#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2213469.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213469_Fobs loop_ _publ_author_name 'Linden, Anthony' 'Wolstenholme, David' 'Basu Baul, Tushar S.' 'Rynjah, Wandondor' _publ_section_title ; Bis{\m-2-hydroxy-5-[(E)-2-(2-methoxyphenyl)diazenyl]benzoato}bis(di-n-butyl{2-hydroxy-5-[(E)-2-(2-methoxyphenyl)diazenyl]benzoato}tin(IV)) ; _journal_coeditor_code LH2373 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1547 _journal_page_last m1548 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.063 _cell_angle_gamma 90.000 _cell_length_a 35.6311 _cell_length_b 10.6333 _cell_length_c 19.5551 _exptl_crystal_F_000 3184.00 _reflns_d_resolution_high 0.8399 _[local]_cod_data_source_file lh2373Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' TSBB-68 (L0401)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 884.76 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 9457.62 3819.63 1539.39 o 6 0 0 242362.00 248509.72 20540.34 o 8 0 0 319649.72 331620.34 4927.60 o 10 0 0 61302.68 61248.18 1013.66 o 12 0 0 40993.88 44770.80 799.17 o 14 0 0 13122.45 11082.05 274.46 o 16 0 0 63935.57 61439.74 1029.76 o 18 0 0 10877.90 10183.20 310.59 o 20 0 0 7523.99 8038.57 275.76 o 22 0 0 12922.03 11997.72 385.13 o 24 0 0 34756.62 35257.79 765.97 o 26 0 0 16475.50 17798.81 832.53 o 28 0 0 4190.92 4460.28 277.11 o 30 0 0 1921.69 2107.37 258.93 o 32 0 0 18019.72 19407.82 672.59 o 34 0 0 8168.54 8754.78 454.65 o 36 0 0 5845.30 5709.78 429.15 o 38 0 0 119.28 488.06 362.20 o 40 0 0 4332.80 4569.35 497.59 o 1 1 0 533.06 356.03 107.42 o 3 1 0 9645.73 3214.34 606.87 o 5 1 0 8509.58 10876.87 875.17 o 7 1 0 16403.50 16669.54 225.63 o 9 1 0 15025.14 13149.54 197.89 o 11 1 0 4.44 522.45 55.36 o 13 1 0 3341.95 2494.45 222.05 o 15 1 0 223.79 174.07 60.46 o 17 1 0 57655.39 61045.63 755.23 o 19 1 0 22.17 -42.83 57.55 o 21 1 0 320.60 554.86 101.41 o 23 1 0 8401.73 8720.30 242.19 o 25 1 0 404.34 367.82 113.44 o 27 1 0 2418.47 2408.23 179.84 o 29 1 0 7.67 330.97 131.13 o 31 1 0 0.96 293.63 135.66 o 33 1 0 340.76 395.17 170.45 o 35 1 0 665.43 868.16 173.27 o 37 1 0 138.71 138.72 215.87 o 39 1 0 43.36 347.51 253.57 o 41 1 0 165.66 -249.00 249.00 o 0 2 0 254979.61 236150.59 19181.15 o 2 2 0 42569.36 39027.11 932.44 o 4 2 0 1.47 953.04 37.40 o 6 2 0 14746.60 13342.97 166.82 o 8 2 0 222448.34 226499.77 2128.87 o 10 2 0 12442.80 12204.76 198.75 o 12 2 0 6541.02 6795.01 130.88 o 14 2 0 9787.47 7733.99 165.39 o 16 2 0 115367.17 118434.39 1383.84 o 18 2 0 10391.76 9935.33 208.81 o 20 2 0 3071.88 3415.25 123.20 o 22 2 0 4632.26 4344.42 134.22 o 24 2 0 40888.16 41554.00 623.28 o 26 2 0 7535.04 8589.24 238.00 o 28 2 0 8499.63 9678.22 262.06 o 30 2 0 118.25 119.42 126.13 o 32 2 0 6619.54 6658.64 267.82 o 34 2 0 19686.91 21892.63 495.57 o 36 2 0 5965.70 6246.93 409.97 o 38 2 0 112.62 -91.29 181.53 o 40 2 0 2777.60 2374.07 313.80 o 1 3 0 10653.64 12102.32 167.40 o 3 3 0 8520.76 10230.66 148.16 o 5 3 0 11111.35 9578.46 143.02 o 7 3 0 7591.96 7130.32 115.84 o 9 3 0 704.44 667.87 57.98 o 11 3 0 4231.31 3920.46 96.28 o 13 3 0 2378.46 3368.78 99.53 o 15 3 0 7216.51 5898.90 155.72 o 17 3 0 12820.99 11677.63 207.76 o 19 3 0 8.96 194.67 80.73 o 21 3 0 256.55 293.39 81.67 o 23 3 0 1990.26 1971.68 130.40 o 25 3 0 4345.59 4069.85 146.48 o 27 3 0 720.80 995.28 126.51 o 29 3 0 1510.12 1791.74 157.24 o 31 3 0 232.45 278.03 151.76 o 33 3 0 8.14 55.32 161.68 o 35 3 0 2257.58 2051.06 223.84 o 37 3 0 254.48 72.88 216.88 o 39 3 0 274.92 211.58 244.06 o 0 4 0 51674.18 49049.54 829.44 o 2 4 0 51443.49 50242.17 571.81 o 4 4 0 1.06 589.64 55.39 o 6 4 0 26084.27 23580.46 294.64 o 8 4 0 121325.66 126146.42 1209.37 o 10 4 0 48878.53 53142.96 600.64 o 12 4 0 3.57 141.22 66.26 o 14 4 0 21069.97 22612.79 302.25 o 16 4 0 59387.33 61618.61 700.20 o 18 4 0 12078.53 13624.02 251.75 o 20 4 0 597.85 515.47 97.65 o 22 4 0 156.30 229.27 96.61 o 24 4 0 20157.28 21192.15 370.59 o 26 4 0 5864.88 6245.03 223.56 o 28 4 0 2143.02 2143.85 130.44 o 30 4 0 8.76 -108.48 108.48 o 32 4 0 4444.82 4125.76 308.55 o 34 4 0 6844.30 6391.50 289.57 o 36 4 0 2799.08 2568.91 245.11 o 38 4 0 175.81 -170.86 235.70 o 1 5 0 37563.64 37915.96 471.39 o 3 5 0 4037.61 3928.15 107.49 o 5 5 0 4664.90 5512.87 144.71 o 7 5 0 46512.19 51549.35 590.32 o 9 5 0 9098.91 8315.08 151.82 o 11 5 0 37.78 257.19 84.98 o 13 5 0 0.53 363.61 77.14 o 15 5 0 6099.04 6262.12 167.28 o 17 5 0 9823.43 10947.27 246.15 o 19 5 0 6524.73 6616.11 255.16 o 21 5 0 80.53 81.12 91.84 o 23 5 0 3931.78 4634.54 241.92 o 25 5 0 255.06 423.78 111.01 o 27 5 0 9731.06 9843.32 271.10 o 29 5 0 1795.44 1673.66 181.93 o 31 5 0 4754.07 5119.37 217.73 o 33 5 0 1497.17 1802.80 171.27 o 35 5 0 1254.48 767.25 179.97 o 37 5 0 55.43 181.23 224.86 o 0 6 0 17160.31 17367.58 366.66 o 2 6 0 12406.81 12479.20 220.46 o 4 6 0 5326.64 4914.45 137.84 o 6 6 0 1090.49 979.30 79.44 o 8 6 0 27422.74 28317.45 367.20 o 10 6 0 7101.81 6936.16 149.10 o 12 6 0 178.32 364.45 75.51 o 14 6 0 558.70 589.21 96.42 o 16 6 0 14080.25 14951.21 276.39 o 18 6 0 8612.56 8473.49 213.38 o 20 6 0 436.87 385.61 118.52 o 22 6 0 38.47 261.61 116.29 o 24 6 0 1065.43 1173.36 198.93 o 26 6 0 431.37 529.47 151.60 o 28 6 0 11664.69 12448.84 421.54 o 30 6 0 776.57 915.28 181.15 o 32 6 0 1421.65 978.08 165.78 o 34 6 0 667.24 705.25 178.83 o 36 6 0 1731.27 1584.52 283.27 o 1 7 0 7884.82 8422.40 183.08 o 3 7 0 794.10 1025.31 84.42 o 5 7 0 1848.86 1840.00 103.31 o 7 7 0 14194.19 14962.24 270.76 o 9 7 0 2080.99 2552.23 110.89 o 11 7 0 3742.13 4057.46 146.34 o 13 7 0 1235.71 1124.31 103.59 o 15 7 0 7550.64 8491.87 227.26 o 17 7 0 6836.52 7239.36 209.92 o 19 7 0 6149.70 6675.76 222.19 o 21 7 0 2669.87 2613.04 174.17 o 23 7 0 307.46 398.20 141.92 o 25 7 0 6759.22 7175.96 420.75 o 27 7 0 1801.95 1718.53 210.88 o 29 7 0 1166.73 1463.75 203.45 o 31 7 0 712.01 598.31 212.90 o 33 7 0 1959.02 1742.82 261.57 o 0 8 0 2882.60 2593.43 176.90 o 2 8 0 2525.26 2135.21 145.67 o 4 8 0 0.11 -86.26 86.26 o 6 8 0 9154.34 9172.95 323.62 o 8 8 0 4137.86 3858.90 161.83 o 10 8 0 62.55 138.24 102.39 o 12 8 0 15.61 263.09 99.18 o 14 8 0 579.05 549.59 116.69 o 16 8 0 4080.35 3827.63 174.81 o 18 8 0 3707.55 3362.11 172.01 o 20 8 0 2359.05 2358.94 159.46 o 22 8 0 938.37 792.96 140.17 o 24 8 0 3845.23 3595.48 224.78 o 26 8 0 1797.68 2049.27 274.79 o 28 8 0 553.17 227.27 190.44 o 30 8 0 362.65 158.16 214.56 o 1 9 0 19011.16 20828.12 374.32 o 3 9 0 4810.06 5129.46 172.09 o 5 9 0 6499.77 6106.02 200.05 o 7 9 0 10535.46 10603.67 305.13 o 9 9 0 7411.97 7757.67 233.17 o 11 9 0 1236.95 1040.28 125.87 o 13 9 0 144.64 75.54 106.75 o 15 9 0 6791.32 6378.58 250.60 o 17 9 0 4973.15 5635.94 253.43 o 19 9 0 1667.54 1830.63 165.79 o 21 9 0 293.09 191.69 167.80 o 23 9 0 2026.18 2255.78 203.04 o 25 9 0 2771.09 3322.30 245.58 o 27 9 0 601.66 -80.37 238.72 o 0 10 0 2092.57 2028.32 251.65 o 2 10 0 622.34 434.71 114.62 o 4 10 0 7926.37 7958.31 299.31 o 6 10 0 3295.27 2766.21 158.53 o 8 10 0 845.99 672.79 99.08 o 10 10 0 157.17 274.07 133.35 o 12 10 0 0.90 335.08 132.12 o 14 10 0 91.47 515.63 136.18 o 16 10 0 1.59 278.53 143.42 o 18 10 0 216.88 548.59 166.14 o 20 10 0 10.23 -90.02 169.43 o 22 10 0 28.73 152.46 193.84 o 24 10 0 30.92 389.29 248.64 o 1 11 0 5435.00 5821.91 267.33 o 3 11 0 21.93 66.85 135.04 o 5 11 0 25.02 -76.52 143.45 o 7 11 0 3036.84 3155.33 189.52 o 9 11 0 2664.20 2683.73 202.00 o 11 11 0 1861.84 1755.75 264.73 o 13 11 0 383.89 255.57 155.43 o 15 11 0 1832.39 1913.80 224.11 o 17 11 0 2901.38 3435.91 330.62 o 19 11 0 129.01 359.11 283.79 o 0 12 0 50.18 2.21 238.16 o 2 12 0 5.92 19.50 150.68 o 4 12 0 21.78 -187.04 204.79 o 6 12 0 159.06 96.11 212.19 o 8 12 0 474.45 449.43 229.90 o 10 12 0 0.64 137.57 229.67 o 12 12 0 8.63 -273.76 273.76 o -41 1 1 351.96 229.43 279.36 o -39 1 1 4809.12 5247.27 334.23 o -37 1 1 6761.15 6549.96 322.11 o -35 1 1 2134.74 1947.22 201.27 o -33 1 1 100.77 -130.19 130.19 o -31 1 1 6484.45 7907.15 265.26 o -29 1 1 26344.32 26800.72 482.41 o -27 1 1 10635.92 10512.05 275.45 o -25 1 1 560.49 822.38 117.93 o -23 1 1 19426.09 20539.47 376.88 o -21 1 1 116420.70 120423.86 1307.29 o -19 1 1 4858.91 3514.21 117.91 o -17 1 1 2418.52 3523.13 112.33 o -15 1 1 31541.88 29657.78 388.08 o -13 1 1 104518.52 94810.77 1072.63 o -11 1 1 39540.03 34822.80 435.50 o -9 1 1 24030.07 23953.74 312.94 o -7 1 1 84276.58 75301.11 808.69 o -5 1 1 301154.38 290456.94 28983.88 o -3 1 1 33491.34 19102.92 3955.24 o -1 1 1 29874.11 10913.45 4547.77 o 1 1 1 48.25 22.21 11.77 o 3 1 1 79148.94 59701.39 10367.11 o 5 1 1 183017.28 205018.70 2711.24 o 7 1 1 40801.23 45089.46 544.48 o 9 1 1 8435.15 6394.94 117.56 o 11 1 1 7614.38 5982.51 135.35 o 13 1 1 83648.94 79994.61 893.19 o 15 1 1 41819.23 41522.10 1336.82 o 17 1 1 30516.09 36412.87 450.70 o 19 1 1 33364.04 31489.50 440.49 o 21 1 1 60910.14 60751.64 785.84 o 23 1 1 31272.63 32098.99 496.40 o 25 1 1 4447.02 4059.96 178.25 o 27 1 1 13640.34 15132.69 359.88 o 29 1 1 9598.43 9695.66 344.24 o 31 1 1 10335.20 10164.11 337.79 o 33 1 1 223.34 638.01 185.14 o 35 1 1 481.41 719.53 202.67 o 37 1 1 5916.43 5585.40 431.64 o 39 1 1 5111.90 5753.34 367.20 o -40 2 1 880.38 716.87 235.54 o -38 2 1 522.11 620.74 217.66 o -36 2 1 1908.67 1770.18 289.59 o -34 2 1 584.85 686.26 183.92 o -32 2 1 2952.28 3384.73 196.74 o -30 2 1 924.78 764.00 131.82 o -28 2 1 3349.78 3495.34 120.43 o -26 2 1 3545.36 3258.33 126.47 o -24 2 1 373.30 443.55 80.21 o -22 2 1 3013.76 2890.16 113.22 o -20 2 1 2048.59 2037.62 94.16 o -18 2 1 9142.58 8863.87 170.98 o -16 2 1 14.14 283.49 62.05 o -14 2 1 3195.27 2265.50 86.70 o -12 2 1 365.17 661.57 57.85 o -10 2 1 115.47 243.38 38.70 o -8 2 1 29758.31 28773.96 304.96 o -6 2 1 415.71 329.42 30.14 o -4 2 1 63630.36 58994.66 1788.31 o -2 2 1 5576.13 6146.97 483.80 o 0 2 1 8071.27 9885.53 138.53 o 2 2 1 13201.05 17094.35 206.24 o 4 2 1 6467.84 8610.20 122.01 o 6 2 1 427.57 1205.50 56.30 o 8 2 1 6442.06 6467.95 131.11 o 10 2 1 5380.17 4193.39 105.47 o 12 2 1 493.92 238.13 59.62 o 14 2 1 6431.31 6284.24 174.00 o 16 2 1 2583.46 2455.51 107.10 o 18 2 1 32.98 335.68 85.54 o 20 2 1 3941.80 3648.50 164.38 o 22 2 1 3740.57 2606.22 371.21 o 24 2 1 1.10 175.70 75.55 o 26 2 1 4173.75 4339.03 207.76 o 28 2 1 1242.09 802.27 142.82 o 30 2 1 970.50 1052.00 167.60 o 32 2 1 1783.76 1612.10 189.23 o 34 2 1 43.29 205.37 163.08 o 36 2 1 403.22 283.80 208.54 o 38 2 1 1621.85 1287.56 247.17 o 40 2 1 364.22 -239.73 239.73 o -39 3 1 4571.93 4109.11 299.55 o -37 3 1 5819.90 5333.04 326.08 o -35 3 1 3229.55 2692.44 212.20 o -33 3 1 499.30 616.04 202.54 o -31 3 1 9924.48 10961.63 343.74 o -29 3 1 37568.11 41493.84 610.58 o -27 3 1 4661.16 4345.62 163.33 o -25 3 1 4379.25 4529.52 160.25 o -23 3 1 12667.86 13528.12 259.94 o -21 3 1 38852.50 39965.35 558.02 o -19 3 1 28048.84 26784.40 384.02 o -17 3 1 10014.49 9154.66 183.47 o -15 3 1 24925.23 25939.54 354.31 o -13 3 1 84001.60 82516.33 868.92 o -11 3 1 60609.66 58402.44 602.13 o -9 3 1 317.18 157.19 37.23 o -7 3 1 4104.67 4478.34 85.40 o -5 3 1 66917.14 64440.64 673.97 o -3 3 1 1562.90 1809.69 89.82 o -1 3 1 18170.95 18702.02 689.60 o 1 3 1 1858.52 1007.44 51.02 o 3 3 1 15502.75 13844.13 185.68 o 5 3 1 39664.99 35305.66 400.77 o 7 3 1 52472.56 51240.35 558.87 o 9 3 1 845.12 664.92 52.96 o 11 3 1 57595.69 57365.90 655.87 o 13 3 1 49099.46 50427.58 563.34 o 15 3 1 29899.19 29797.04 371.62 o 17 3 1 490.13 526.37 76.89 o 19 3 1 15933.06 17856.12 299.20 o 21 3 1 27667.25 28698.11 412.22 o 23 3 1 24895.05 25232.94 698.76 o 25 3 1 4684.95 4078.54 160.19 o 27 3 1 5577.95 5658.67 173.66 o 29 3 1 34658.39 37929.66 628.99 o 31 3 1 10247.97 10371.88 309.89 o 33 3 1 217.94 208.38 167.94 o 35 3 1 707.48 489.76 201.69 o 37 3 1 6932.78 7403.16 354.83 o 39 3 1 3788.40 3489.47 340.33 o -38 4 1 873.39 617.41 223.17 o -36 4 1 1112.21 1170.35 204.98 o -34 4 1 81.67 16.39 122.66 o -32 4 1 258.49 506.13 122.84 o -30 4 1 480.99 738.00 175.98 o -28 4 1 14518.31 15321.98 318.33 o -26 4 1 500.45 511.36 100.91 o -24 4 1 146.83 251.17 98.14 o -22 4 1 11036.82 10323.19 335.40 o -20 4 1 2287.23 1758.64 108.83 o -18 4 1 2688.30 2057.19 106.92 o -16 4 1 16.67 523.02 75.26 o -14 4 1 11292.36 11506.94 211.90 o -12 4 1 15292.64 15990.18 276.28 o -10 4 1 3744.72 3544.54 109.61 o -8 4 1 70109.93 75961.20 758.33 o -6 4 1 24873.27 25194.15 306.02 o -4 4 1 3786.59 4174.96 96.63 o -2 4 1 28475.89 27085.04 337.20 o 0 4 1 1963.40 2333.54 71.93 o 2 4 1 16494.39 16680.37 258.15 o 4 4 1 47130.88 44095.33 493.42 o 6 4 1 48859.06 47105.79 526.71 o 8 4 1 36220.13 39037.16 452.24 o 10 4 1 12281.38 11816.68 203.52 o 12 4 1 12543.68 12623.50 223.88 o 14 4 1 8334.68 6788.66 152.80 o 16 4 1 4498.37 4083.02 128.33 o 18 4 1 3453.20 4039.73 132.50 o 20 4 1 449.36 675.42 89.92 o 22 4 1 4253.95 4163.45 147.33 o 24 4 1 222.80 439.15 106.97 o 26 4 1 2919.09 3145.40 227.46 o 28 4 1 803.71 836.15 110.04 o 30 4 1 1499.95 1837.32 130.08 o 32 4 1 189.63 282.68 141.88 o 34 4 1 95.45 57.45 154.48 o 36 4 1 703.05 784.12 208.60 o 38 4 1 1274.08 844.56 308.14 o -37 5 1 3035.69 3146.95 279.49 o -35 5 1 1299.93 1181.13 170.86 o -33 5 1 230.25 234.40 136.53 o -31 5 1 1171.39 1229.72 152.63 o -29 5 1 10589.24 10989.04 278.07 o -27 5 1 2863.05 2797.06 179.61 o -25 5 1 2382.17 2159.58 150.07 o -23 5 1 10986.75 12013.65 313.25 o -21 5 1 16738.79 17762.17 413.38 o -19 5 1 8458.82 8619.07 233.80 o -17 5 1 1775.29 1474.34 105.99 o -15 5 1 12199.15 14695.32 249.60 o -13 5 1 43839.97 45172.36 549.21 o -11 5 1 24031.10 23818.72 307.20 o -9 5 1 93.07 291.46 51.87 o -7 5 1 32851.20 37524.43 456.09 o -5 5 1 48145.69 49199.32 586.80 o -3 5 1 14203.16 13765.17 213.04 o -1 5 1 1355.91 1573.26 69.86 o 1 5 1 339.77 440.72 57.53 o 3 5 1 42297.34 40704.49 496.11 o 5 5 1 32688.82 32607.82 401.36 o 7 5 1 76911.78 85713.90 910.05 o 9 5 1 5421.61 6247.48 146.77 o 11 5 1 8968.08 9654.27 188.29 o 13 5 1 32893.29 35997.68 486.53 o 15 5 1 16511.40 16834.97 379.14 o 17 5 1 1550.66 1663.40 112.99 o 19 5 1 2088.35 2222.16 114.73 o 21 5 1 8225.68 8814.16 206.45 o 23 5 1 10060.78 10234.58 237.64 o 25 5 1 2775.18 2322.09 152.21 o 27 5 1 15.26 -89.31 111.53 o 29 5 1 10595.43 11008.03 319.75 o 31 5 1 1725.86 1409.73 149.03 o 33 5 1 325.23 394.25 147.17 o 35 5 1 519.39 230.38 213.45 o 37 5 1 3304.67 3145.18 366.79 o -36 6 1 1688.18 2038.37 287.32 o -34 6 1 410.54 620.61 170.35 o -32 6 1 426.60 445.28 168.49 o -30 6 1 10591.96 10123.48 438.36 o -28 6 1 6857.51 6768.72 263.67 o -26 6 1 2651.60 2054.24 181.75 o -24 6 1 12267.86 12984.45 391.62 o -22 6 1 8386.66 9659.71 305.83 o -20 6 1 3568.23 4143.88 181.27 o -18 6 1 640.17 695.61 100.29 o -16 6 1 246.44 456.22 88.03 o -14 6 1 3183.87 2972.34 129.08 o -12 6 1 18873.05 19571.76 284.96 o -10 6 1 2351.60 1949.88 86.72 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