#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2213502.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213502_Fobs loop_ _publ_author_name 'Fletcher Claville, Michelle O.' 'Payne, Roosevelt J.' 'Parker, Brandon C.' 'Fronczek, Frank R.' _publ_section_title ; (Bromomethyl)trimethylammonium bromide ; _journal_coeditor_code PK2016 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2601 _journal_volume 63 _journal_year 2007 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 19.6740 _cell_length_b 6.9319 _cell_length_c 5.7038 _exptl_crystal_F_000 448.00 _reflns_d_resolution_high 0.6803 _[local]_cod_data_source_file pk2016Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Shelly1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 262.55 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x, y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z-1/2' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 56787.76 45631.71 635.20 o 12 0 0 24225.40 25659.08 433.26 o 18 0 0 8300.29 10604.02 256.07 o 24 0 0 4897.59 6787.40 163.13 o 26 0 0 34.58 60.31 29.12 o 2 1 0 1201.32 1295.64 17.85 o 4 1 0 6004.62 6646.29 106.75 o 6 1 0 670.88 606.49 12.14 o 8 1 0 12634.03 9979.57 146.54 o 10 1 0 4607.05 3912.77 62.19 o 12 1 0 1282.03 1180.78 28.87 o 14 1 0 5900.00 6358.76 91.15 o 16 1 0 2921.77 3584.14 71.11 o 18 1 0 1357.26 1543.23 44.63 o 20 1 0 4751.85 6187.21 155.86 o 22 1 0 307.66 434.32 64.78 o 24 1 0 248.91 284.58 21.65 o 26 1 0 1749.19 2308.48 64.07 o 28 1 0 9.56 34.72 22.37 o 0 2 0 68934.80 69090.10 924.16 o 2 2 0 2077.31 2069.97 22.59 o 4 2 0 3877.13 3654.89 45.13 o 6 2 0 35925.93 33762.91 620.68 o 8 2 0 1183.85 1111.17 29.68 o 10 2 0 3072.95 2989.81 46.04 o 12 2 0 23583.21 22993.11 254.41 o 14 2 0 1483.96 1371.03 27.46 o 16 2 0 529.58 456.50 17.89 o 18 2 0 10163.15 11419.35 212.91 o 20 2 0 647.14 747.28 48.57 o 22 2 0 473.34 572.49 30.67 o 24 2 0 5103.58 7384.39 123.38 o 26 2 0 116.11 136.02 18.97 o 28 2 0 196.25 230.79 38.19 o 2 3 0 7933.98 7747.96 79.37 o 4 3 0 5986.56 5855.94 61.05 o 6 3 0 1.70 6.69 3.04 o 8 3 0 10064.52 10886.74 167.20 o 10 3 0 2463.00 2113.12 45.48 o 12 3 0 352.21 327.86 17.89 o 14 3 0 4451.61 4151.07 83.02 o 16 3 0 1315.86 1290.56 28.41 o 18 3 0 922.13 969.94 52.25 o 20 3 0 2727.60 3175.68 80.76 o 22 3 0 172.16 209.56 15.02 o 24 3 0 416.46 521.67 34.92 o 26 3 0 1124.79 1442.37 63.76 o 0 4 0 37188.62 36108.58 494.16 o 2 4 0 1048.14 983.81 15.49 o 4 4 0 1061.67 975.97 15.43 o 6 4 0 24021.15 22096.38 249.78 o 8 4 0 1006.75 919.24 15.00 o 10 4 0 1235.55 1119.57 18.17 o 12 4 0 15342.07 15129.47 203.54 o 14 4 0 1090.28 989.02 18.65 o 16 4 0 363.14 297.26 24.64 o 18 4 0 6742.49 7281.41 105.83 o 20 4 0 422.52 493.90 30.72 o 22 4 0 376.08 487.27 32.67 o 24 4 0 3604.06 4881.93 117.49 o 26 4 0 53.96 -53.08 53.08 o 2 5 0 1649.05 1590.42 23.63 o 4 5 0 2618.59 2415.99 36.47 o 6 5 0 359.78 305.03 8.64 o 8 5 0 4227.26 4028.78 56.59 o 10 5 0 2389.71 2155.21 36.73 o 12 5 0 676.18 528.80 21.55 o 14 5 0 3232.85 2867.15 55.60 o 16 5 0 1813.26 1798.16 46.05 o 18 5 0 624.63 612.26 31.77 o 20 5 0 2756.35 3185.62 72.55 o 22 5 0 246.84 251.43 30.53 o 24 5 0 97.96 156.27 29.00 o 0 6 0 23446.24 23793.79 389.74 o 2 6 0 296.44 300.65 11.13 o 4 6 0 52.01 63.05 7.42 o 6 6 0 14068.27 13934.72 171.26 o 8 6 0 738.76 664.88 15.28 o 10 6 0 274.39 242.95 20.01 o 12 6 0 7936.31 7058.67 129.34 o 14 6 0 944.23 853.71 30.27 o 16 6 0 146.82 177.99 23.72 o 18 6 0 3062.14 3032.67 70.81 o 20 6 0 260.57 277.10 38.56 o 22 6 0 361.08 371.97 41.85 o 2 7 0 1268.82 1299.06 24.93 o 4 7 0 1585.93 1658.09 42.26 o 6 7 0 65.45 60.74 18.06 o 8 7 0 2650.59 2688.71 58.95 o 10 7 0 1183.88 1135.09 39.90 o 12 7 0 223.61 231.54 29.25 o 14 7 0 1638.76 1445.67 52.55 o 16 7 0 920.46 767.80 43.78 o 18 7 0 346.22 333.09 37.83 o 20 7 0 1346.16 1352.39 70.78 o 0 8 0 7729.12 8179.10 233.45 o 2 8 0 118.77 66.22 31.68 o 4 8 0 233.73 249.91 20.25 o 6 8 0 5354.97 6009.09 115.19 o 8 8 0 34.80 38.91 23.10 o 10 8 0 332.78 295.50 28.83 o 12 8 0 4360.32 4350.42 97.93 o 14 8 0 100.60 80.99 25.72 o 16 8 0 24.03 -12.77 25.60 o 2 9 0 1006.22 1144.52 61.80 o 4 9 0 925.25 986.61 57.35 o 6 9 0 0.72 -20.12 39.64 o 8 9 0 1561.19 1546.40 77.64 o 10 9 0 469.33 309.30 50.31 o 12 9 0 27.47 -56.54 86.76 o 2 10 0 9.77 -15.75 71.07 o 4 10 0 2.91 23.10 79.64 o 1 0 1 487.68 564.16 8.25 o 2 0 1 3681.95 3875.60 43.68 o 3 0 1 177.95 189.58 2.74 o 4 0 1 3563.19 3899.35 37.41 o 5 0 1 707.92 758.95 10.87 o 6 0 1 921.55 928.67 13.56 o 7 0 1 7829.81 7500.53 86.92 o 8 0 1 187.75 157.64 6.81 o 9 0 1 63.75 78.38 5.66 o 10 0 1 4419.13 3832.06 46.16 o 11 0 1 929.85 748.57 16.22 o 12 0 1 46.49 32.71 8.45 o 13 0 1 7632.02 5970.18 84.69 o 14 0 1 1533.63 1248.07 26.18 o 15 0 1 6.60 7.36 9.12 o 16 0 1 1904.96 1816.85 33.70 o 17 0 1 514.11 543.51 16.13 o 18 0 1 146.17 170.16 13.50 o 19 0 1 4443.88 4821.48 75.67 o 20 0 1 572.14 729.73 28.00 o 21 0 1 328.06 374.85 22.93 o 22 0 1 1319.89 1765.18 56.00 o 23 0 1 99.68 132.07 24.93 o 24 0 1 37.03 43.65 19.58 o 25 0 1 1352.91 1711.41 65.37 o 26 0 1 290.15 392.19 39.05 o 27 0 1 386.83 496.02 40.64 o 28 0 1 376.42 370.09 43.68 o 0 1 1 332.19 412.86 6.03 o 1 1 1 36456.63 39854.43 268.61 o 2 1 1 6000.50 6146.81 120.54 o 3 1 1 195.96 215.85 3.08 o 4 1 1 7442.26 7615.38 51.23 o 5 1 1 20982.24 22339.78 151.18 o 6 1 1 3285.13 3361.45 67.80 o 7 1 1 19823.13 20841.33 154.44 o 8 1 1 2824.12 2596.23 89.77 o 9 1 1 415.84 410.40 7.08 o 10 1 1 5778.28 5187.23 73.47 o 11 1 1 9491.36 7614.17 67.68 o 12 1 1 571.99 489.98 27.71 o 13 1 1 10524.28 10149.03 101.45 o 14 1 1 2588.61 2088.61 25.59 o 15 1 1 465.93 411.26 16.04 o 16 1 1 983.92 899.84 15.15 o 17 1 1 4201.14 4041.56 45.29 o 18 1 1 359.85 339.16 42.31 o 19 1 1 3993.34 4352.92 96.37 o 20 1 1 1175.34 1369.26 31.07 o 21 1 1 222.74 245.98 16.70 o 22 1 1 590.49 668.25 23.77 o 23 1 1 2713.02 3590.86 69.53 o 24 1 1 19.03 53.63 18.13 o 25 1 1 1290.28 1616.26 48.52 o 26 1 1 352.88 452.34 26.33 o 27 1 1 37.81 29.03 19.29 o 28 1 1 151.01 208.09 42.69 o 1 2 1 3177.60 3165.67 60.21 o 2 2 1 10243.41 10715.85 261.01 o 3 2 1 63.77 63.31 3.71 o 4 2 1 4827.51 4754.30 37.15 o 5 2 1 3248.41 3419.14 33.83 o 6 2 1 36.02 38.00 3.87 o 7 2 1 5654.95 5866.90 114.33 o 8 2 1 1326.72 1275.61 34.54 o 9 2 1 263.30 243.98 5.14 o 10 2 1 2702.79 2694.18 26.29 o 11 2 1 1052.43 1030.53 13.45 o 12 2 1 55.11 50.63 4.46 o 13 2 1 4577.05 4591.90 56.89 o 14 2 1 1106.11 916.37 32.18 o 15 2 1 68.07 61.30 5.01 o 16 2 1 915.31 749.65 22.33 o 17 2 1 206.29 199.61 8.36 o 18 2 1 130.82 105.95 10.24 o 19 2 1 3178.63 3300.96 49.15 o 20 2 1 177.94 223.00 16.02 o 21 2 1 190.85 237.47 20.68 o 22 2 1 948.44 1136.31 61.78 o 23 2 1 17.10 23.55 22.74 o 24 2 1 0.53 12.52 15.23 o 25 2 1 1261.61 1568.59 84.85 o 26 2 1 142.24 219.53 30.08 o 27 2 1 210.33 161.23 182.41 o 0 3 1 61.57 81.00 4.86 o 1 3 1 17667.40 17537.86 124.60 o 2 3 1 3307.27 3335.57 29.35 o 3 3 1 37.47 36.54 2.80 o 4 3 1 1738.66 1732.11 56.43 o 5 3 1 14697.14 15756.23 171.26 o 6 3 1 882.74 906.29 14.88 o 7 3 1 10581.67 10607.03 224.42 o 8 3 1 3445.92 3363.61 112.21 o 9 3 1 225.15 231.07 6.61 o 10 3 1 2467.44 2412.80 48.68 o 11 3 1 8982.96 8349.72 163.53 o 12 3 1 663.49 631.80 15.18 o 13 3 1 7333.52 7524.44 118.77 o 14 3 1 2843.39 2973.86 48.62 o 15 3 1 116.69 104.62 3.59 o 16 3 1 906.46 783.49 25.73 o 17 3 1 3828.31 3460.07 40.06 o 18 3 1 694.95 612.70 17.84 o 19 3 1 3548.36 3603.23 68.44 o 20 3 1 1059.57 1199.23 37.82 o 21 3 1 60.63 47.05 35.02 o 22 3 1 788.11 917.54 81.27 o 23 3 1 2055.43 2895.97 78.11 o 24 3 1 64.90 53.50 23.36 o 25 3 1 1282.34 1732.60 61.94 o 26 3 1 189.73 228.88 93.26 o 1 4 1 1677.55 1592.15 15.17 o 2 4 1 3674.46 3696.44 31.77 o 3 4 1 0.87 2.77 3.35 o 4 4 1 2668.52 2603.14 69.26 o 5 4 1 1489.20 1364.01 20.06 o 6 4 1 1.61 5.13 6.66 o 7 4 1 3754.37 4033.65 124.40 o 8 4 1 1049.85 1078.34 17.01 o 9 4 1 63.03 74.44 13.41 o 10 4 1 2069.11 2050.86 58.22 o 11 4 1 744.89 755.76 13.44 o 12 4 1 15.29 26.46 6.62 o 13 4 1 3549.43 3458.56 46.13 o 14 4 1 814.59 765.50 17.55 o 15 4 1 26.58 40.10 13.68 o 16 4 1 816.56 700.68 72.64 o 17 4 1 221.23 186.40 19.26 o 18 4 1 76.19 89.58 18.57 o 19 4 1 2465.33 2556.67 64.72 o 20 4 1 184.73 216.11 25.61 o 21 4 1 147.49 189.57 23.86 o 22 4 1 731.07 807.94 68.05 o 23 4 1 32.59 -0.15 27.20 o 24 4 1 1.41 35.53 23.85 o 25 4 1 923.15 1127.96 40.22 o 26 4 1 128.25 22.84 47.73 o 0 5 1 755.50 768.16 15.05 o 1 5 1 10647.73 10539.88 83.19 o 2 5 1 2261.52 2233.04 24.52 o 3 5 1 72.60 92.20 6.26 o 4 5 1 2720.32 2683.42 54.99 o 5 5 1 7237.43 7026.90 251.16 o 6 5 1 1103.00 1040.22 17.46 o 7 5 1 7749.48 7335.65 212.63 o 8 5 1 1199.09 1169.45 21.95 o 9 5 1 65.40 56.14 5.51 o 10 5 1 2296.25 2290.98 41.39 o 11 5 1 4131.24 4091.09 79.15 o 12 5 1 304.23 263.11 14.34 o 13 5 1 4828.76 4541.50 85.02 o 14 5 1 1052.11 913.53 25.45 o 15 5 1 161.86 146.80 18.75 o 16 5 1 542.15 495.53 26.96 o 17 5 1 1932.89 1825.63 40.87 o 18 5 1 184.82 156.66 34.00 o 19 5 1 1900.13 2001.59 62.05 o 20 5 1 588.21 627.74 29.25 o 21 5 1 93.76 101.15 20.86 o 22 5 1 265.86 289.42 24.02 o 23 5 1 1430.31 1711.87 74.39 o 24 5 1 15.03 -24.52 41.19 o 1 6 1 739.25 751.75 24.36 o 2 6 1 1051.89 1061.86 29.74 o 3 6 1 8.71 10.63 5.14 o 4 6 1 1150.55 1109.04 15.10 o 5 6 1 550.12 544.68 9.96 o 6 6 1 66.59 60.35 6.08 o 7 6 1 2179.11 2033.79 33.34 o 8 6 1 319.01 296.00 10.31 o 9 6 1 1.20 -7.93 7.93 o 10 6 1 1529.78 1395.83 28.03 o 11 6 1 437.93 400.84 39.61 o 12 6 1 16.68 22.74 12.34 o 13 6 1 2565.39 2316.66 42.68 o 14 6 1 601.43 557.50 20.98 o 15 6 1 2.01 9.73 18.76 o 16 6 1 802.77 712.40 25.56 o 17 6 1 251.80 247.09 76.82 o 18 6 1 39.62 65.14 23.43 o 19 6 1 1760.50 1810.21 47.31 o 20 6 1 265.09 243.81 36.43 o 21 6 1 104.96 92.99 26.04 o 22 6 1 558.52 577.11 35.91 o 23 6 1 73.66 57.28 107.13 o 0 7 1 215.19 201.80 10.52 o 1 7 1 4661.89 4784.66 48.27 o 2 7 1 1038.26 1105.84 23.09 o 3 7 1 46.15 48.40 7.97 o 4 7 1 1014.73 1040.75 55.40 o 5 7 1 3589.36 3754.80 51.45 o 6 7 1 601.62 575.24 26.05 o 7 7 1 3402.66 3539.43 52.03 o 8 7 1 742.38 753.20 57.50 o 9 7 1 4.84 11.00 15.20 o 10 7 1 1070.06 1039.97 73.06 o 11 7 1 2236.70 2088.46 190.68 o 12 7 1 251.48 218.42 39.20 o 13 7 1 2348.40 2176.49 137.59 o 14 7 1 702.33 689.30 63.91 o 15 7 1 25.09 37.53 52.26 o 16 7 1 276.97 222.91 23.64 o 17 7 1 1033.50 948.26 52.46 o 18 7 1 192.69 154.84 23.43 o 19 7 1 1057.49 982.10 38.25 o 20 7 1 342.78 305.20 48.36 o 1 8 1 706.02 735.13 28.18 o 2 8 1 1324.43 1338.37 73.45 o 3 8 1 4.87 27.33 21.95 o 4 8 1 813.49 856.68 44.59 o 5 8 1 631.63 682.92 24.98 o 6 8 1 11.65 17.41 15.88 o 7 8 1 988.60 988.04 26.86 o 8 8 1 372.62 379.20 19.65 o 9 8 1 44.61 47.86 15.50 o 10 8 1 502.09 524.25 65.10 o 11 8 1 299.54 336.29 23.00 o 12 8 1 19.81 16.37 22.80 o 13 8 1 915.14 815.33 86.69 o 14 8 1 264.18 254.61 24.48 o 15 8 1 6.11 -4.01 27.02 o 16 8 1 174.04 146.28 36.27 o 17 8 1 75.74 113.70 52.72 o 0 9 1 30.26 14.59 32.22 o 1 9 1 1701.45 1870.27 54.36 o 2 9 1 391.74 426.50 27.99 o 3 9 1 21.88 90.54 33.70 o 4 9 1 245.34 264.64 31.10 o 5 9 1 1558.74 1659.19 52.61 o 6 9 1 229.88 272.77 37.71 o 7 9 1 1157.50 1361.47 53.41 o 8 9 1 456.67 491.97 40.13 o 9 9 1 1.91 -46.21 46.21 o 10 9 1 329.44 399.29 109.15 o 11 9 1 1109.12 973.91 89.33 o 12 9 1 193.24 -107.34 107.34 o 2 10 1 401.52 488.35 85.04 o 3 10 1 0.68 35.87 78.61 o 4 10 1 319.53 329.14 137.49 o 0 0 2 6418.59 6389.12 100.14 o 1 0 2 22.69 22.44 3.04 o 2 0 2 5056.58 5064.54 56.83 o 3 0 2 34506.25 37587.20 369.49 o 4 0 2 5102.27 5096.33 60.50 o 5 0 2 608.37 600.98 9.69 o 6 0 2 10194.80 10699.57 104.01 o 7 0 2 591.78 688.49 10.36 o 8 0 2 5585.07 6076.59 62.07 o 9 0 2 21358.55 22799.04 199.88 o 10 0 2 1450.55 1330.24 21.62 o 11 0 2 566.39 563.50 12.91 o 12 0 2 3383.50 3174.61 41.89 o 13 0 2 61.54 43.66 7.18 o 14 0 2 2482.75 2207.61 34.86 o 15 0 2 8861.02 7456.34 111.78 o 16 0 2 2122.22 1896.05 38.72 o 17 0 2 3.74 24.32 12.16 o 18 0 2 1940.35 1706.08 38.75 o 19 0 2 248.13 232.29 18.79 o 20 0 2 1055.74 915.57 34.35 o 21 0 2 3578.69 3663.08 83.81 o 22 0 2 725.18 833.26 37.01 o 23 0 2 22.19 40.80 24.26 o 24 0 2 541.12 593.94 34.87 o 25 0 2 156.92 144.24 29.61 o 26 0 2 414.05 439.53 40.33 o 27 0 2 1369.38 1501.58 91.80 o 28 0 2 443.01 558.34 48.97 o 1 1 2 10423.07 10829.80 74.30 o 2 1 2 312.80 310.39 4.58 o 3 1 2 137.88 141.19 3.07 o 4 1 2 39.69 41.16 2.42 o 5 1 2 5663.24 5646.77 59.95 o 6 1 2 397.11 441.97 5.88 o 7 1 2 5035.96 5214.24 37.85 o 8 1 2 4.17 6.37 3.01 o 9 1 2 914.11 960.90 10.68 o 10 1 2 8.80 8.51 3.89 o 11 1 2 4638.59 4680.49 47.56 o 12 1 2 653.67 679.04 16.75 o 13 1 2 2532.34 2430.23 63.41 o 14 1 2 583.71 554.95 11.63 o 15 1 2 90.90 100.50 6.75 o 16 1 2 52.96 44.62 9.58 o 17 1 2 3658.34 3126.67 56.81 o 18 1 2 231.90 180.34 13.50 o 19 1 2 793.82 741.26 20.62 o 20 1 2 357.72 341.60 22.81 o 21 1 2 173.77 180.28 14.88 o 22 1 2 30.23 29.61 27.75 o 23 1 2 2020.39 2439.22 52.10 o 24 1 2 235.44 255.27 22.62 o 25 1 2 441.75 512.36 39.00 o 26 1 2 401.14 456.06 29.96 o 27 1 2 114.93 183.94 40.13 o 0 2 2 9083.03 9490.77 97.81 o 1 2 2 1033.18 1101.90 10.45 o 2 2 2 3580.19 3461.19 39.45 o 3 2 2 17544.29 17515.81 121.36 o 4 2 2 2939.44 2879.00 22.57 o 5 2 2 43.61 46.99 2.50 o 6 2 2 8189.56 8196.82 57.58 o 7 2 2 83.80 78.59 2.73 o 8 2 2 4462.38 4761.88 113.21 o 9 2 2 18210.54 19165.21 603.04 o 10 2 2 1455.36 1479.80 24.66 o 11 2 2 0.51 9.69 13.65 o 12 2 2 3074.43 2941.62 33.18 o 13 2 2 200.76 193.78 6.73 o 14 2 2 2299.59 2129.73 67.37 o 15 2 2 10372.95 9761.67 91.06 o 16 2 2 1697.15 1638.91 22.50 o 17 2 2 73.60 65.58 7.60 o 18 2 2 1496.53 1307.70 30.45 o 19 2 2 55.91 39.55 13.04 o 20 2 2 1013.46 835.68 87.73 o 21 2 2 4367.71 4535.02 87.11 o 22 2 2 773.90 794.91 112.89 o 23 2 2 43.32 19.02 27.30 o 24 2 2 415.23 488.36 35.62 o 25 2 2 18.80 28.86 43.17 o 26 2 2 317.44 292.19 34.93 o 27 2 2 1276.63 1708.86 95.87 o 1 3 2 10731.60 11403.14 190.13 o 2 3 2 56.67 85.59 3.86 o 3 3 2 30.93 39.71 3.27 o 4 3 2 77.34 86.57 5.69 o 5 3 2 7613.28 7632.28 102.37 o 6 3 2 448.74 472.13 6.68 o 7 3 2 3323.86 3351.54 141.07 o 8 3 2 4.99 -0.24 5.08 o 9 3 2 56.60 67.65 5.75 o 10 3 2 14.12 15.10 6.45 o 11 3 2 4105.79 4186.64 49.87 o 12 3 2 576.65 555.57 13.39 o 13 3 2 1107.77 1070.22 20.19 o 14 3 2 410.56 415.66 13.38 o 15 3 2 4.27 19.28 7.53 o 16 3 2 6.30 29.72 15.40 o 17 3 2 2181.32 1914.31 41.19 o 18 3 2 229.39 193.11 19.96 o 19 3 2 324.68 290.71 23.48 o 20 3 2 393.51 327.82 25.31 o 21 3 2 233.52 234.38 58.87 o 22 3 2 11.22 -7.82 24.82 o 23 3 2 1141.05 1340.29 48.43 o 24 3 2 132.05 188.32 45.45 o 25 3 2 404.14 506.85 127.84 o 26 3 2 386.34 366.98 42.17 o 0 4 2 5795.93 6073.55 73.62 o 1 4 2 256.65 265.68 14.39 o 2 4 2 2054.04 2009.35 74.03 o 3 4 2 12918.08 13208.57 533.80 o 4 4 2 1728.72 1710.41 47.97 o 5 4 2 25.16 28.30 3.18 o 6 4 2 4834.98 4716.86 44.24 o 7 4 2 0.86 4.10 5.82 o 8 4 2 2732.67 2758.62 107.51 o 9 4 2 12178.52 12010.71 123.72 o 10 4 2 1018.20 1053.59 29.58 o 11 4 2 11.28 13.16 6.28 o 12 4 2 1979.65 1962.94 28.61 o 13 4 2 83.21 89.72 8.79 o 14 4 2 1609.11 1583.44 65.01 o 15 4 2 6908.56 7079.66 95.67 o 16 4 2 1101.40 1027.55 61.19 o 17 4 2 46.87 34.54 19.65 o 18 4 2 1020.41 954.47 44.73 o 19 4 2 47.17 59.50 22.02 o 20 4 2 703.67 652.62 81.80 o 21 4 2 3026.28 3180.36 70.95 o 22 4 2 542.76 569.65 33.68 o 23 4 2 18.76 102.15 48.43 o 24 4 2 291.20 348.94 35.71 o 25 4 2 20.10 55.55 74.39 o 1 5 2 3730.76 3813.38 76.41 o 2 5 2 58.86 60.47 9.36 o 3 5 2 47.50 48.52 13.01 o 4 5 2 4.44 10.59 3.34 o 5 5 2 2480.21 2533.38 62.02 o 6 5 2 81.82 78.22 3.98 o 7 5 2 2483.43 2478.13 77.35 o 8 5 2 31.76 26.50 7.31 o 9 5 2 488.53 474.34 18.74 o 10 5 2 2.26 0.29 9.12 o 11 5 2 2356.75 2334.40 37.14 o 12 5 2 236.80 231.27 12.47 o 13 5 2 1639.83 1604.26 37.56 o 14 5 2 251.81 242.22 31.26 o 15 5 2 57.42 44.86 20.49 o 16 5 2 19.98 30.81 22.18 o 17 5 2 2134.35 2157.34 50.70 o 18 5 2 127.53 96.06 26.81 o 19 5 2 552.58 577.12 33.23 o 20 5 2 171.04 225.59 28.45 o 21 5 2 71.68 132.39 114.40 o 22 5 2 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3777.59 3957.69 90.34 o 9 5 3 2454.10 2460.83 77.18 o 10 5 3 3624.30 3676.69 52.92 o 11 5 3 19.95 14.91 11.14 o 12 5 3 39.81 38.98 11.04 o 13 5 3 45.78 39.54 24.38 o 14 5 3 2625.64 2857.97 63.66 o 15 5 3 1601.51 1711.57 129.14 o 16 5 3 1769.96 1837.98 90.79 o 17 5 3 112.75 163.62 28.51 o 18 5 3 0.27 -25.25 25.25 o 19 5 3 34.13 4.21 26.27 o 20 5 3 1401.93 1360.08 57.84 o 21 5 3 883.84 745.35 73.08 o 22 5 3 660.13 766.38 101.84 o 1 6 3 362.33 363.60 32.55 o 2 6 3 1213.06 1286.48 23.78 o 3 6 3 25.98 31.89 10.61 o 4 6 3 1896.83 2015.30 39.96 o 5 6 3 813.58 791.62 19.35 o 6 6 3 2.11 -3.13 10.72 o 7 6 3 628.40 636.79 62.33 o 8 6 3 675.12 685.94 19.51 o 9 6 3 0.36 9.78 11.22 o 10 6 3 1545.22 1617.10 70.38 o 11 6 3 863.52 913.75 33.20 o 12 6 3 18.43 12.67 19.62 o 13 6 3 340.47 362.16 25.47 o 14 6 3 292.92 300.65 24.94 o 15 6 3 110.36 100.77 31.95 o 16 6 3 1190.85 1179.54 59.02 o 17 6 3 520.91 466.35 44.33 o 18 6 3 57.93 64.17 53.47 o 19 6 3 168.93 116.66 30.80 o 20 6 3 169.45 188.88 43.24 o 0 7 3 39.09 31.62 13.32 o 1 7 3 13.34 30.36 12.79 o 2 7 3 2230.67 2393.83 37.59 o 3 7 3 1916.39 2053.10 54.84 o 4 7 3 2407.48 2484.19 44.35 o 5 7 3 12.91 14.04 17.75 o 6 7 3 27.91 47.30 19.33 o 7 7 3 208.93 177.38 33.91 o 8 7 3 2067.92 2244.35 49.30 o 9 7 3 1280.27 1316.28 37.92 o 10 7 3 1654.68 1772.07 60.93 o 11 7 3 4.62 -2.29 6.05 o 12 7 3 70.95 63.67 28.79 o 13 7 3 28.01 15.06 25.54 o 14 7 3 1491.35 1556.15 161.72 o 15 7 3 1040.91 990.00 98.31 o 16 7 3 969.38 933.99 81.83 o 17 7 3 22.22 13.45 31.99 o 1 8 3 546.98 561.46 31.92 o 2 8 3 838.32 968.25 46.45 o 3 8 3 8.31 4.17 16.60 o 4 8 3 1063.14 1103.77 69.97 o 5 8 3 1015.74 1086.06 35.56 o 6 8 3 8.22 30.76 73.32 o 7 8 3 279.96 310.69 91.93 o 8 8 3 507.68 563.18 27.10 o 9 8 3 122.49 141.01 33.63 o 10 8 3 636.47 704.52 50.63 o 11 8 3 556.33 460.23 77.43 o 12 8 3 37.41 48.86 30.09 o 13 8 3 32.25 13.31 30.95 o 14 8 3 134.72 92.98 50.41 o 0 9 3 34.61 21.95 57.76 o 1 9 3 24.70 -4.45 31.36 o 2 9 3 930.32 1004.30 87.73 o 3 9 3 572.98 499.21 91.55 o 4 9 3 941.40 998.69 191.41 o 5 9 3 0.81 14.04 38.97 o 6 9 3 30.72 6.08 52.89 o 7 9 3 210.37 192.78 50.66 o 8 9 3 957.00 957.34 68.73 o 0 0 4 4226.67 4382.45 114.90 o 1 0 4 3164.10 3195.19 55.97 o 2 0 4 2952.41 2976.06 54.04 o 3 0 4 5852.60 5949.80 91.95 o 4 0 4 2169.45 2255.91 35.21 o 5 0 4 2892.37 2886.14 47.89 o 6 0 4 3353.41 3330.44 54.31 o 7 0 4 4350.97 4524.40 73.34 o 8 0 4 2037.18 2106.39 40.86 o 9 0 4 4391.44 4602.56 77.30 o 10 0 4 1347.54 1405.05 37.01 o 11 0 4 1145.29 1142.20 33.40 o 12 0 4 1422.96 1468.67 39.75 o 13 0 4 1804.26 1805.04 50.40 o 14 0 4 924.44 891.70 35.39 o 15 0 4 3239.35 3246.81 84.53 o 16 0 4 774.74 784.28 33.18 o 17 0 4 1152.40 1108.61 44.35 o 18 0 4 958.44 915.33 38.85 o 19 0 4 871.35 770.55 38.36 o 20 0 4 665.85 526.39 35.12 o 21 0 4 1494.34 1223.61 58.75 o 22 0 4 380.03 356.96 34.49 o 23 0 4 310.72 264.95 32.91 o 24 0 4 628.91 564.35 49.23 o 25 0 4 268.38 242.18 32.23 o 1 1 4 124.76 125.34 7.63 o 2 1 4 4219.15 4217.85 74.11 o 3 1 4 45.29 62.87 10.97 o 4 1 4 3678.89 3843.13 105.96 o 5 1 4 701.32 715.61 11.10 o 6 1 4 65.18 71.84 6.94 o 7 1 4 52.48 62.73 8.71 o 8 1 4 3579.32 3605.93 43.42 o 9 1 4 2.22 -5.24 7.28 o 10 1 4 3278.27 3405.77 43.03 o 11 1 4 577.37 593.23 18.11 o 12 1 4 11.21 16.28 9.83 o 13 1 4 38.09 -7.60 14.83 o 14 1 4 1841.80 1793.75 38.37 o 15 1 4 352.03 361.54 21.11 o 16 1 4 1946.45 1869.80 41.36 o 17 1 4 365.83 370.76 17.41 o 18 1 4 0.23 7.02 13.37 o 19 1 4 15.76 -2.42 14.57 o 20 1 4 491.42 421.96 43.38 o 21 1 4 181.82 174.53 18.98 o 22 1 4 653.47 555.19 45.61 o 23 1 4 224.08 167.15 20.79 o 24 1 4 0.66 20.12 32.28 o 25 1 4 112.61 122.04 27.24 o 0 2 4 2506.91 2553.16 44.96 o 1 2 4 2011.06 2088.71 50.92 o 2 2 4 2404.96 2433.68 29.85 o 3 2 4 6328.55 6512.12 74.07 o 4 2 4 906.22 918.53 26.84 o 5 2 4 2924.71 2889.54 37.48 o 6 2 4 2134.93 2173.79 30.83 o 7 2 4 2854.42 2999.44 50.20 o 8 2 4 3025.93 3095.20 37.91 o 9 2 4 3910.87 4025.84 50.53 o 10 2 4 498.44 496.26 14.41 o 11 2 4 1400.90 1441.20 76.85 o 12 2 4 1855.54 1885.50 42.71 o 13 2 4 1318.51 1410.41 29.59 o 14 2 4 1608.98 1647.02 34.18 o 15 2 4 2446.45 2317.78 46.32 o 16 2 4 822.55 794.87 34.37 o 17 2 4 1330.14 1142.39 34.37 o 18 2 4 1491.54 1384.84 32.65 o 19 2 4 894.85 720.45 42.19 o 20 2 4 677.64 611.27 44.82 o 21 2 4 1028.17 966.74 61.38 o 22 2 4 605.26 565.50 48.07 o 23 2 4 262.19 256.96 41.11 o 24 2 4 740.94 664.61 54.71 o 1 3 4 3.35 20.38 7.49 o 2 3 4 4664.33 4626.76 56.63 o 3 3 4 154.88 141.16 13.11 o 4 3 4 3429.97 3405.27 46.83 o 5 3 4 195.94 204.36 17.88 o 6 3 4 377.00 369.42 16.06 o 7 3 4 75.24 69.58 7.80 o 8 3 4 4110.28 4031.34 102.36 o 9 3 4 69.95 68.89 7.15 o 10 3 4 1880.98 1818.13 163.88 o 11 3 4 362.00 352.44 30.85 o 12 3 4 182.69 155.05 15.36 o 13 3 4 0.06 0.15 12.77 o 14 3 4 1232.87 1106.06 88.59 o 15 3 4 434.40 348.29 62.30 o 16 3 4 985.94 904.56 36.32 o 17 3 4 415.48 430.53 33.25 o 18 3 4 0.54 41.92 22.84 o 19 3 4 2.98 3.69 47.18 o 20 3 4 196.46 161.58 31.95 o 21 3 4 115.67 51.14 36.67 o 22 3 4 445.15 420.14 97.10 o 23 3 4 294.88 233.80 44.52 o 0 4 4 2276.13 2313.25 59.44 o 1 4 4 1291.47 1278.80 100.46 o 2 4 4 1784.83 1753.19 30.70 o 3 4 4 4231.55 4280.42 58.40 o 4 4 4 803.53 804.31 18.12 o 5 4 4 1951.03 1923.11 59.36 o 6 4 4 1687.61 1718.50 34.74 o 7 4 4 1897.36 1962.84 80.61 o 8 4 4 1973.81 1975.80 54.86 o 9 4 4 2675.82 2680.19 99.81 o 10 4 4 422.59 425.70 35.53 o 11 4 4 897.74 887.02 32.40 o 12 4 4 1311.49 1394.91 105.67 o 13 4 4 890.21 922.69 26.65 o 14 4 4 1033.46 996.66 71.62 o 15 4 4 1745.10 1607.95 40.32 o 16 4 4 602.86 613.10 35.06 o 17 4 4 904.50 973.94 48.40 o 18 4 4 1041.15 972.13 47.91 o 19 4 4 615.84 498.97 38.14 o 20 4 4 500.68 396.06 36.28 o 21 4 4 746.45 622.12 45.73 o 22 4 4 406.47 221.92 149.16 o 1 5 4 84.42 104.27 11.60 o 2 5 4 1787.74 1863.33 34.84 o 3 5 4 21.65 22.39 11.37 o 4 5 4 1841.57 1900.74 170.33 o 5 5 4 396.90 403.38 15.22 o 6 5 4 12.60 19.66 10.27 o 7 5 4 38.99 34.38 12.10 o 8 5 4 1915.48 1985.82 115.51 o 9 5 4 3.11 -1.00 11.82 o 10 5 4 1951.15 2050.70 56.85 o 11 5 4 296.78 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8 5 5 746.99 702.99 56.06 o 9 5 5 872.21 932.81 32.37 o 10 5 5 92.81 118.90 18.83 o 11 5 5 444.09 454.05 30.78 o 12 5 5 1848.42 1969.96 67.52 o 13 5 5 155.18 176.66 38.80 o 14 5 5 331.83 324.79 122.72 o 15 5 5 546.82 587.49 93.22 o 16 5 5 310.71 214.79 132.11 o 17 5 5 478.32 355.12 41.86 o 1 6 5 1241.17 1224.56 28.68 o 2 6 5 201.17 165.41 18.09 o 3 6 5 31.56 4.09 13.41 o 4 6 5 181.86 152.05 35.70 o 5 6 5 1036.38 1054.34 27.73 o 6 6 5 161.22 157.55 15.67 o 7 6 5 747.64 821.23 32.69 o 8 6 5 119.79 141.30 40.38 o 9 6 5 1.17 26.44 25.86 o 10 6 5 172.51 140.38 45.73 o 11 6 5 746.35 752.88 54.95 o 12 6 5 137.87 193.44 124.11 o 13 6 5 634.29 702.05 78.04 o 14 6 5 403.28 463.60 46.72 o 0 7 5 1393.25 1519.00 55.81 o 1 7 5 182.55 151.54 36.76 o 2 7 5 264.57 290.01 21.23 o 3 7 5 530.97 493.75 78.19 o 4 7 5 161.90 191.66 39.89 o 5 7 5 535.73 539.49 43.10 o 6 7 5 1595.39 1710.37 74.99 o 7 7 5 166.74 122.67 61.48 o 8 7 5 248.98 263.28 46.47 o 9 7 5 530.23 573.19 44.97 o 10 7 5 74.10 26.98 199.55 o 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43.89 o 8 5 6 154.36 125.90 25.11 o 9 5 6 1.65 5.17 40.79 o 10 5 6 25.33 8.18 17.59 o 11 5 6 298.57 342.17 135.24 o 12 5 6 5.22 17.11 30.98 o 13 5 6 799.10 682.62 170.18 o 0 6 6 74.82 82.81 35.45 o 1 6 6 1494.83 1630.93 78.24 o 2 6 6 43.22 60.95 19.29 o 3 6 6 220.04 168.39 26.29 o 4 6 6 176.51 205.20 28.55 o 5 6 6 797.63 770.46 43.98 o 6 6 6 295.83 308.02 34.06 o 7 6 6 1353.46 1470.85 148.12 o 8 6 6 0.82 7.83 70.55 o 9 6 6 152.26 197.25 62.27 o 10 6 6 77.53 -142.46 147.14 o 1 7 6 661.28 574.13 33.75 o 2 7 6 237.88 164.09 34.48 o 3 7 6 6.24 53.40 37.23 o 1 0 7 4.85 28.64 18.18 o 2 0 7 912.89 1077.02 35.62 o 3 0 7 7.80 10.27 16.42 o 4 0 7 1148.46 1268.24 43.98 o 5 0 7 25.92 24.81 31.43 o 6 0 7 13.43 9.67 35.08 o 7 0 7 82.06 94.37 26.81 o 8 0 7 1183.63 1217.81 41.36 o 9 0 7 135.11 78.38 31.44 o 10 0 7 469.26 446.81 42.77 o 11 0 7 224.64 277.08 29.56 o 12 0 7 10.46 34.72 35.14 o 13 0 7 302.51 226.32 32.66 o 14 0 7 543.11 478.73 45.33 o 15 0 7 106.59 80.99 34.17 o 0 1 7 3276.30 3698.66 84.22 o 1 1 7 43.47 72.10 13.24 o 2 1 7 1.13 -13.77 17.05 o 3 1 7 1866.53 2058.94 42.62 o 4 1 7 6.80 -4.78 14.17 o 5 1 7 77.21 84.92 15.46 o 6 1 7 2234.80 2669.54 81.97 o 7 1 7 34.07 39.27 28.48 o 8 1 7 5.65 -4.52 16.74 o 9 1 7 857.23 835.20 29.12 o 10 1 7 7.14 1.54 16.36 o 11 1 7 306.33 317.72 27.52 o 12 1 7 2076.68 2124.48 161.67 o 13 1 7 39.43 18.61 22.99 o 14 1 7 4.22 7.45 23.34 o 15 1 7 314.38 190.96 21.84 o 1 2 7 90.61 138.76 16.45 o 2 2 7 715.06 777.69 30.13 o 3 2 7 8.36 -2.76 15.82 o 4 2 7 981.23 1062.55 74.96 o 5 2 7 215.22 241.35 20.53 o 6 2 7 25.91 46.01 17.96 o 7 2 7 50.54 98.14 19.67 o 8 2 7 964.54 1048.23 49.87 o 9 2 7 1.54 2.44 14.58 o 10 2 7 467.30 463.25 36.17 o 11 2 7 262.31 252.10 55.83 o 12 2 7 27.79 51.25 17.93 o 13 2 7 77.96 42.53 20.33 o 14 2 7 479.82 360.71 36.56 o 0 3 7 2923.61 3315.60 96.74 o 1 3 7 133.51 136.43 22.94 o 2 3 7 0.07 6.80 21.65 o 3 3 7 956.29 1006.18 43.02 o 4 3 7 22.13 8.07 21.19 o 5 3 7 19.67 12.37 24.05 o 6 3 7 1949.78 2199.04 61.28 o 7 3 7 181.55 131.15 17.85 o 8 3 7 1.97 16.22 15.87 o 9 3 7 683.69 620.58 105.95 o 10 3 7 0.01 32.09 16.94 o 11 3 7 65.21 24.37 13.52 o 12 3 7 1691.96 1621.29 81.48 o 13 3 7 64.40 120.39 41.10 o 1 4 7 44.28 52.51 19.28 o 2 4 7 523.01 509.80 28.65 o 3 4 7 2.82 5.17 18.44 o 4 4 7 751.19 719.89 64.15 o 5 4 7 114.23 124.68 26.24 o 6 4 7 22.10 43.63 20.44 o 7 4 7 42.63 20.89 20.80 o 8 4 7 738.64 706.97 34.92 o 9 4 7 9.47 -23.51 23.51 o 10 4 7 380.86 361.57 35.65 o 11 4 7 189.01 178.67 41.54 o 0 5 7 1885.54 1772.23 83.16 o 1 5 7 6.36 12.08 21.06 o 2 5 7 0.38 16.11 38.24 o 3 5 7 1159.50 1163.96 46.44 o 4 5 7 12.53 71.26 27.69 o 5 5 7 35.45 55.68 23.51 o 6 5 7 1252.60 1161.60 63.95 o 7 5 7 2.28 -15.75 29.18 o 0 0 8 289.79 264.15 37.65 o 1 0 8 128.53 142.47 26.51 o 2 0 8 1228.04 1266.49 52.68 o 3 0 8 12.78 -7.90 29.12 o 4 0 8 1034.10 1044.91 54.25 o 5 0 8 267.60 254.59 37.77 o 7 0 8 27.79 29.18 42.62 o 1 1 8 114.51 115.71 29.22 o 2 1 8 413.06 414.23 22.96 o 3 1 8 3.43 12.51 18.51 o 4 1 8 347.71 318.42 28.05 o 5 1 8 147.33 157.53 24.54 o 6 1 8 0.64 -10.27 27.36 o 7 1 8 132.30 168.26 42.87 o 8 1 8 224.42 158.79 32.96 o 0 2 8 150.31 126.97 38.92 o 1 2 8 255.35 291.32 73.12 o 2 2 8 1068.36 1040.44 71.24 o 3 2 8 117.99 81.91 37.03 o 4 2 8 717.34 733.72 61.47 o 5 2 8 178.78 158.78 32.96 o 6 2 8 224.21 298.85 46.04 o