o -4 1 0 578.40 676.63 3.63 o -3 1 0 849.08 1036.18 3.69 o -2 1 0 74.17 93.28 0.96 o -1 1 0 445.79 513.95 4.42 o 0 1 0 4181.13 3246.86 37.51 o 1 1 0 8279.98 6973.67 18.94 o 2 1 0 1515.00 1795.37 12.64 o 3 1 0 1.45 1.42 0.17 o 4 1 0 16.78 20.02 0.74 o 5 1 0 46.60 51.60 1.59 o 6 1 0 8.76 7.82 0.40 o -7 2 0 25.59 24.67 0.96 o -6 2 0 22.32 22.68 1.02 o -5 2 0 31.15 37.65 1.30 o -4 2 0 466.03 548.99 3.23 o -3 2 0 509.71 563.40 2.72 o -2 2 0 905.59 1105.64 9.07 o -1 2 0 1212.61 1343.11 8.62 o 0 2 0 2.09 5.27 3.46 o 1 2 0 1544.98 1648.46 11.51 o 2 2 0 589.43 604.34 2.95 o 3 2 0 101.08 101.33 1.64 o 4 2 0 53.90 53.58 1.53 o 5 2 0 0.59 0.06 1.08 o 6 2 0 2.36 2.78 0.40 o -7 3 0 64.04 56.76 2.15 o -6 3 0 25.81 30.05 1.30 o -5 3 0 30.40 31.98 1.19 o -4 3 0 1.24 0.57 0.79 o -3 3 0 419.05 444.89 2.61 o -2 3 0 1036.71 1149.30 10.43 o -1 3 0 138.42 127.41 1.19 o 0 3 0 645.72 581.53 8.79 o 1 3 0 111.29 110.46 1.36 o 2 3 0 47.76 49.84 1.19 o 3 3 0 61.66 63.39 1.53 o 4 3 0 7.82 8.79 0.34 o 5 3 0 9.81 10.38 0.40 o -7 4 0 40.12 36.18 1.64 o -6 4 0 206.91 205.72 2.95 o -5 4 0 81.34 85.45 1.76 o -4 4 0 79.81 80.40 1.53 o -3 4 0 1.83 1.47 0.17 o -2 4 0 293.94 292.81 2.15 o -1 4 0 413.64 386.48 2.38 o 0 4 0 304.46 287.28 1.64 o 1 4 0 36.90 33.34 1.02 o 2 4 0 69.50 66.63 1.47 o 3 4 0 12.75 13.27 0.51 o 4 4 0 0.79 -0.06 1.13 o -7 5 0 0.52 1.13 1.42 o -6 5 0 95.14 92.20 2.21 o -5 5 0 156.07 154.97 2.32 o -4 5 0 133.51 138.58 2.04 o -3 5 0 110.64 105.98 1.64 o -2 5 0 47.98 48.71 1.19 o -1 5 0 372.61 357.57 2.72 o 0 5 0 117.48 109.58 1.20 o 1 5 0 80.41 76.83 1.64 o 2 5 0 40.69 40.60 1.47 o 3 5 0 7.23 7.54 0.34 o 4 5 0 3.67 4.99 0.40 o -6 6 0 2.55 2.78 0.40 o -5 6 0 54.12 52.00 1.70 o -4 6 0 162.43 160.41 2.38 o -3 6 0 35.53 40.60 1.36 o -2 6 0 0.88 0.91 0.23 o -1 6 0 2.83 2.32 0.23 o 0 6 0 58.35 59.06 1.08 o 1 6 0 69.01 68.10 1.81 o 2 6 0 14.50 13.67 0.62 o 3 6 0 13.82 14.46 0.57 o -6 7 0 1.74 -1.08 1.36 o -5 7 0 18.57 17.41 0.74 o -4 7 0 4.97 6.01 0.34 o -3 7 0 64.81 67.14 1.76 o -2 7 0 74.65 75.30 1.87 o -1 7 0 13.77 13.50 0.68 o 0 7 0 47.63 50.53 1.22 o 1 7 0 10.29 10.66 0.45 o 2 7 0 6.15 6.86 0.40 o -5 8 0 6.66 6.52 0.40 o -4 8 0 24.27 26.48 0.96 o -3 8 0 17.68 18.20 0.68 o -2 8 0 6.26 6.92 0.34 o -1 8 0 46.72 50.24 1.93 o 0 8 0 38.61 37.32 1.39 o 0 -8 1 78.93 75.28 1.81 o 1 -8 1 67.37 66.17 2.04 o 2 -8 1 8.67 8.85 0.34 o 3 -8 1 33.43 31.75 1.42 o 4 -8 1 31.86 32.83 1.42 o 5 -8 1 46.33 43.32 1.76 o -2 -7 1 6.29 7.54 0.40 o -1 -7 1 4.30 4.71 0.34 o 0 -7 1 81.67 83.92 1.50 o 1 -7 1 231.27 230.38 2.95 o 2 -7 1 241.29 229.08 2.84 o 3 -7 1 48.65 51.26 1.59 o 4 -7 1 8.88 8.39 0.34 o 5 -7 1 77.17 74.96 2.04 o 6 -7 1 39.60 34.19 1.64 o -3 -6 1 21.91 22.11 0.91 o -2 -6 1 40.31 44.74 1.70 o -1 -6 1 86.48 82.90 1.93 o 0 -6 1 8.96 10.52 0.34 o 1 -6 1 164.02 156.78 2.15 o 2 -6 1 606.86 588.63 3.86 o 3 -6 1 191.63 191.88 2.32 o 4 -6 1 100.23 96.28 1.93 o 5 -6 1 10.60 10.66 0.45 o 6 -6 1 15.88 14.06 0.74 o -4 -5 1 3.11 3.23 0.40 o -3 -5 1 13.99 13.95 0.68 o -2 -5 1 115.50 117.15 2.10 o -1 -5 1 161.62 157.75 2.15 o 0 -5 1 189.35 178.59 1.44 o 1 -5 1 234.63 234.92 2.21 o 2 -5 1 113.43 111.42 1.59 o 3 -5 1 246.94 241.33 2.32 o 4 -5 1 151.82 150.83 2.10 o 5 -5 1 38.43 39.69 1.47 o 6 -5 1 26.74 26.14 1.08 o 7 -5 1 4.84 4.65 0.45 o -4 -4 1 0.21 -1.02 1.13 o -3 -4 1 10.10 9.53 0.34 o -2 -4 1 137.99 133.31 1.93 o -1 -4 1 82.09 86.19 1.42 o 0 -4 1 542.98 489.84 1.94 o 1 -4 1 525.23 511.68 2.67 o 2 -4 1 323.68 316.63 2.21 o 3 -4 1 209.61 224.83 2.04 o 4 -4 1 27.04 26.25 1.08 o 5 -4 1 22.01 22.34 0.85 o 6 -4 1 83.01 85.28 2.10 o 7 -4 1 10.81 10.43 0.45 o -5 -3 1 10.78 10.21 0.40 o -4 -3 1 31.91 32.55 1.25 o -3 -3 1 12.61 12.70 0.51 o -2 -3 1 2.76 4.59 0.23 o -1 -3 1 395.36 378.49 2.32 o 0 -3 1 290.53 256.72 2.52 o 1 -3 1 198.80 184.96 1.42 o 2 -3 1 1208.89 1389.61 11.40 o 3 -3 1 349.91 388.24 2.44 o 4 -3 1 18.80 19.34 0.91 o 5 -3 1 32.02 34.65 1.36 o 6 -3 1 1.14 2.04 1.19 o 7 -3 1 56.42 45.82 1.81 o -6 -2 1 0.21 0.85 1.30 o -5 -2 1 2.08 1.98 1.08 o -4 -2 1 139.33 138.01 2.15 o -3 -2 1 119.11 122.70 1.70 o -2 -2 1 9.83 13.67 0.57 o -1 -2 1 35.62 25.01 0.68 o 0 -2 1 56.16 57.08 0.60 o 1 -2 1 658.23 728.23 6.41 o 2 -2 1 599.04 681.05 2.49 o 3 -2 1 247.74 287.25 2.04 o 4 -2 1 474.04 529.03 3.29 o 5 -2 1 2.38 3.06 0.28 o 6 -2 1 24.07 25.12 0.96 o 7 -2 1 4.70 5.39 0.45 o -6 -1 1 0.37 -1.02 1.30 o -5 -1 1 6.05 8.22 0.34 o -4 -1 1 7.89 7.65 0.40 o -3 -1 1 139.12 157.18 1.70 o -2 -1 1 987.50 1029.04 3.29 o -1 -1 1 354.72 376.84 1.59 o 0 -1 1 263.86 255.61 5.98 o 1 -1 1 899.59 1091.69 6.52 o 2 -1 1 112.23 128.03 1.13 o 3 -1 1 705.18 737.93 3.12 o 4 -1 1 204.41 230.04 2.21 o 5 -1 1 115.84 118.91 2.04 o 6 -1 1 18.27 18.43 0.68 o -6 0 1 36.04 36.35 1.36 o -5 0 1 26.83 28.41 1.19 o -4 0 1 14.36 14.52 0.62 o -3 0 1 91.64 104.84 1.36 o -2 0 1 50.11 52.68 0.79 o -1 0 1 494.81 666.48 4.99 o 0 0 1 2339.97 1529.51 25.20 o 1 0 1 1721.30 1809.49 8.39 o 2 0 1 569.65 670.17 2.49 o 3 0 1 258.83 273.42 2.04 o 4 0 1 103.89 108.13 1.64 o 5 0 1 165.82 167.50 2.44 o 6 0 1 48.07 47.46 1.87 o -7 1 1 17.96 16.50 0.74 o -6 1 1 94.57 95.32 2.21 o -5 1 1 28.59 31.07 1.25 o -4 1 1 280.24 341.41 2.61 o -3 1 1 696.95 839.99 3.35 o -2 1 1 40.47 56.59 0.85 o -1 1 1 317.89 285.50 1.25 o 0 1 1 497.35 519.25 5.24 o 1 1 1 4943.75 4618.59 16.16 o 2 1 1 3188.57 3569.71 18.20 o 3 1 1 45.84 60.90 1.19 o 4 1 1 47.75 46.55 1.36 o 5 1 1 51.53 55.40 1.70 o 6 1 1 27.55 25.40 1.02 o -7 2 1 29.43 29.20 1.25 o -6 2 1 31.10 34.13 1.30 o -5 2 1 186.08 224.88 2.61 o -4 2 1 241.09 256.81 2.27 o -3 2 1 439.29 491.67 2.61 o -2 2 1 2558.13 2754.78 14.57 o -1 2 1 94.85 85.56 0.91 o 0 2 1 8.79 14.60 1.08 o 1 2 1 1155.17 1224.26 10.26 o 2 2 1 1831.54 2042.25 15.71 o 3 2 1 754.07 746.21 4.03 o 4 2 1 41.11 39.92 1.47 o 5 2 1 0.26 -0.62 1.13 o -7 3 1 37.50 42.07 1.59 o -6 3 1 15.23 15.88 0.68 o -5 3 1 184.29 197.61 2.44 o -4 3 1 244.19 252.89 2.32 o -3 3 1 291.62 302.39 2.21 o -2 3 1 1305.80 1438.94 11.91 o -1 3 1 760.07 742.35 2.84 o 0 3 1 513.67 471.31 1.68 o 1 3 1 27.98 25.06 0.85 o 2 3 1 130.63 128.32 1.70 o 3 3 1 520.70 499.49 3.74 o 4 3 1 91.24 96.96 2.15 o 5 3 1 4.94 5.16 0.40 o -7 4 1 58.27 54.89 2.04 o -6 4 1 169.14 167.84 2.72 o -5 4 1 39.30 40.77 1.42 o -4 4 1 103.36 110.46 1.70 o -3 4 1 400.23 405.93 2.72 o -2 4 1 84.85 79.78 1.25 o -1 4 1 630.03 600.59 3.01 o 0 4 1 414.85 399.12 4.48 o 1 4 1 54.02 52.39 1.25 o 2 4 1 46.34 45.87 1.36 o 3 4 1 19.63 19.17 0.85 o 4 4 1 40.14 37.25 1.64 o -6 5 1 119.45 108.47 2.44 o -5 5 1 204.43 205.43 2.72 o -4 5 1 177.44 177.37 2.27 o -3 5 1 17.27 17.07 0.68 o -2 5 1 3.19 3.69 0.23 o -1 5 1 141.76 136.03 1.81 o 0 5 1 119.19 115.44 2.49 o 1 5 1 99.61 97.81 1.81 o 2 5 1 23.43 22.85 0.91 o 3 5 1 0.91 1.64 1.08 o 4 5 1 5.79 5.95 0.40 o -6 6 1 0.71 0.28 1.30 o -5 6 1 115.36 110.51 2.27 o -4 6 1 305.77 294.46 3.12 o -3 6 1 67.72 67.14 1.59 o -2 6 1 4.56 5.16 0.28 o -1 6 1 42.08 44.74 1.36 o 0 6 1 18.64 21.24 1.42 o 1 6 1 76.00 74.22 1.93 o 2 6 1 7.26 8.22 0.34 o 3 6 1 5.95 7.03 0.40 o -5 7 1 1.15 1.53 1.25 o -4 7 1 15.04 13.44 0.51 o -3 7 1 191.61 195.11 2.72 o -2 7 1 49.69 50.52 1.64 o -1 7 1 8.48 8.56 0.40 o 0 7 1 4.31 4.25 0.24 o 1 7 1 2.05 1.47 0.34 o -4 8 1 1.48 1.53 0.34 o -3 8 1 12.20 10.94 0.51 o -2 8 1 23.59 25.69 1.02 o -1 8 1 30.66 32.83 1.30 o 0 8 1 0.16 -0.01 0.86 o 0 -8 2 15.25 16.62 0.54 o 1 -8 2 23.45 25.80 0.96 o 2 -8 2 17.88 18.71 0.74 o 3 -8 2 33.67 34.08 1.36 o 4 -8 2 5.58 5.50 0.34 o 5 -8 2 20.70 20.53 0.74 o -2 -7 2 1.59 1.59 0.34 o -1 -7 2 15.06 14.63 0.57 o 0 -7 2 41.60 42.43 1.10 o 1 -7 2 55.45 54.89 1.64 o 2 -7 2 191.43 183.43 2.61 o 3 -7 2 50.35 49.95 1.59 o 4 -7 2 29.78 28.35 1.13 o 5 -7 2 54.11 51.26 1.87 o 6 -7 2 24.59 23.30 0.96 o -3 -6 2 5.25 5.84 0.40 o -2 -6 2 30.65 28.41 1.19 o -1 -6 2 61.33 60.44 1.64 o 0 -6 2 8.86 9.38 0.96 o 1 -6 2 95.98 89.02 1.70 o 2 -6 2 477.89 463.60 3.46 o 3 -6 2 425.19 419.43 3.40 o 4 -6 2 158.36 152.76 2.32 o 5 -6 2 29.23 28.75 1.19 o 6 -6 2 27.98 27.95 1.13 o -4 -5 2 8.92 11.17 0.40 o -3 -5 2 2.03 1.64 0.34 o -2 -5 2 103.15 102.18 1.98 o -1 -5 2 213.75 210.03 2.38 o 0 -5 2 211.73 198.99 1.98 o 1 -5 2 101.83 100.93 1.47 o 2 -5 2 38.96 37.99 1.08 o 3 -5 2 1182.23 1145.39 4.93 o 4 -5 2 821.84 924.76 4.82 o 5 -5 2 63.13 61.52 1.70 o 6 -5 2 30.00 28.97 1.25 o 7 -5 2 8.43 9.53 0.57 o -5 -4 2 7.20 8.17 0.45 o -4 -4 2 6.62 6.86 0.34 o -3 -4 2 48.68 46.10 1.53 o -2 -4 2 37.62 36.91 1.19 o -1 -4 2 218.56 231.01 2.10 o 0 -4 2 1233.31 1351.56 9.14 o 1 -4 2 534.21 547.58 2.78 o 2 -4 2 139.13 140.57 1.53 o 3 -4 2 196.69 210.76 1.98 o 4 -4 2 641.55 669.37 3.91 o 5 -4 2 468.07 495.41 3.91 o 6 -4 2 38.21 39.86 1.64 o 7 -4 2 1.48 -0.68 1.53 o -5 -3 2 10.01 10.32 0.40 o -4 -3 2 19.37 18.14 1.02 o -3 -3 2 87.27 84.88 1.64 o -2 -3 2 34.61 34.48 1.02 o -1 -3 2 398.23 371.23 2.27 o 0 -3 2 769.69 864.43 6.21 o 1 -3 2 742.15 875.77 8.56 o 2 -3 2 1746.27 1931.29 13.55 o 3 -3 2 127.40 144.87 1.59 o 4 -3 2 116.62 125.77 1.76 o 5 -3 2 232.94 261.85 2.84 o 6 -3 2 29.51 32.43 1.19 o 7 -3 2 18.36 16.56 0.79 o -6 -2 2 5.51 5.44 0.40 o -5 -2 2 20.75 20.19 0.74 o -4 -2 2 132.29 135.12 2.10 o -3 -2 2 47.85 45.42 1.19 o -2 -2 2 245.26 242.06 1.87 o -1 -2 2 174.21 168.35 1.36 o 0 -2 2 136.05 116.64 0.72 o 1 -2 2 1904.20 1947.62 10.66 o 2 -2 2 278.95 334.60 1.87 o 3 -2 2 605.53 825.76 3.46 o 4 -2 2 302.09 330.69 2.67 o 5 -2 2 16.29 16.61 0.79 o 6 -2 2 11.03 11.57 0.40 o 7 -2 2 0.99 1.98 1.42 o -6 -1 2 11.73 12.19 0.51 o -5 -1 2 15.01 16.90 0.74 o -4 -1 2 14.74 16.44 0.68 o -3 -1 2 309.82 335.74 2.38 o -2 -1 2 1203.97 1459.98 11.45 o -1 -1 2 5.25 4.71 0.17 o 0 -1 2 231.01 232.91 0.94 o 1 -1 2 514.27 591.69 5.27 o 2 -1 2 192.65 209.01 1.47 o 3 -1 2 416.36 429.18 2.49 o 4 -1 2 156.79 156.27 1.93 o 5 -1 2 61.93 61.69 1.59 o 6 -1 2 20.42 20.30 0.74 o -6 0 2 87.68 83.13 2.27 o -5 0 2 56.97 59.71 1.64 o -4 0 2 27.24 28.86 1.08 o -3 0 2 83.77 99.06 1.30 o -2 0 2 401.28 454.64 2.10 o -1 0 2 2145.40 2307.57 10.04 o 0 0 2 192.83 177.57 1.36 o 1 0 2 2108.97 2086.03 9.98 o 2 0 2 465.27 419.49 2.10 o 3 0 2 214.60 229.42 1.98 o 4 0 2 55.62 51.88 1.30 o 5 0 2 91.99 94.64 1.98 o 6 0 2 16.29 15.71 0.51 o -7 1 2 37.50 36.46 1.42 o -6 1 2 73.96 79.72 2.10 o -5 1 2 127.13 141.81 2.15 o -4 1 2 212.70 242.86 2.27 o -3 1 2 57.62 87.15 1.25 o -2 1 2 23.18 35.44 0.74 o -1 1 2 965.99 956.80 6.92 o 0 1 2 855.48 832.13 13.72 o 1 1 2 84.97 76.55 0.91 o 2 1 2 14.36 10.32 0.45 o 3 1 2 63.20 70.25 1.30 o 4 1 2 106.70 103.48 1.81 o 5 1 2 23.98 22.23 0.96 o 6 1 2 14.15 13.21 0.57 o -7 2 2 62.27 56.93 2.27 o -6 2 2 55.62 56.65 1.87 o -5 2 2 139.84 162.28 2.32 o -4 2 2 355.45 362.90 2.72 o -3 2 2 58.65 51.37 1.02 o -2 2 2 206.77 185.25 1.47 o -1 2 2 9.90 11.51 0.45 o 0 2 2 8.56 6.67 0.88 o 1 2 2 902.14 850.48 3.12 o 2 2 2 106.15 114.77 1.47 o 3 2 2 205.49 202.60 2.27 o 4 2 2 85.02 89.02 1.87 o 5 2 2 3.64 4.14 0.34 o -7 3 2 22.83 22.85 0.91 o -6 3 2 83.00 77.34 1.98 o -5 3 2 186.14 178.22 2.32 o -4 3 2 81.09 82.50 1.47 o -3 3 2 477.43 497.73 2.84 o -2 3 2 307.90 286.23 1.98 o -1 3 2 333.60 319.86 1.98 o 0 3 2 342.37 311.35 5.13 o 1 3 2 2.08 2.44 0.17 o 2 3 2 126.38 125.37 1.76 o 3 3 2 217.86 209.01 2.61 o 4 3 2 94.52 83.69 2.10 o 5 3 2 25.07 25.35 0.91 o -7 4 2 84.68 79.78 2.38 o -6 4 2 112.36 107.79 2.32 o -5 4 2 53.29 50.92 1.53 o -4 4 2 109.26 119.19 1.81 o -3 4 2 434.86 415.91 2.84 o -2 4 2 177.87 175.72 1.76 o -1 4 2 359.93 343.96 2.44 o 0 4 2 464.51 434.65 3.52 o 1 4 2 61.11 55.40 1.30 o 2 4 2 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42.32 1.45 o 1 2 9 74.82 73.26 1.64 o 2 2 9 34.26 34.76 1.42 o 3 2 9 1.65 1.98 1.08 o 4 2 9 0.33 -0.91 1.19 o -6 3 9 75.74 72.35 2.32 o -5 3 9 27.25 26.37 0.96 o -4 3 9 129.95 121.46 2.27 o -3 3 9 231.63 235.66 2.78 o -2 3 9 122.53 124.01 2.04 o -1 3 9 28.62 28.97 1.13 o 0 3 9 52.76 50.66 1.06 o 1 3 9 3.01 3.57 0.28 o 2 3 9 46.44 48.99 1.70 o 3 3 9 4.33 4.42 0.34 o -5 4 9 66.80 66.91 2.04 o -4 4 9 20.43 19.68 0.96 o -3 4 9 35.89 32.89 1.36 o -2 4 9 159.48 161.09 2.44 o -1 4 9 45.28 48.99 1.59 o 0 4 9 0.40 -0.35 0.70 o 1 4 9 12.38 10.77 0.62 o 2 4 9 0.13 0.06 1.13 o -5 5 9 25.99 25.80 0.96 o -4 5 9 15.12 15.48 0.74 o -3 5 9 13.61 12.93 0.51 o -2 5 9 37.08 39.29 1.53 o -1 5 9 25.41 26.76 1.19 o 0 5 9 26.12 28.60 0.79 o 1 5 9 0.17 2.04 1.19 o -3 6 9 18.52 19.51 0.85 o -2 6 9 1.14 -0.74 1.30 o -1 6 9 24.22 28.63 1.13 o 0 -8 10 15.02 15.64 0.60 o 1 -8 10 25.29 27.90 1.13 o 2 -8 10 16.96 15.88 0.62 o 3 -8 10 12.31 11.91 0.45 o -1 -7 10 28.21 26.25 1.13 o 0 -7 10 44.18 46.66 2.35 o 1 -7 10 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