#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/34/2213475.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213475_Fobs loop_ _publ_author_name 'Gowda, B. Thimme' 'Foro, Sabine' 'Fuess, Hartmut' _publ_section_title ; N-(3-Chlorophenyl)methanesulfonamide ; _journal_coeditor_code LW2009 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2569 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.050 _cell_angle_gamma 90.000 _cell_length_a 23.4880 _cell_length_b 8.5230 _cell_length_c 9.2160 _exptl_crystal_F_000 848.00 _reflns_d_resolution_high 0.8378 _[local]_cod_data_source_file lw2009Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' GM2 C2/C' _shelx_refln_list_code 4 _shelx_f_calc_maximum 327.43 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 109.64 36.71 2.72 o 4 0 0 871.01 608.31 78.31 o 6 0 0 5158.55 4596.98 595.29 o 8 0 0 81.98 65.41 5.96 o 10 0 0 2861.06 2887.79 220.79 o 12 0 0 514.80 531.91 29.21 o 14 0 0 53.36 75.11 8.42 o 16 0 0 3429.74 4738.60 203.45 o 18 0 0 809.56 878.32 57.47 o 20 0 0 19.35 31.13 1.29 o 22 0 0 220.89 214.95 6.26 o 24 0 0 335.01 259.05 13.12 o 26 0 0 2.04 3.08 0.61 o 1 1 0 5798.98 3328.36 277.84 o 3 1 0 22646.22 14238.91 2412.32 o 5 1 0 19446.20 18119.92 2001.35 o 7 1 0 1257.01 1156.17 101.90 o 9 1 0 1055.83 1086.36 105.77 o 11 1 0 2105.13 2325.63 186.44 o 13 1 0 353.89 382.50 20.35 o 15 1 0 728.75 824.31 48.96 o 17 1 0 158.08 178.16 10.62 o 19 1 0 441.39 492.09 22.62 o 21 1 0 335.08 339.89 14.13 o 23 1 0 22.98 17.54 1.70 o 25 1 0 20.90 20.15 0.90 o 0 2 0 1912.82 2293.59 13.30 o 2 2 0 22208.34 17517.01 847.49 o 4 2 0 5310.17 4162.62 600.43 o 6 2 0 6813.00 7170.54 789.03 o 8 2 0 1002.88 797.10 77.72 o 10 2 0 1026.50 1185.34 119.59 o 12 2 0 296.50 418.85 40.56 o 14 2 0 898.35 1110.86 116.33 o 16 2 0 82.98 78.68 5.05 o 18 2 0 786.16 935.83 70.14 o 20 2 0 382.66 387.90 36.06 o 22 2 0 162.45 139.44 8.66 o 24 2 0 26.68 25.23 1.39 o 26 2 0 121.36 92.59 3.80 o 1 3 0 8005.02 7368.65 27.44 o 3 3 0 31.16 46.50 4.69 o 5 3 0 4506.77 4376.19 429.56 o 7 3 0 336.02 425.57 62.97 o 9 3 0 1309.86 1391.21 235.68 o 11 3 0 2729.05 3446.86 568.35 o 13 3 0 48.09 42.81 7.56 o 15 3 0 324.48 382.70 41.34 o 17 3 0 21.00 27.24 3.80 o 19 3 0 128.83 142.35 12.29 o 21 3 0 135.51 145.42 20.08 o 23 3 0 11.08 10.55 1.11 o 25 3 0 85.31 76.97 3.84 o 0 4 0 156.34 141.63 3.93 o 2 4 0 4042.92 4129.25 120.42 o 4 4 0 5813.99 6071.69 208.58 o 6 4 0 12.61 9.91 0.91 o 8 4 0 4787.97 6091.08 813.90 o 10 4 0 792.79 1021.99 166.55 o 12 4 0 70.80 93.83 20.44 o 14 4 0 119.76 150.33 21.01 o 16 4 0 22.59 33.00 5.88 o 18 4 0 2.92 11.75 2.35 o 20 4 0 77.47 104.53 11.27 o 22 4 0 63.54 55.74 5.05 o 24 4 0 12.70 9.39 0.70 o 1 5 0 954.31 998.80 55.07 o 3 5 0 4700.73 4128.52 1067.55 o 5 5 0 0.32 3.46 1.77 o 7 5 0 831.25 932.75 108.70 o 9 5 0 1386.88 1752.30 240.75 o 11 5 0 281.54 356.01 66.62 o 13 5 0 1373.51 1743.06 308.88 o 15 5 0 6.96 5.20 2.68 o 17 5 0 51.36 44.30 3.50 o 19 5 0 596.38 687.37 86.02 o 21 5 0 374.47 366.50 26.12 o 23 5 0 0.14 0.16 1.11 o 0 6 0 927.93 901.09 12.64 o 2 6 0 168.78 154.15 4.36 o 4 6 0 658.57 523.29 10.60 o 6 6 0 242.58 230.90 5.34 o 8 6 0 3865.93 3441.46 415.26 o 10 6 0 974.85 968.29 145.81 o 12 6 0 0.75 1.15 1.30 o 14 6 0 160.11 184.82 24.68 o 16 6 0 435.17 552.97 73.84 o 18 6 0 255.45 252.25 28.71 o 20 6 0 19.17 20.32 3.44 o 1 7 0 35.15 45.36 12.82 o 3 7 0 22.32 19.39 1.44 o 5 7 0 5100.38 4471.69 106.51 o 7 7 0 29.00 22.91 2.81 o 9 7 0 58.78 58.95 9.08 o 11 7 0 348.71 360.13 41.12 o 13 7 0 466.52 486.50 130.19 o 15 7 0 291.42 346.98 46.07 o 17 7 0 2.70 2.41 0.98 o 19 7 0 119.23 97.94 7.31 o 0 8 0 493.19 412.71 8.62 o 2 8 0 298.49 275.49 5.12 o 4 8 0 110.11 117.21 4.68 o 6 8 0 187.08 164.23 7.78 o 8 8 0 12.52 8.76 0.87 o 10 8 0 535.79 516.92 43.04 o 12 8 0 181.66 205.58 42.88 o 14 8 0 0.60 -0.64 1.48 o 16 8 0 29.00 26.43 0.84 o 1 9 0 71.54 73.50 1.61 o 3 9 0 113.80 112.34 2.42 o 5 9 0 47.47 52.17 1.88 o 7 9 0 10.30 10.14 1.19 o 9 9 0 81.22 89.11 15.45 o 11 9 0 168.32 237.79 3.75 o 0 10 0 55.65 48.48 1.52 o 2 10 0 90.08 101.00 4.96 o 4 10 0 164.63 210.68 7.05 o -27 1 1 0.25 -1.01 1.42 o -25 1 1 292.21 277.40 6.36 o -23 1 1 460.59 460.91 9.54 o -21 1 1 123.64 135.67 3.82 o -19 1 1 1194.52 1318.17 17.94 o -17 1 1 2919.48 3811.72 31.92 o -15 1 1 1123.74 1463.50 17.51 o -13 1 1 904.55 909.12 12.92 o -11 1 1 138.94 133.75 3.93 o -9 1 1 1879.24 1440.83 14.22 o -7 1 1 859.88 660.28 8.24 o -5 1 1 3527.23 2433.53 16.03 o -3 1 1 12896.99 11134.15 47.05 o -1 1 1 482.60 536.51 4.42 o 1 1 1 773.74 905.87 6.80 o 3 1 1 12288.13 12769.55 55.19 o 5 1 1 107213.16 101137.04 741.14 o 7 1 1 1160.16 863.90 10.46 o 9 1 1 1351.55 1333.60 14.32 o 11 1 1 5689.44 7165.85 43.22 o 13 1 1 3.71 5.26 1.37 o 15 1 1 870.57 997.10 14.97 o 17 1 1 216.02 298.21 8.58 o 19 1 1 507.18 700.56 12.71 o 21 1 1 637.12 756.65 12.57 o 23 1 1 0.29 1.32 2.28 o 25 1 1 11.96 16.46 1.11 o -26 2 1 86.23 76.66 2.44 o -24 2 1 583.56 557.73 9.55 o -22 2 1 179.35 182.49 5.56 o -20 2 1 1.91 1.82 1.62 o -18 2 1 259.79 260.37 7.01 o -16 2 1 89.53 63.62 2.24 o -14 2 1 1350.47 1479.50 17.90 o -12 2 1 363.09 376.02 8.20 o -10 2 1 4.30 13.52 1.11 o -8 2 1 2407.71 1466.37 14.86 o -6 2 1 7553.05 4775.98 29.70 o -4 2 1 2498.73 1966.40 14.37 o -2 2 1 11.33 8.97 0.61 o 0 2 1 16989.82 17766.82 161.73 o 2 2 1 16699.00 16295.86 69.97 o 4 2 1 10464.68 9582.33 48.03 o 6 2 1 1962.55 1569.70 14.87 o 8 2 1 7385.08 8872.14 48.98 o 10 2 1 9897.91 13754.85 69.84 o 12 2 1 61.61 96.61 3.05 o 14 2 1 65.03 92.64 2.84 o 16 2 1 1560.35 2037.14 22.41 o 18 2 1 120.13 132.96 4.17 o 20 2 1 127.43 145.26 4.32 o 22 2 1 4.98 5.32 1.32 o 24 2 1 45.46 38.91 1.37 o -25 3 1 6.25 6.53 0.91 o -23 3 1 439.28 410.18 8.35 o -21 3 1 1165.67 1202.95 16.11 o -19 3 1 77.72 99.11 2.94 o -17 3 1 2453.44 2716.39 26.96 o -15 3 1 294.66 271.45 7.33 o -13 3 1 777.04 813.31 13.21 o -11 3 1 5575.15 5452.54 38.26 o -9 3 1 277.66 188.45 5.60 o -7 3 1 5582.98 4521.32 31.17 o -5 3 1 2238.26 1815.44 16.00 o -3 3 1 4645.92 4295.20 25.76 o -1 3 1 67.59 94.87 2.80 o 1 3 1 6513.48 6210.70 33.53 o 3 3 1 2171.41 2026.35 17.03 o 5 3 1 4734.60 4212.96 29.18 o 7 3 1 14106.24 16404.82 81.00 o 9 3 1 1841.03 2299.22 21.66 o 11 3 1 520.31 699.96 11.77 o 13 3 1 3646.11 4962.71 37.11 o 15 3 1 224.29 273.86 8.23 o 17 3 1 9.12 13.67 1.67 o 19 3 1 539.33 632.32 11.90 o 21 3 1 32.88 32.94 1.67 o 23 3 1 344.54 371.66 6.99 o -24 4 1 93.84 76.78 2.19 o -22 4 1 476.18 432.08 8.47 o -20 4 1 0.32 0.71 2.94 o -18 4 1 340.59 390.41 9.75 o -16 4 1 2279.35 2340.40 25.12 o -14 4 1 2273.57 2376.87 25.35 o -12 4 1 2535.54 2615.40 25.93 o -10 4 1 2720.67 2626.59 25.13 o -8 4 1 3342.30 2974.74 26.21 o -6 4 1 90.97 46.95 1.68 o -4 4 1 92.57 68.59 2.09 o -2 4 1 1120.69 1335.89 12.60 o 0 4 1 270.58 281.83 5.66 o 2 4 1 1248.57 1188.91 13.59 o 4 4 1 576.77 664.54 10.54 o 6 4 1 3093.80 3352.21 27.82 o 8 4 1 1668.87 1969.54 20.91 o 10 4 1 817.95 1166.77 15.90 o 12 4 1 1047.46 1306.27 17.45 o 14 4 1 1249.56 1648.19 20.27 o 16 4 1 0.52 -0.86 2.73 o 18 4 1 442.62 527.24 10.61 o 20 4 1 14.07 11.34 1.37 o 22 4 1 98.87 115.83 3.71 o -23 5 1 5.60 6.89 0.96 o -21 5 1 364.28 360.05 7.56 o -19 5 1 1148.80 1114.95 15.26 o -17 5 1 138.52 149.04 4.53 o -15 5 1 1.06 2.89 1.57 o -13 5 1 1971.84 2007.21 23.55 o -11 5 1 1062.79 1129.62 16.87 o -9 5 1 415.37 449.59 10.36 o -7 5 1 663.06 687.40 12.41 o -5 5 1 18.27 17.63 1.01 o -3 5 1 86.48 59.07 1.88 o -1 5 1 108.49 102.95 3.10 o 1 5 1 523.74 451.90 7.84 o 3 5 1 469.80 499.04 10.04 o 5 5 1 770.48 858.79 13.74 o 7 5 1 194.45 276.44 8.17 o 9 5 1 1873.19 2624.53 26.05 o 11 5 1 5.86 7.59 1.52 o 13 5 1 57.64 55.81 2.18 o 15 5 1 226.51 294.53 8.43 o 17 5 1 9.36 13.97 1.47 o 19 5 1 22.05 26.90 1.57 o 21 5 1 104.79 120.36 3.51 o -22 6 1 165.52 165.32 3.93 o -20 6 1 213.39 206.04 5.47 o -18 6 1 87.69 86.37 2.64 o -16 6 1 91.81 106.18 3.10 o -14 6 1 120.10 144.75 4.43 o -12 6 1 441.01 336.66 8.19 o -10 6 1 292.28 236.11 6.71 o -8 6 1 618.47 450.60 8.93 o -6 6 1 809.37 520.23 9.43 o -4 6 1 400.50 314.67 7.26 o -2 6 1 196.11 212.13 6.13 o 0 6 1 429.95 387.90 8.10 o 2 6 1 388.36 307.27 7.05 o 4 6 1 3.06 5.26 1.06 o 6 6 1 22.74 19.91 1.27 o 8 6 1 890.96 894.87 12.91 o 10 6 1 1516.85 1966.40 22.98 o 12 6 1 94.41 133.73 4.17 o 14 6 1 106.71 149.97 4.37 o 16 6 1 14.79 15.40 1.47 o 18 6 1 104.22 136.49 4.07 o 20 6 1 38.58 39.41 1.37 o -19 7 1 565.43 578.71 7.86 o -17 7 1 118.65 122.08 3.56 o -15 7 1 80.65 91.32 2.64 o -13 7 1 173.04 159.05 4.59 o -11 7 1 226.38 216.38 6.28 o -9 7 1 33.13 34.26 1.67 o -7 7 1 222.55 217.38 6.54 o -5 7 1 148.34 118.24 3.77 o -3 7 1 2761.89 2462.02 23.01 o -1 7 1 652.07 612.17 10.60 o 1 7 1 75.66 67.02 1.98 o 3 7 1 51.89 40.63 1.72 o 5 7 1 107.91 98.93 3.00 o 7 7 1 769.06 762.86 12.00 o 9 7 1 90.28 103.94 3.10 o 11 7 1 56.63 52.91 1.88 o 13 7 1 699.51 1008.67 14.12 o 15 7 1 266.60 397.57 7.89 o 17 7 1 0.65 1.72 1.72 o -16 8 1 308.79 352.09 6.27 o -14 8 1 895.10 1007.96 12.38 o -12 8 1 4.07 0.86 2.08 o -10 8 1 1.27 0.81 0.96 o -8 8 1 1198.14 1040.37 13.38 o -6 8 1 524.14 485.50 9.51 o -4 8 1 51.71 51.08 1.83 o -2 8 1 2.11 3.64 1.11 o 0 8 1 2168.59 2056.34 20.22 o 2 8 1 320.67 307.71 7.74 o 4 8 1 11.81 12.96 1.32 o 6 8 1 30.50 34.61 1.47 o 8 8 1 20.79 21.43 1.37 o 10 8 1 1065.44 1256.36 13.86 o 12 8 1 13.74 28.72 1.57 o 14 8 1 165.94 219.34 5.21 o -13 9 1 106.96 123.94 3.56 o -11 9 1 378.62 480.21 7.79 o -9 9 1 164.40 146.54 4.18 o -7 9 1 47.46 43.47 1.37 o -5 9 1 958.11 901.41 11.18 o -3 9 1 728.68 747.18 10.28 o -1 9 1 521.00 483.45 8.49 o 1 9 1 3.40 1.82 1.92 o 3 9 1 214.85 213.15 5.42 o 5 9 1 326.49 335.29 6.68 o 7 9 1 288.36 310.67 6.21 o 9 9 1 39.00 52.23 1.72 o 11 9 1 82.53 103.21 3.00 o -4 10 1 61.21 79.28 2.34 o -2 10 1 10.43 10.08 0.86 o 0 10 1 480.98 574.15 9.45 o 2 10 1 493.82 630.68 10.19 o -26 0 2 25.86 22.50 1.32 o -24 0 2 423.88 419.22 8.86 o -22 0 2 455.55 473.70 10.31 o -20 0 2 619.61 687.76 12.92 o -18 0 2 503.49 475.05 10.55 o -16 0 2 375.74 370.28 8.85 o -14 0 2 5759.13 5643.13 38.77 o -12 0 2 11486.47 10846.33 58.98 o -10 0 2 4909.82 4160.56 27.76 o -8 0 2 6893.67 6232.77 33.73 o -6 0 2 705.39 500.87 6.19 o -4 0 2 44222.82 39445.13 300.39 o -2 0 2 2783.24 3028.67 15.65 o 0 0 2 1058.67 1390.66 9.23 o 2 0 2 91679.00 112191.50 678.09 o 4 0 2 18740.29 22996.68 93.71 o 6 0 2 65.38 43.88 1.37 o 8 0 2 3713.18 3455.43 25.32 o 10 0 2 22879.94 24676.32 114.50 o 12 0 2 7665.01 9179.15 54.77 o 14 0 2 1706.32 1867.37 20.85 o 16 0 2 527.22 632.01 12.10 o 18 0 2 544.62 696.83 12.78 o 20 0 2 319.16 294.34 7.85 o 22 0 2 73.10 80.17 2.34 o 24 0 2 61.63 63.41 1.88 o -27 1 2 416.88 330.91 5.89 o -25 1 2 118.78 108.52 3.15 o -23 1 2 72.33 77.92 2.49 o -21 1 2 3.55 2.43 2.83 o -19 1 2 1464.24 1555.79 19.68 o -17 1 2 600.51 646.45 12.00 o -15 1 2 24.65 13.73 1.27 o -13 1 2 47.29 39.37 1.42 o -11 1 2 553.79 539.90 8.77 o -9 1 2 4101.73 3123.24 22.27 o -7 1 2 105.86 99.57 2.70 o -5 1 2 368.56 236.57 4.08 o -3 1 2 20443.69 18630.93 74.13 o -1 1 2 11801.60 14443.14 57.37 o 1 1 2 5928.33 7194.31 32.89 o 3 1 2 305.20 336.87 5.30 o 5 1 2 2696.46 2623.72 18.95 o 7 1 2 3569.61 2981.61 22.60 o 9 1 2 772.89 556.66 9.54 o 11 1 2 176.12 168.63 5.11 o 13 1 2 989.73 1152.58 15.64 o 15 1 2 2576.42 3006.76 27.79 o 17 1 2 618.60 679.30 12.56 o 19 1 2 28.87 31.47 1.93 o 21 1 2 226.26 235.72 6.80 o 23 1 2 38.61 36.61 1.37 o -26 2 2 51.43 33.23 1.32 o -24 2 2 482.93 453.20 9.04 o -22 2 2 534.43 538.84 11.02 o -20 2 2 50.15 50.46 2.28 o -18 2 2 727.50 788.05 13.56 o -16 2 2 823.91 755.01 13.11 o -14 2 2 758.86 763.64 12.47 o -12 2 2 11598.16 8711.45 52.97 o -10 2 2 472.37 300.41 6.55 o -8 2 2 85.20 47.59 1.43 o -6 2 2 21920.52 18861.80 82.63 o -4 2 2 5.22 34.48 1.06 o -2 2 2 16798.99 20878.23 182.47 o 0 2 2 3406.33 3780.06 20.89 o 2 2 2 4050.69 4794.25 26.43 o 4 2 2 7.99 10.89 0.96 o 6 2 2 355.30 346.76 6.93 o 8 2 2 13.66 17.07 1.27 o 10 2 2 15.25 25.98 1.52 o 12 2 2 1168.25 1274.82 16.62 o 14 2 2 1.16 -1.77 2.99 o 16 2 2 639.53 705.44 12.78 o 18 2 2 113.13 112.88 3.20 o 20 2 2 53.58 59.20 2.18 o 22 2 2 27.44 26.61 1.47 o 24 2 2 235.83 179.75 4.25 o -25 3 2 26.66 32.84 1.32 o -23 3 2 162.64 162.43 4.84 o -21 3 2 427.00 438.39 9.89 o -19 3 2 9.98 8.71 1.72 o -17 3 2 474.32 447.04 10.58 o -15 3 2 11.10 16.00 1.62 o -13 3 2 2108.77 1640.76 19.16 o -11 3 2 178.51 113.88 3.68 o -9 3 2 9.04 12.20 0.96 o -7 3 2 9590.53 8475.11 46.37 o -5 3 2 4419.08 4477.12 27.10 o -3 3 2 2020.06 2531.60 17.12 o -1 3 2 293.97 293.00 5.01 o 1 3 2 4536.73 4999.42 28.59 o 3 3 2 1357.62 1452.36 13.84 o 5 3 2 1425.14 1541.70 15.61 o 7 3 2 3820.28 3626.79 28.17 o 9 3 2 1754.42 1833.55 19.82 o 11 3 2 307.69 338.27 8.62 o 13 3 2 738.18 942.75 14.61 o 15 3 2 1.68 8.35 1.67 o 17 3 2 285.89 289.71 8.40 o 19 3 2 68.16 65.98 2.23 o 21 3 2 14.78 16.92 1.27 o 23 3 2 0.70 1.82 0.86 o -24 4 2 151.05 125.30 3.62 o -22 4 2 2.08 2.83 1.21 o -20 4 2 53.92 58.84 2.28 o -18 4 2 413.66 426.08 10.45 o -16 4 2 2158.71 2170.02 24.36 o -14 4 2 0.13 1.06 2.38 o -12 4 2 1290.90 922.74 14.66 o -10 4 2 104.29 65.16 1.98 o -8 4 2 551.90 431.16 8.37 o -6 4 2 529.95 354.23 7.23 o -4 4 2 993.19 1253.45 12.74 o -2 4 2 7619.89 8604.87 43.62 o 0 4 2 1600.27 1611.15 14.67 o 2 4 2 1473.12 1586.59 15.53 o 4 4 2 3903.27 4141.32 30.11 o 6 4 2 820.96 787.04 12.15 o 8 4 2 2.66 1.72 2.13 o 10 4 2 778.29 981.69 14.91 o 12 4 2 1151.76 1386.41 18.24 o 14 4 2 530.11 615.70 12.26 o 16 4 2 5.68 9.82 1.42 o 18 4 2 292.18 362.66 8.66 o 20 4 2 58.39 61.81 1.78 o 22 4 2 24.59 24.02 1.11 o -23 5 2 260.74 256.30 5.54 o -21 5 2 8.55 14.23 1.27 o -19 5 2 266.04 270.39 7.83 o -17 5 2 2202.73 2336.78 24.97 o -15 5 2 70.78 75.94 2.74 o -13 5 2 323.22 312.04 8.93 o -11 5 2 4566.36 3690.02 33.36 o -9 5 2 911.25 792.36 13.11 o 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305.71 6.47 o -13 1 10 24.12 27.87 1.27 o -11 1 10 98.08 97.61 2.90 o -9 1 10 51.90 43.48 1.57 o -7 1 10 255.59 267.59 6.76 o -5 1 10 1083.67 1101.97 13.63 o -3 1 10 71.02 79.93 2.34 o -1 1 10 48.69 37.85 1.52 o 1 1 10 331.13 293.54 6.28 o 3 1 10 393.72 326.28 6.05 o -16 2 10 30.64 24.54 1.22 o -14 2 10 205.89 220.31 5.27 o -12 2 10 122.90 144.48 4.02 o -10 2 10 18.37 22.24 1.17 o -8 2 10 98.80 103.21 3.25 o -6 2 10 5.20 6.43 1.06 o -4 2 10 1.48 0.25 1.97 o -2 2 10 489.56 492.53 8.50 o 0 2 10 3.02 5.82 0.96 o 2 2 10 0.41 0.71 0.81 o -15 3 10 5.25 7.09 0.81 o -13 3 10 110.29 133.47 3.92 o -11 3 10 12.39 16.71 1.06 o -9 3 10 0.42 0.35 0.81 o -7 3 10 11.90 8.71 0.96 o -5 3 10 304.20 288.34 6.22 o -3 3 10 38.37 42.80 1.52 o -1 3 10 12.14 14.08 0.96 o -10 4 10 42.08 43.63 1.32 o -8 4 10 216.19 228.08 5.07 o -6 4 10 7.66 10.23 0.91 o -4 4 10 29.29 31.08 1.17 o