#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:29:10 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/34/2213457.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213457_Fobs loop_ _publ_author_name 'Zinczuk, Juan' 'Ruveda, Edmundo A.' 'Lalancette, Roger A.' 'Thompson, Hugh W.' _publ_section_title ; (--)-Metasantonic acid: alteration of the hydrogen-bonding mode in a diastereomer of santonic acid ; _journal_coeditor_code LH2356 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2370 _journal_page_last o2372 _journal_volume 63 _journal_year 2007 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.4191 _cell_length_b 11.7706 _cell_length_c 12.2382 _exptl_crystal_F_000 568.00 _reflns_d_resolution_high 0.8505 _cod_data_source_file lh2356Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' RLL01A in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 118.78 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 14.51 14.46 0.51 o 4 0 0 777.22 808.00 18.24 o 6 0 0 1469.07 1413.17 26.59 o 8 0 0 773.42 790.56 11.78 o 1 1 0 182.55 158.99 2.46 o 2 1 0 2178.22 2185.59 27.45 o 3 1 0 33.63 31.16 0.68 o 4 1 0 431.26 476.12 7.71 o 5 1 0 33.38 34.69 1.29 o 6 1 0 832.78 789.61 10.61 o 7 1 0 182.56 192.61 4.10 o 8 1 0 31.20 30.32 0.65 o 9 1 0 733.07 715.79 9.91 o 10 1 0 20.04 17.68 0.76 o 0 2 0 8190.78 7911.08 137.67 o 1 2 0 1827.65 1730.22 28.77 o 2 2 0 418.54 421.21 5.92 o 3 2 0 110.61 81.88 1.43 o 4 2 0 547.23 599.64 10.16 o 5 2 0 454.64 450.63 6.71 o 6 2 0 440.14 440.96 6.87 o 7 2 0 59.05 59.08 1.59 o 8 2 0 986.67 936.13 13.80 o 9 2 0 298.07 294.96 4.63 o 10 2 0 1.76 3.96 0.38 o 1 3 0 413.64 434.63 6.69 o 2 3 0 1062.45 1097.54 18.33 o 3 3 0 655.08 686.36 11.55 o 4 3 0 11.35 10.12 0.72 o 5 3 0 32.53 32.37 0.79 o 6 3 0 2.14 3.22 0.27 o 7 3 0 159.93 158.08 10.45 o 8 3 0 7.92 9.29 0.68 o 9 3 0 43.74 54.46 1.96 o 10 3 0 236.82 239.13 5.82 o 0 4 0 82.07 73.41 1.76 o 1 4 0 20.77 14.08 0.54 o 2 4 0 1611.91 1699.60 28.33 o 3 4 0 9041.49 9327.74 203.30 o 4 4 0 1069.26 1130.09 15.10 o 5 4 0 85.78 78.72 1.53 o 6 4 0 65.26 57.51 1.57 o 7 4 0 4.74 6.99 0.62 o 8 4 0 40.67 40.13 0.91 o 9 4 0 269.87 281.27 7.78 o 10 4 0 73.93 87.33 2.37 o 1 5 0 8.56 10.53 0.88 o 2 5 0 267.49 298.45 5.25 o 3 5 0 1545.97 1600.00 26.73 o 4 5 0 541.47 554.35 11.75 o 5 5 0 36.87 37.99 1.04 o 6 5 0 167.82 161.13 3.60 o 7 5 0 48.49 44.71 0.98 o 8 5 0 53.95 50.75 1.08 o 9 5 0 0.43 1.07 0.23 o 10 5 0 0.97 1.37 0.23 o 0 6 0 156.24 200.68 7.73 o 1 6 0 1401.65 1463.74 35.99 o 2 6 0 1292.80 1327.50 26.74 o 3 6 0 60.57 68.36 1.36 o 4 6 0 858.14 878.35 19.19 o 5 6 0 66.64 63.03 1.68 o 6 6 0 15.23 18.34 0.56 o 7 6 0 32.90 26.95 0.71 o 8 6 0 1.07 1.04 0.65 o 9 6 0 146.40 133.05 3.44 o 1 7 0 368.92 384.20 8.13 o 2 7 0 118.45 101.90 2.51 o 3 7 0 139.50 137.53 3.26 o 5 7 0 853.75 753.25 17.49 o 6 7 0 78.15 78.62 2.21 o 7 7 0 2.24 1.30 0.30 o 8 7 0 106.35 90.13 2.44 o 9 7 0 26.78 31.79 1.07 o 0 8 0 440.47 468.22 12.21 o 1 8 0 24.48 28.20 0.85 o 2 8 0 17.09 14.71 0.99 o 3 8 0 164.42 174.86 6.50 o 4 8 0 1413.03 1392.67 32.11 o 5 8 0 332.62 287.60 4.86 o 6 8 0 1.29 2.48 0.27 o 7 8 0 18.79 17.45 0.76 o 8 8 0 26.76 39.19 1.22 o 1 9 0 6.82 7.30 0.56 o 2 9 0 1008.06 987.51 16.84 o 3 9 0 3.48 4.84 0.29 o 4 9 0 162.28 178.42 2.49 o 5 9 0 75.81 58.27 1.01 o 6 9 0 1.21 2.51 0.24 o 7 9 0 43.70 47.06 1.45 o 8 9 0 106.59 127.30 3.21 o 0 10 0 0.33 0.76 0.24 o 1 10 0 385.89 395.59 5.20 o 2 10 0 1684.42 1725.63 18.71 o 3 10 0 264.82 282.64 3.78 o 4 10 0 264.33 302.02 3.75 o 5 10 0 0.07 0.82 0.18 o 6 10 0 2.25 2.68 0.21 o 7 10 0 1.21 1.16 0.14 o 1 11 0 54.06 58.75 1.06 o 2 11 0 125.38 136.83 2.19 o 3 11 0 11.56 12.72 0.48 o 4 11 0 101.24 97.06 1.39 o 5 11 0 94.54 74.62 1.17 o 6 11 0 8.02 11.47 0.39 o 0 12 0 69.33 68.98 3.32 o 1 12 0 240.41 237.57 3.48 o 2 12 0 2.82 5.30 0.42 o 3 12 0 3.99 5.50 0.35 o 4 12 0 45.78 54.04 1.10 o 5 12 0 117.86 140.54 2.43 o 1 13 0 101.81 115.12 2.60 o 2 13 0 0.02 1.23 0.19 o 3 13 0 3.69 5.36 0.27 o 1 0 1 6643.12 6409.63 81.54 o 2 0 1 1066.61 1072.57 13.52 o 3 0 1 2485.38 2558.02 34.15 o 4 0 1 1872.87 1971.16 31.05 o 5 0 1 208.97 221.69 2.67 o 6 0 1 285.79 266.27 3.78 o 8 0 1 150.73 151.07 1.89 o 9 0 1 249.75 241.52 5.05 o 10 0 1 335.68 326.92 7.91 o -10 1 1 35.99 39.04 1.30 o -9 1 1 15.51 17.48 0.51 o -8 1 1 110.03 112.05 1.99 o -7 1 1 466.00 448.63 12.40 o -6 1 1 615.36 600.15 8.26 o -5 1 1 511.50 489.98 7.23 o -4 1 1 36.34 42.39 1.29 o -3 1 1 420.28 412.70 6.09 o -2 1 1 4061.64 4026.62 64.52 o -1 1 1 4806.90 4677.03 65.97 o 0 1 1 1268.38 1245.20 13.92 o 1 1 1 4823.05 4471.01 66.01 o 2 1 1 4053.70 4167.21 51.61 o 3 1 1 421.37 415.93 5.64 o 4 1 1 36.56 39.99 0.75 o 5 1 1 509.63 485.36 7.23 o 6 1 1 617.45 614.77 8.26 o 7 1 1 470.89 469.75 9.11 o 8 1 1 110.14 112.08 1.67 o 9 1 1 15.61 17.79 0.53 o 10 1 1 37.05 39.27 1.30 o -10 2 1 126.85 133.83 3.44 o -9 2 1 31.36 33.27 0.74 o -8 2 1 221.63 213.22 3.20 o -7 2 1 13.30 15.86 0.72 o -6 2 1 141.71 145.87 2.76 o -5 2 1 75.69 71.02 1.30 o -4 2 1 904.51 970.38 18.24 o -3 2 1 1491.34 1582.87 25.00 o -2 2 1 2961.21 2973.52 42.98 o -1 2 1 3772.17 3706.98 60.04 o 0 2 1 3055.03 2975.61 33.81 o 1 2 1 3759.27 3553.36 43.25 o 2 2 1 2949.26 2989.33 39.98 o 3 2 1 1493.11 1585.97 22.90 o 4 2 1 899.72 960.50 16.14 o 5 2 1 76.43 71.74 1.20 o 6 2 1 141.32 142.08 2.75 o 7 2 1 13.24 16.05 0.70 o 8 2 1 220.02 211.93 2.92 o 9 2 1 30.00 32.25 0.83 o -10 3 1 260.76 268.04 6.52 o -9 3 1 6.55 9.96 0.95 o -8 3 1 93.52 92.41 1.74 o -7 3 1 138.68 133.50 2.28 o -6 3 1 11.12 14.24 0.58 o -5 3 1 1028.52 1055.45 15.96 o -4 3 1 69.61 69.38 1.35 o -3 3 1 5717.38 6020.01 112.60 o -2 3 1 1544.35 1683.53 28.07 o -1 3 1 2006.92 1963.70 32.42 o 0 3 1 1633.40 1532.67 20.48 o 1 3 1 2003.86 1945.78 24.53 o 2 3 1 1549.02 1695.27 28.06 o 3 3 1 5715.80 6040.67 99.94 o 4 3 1 69.69 68.41 1.38 o 5 3 1 1031.77 1066.05 15.96 o 6 3 1 11.59 15.30 0.53 o 7 3 1 138.32 135.10 2.30 o 8 3 1 94.43 95.57 2.12 o 9 3 1 6.32 9.72 0.42 o -10 4 1 37.55 43.47 1.30 o -9 4 1 159.54 151.58 3.68 o -8 4 1 98.81 88.68 1.65 o -7 4 1 515.36 486.52 7.47 o -6 4 1 300.42 311.20 6.37 o -5 4 1 194.17 199.13 3.34 o -4 4 1 125.67 124.38 1.94 o -3 4 1 50.15 47.41 1.21 o -2 4 1 1337.86 1469.79 27.77 o -1 4 1 1773.96 1677.58 28.98 o 0 4 1 11.04 10.53 0.27 o 1 4 1 1779.68 1669.66 27.75 o 2 4 1 1336.81 1485.08 24.62 o 3 4 1 47.68 45.12 1.02 o 4 4 1 124.13 125.90 1.94 o 5 4 1 194.78 201.44 3.84 o 6 4 1 300.86 311.92 6.36 o 7 4 1 517.29 497.86 7.49 o 8 4 1 99.49 89.91 1.67 o 9 4 1 161.02 154.20 3.94 o 10 4 1 38.23 43.39 1.37 o -10 5 1 28.18 25.62 0.84 o -9 5 1 26.65 23.63 0.84 o -8 5 1 29.05 27.33 0.71 o -7 5 1 123.58 124.80 2.18 o -6 5 1 39.58 36.82 1.21 o -5 5 1 152.65 165.49 3.86 o -4 5 1 385.15 386.01 5.57 o -3 5 1 1316.58 1372.17 20.68 o -2 5 1 80.92 87.58 2.00 o -1 5 1 21.25 24.03 0.76 o 0 5 1 148.52 125.13 3.55 o 1 5 1 22.59 25.80 0.66 o 2 5 1 81.70 87.76 1.76 o 3 5 1 1317.46 1393.79 26.05 o 4 5 1 383.22 388.08 6.17 o 5 5 1 153.72 167.49 4.66 o 6 5 1 39.57 38.46 1.20 o 7 5 1 124.58 126.88 2.19 o 8 5 1 30.02 27.84 0.73 o 9 5 1 26.09 22.26 0.91 o -9 6 1 35.44 37.82 1.22 o -8 6 1 58.95 51.67 1.73 o -7 6 1 203.41 204.51 3.38 o -6 6 1 140.48 137.19 2.33 o -5 6 1 775.30 760.17 14.81 o -4 6 1 74.53 59.32 1.87 o -3 6 1 306.41 313.92 5.93 o -2 6 1 145.95 134.46 2.83 o -1 6 1 844.51 861.79 21.55 o 0 6 1 159.76 184.65 5.12 o 1 6 1 839.39 865.00 21.55 o 2 6 1 148.42 145.19 3.20 o 3 6 1 306.98 318.14 8.43 o 4 6 1 73.69 57.36 2.25 o 5 6 1 784.74 772.88 15.53 o 6 6 1 137.38 132.94 2.51 o 7 6 1 201.64 208.91 3.68 o 8 6 1 59.02 50.98 1.18 o 9 6 1 35.88 39.58 1.30 o -9 7 1 17.31 20.43 0.76 o -8 7 1 70.93 72.66 1.98 o -7 7 1 39.23 35.15 1.14 o -6 7 1 107.57 91.02 2.19 o -5 7 1 379.65 372.77 7.65 o -4 7 1 111.23 105.21 3.21 o -3 7 1 7.01 9.58 0.51 o -2 7 1 276.88 294.16 5.55 o -1 7 1 975.19 977.72 17.35 o 0 7 1 791.60 820.33 16.75 o 1 7 1 971.46 1001.25 20.08 o 2 7 1 277.86 303.78 6.45 o 3 7 1 7.13 9.15 0.76 o 5 7 1 377.34 385.64 8.99 o 6 7 1 106.99 88.29 2.60 o 7 7 1 40.91 36.53 1.22 o 8 7 1 70.17 71.74 2.06 o 9 7 1 17.47 20.43 0.76 o -9 8 1 6.97 7.85 0.38 o -8 8 1 131.08 138.89 3.52 o -7 8 1 38.13 31.82 1.37 o -6 8 1 4.28 2.73 0.29 o -5 8 1 257.86 260.03 4.41 o -4 8 1 46.03 43.63 1.45 o -3 8 1 104.66 113.73 3.21 o -2 8 1 128.27 140.53 4.23 o -1 8 1 271.89 286.14 5.40 o 0 8 1 332.24 337.37 6.26 o 1 8 1 273.82 288.43 6.28 o 2 8 1 130.96 134.81 3.86 o 4 8 1 46.47 45.92 1.45 o 5 8 1 254.70 258.47 3.41 o 6 8 1 4.35 2.11 0.24 o 7 8 1 37.35 29.82 1.07 o 8 8 1 132.75 142.64 3.59 o -8 9 1 42.51 48.13 1.37 o -7 9 1 58.11 72.50 1.43 o -6 9 1 21.90 17.36 0.45 o -5 9 1 66.47 71.60 1.10 o -4 9 1 496.05 465.29 5.57 o -3 9 1 48.78 51.72 0.83 o -2 9 1 189.98 185.87 4.05 o -1 9 1 299.06 299.50 7.76 o 0 9 1 454.17 447.21 11.41 o 1 9 1 302.85 296.48 7.76 o 2 9 1 187.55 183.74 6.96 o 3 9 1 48.77 50.60 0.94 o 4 9 1 498.21 461.52 5.88 o 5 9 1 64.79 70.71 1.17 o 6 9 1 22.32 17.36 0.56 o 7 9 1 57.60 70.63 1.53 o 8 9 1 43.42 49.89 1.45 o -7 10 1 63.84 70.22 1.35 o -6 10 1 0.57 1.36 0.57 o -5 10 1 32.38 32.31 1.13 o -4 10 1 28.27 25.55 0.57 o -3 10 1 53.60 52.40 0.90 o -2 10 1 550.85 546.74 6.19 o -1 10 1 410.66 410.80 4.75 o 0 10 1 3.41 5.19 0.37 o 1 10 1 406.86 412.78 6.43 o 2 10 1 557.73 554.08 8.14 o 3 10 1 53.91 51.44 1.15 o 4 10 1 28.21 25.39 0.61 o 5 10 1 32.59 31.13 0.66 o 6 10 1 0.59 1.29 0.30 o 7 10 1 63.45 70.14 1.98 o -6 11 1 36.80 33.79 0.64 o -5 11 1 91.72 97.47 1.27 o -4 11 1 7.26 9.61 0.88 o -3 11 1 167.92 190.40 2.49 o -2 11 1 221.14 217.47 2.74 o -1 11 1 571.84 578.62 7.33 o 0 11 1 211.68 228.28 3.00 o 1 11 1 569.46 580.97 8.93 o 2 11 1 224.11 225.79 3.26 o 3 11 1 167.26 191.43 2.87 o 4 11 1 7.71 9.88 0.46 o 5 11 1 91.84 97.38 1.72 o 6 11 1 37.08 34.91 0.83 o -5 12 1 92.39 103.85 1.29 o -4 12 1 14.08 11.76 0.32 o -3 12 1 208.15 242.00 3.21 o -2 12 1 224.40 229.41 4.33 o -1 12 1 0.65 0.65 0.15 o 0 12 1 9.30 9.56 0.38 o 1 12 1 0.77 0.80 0.24 o 2 12 1 223.18 234.08 4.87 o 3 12 1 207.89 245.58 3.79 o 4 12 1 14.03 11.78 0.46 o 5 12 1 93.48 106.07 1.89 o -3 13 1 36.36 39.49 0.70 o -2 13 1 174.31 199.58 2.62 o -1 13 1 132.36 140.98 3.13 o 0 13 1 65.91 71.36 1.76 o 1 13 1 131.41 143.34 3.06 o 2 13 1 173.04 202.97 3.13 o 3 13 1 35.72 40.57 1.22 o 0 0 2 201.06 229.32 5.90 o 1 0 2 1622.43 1687.22 28.96 o 2 0 2 1674.08 1778.79 23.84 o 3 0 2 3250.13 3432.16 49.39 o 4 0 2 186.25 219.32 3.67 o 5 0 2 97.31 105.54 1.31 o 6 0 2 500.02 494.84 6.36 o 7 0 2 6.23 7.15 0.88 o 8 0 2 3.24 3.19 0.27 o 9 0 2 568.73 567.54 11.14 o 10 0 2 39.32 34.09 1.14 o -10 1 2 66.96 75.93 2.14 o -9 1 2 194.51 194.34 3.15 o -8 1 2 35.99 35.50 0.83 o -7 1 2 128.01 118.18 2.73 o -6 1 2 129.22 123.19 1.85 o -5 1 2 123.81 134.02 2.00 o -4 1 2 119.12 116.74 2.10 o -3 1 2 6073.16 6271.34 108.93 o -2 1 2 612.75 613.85 8.28 o -1 1 2 1288.48 1306.11 17.95 o 0 1 2 14107.87 13552.20 198.18 o 1 1 2 1287.82 1269.04 23.28 o 2 1 2 613.92 619.20 8.40 o 3 1 2 6081.42 6281.65 110.51 o 4 1 2 120.06 122.00 2.12 o 5 1 2 125.09 138.07 1.77 o 6 1 2 130.04 126.01 1.84 o 7 1 2 128.39 120.82 2.74 o 8 1 2 35.13 35.10 0.84 o 9 1 2 195.58 191.68 3.18 o 10 1 2 67.39 76.85 2.14 o -10 2 2 47.84 50.80 1.53 o -9 2 2 33.53 34.25 0.92 o -8 2 2 59.84 58.01 1.15 o -7 2 2 427.45 418.53 6.36 o -6 2 2 101.53 103.89 2.70 o -5 2 2 406.69 386.33 6.11 o -4 2 2 488.15 539.53 8.96 o -3 2 2 2105.06 2234.55 31.88 o -2 2 2 1095.10 1179.64 17.10 o -1 2 2 520.92 507.74 8.47 o 0 2 2 1045.26 962.19 12.58 o 1 2 2 514.78 499.04 6.82 o 2 2 2 1094.93 1182.99 15.86 o 3 2 2 2108.44 2235.59 35.40 o 4 2 2 486.73 534.31 7.36 o 5 2 2 407.28 405.32 7.88 o 6 2 2 101.45 100.33 3.91 o 7 2 2 428.97 418.09 6.41 o 8 2 2 59.43 58.77 1.21 o 9 2 2 33.59 34.33 0.82 o 10 2 2 47.32 47.67 1.53 o -10 3 2 52.11 57.83 1.68 o -9 3 2 163.37 163.02 2.48 o -8 3 2 851.93 818.85 11.22 o -7 3 2 274.91 261.17 3.80 o -6 3 2 291.69 284.52 5.25 o -5 3 2 763.54 735.54 11.25 o -4 3 2 1000.44 1017.79 13.67 o -3 3 2 654.70 680.41 12.95 o -2 3 2 462.11 509.15 8.64 o -1 3 2 264.51 239.60 4.11 o 0 3 2 481.40 407.98 6.44 o 1 3 2 259.81 235.90 3.02 o 2 3 2 466.46 510.06 7.53 o 3 3 2 655.14 678.74 11.46 o 4 3 2 997.70 1015.73 16.29 o 5 3 2 767.58 746.71 11.31 o 6 3 2 291.43 284.61 5.81 o 7 3 2 274.45 261.68 3.50 o 8 3 2 857.25 819.15 10.27 o 9 3 2 158.98 154.47 6.65 o -10 4 2 82.74 81.93 2.14 o -9 4 2 25.03 22.66 0.68 o -8 4 2 53.19 52.35 1.00 o -7 4 2 56.35 56.40 1.05 o -6 4 2 879.41 846.03 14.40 o -5 4 2 25.80 29.86 0.79 o -4 4 2 95.92 94.62 1.56 o -3 4 2 151.90 173.56 3.67 o -2 4 2 133.78 135.20 2.86 o -1 4 2 110.25 122.35 2.27 o 0 4 2 1195.35 1190.78 17.21 o 1 4 2 110.72 122.46 2.24 o 2 4 2 132.25 137.15 2.77 o 3 4 2 154.50 178.80 3.65 o 4 4 2 92.93 91.34 1.89 o 5 4 2 26.35 29.41 0.85 o 6 4 2 874.99 854.39 16.38 o 7 4 2 53.93 56.52 1.78 o 8 4 2 54.11 52.91 1.12 o -10 5 2 30.86 35.08 1.07 o -9 5 2 119.45 114.77 2.98 o -8 5 2 187.95 189.83 3.07 o -7 5 2 8.85 11.91 0.43 o -6 5 2 98.69 96.74 2.46 o -5 5 2 144.82 142.74 2.17 o -4 5 2 445.46 473.81 6.53 o -3 5 2 388.45 391.25 5.11 o -2 5 2 542.77 555.08 10.81 o -1 5 2 290.46 311.32 6.85 o 0 5 2 2133.21 2076.36 48.84 o 1 5 2 289.88 310.84 6.63 o 2 5 2 551.69 562.67 9.54 o 3 5 2 388.32 394.57 5.90 o 4 5 2 442.00 467.60 8.11 o 5 5 2 147.28 150.43 6.87 o 6 5 2 100.85 101.43 2.41 o 7 5 2 8.67 11.55 0.48 o 8 5 2 185.00 188.42 3.41 o -9 6 2 29.32 32.25 1.07 o -8 6 2 106.82 108.07 1.78 o -7 6 2 47.83 45.32 0.90 o -6 6 2 139.27 136.29 1.82 o -5 6 2 18.99 20.51 0.68 o -4 6 2 89.18 85.81 1.72 o -3 6 2 540.88 548.93 8.94 o -2 6 2 111.69 120.55 2.25 o -1 6 2 499.02 504.16 10.49 o 0 6 2 624.52 606.00 12.43 o 1 6 2 497.13 512.08 10.49 o 2 6 2 111.80 122.50 2.84 o 3 6 2 543.22 565.87 14.23 o 4 6 2 89.28 86.17 4.01 o 5 6 2 18.51 19.82 0.91 o 6 6 2 141.58 135.72 4.01 o 7 6 2 46.90 45.94 1.07 o 8 6 2 106.64 108.59 3.09 o -9 7 2 5.61 5.94 0.38 o -8 7 2 59.52 61.19 1.75 o -7 7 2 92.85 78.53 1.68 o -6 7 2 111.33 107.92 1.73 o -5 7 2 525.09 471.46 8.34 o -4 7 2 738.79 740.35 15.30 o -3 7 2 78.25 69.90 1.49 o -2 7 2 409.84 387.16 9.39 o -1 7 2 944.13 941.67 16.80 o 0 7 2 8.32 10.17 0.55 o 1 7 2 942.38 976.20 19.42 o 2 7 2 411.71 405.98 8.33 o 3 7 2 77.54 70.84 3.97 o 5 7 2 530.67 487.34 11.34 o 6 7 2 110.19 103.20 2.37 o 7 7 2 93.07 82.77 2.29 o -8 8 2 126.59 149.13 3.67 o -7 8 2 196.89 200.59 3.08 o -6 8 2 34.44 28.46 0.72 o -5 8 2 408.21 388.12 5.81 o -4 8 2 46.59 43.08 1.01 o -3 8 2 70.59 74.40 2.48 o -2 8 2 207.72 198.70 5.31 o -1 8 2 447.57 439.87 11.20 o 0 8 2 76.35 73.13 2.35 o 1 8 2 446.68 445.61 15.72 o 4 8 2 46.38 43.02 1.45 o 5 8 2 408.86 385.50 4.94 o 6 8 2 33.78 24.49 0.73 o 7 8 2 195.96 195.21 6.05 o -8 9 2 103.52 119.13 2.98 o -7 9 2 53.34 58.38 1.21 o -6 9 2 14.99 15.94 0.71 o -5 9 2 241.42 221.17 2.90 o -4 9 2 22.29 23.01 0.51 o -3 9 2 204.61 195.61 2.87 o -2 9 2 943.81 897.77 19.44 o -1 9 2 47.94 46.69 1.36 o 0 9 2 290.06 300.21 7.81 o 1 9 2 46.29 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263.55 254.72 4.18 o -2 1 14 12.19 12.71 0.40 o -1 1 14 131.20 134.13 3.29 o 0 1 14 1.23 2.40 0.22 o 1 1 14 129.44 131.98 1.90 o 2 1 14 12.07 12.39 0.40 o -2 2 14 7.36 9.13 0.34 o -1 2 14 58.68 53.27 1.45 o 0 2 14 0.05 0.23 0.15 o 1 2 14 59.61 52.07 0.87 o 2 2 14 6.86 8.38 0.46 o 0 3 14 50.33 57.38 1.60 o