#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:29:10 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181054 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/34/2213465.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213465_Fobs loop_ _publ_author_name 'Khawar Rauf, M.' 'Badshah, Amin' 'Bolte, Michael' _publ_section_title ; 1-(2,6-Dichlorobenzoyl)-3-(2-methoxyphenyl)thiourea ; _journal_coeditor_code LH2369 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2665 _journal_page_last o2666 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 70.055 _cell_angle_beta 82.438 _cell_angle_gamma 74.299 _cell_length_a 7.3748 _cell_length_b 10.1854 _cell_length_c 11.8404 _exptl_crystal_F_000 364.00 _reflns_d_resolution_high 0.8237 _cod_data_source_file lh2369Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' wa661 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 112.32 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 335.31 271.54 5.34 o 3 0 0 10.13 9.89 0.72 o 4 0 0 300.81 338.20 3.91 o 5 0 0 38.08 50.37 1.36 o 6 0 0 0.23 1.04 0.93 o 7 0 0 1.50 2.74 1.40 o 8 0 0 357.64 329.26 5.86 o -8 1 0 4.01 4.11 1.49 o -7 1 0 158.79 161.07 3.02 o -6 1 0 295.42 295.64 3.69 o -5 1 0 296.01 299.84 12.42 o -4 1 0 1237.57 1237.47 24.96 o -3 1 0 208.17 215.10 3.50 o -2 1 0 592.64 519.67 6.18 o -1 1 0 1011.43 906.18 45.28 o 2 1 0 3438.87 3234.05 43.34 o 3 1 0 861.76 754.93 20.57 o 4 1 0 1.24 0.88 1.22 o 5 1 0 158.17 156.28 3.35 o 6 1 0 0.34 1.38 1.67 o 7 1 0 38.88 38.52 1.70 o 8 1 0 73.66 67.85 2.79 o -8 2 0 123.94 115.29 3.31 o -7 2 0 42.73 44.72 2.42 o -6 2 0 59.85 57.81 1.59 o -5 2 0 69.69 66.67 1.90 o -4 2 0 317.96 313.20 6.26 o -3 2 0 3472.98 3560.63 42.59 o -2 2 0 1499.76 1497.58 37.68 o -1 2 0 1529.49 1470.31 15.88 o 0 2 0 1.03 13.38 11.33 o 1 2 0 0.24 0.01 0.24 o 2 2 0 5649.71 6023.62 69.87 o 3 2 0 3.25 2.28 0.83 o 4 2 0 429.79 449.01 16.08 o 5 2 0 1333.06 1323.48 15.05 o 6 2 0 1139.11 1173.58 14.04 o 7 2 0 17.11 18.67 1.34 o 8 2 0 100.41 107.62 9.19 o -7 3 0 9.98 11.40 1.38 o -6 3 0 121.20 115.64 5.00 o -5 3 0 244.44 267.05 5.73 o -4 3 0 21.26 24.59 1.75 o -3 3 0 667.76 682.39 10.19 o -2 3 0 1506.24 1470.17 15.45 o -1 3 0 35.04 36.83 1.55 o 0 3 0 1639.36 1687.60 34.49 o 1 3 0 957.42 1035.09 34.00 o 2 3 0 1111.13 1092.94 10.02 o 3 3 0 10.59 12.62 1.18 o 4 3 0 403.66 426.58 16.00 o 5 3 0 15.93 22.04 1.00 o 6 3 0 418.25 431.93 10.19 o 7 3 0 13.01 17.81 1.25 o 8 3 0 161.91 169.57 5.98 o -7 4 0 110.62 101.61 2.44 o -6 4 0 0.52 -0.27 1.32 o -5 4 0 12.14 15.20 1.69 o -4 4 0 84.33 85.11 2.19 o -3 4 0 169.82 168.54 3.08 o -2 4 0 1289.55 1371.90 36.52 o -1 4 0 193.71 210.62 4.39 o 0 4 0 323.71 313.88 14.28 o 1 4 0 2693.73 2833.26 49.44 o 2 4 0 201.54 237.02 22.37 o 3 4 0 2294.66 2248.43 22.98 o 4 4 0 95.56 102.26 2.66 o 5 4 0 1002.95 1026.68 8.93 o 6 4 0 862.94 832.39 22.23 o 7 4 0 24.38 22.99 1.33 o 8 4 0 18.56 21.28 1.50 o -6 5 0 273.82 266.98 7.87 o -5 5 0 311.86 307.49 22.47 o -4 5 0 12.72 12.34 1.29 o -3 5 0 70.16 64.44 1.45 o -2 5 0 105.26 113.45 3.26 o -1 5 0 197.94 203.71 6.73 o 0 5 0 107.20 120.64 2.37 o 1 5 0 120.72 108.72 2.02 o 2 5 0 213.79 268.70 22.38 o 3 5 0 1712.22 1704.13 76.78 o 4 5 0 575.90 615.89 7.55 o 5 5 0 101.76 98.10 2.42 o 6 5 0 189.07 178.44 12.37 o 7 5 0 98.20 103.29 2.33 o 8 5 0 485.78 450.39 10.31 o -6 6 0 1.00 3.43 1.89 o -5 6 0 2.10 8.41 1.35 o -4 6 0 18.75 16.71 1.34 o -3 6 0 662.49 674.30 5.59 o -2 6 0 801.39 824.14 6.11 o -1 6 0 5.47 22.14 9.66 o 0 6 0 138.77 163.82 4.34 o 1 6 0 2.90 3.41 1.27 o 2 6 0 754.92 804.21 36.06 o 3 6 0 156.98 170.53 6.77 o 4 6 0 188.76 206.24 3.70 o 5 6 0 126.01 119.25 2.61 o 6 6 0 423.86 422.11 5.81 o 7 6 0 6.73 6.63 1.18 o 8 6 0 117.85 107.39 3.91 o -5 7 0 7.72 11.54 1.58 o -4 7 0 12.41 12.37 1.43 o -3 7 0 7.01 6.07 1.12 o -2 7 0 12.47 11.43 1.10 o -1 7 0 302.23 304.67 2.95 o 0 7 0 1201.13 1224.06 64.54 o 1 7 0 221.44 211.88 2.66 o 2 7 0 54.61 54.96 1.69 o 3 7 0 0.40 2.73 1.16 o 4 7 0 14.80 17.00 3.42 o 5 7 0 103.78 96.82 2.53 o 6 7 0 8.22 8.75 2.03 o 7 7 0 47.23 41.30 1.89 o 8 7 0 2.85 4.70 1.42 o -4 8 0 4.00 5.51 1.35 o -3 8 0 25.79 31.85 1.75 o -2 8 0 55.87 47.85 2.64 o -1 8 0 27.97 32.26 2.06 o 0 8 0 241.39 232.25 8.55 o 1 8 0 0.06 1.20 1.31 o 2 8 0 86.75 86.37 1.80 o 3 8 0 660.65 656.11 45.76 o 4 8 0 74.90 81.97 7.35 o 5 8 0 543.93 516.78 6.97 o 6 8 0 41.03 43.22 2.55 o 7 8 0 4.38 7.38 1.78 o -3 9 0 229.05 213.24 16.02 o -2 9 0 166.34 161.71 7.07 o -1 9 0 427.96 425.63 4.00 o 0 9 0 490.25 455.17 23.45 o 1 9 0 95.72 98.35 2.03 o 2 9 0 4.59 8.01 1.18 o 3 9 0 0.49 2.83 3.11 o 4 9 0 4.73 7.02 1.64 o 5 9 0 83.48 91.69 2.99 o 6 9 0 269.42 258.91 4.44 o 7 9 0 1.70 1.81 1.77 o -2 10 0 184.38 176.96 4.25 o -1 10 0 14.12 16.63 1.62 o 0 10 0 4.46 7.14 1.33 o 1 10 0 32.22 31.45 3.79 o 2 10 0 46.83 48.07 4.31 o 3 10 0 15.20 16.22 2.18 o 4 10 0 69.62 76.72 5.83 o 5 10 0 13.45 19.42 1.97 o 6 10 0 75.89 63.10 2.53 o 0 11 0 39.07 37.46 1.57 o 1 11 0 40.67 34.17 1.42 o 2 11 0 357.03 312.22 29.02 o 3 11 0 16.61 18.82 2.92 o 4 11 0 3.19 7.34 1.86 o -3 -11 1 27.38 32.63 1.79 o -2 -11 1 119.10 118.99 2.55 o -1 -11 1 89.53 86.49 2.59 o -5 -10 1 1.59 4.21 1.77 o -4 -10 1 110.58 117.13 3.21 o -3 -10 1 90.34 88.37 4.59 o -2 -10 1 54.51 52.24 5.26 o -1 -10 1 325.28 312.14 3.64 o 0 -10 1 78.22 71.61 3.48 o 1 -10 1 88.67 78.17 2.35 o 2 -10 1 3.42 3.57 1.99 o -6 -9 1 301.54 314.26 5.63 o -5 -9 1 35.76 30.39 2.07 o -4 -9 1 40.67 43.12 6.91 o -3 -9 1 31.91 29.10 2.62 o -2 -9 1 8.09 9.16 1.26 o -1 -9 1 473.63 490.88 5.93 o 0 -9 1 63.68 59.94 1.96 o 1 -9 1 246.66 246.18 7.76 o 2 -9 1 363.00 346.25 17.98 o 3 -9 1 86.63 89.53 4.92 o -7 -8 1 86.75 82.08 3.11 o -6 -8 1 13.20 14.34 2.31 o -5 -8 1 21.05 20.47 1.77 o -4 -8 1 378.45 403.44 10.03 o -3 -8 1 891.99 948.51 16.61 o -2 -8 1 2.81 2.40 1.31 o -1 -8 1 181.11 203.29 9.79 o 0 -8 1 91.04 90.87 3.20 o 1 -8 1 59.64 66.06 1.85 o 2 -8 1 5.09 4.35 1.14 o 3 -8 1 18.50 16.70 1.34 o 4 -8 1 43.74 44.84 3.32 o -7 -7 1 328.00 330.20 9.31 o -6 -7 1 37.41 37.40 1.96 o -5 -7 1 9.62 10.55 2.31 o -4 -7 1 95.92 102.85 1.94 o -3 -7 1 18.11 15.32 2.14 o -2 -7 1 90.23 98.75 3.24 o -1 -7 1 551.99 577.84 21.19 o 0 -7 1 259.18 276.60 12.04 o 1 -7 1 10.78 13.08 3.33 o 2 -7 1 0.82 1.72 1.60 o 3 -7 1 5.68 6.85 1.02 o 4 -7 1 204.02 197.43 3.61 o 5 -7 1 97.17 97.00 3.46 o -8 -6 1 23.56 21.18 1.35 o -7 -6 1 26.33 26.20 1.47 o -6 -6 1 359.88 362.26 5.56 o -5 -6 1 6.17 5.17 1.36 o -4 -6 1 407.04 412.02 32.29 o -3 -6 1 26.39 25.20 1.25 o -2 -6 1 97.98 108.83 4.61 o -1 -6 1 39.84 43.86 1.51 o 0 -6 1 50.52 56.68 3.27 o 1 -6 1 0.00 0.34 1.18 o 2 -6 1 1828.66 1813.85 38.19 o 3 -6 1 138.15 147.35 2.21 o 4 -6 1 169.66 159.55 2.33 o 5 -6 1 301.79 297.77 5.10 o 6 -6 1 44.90 47.76 2.00 o -8 -5 1 50.06 52.81 3.14 o -7 -5 1 33.74 32.90 1.86 o -6 -5 1 9.87 11.64 1.47 o -5 -5 1 455.06 449.24 6.29 o -4 -5 1 203.57 231.07 4.17 o -3 -5 1 347.25 366.32 21.85 o -2 -5 1 52.79 39.68 1.24 o -1 -5 1 1996.47 2391.92 59.52 o 0 -5 1 83.92 81.15 2.65 o 1 -5 1 66.05 68.25 1.81 o 2 -5 1 172.70 154.13 6.40 o 3 -5 1 500.23 526.64 5.19 o 4 -5 1 14.72 16.76 1.22 o 5 -5 1 97.41 103.50 5.31 o 6 -5 1 235.87 228.08 6.81 o -8 -4 1 2.01 3.59 1.42 o -7 -4 1 20.93 25.31 2.57 o -6 -4 1 7.88 9.24 2.11 o -5 -4 1 906.24 906.87 77.62 o -4 -4 1 148.43 153.97 3.31 o -3 -4 1 1357.43 1509.61 46.10 o -2 -4 1 7.80 26.75 3.96 o -1 -4 1 1133.10 1313.86 57.60 o 0 -4 1 105.80 111.75 6.78 o 1 -4 1 159.44 123.73 5.36 o 2 -4 1 1045.27 1015.36 77.82 o 3 -4 1 30.75 27.33 1.07 o 4 -4 1 1.94 4.65 1.12 o 5 -4 1 127.72 145.73 6.46 o 6 -4 1 9.89 11.09 2.95 o 7 -4 1 108.56 94.62 5.81 o -8 -3 1 113.29 115.71 5.68 o -7 -3 1 3.28 5.03 1.45 o -6 -3 1 130.85 126.74 1.89 o -5 -3 1 33.40 33.77 1.77 o -4 -3 1 2518.67 2694.96 28.97 o -3 -3 1 99.13 130.01 3.71 o -2 -3 1 55.26 60.80 1.53 o -1 -3 1 858.08 934.75 33.10 o 0 -3 1 3371.46 3592.10 48.77 o 1 -3 1 116.14 126.28 3.37 o 2 -3 1 492.39 483.30 10.84 o 3 -3 1 112.52 127.11 5.36 o 4 -3 1 995.78 1063.86 24.19 o 5 -3 1 445.69 470.64 21.66 o 6 -3 1 27.73 26.66 1.81 o 7 -3 1 0.90 1.46 1.13 o -8 -2 1 53.14 58.68 4.37 o -7 -2 1 0.40 1.70 1.48 o -6 -2 1 1123.49 1169.98 27.62 o -5 -2 1 188.86 186.97 2.27 o -4 -2 1 1041.23 1039.51 23.81 o -3 -2 1 17.88 14.97 1.37 o -2 -2 1 511.53 513.94 6.20 o -1 -2 1 1627.65 1623.20 15.31 o 0 -2 1 456.51 409.63 5.34 o 1 -2 1 1039.06 971.99 25.82 o 2 -2 1 599.66 583.80 19.18 o 3 -2 1 488.90 453.75 4.16 o 4 -2 1 37.99 45.42 1.60 o 5 -2 1 7.42 9.56 1.13 o 6 -2 1 6.57 7.02 1.21 o 7 -2 1 121.40 125.77 2.04 o 8 -2 1 83.05 81.25 3.86 o -8 -1 1 1.94 3.09 1.41 o -7 -1 1 119.41 121.78 11.82 o -6 -1 1 29.01 28.65 2.19 o -5 -1 1 4.27 3.87 1.52 o -4 -1 1 816.08 777.64 7.29 o -3 -1 1 2563.16 2403.26 31.37 o -2 -1 1 3173.16 3315.73 80.18 o -1 -1 1 203.98 184.54 4.13 o 1 -1 1 33.29 34.91 14.09 o 2 -1 1 754.88 641.52 20.90 o 3 -1 1 209.78 216.23 2.90 o 4 -1 1 323.88 326.35 3.55 o 5 -1 1 1212.45 1228.80 9.17 o 6 -1 1 393.68 401.14 14.20 o 7 -1 1 3.26 3.80 1.49 o 8 -1 1 69.90 68.01 4.31 o -8 0 1 0.80 3.92 2.02 o -7 0 1 171.99 169.29 3.54 o -6 0 1 174.59 162.88 2.26 o -5 0 1 10.79 14.68 1.17 o -4 0 1 253.57 238.48 6.62 o -3 0 1 143.18 139.18 2.48 o -2 0 1 64.54 65.88 1.47 o 2 0 1 1964.48 1769.99 91.52 o 3 0 1 320.35 296.53 15.39 o 4 0 1 1280.86 1328.86 21.37 o 5 0 1 140.47 138.96 7.09 o 6 0 1 0.18 0.91 0.98 o 7 0 1 53.59 58.98 1.89 o 8 0 1 185.56 190.00 4.28 o -8 1 1 0.34 1.71 1.36 o -7 1 1 34.94 35.59 1.70 o -6 1 1 687.95 665.19 13.29 o -5 1 1 71.92 78.12 1.67 o -4 1 1 1439.30 1501.75 28.64 o -3 1 1 440.56 451.00 7.34 o -2 1 1 931.22 849.27 20.56 o -1 1 1 232.34 169.73 2.87 o 2 1 1 8085.59 7968.77 68.74 o 3 1 1 3123.50 3171.80 66.75 o 4 1 1 824.32 833.31 16.96 o 5 1 1 663.54 627.21 12.65 o 6 1 1 15.02 14.57 1.28 o 7 1 1 0.04 -2.00 2.00 o 8 1 1 85.46 86.52 3.04 o -8 2 1 18.19 16.44 1.96 o -7 2 1 17.33 16.21 1.63 o -6 2 1 332.80 339.38 4.06 o -5 2 1 489.42 508.98 16.50 o -4 2 1 0.14 0.58 0.89 o -3 2 1 23.20 13.72 1.01 o -2 2 1 396.57 419.47 4.24 o -1 2 1 10441.92 12256.74 272.64 o 0 2 1 497.86 479.38 5.74 o 1 2 1 3515.52 3293.89 42.87 o 3 2 1 7.75 5.63 0.68 o 4 2 1 163.88 149.32 3.13 o 5 2 1 8.51 10.77 1.56 o 6 2 1 189.75 196.99 3.91 o 7 2 1 274.49 263.70 4.68 o 8 2 1 269.35 257.64 4.80 o -7 3 1 12.36 14.27 1.77 o -6 3 1 269.57 287.37 3.01 o -5 3 1 78.84 91.16 2.79 o -4 3 1 2.51 3.27 1.12 o -3 3 1 181.82 159.37 9.23 o -2 3 1 52.31 61.00 2.14 o -1 3 1 4065.87 4396.95 34.30 o 0 3 1 49.48 63.10 3.37 o 1 3 1 956.05 869.95 43.44 o 2 3 1 10025.48 9636.85 104.56 o 3 3 1 53.85 62.96 1.99 o 4 3 1 3598.77 3903.59 32.37 o 5 3 1 114.89 126.23 6.84 o 6 3 1 264.47 256.85 4.55 o 7 3 1 3.19 2.81 1.32 o 8 3 1 59.55 69.36 2.55 o -7 4 1 15.60 15.88 1.50 o -6 4 1 13.45 12.63 1.29 o -5 4 1 288.29 281.18 7.21 o -4 4 1 317.67 324.70 27.16 o -3 4 1 168.62 149.37 2.35 o -2 4 1 110.45 91.65 1.83 o -1 4 1 1433.29 1537.33 25.29 o 0 4 1 1810.36 1754.86 18.12 o 1 4 1 359.14 341.71 9.13 o 2 4 1 595.70 599.21 32.70 o 3 4 1 11.27 13.31 1.16 o 4 4 1 59.57 70.16 2.33 o 5 4 1 1366.15 1458.19 9.40 o 6 4 1 101.64 99.27 2.02 o 7 4 1 21.56 24.04 2.66 o 8 4 1 82.14 84.30 7.11 o -6 5 1 515.23 491.50 6.02 o -5 5 1 51.94 63.06 7.62 o -4 5 1 142.60 126.06 5.39 o -3 5 1 101.06 91.02 4.63 o -2 5 1 217.39 212.53 5.57 o -1 5 1 1847.58 1905.25 68.77 o 0 5 1 68.54 64.08 1.85 o 1 5 1 1714.14 1882.80 112.67 o 2 5 1 4.93 8.24 1.41 o 3 5 1 192.63 196.11 3.53 o 4 5 1 324.55 354.32 4.95 o 5 5 1 206.81 205.33 3.63 o 6 5 1 223.86 209.82 7.46 o 7 5 1 492.99 486.75 18.10 o 8 5 1 87.30 100.76 2.27 o -6 6 1 77.27 82.69 2.87 o -5 6 1 8.84 8.57 1.66 o -4 6 1 80.63 73.91 3.13 o -3 6 1 1006.68 1025.73 33.43 o -2 6 1 16.01 14.51 1.12 o -1 6 1 134.82 133.46 3.43 o 0 6 1 741.93 773.15 52.85 o 1 6 1 357.93 436.74 4.38 o 2 6 1 1108.20 1169.92 67.37 o 3 6 1 7.52 9.43 1.13 o 4 6 1 522.66 531.79 6.64 o 5 6 1 1285.53 1208.24 12.13 o 6 6 1 11.80 10.65 1.44 o 7 6 1 15.15 11.18 1.12 o 8 6 1 16.37 14.92 1.71 o -5 7 1 2.96 3.88 1.43 o -4 7 1 37.30 41.53 1.60 o -3 7 1 1.16 2.85 1.07 o -2 7 1 25.25 24.67 1.31 o -1 7 1 29.19 24.71 1.14 o 0 7 1 1256.91 1307.32 45.63 o 1 7 1 27.89 32.89 1.55 o 2 7 1 586.89 629.68 26.88 o 3 7 1 784.50 885.33 39.70 o 4 7 1 166.54 179.73 3.54 o 5 7 1 53.25 49.65 2.37 o 6 7 1 10.40 12.50 1.91 o 7 7 1 122.57 114.71 5.18 o 8 7 1 109.69 96.25 1.83 o -4 8 1 170.67 181.02 8.33 o -3 8 1 205.85 190.46 2.98 o -2 8 1 16.70 12.99 1.10 o -1 8 1 10.23 10.52 2.05 o 0 8 1 127.71 132.96 1.97 o 1 8 1 10.63 27.75 10.58 o 2 8 1 80.60 88.37 2.76 o 3 8 1 105.26 103.73 3.85 o 4 8 1 18.57 17.60 1.81 o 5 8 1 297.71 274.31 4.28 o 6 8 1 72.63 72.65 2.67 o 7 8 1 1.97 2.43 1.60 o -3 9 1 59.02 61.96 2.70 o -2 9 1 6.61 6.93 1.03 o -1 9 1 403.46 391.83 10.09 o 0 9 1 204.68 214.32 3.24 o 1 9 1 0.09 0.76 1.10 o 2 9 1 0.03 0.58 1.17 o 3 9 1 32.85 36.00 1.72 o 4 9 1 7.16 4.09 1.69 o 5 9 1 160.38 149.97 3.10 o 6 9 1 40.21 42.96 2.77 o 7 9 1 142.40 135.04 3.68 o -2 10 1 234.17 246.09 8.79 o -1 10 1 2.63 3.37 1.01 o 0 10 1 7.41 3.81 1.31 o 1 10 1 187.56 173.20 3.60 o 2 10 1 692.90 678.05 8.58 o 3 10 1 43.05 44.80 3.29 o 4 10 1 121.95 131.21 2.30 o 5 10 1 0.30 -2.08 2.53 o 6 10 1 45.55 46.99 2.25 o -1 11 1 27.15 26.21 1.49 o 0 11 1 45.92 39.24 2.79 o 1 11 1 19.61 14.69 1.39 o 2 11 1 8.91 12.25 2.45 o 3 11 1 0.62 2.53 1.57 o 4 11 1 14.25 16.51 1.56 o 5 11 1 179.80 179.38 3.68 o -5 -10 2 196.14 190.89 20.20 o -4 -10 2 156.38 155.43 2.84 o -3 -10 2 65.59 54.97 3.54 o -2 -10 2 30.75 31.87 3.17 o -1 -10 2 238.44 251.98 3.28 o 0 -10 2 7.53 9.38 1.83 o 1 -10 2 77.24 72.03 4.32 o -6 -9 2 181.89 170.06 3.60 o -5 -9 2 105.78 111.24 4.19 o -4 -9 2 1.48 4.62 1.20 o -3 -9 2 29.17 31.66 1.62 o -2 -9 2 26.86 30.97 1.39 o -1 -9 2 91.45 84.84 3.49 o 0 -9 2 30.85 34.99 1.85 o 1 -9 2 236.73 212.57 7.01 o 2 -9 2 283.52 272.07 10.90 o 3 -9 2 26.37 24.33 3.45 o -7 -8 2 61.65 62.67 3.20 o -6 -8 2 1.96 2.19 2.43 o -5 -8 2 76.94 77.88 8.58 o -4 -8 2 174.44 200.70 2.72 o -3 -8 2 814.09 849.82 6.62 o -2 -8 2 152.71 145.80 2.51 o -1 -8 2 218.64 226.32 16.80 o 0 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14 3.58 4.46 1.16 o 1 2 14 7.81 7.10 1.03 o 0 3 14 6.43 8.10 1.33 o 1 3 14 0.37 1.03 1.00 o 2 3 14 439.85 438.72 7.97 o 0 4 14 321.27 319.54 5.00 o 1 4 14 24.75 25.54 1.14 o 2 4 14 57.70 56.90 2.05 o 3 4 14 8.78 10.66 1.12 o 0 5 14 9.60 6.93 1.49 o 1 5 14 9.85 6.12 2.21 o 2 5 14 81.19 83.15 3.90 o 3 5 14 112.67 110.20 6.69 o 1 6 14 7.91 8.17 1.82 o 2 6 14 75.39 75.19 8.84 o