#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2213529.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213529_Fobs loop_ _publ_author_name 'Bokach, Nadezhda A.' 'Izotova, Yulia A.' 'Haukka, Matti' _publ_section_title ; Bis(benzyltriphenylphosphonium) tetrachloridoplatinate(II) trichloromethane disolvate ; _journal_coeditor_code SA2042 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1261 _journal_page_last m1262 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 98.287 _cell_angle_beta 105.042 _cell_angle_gamma 108.979 _cell_length_a 9.8900 _cell_length_b 11.2570 _cell_length_c 13.0180 _exptl_crystal_F_000 636.00 _reflns_d_resolution_high 0.7685 _[local]_cod_data_source_file sa2042Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bn304dx in P-1 (colorless plate)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 162.48 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3070.51 3088.16 49.04 o 3 0 0 8648.66 8351.99 164.18 o 4 0 0 87.03 193.69 52.85 o 5 0 0 6788.68 6866.41 170.24 o 6 0 0 49.18 51.33 21.03 o 7 0 0 563.58 589.11 47.46 o 8 0 0 4587.33 4796.13 114.39 o 9 0 0 1915.38 1926.34 82.77 o 10 0 0 765.69 768.87 64.37 o 11 0 0 27.05 64.33 138.29 o -11 1 0 151.98 162.51 95.11 o -10 1 0 570.62 602.90 55.26 o -9 1 0 1732.18 1870.51 91.83 o -8 1 0 141.13 70.00 36.47 o -7 1 0 44.80 17.32 20.17 o -6 1 0 540.29 590.97 29.17 o -5 1 0 3349.25 3299.69 87.34 o -4 1 0 10678.92 10958.84 180.48 o -3 1 0 19831.83 19108.52 403.68 o -2 1 0 7475.77 7233.71 132.59 o 1 1 0 633.23 774.44 40.92 o 2 1 0 4462.71 4405.72 93.12 o 3 1 0 1927.94 2002.97 40.56 o 4 1 0 2571.25 2513.87 62.44 o 5 1 0 6759.99 6960.64 138.39 o 6 1 0 2675.94 2703.76 75.64 o 7 1 0 1871.42 1988.09 47.76 o 8 1 0 3492.61 3630.95 111.02 o 9 1 0 2534.44 2235.08 110.28 o 10 1 0 398.07 314.35 91.30 o 11 1 0 1041.76 1047.17 288.35 o -12 2 0 454.13 466.15 96.88 o -11 2 0 210.80 59.09 112.32 o -10 2 0 614.25 473.97 32.64 o -9 2 0 1416.43 1490.19 61.22 o -8 2 0 433.36 473.20 38.84 o -7 2 0 1397.05 1359.50 52.16 o -6 2 0 2568.44 2527.08 71.89 o -5 2 0 3771.70 3648.96 69.01 o -4 2 0 7952.21 7963.05 183.48 o -3 2 0 313.75 249.17 17.90 o -2 2 0 3561.31 3782.71 65.99 o -1 2 0 7917.93 8118.17 185.24 o 0 2 0 91.23 165.85 16.45 o 1 2 0 1336.96 1459.29 25.34 o 2 2 0 1300.70 1209.95 26.64 o 3 2 0 5124.52 5201.65 89.86 o 4 2 0 13056.13 12962.73 251.86 o 5 2 0 3495.60 3479.24 72.76 o 6 2 0 3249.17 3319.46 77.22 o 7 2 0 814.63 816.79 35.07 o 8 2 0 857.51 815.22 37.03 o 9 2 0 1424.18 1613.56 94.00 o 10 2 0 554.14 596.02 90.29 o -12 3 0 218.64 156.87 77.94 o -11 3 0 195.70 71.77 59.01 o -10 3 0 868.71 494.65 87.25 o -9 3 0 2205.48 2155.10 93.74 o -8 3 0 5899.65 6000.67 164.73 o -7 3 0 1227.83 1282.46 40.91 o -6 3 0 7276.78 7305.25 131.27 o -5 3 0 3075.13 2953.59 62.11 o 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130.39 o 6 4 0 369.86 371.81 23.10 o 7 4 0 288.72 334.01 48.00 o 8 4 0 645.48 622.31 97.56 o 9 4 0 607.72 705.11 198.45 o -12 5 0 1580.35 1718.18 170.03 o -11 5 0 534.42 410.65 71.59 o -10 5 0 1236.58 1167.39 91.58 o -9 5 0 2052.58 1999.63 82.18 o -8 5 0 47.29 58.22 26.36 o -7 5 0 1367.43 1352.65 44.67 o -6 5 0 95.64 122.46 22.11 o -5 5 0 1197.24 1143.52 46.34 o -4 5 0 15013.45 14780.07 222.93 o -3 5 0 3551.09 3657.76 65.03 o -2 5 0 8009.82 8137.06 124.58 o -1 5 0 4825.12 5139.31 96.00 o 0 5 0 2720.00 2709.34 60.96 o 1 5 0 6563.06 6671.32 126.25 o 2 5 0 931.27 901.27 32.96 o 3 5 0 2113.28 2178.85 45.76 o 4 5 0 3256.28 3435.75 97.54 o 5 5 0 797.20 756.60 40.87 o 6 5 0 1322.97 1264.77 60.77 o 7 5 0 155.64 246.08 41.32 o 8 5 0 593.09 593.62 132.82 o 9 5 0 728.78 811.69 135.12 o -12 6 0 609.64 627.14 144.77 o -11 6 0 80.44 237.58 138.57 o -10 6 0 113.91 117.10 36.17 o -9 6 0 304.93 382.25 45.38 o -8 6 0 2020.08 1988.27 74.76 o -7 6 0 706.79 685.80 37.12 o -6 6 0 2576.77 2558.24 63.21 o -5 6 0 3638.50 3563.98 75.93 o -4 6 0 8604.32 8463.34 136.84 o -3 6 0 3186.02 3107.93 63.23 o -2 6 0 431.70 457.49 21.08 o -1 6 0 5790.30 5721.70 117.13 o 0 6 0 2776.13 2760.54 82.37 o 1 6 0 1592.66 1515.92 38.01 o 2 6 0 1615.73 1596.45 40.91 o 3 6 0 159.84 165.70 30.50 o 4 6 0 2913.18 3118.25 84.49 o 5 6 0 1195.71 1379.62 99.20 o 6 6 0 397.09 350.96 49.75 o 7 6 0 870.92 779.64 80.91 o 8 6 0 848.01 799.29 80.19 o -12 7 0 169.98 191.57 116.49 o -11 7 0 139.83 215.27 92.36 o -10 7 0 285.21 132.98 68.02 o -9 7 0 2781.99 3002.54 119.26 o -8 7 0 3033.20 3103.14 103.13 o -7 7 0 2006.03 1890.31 53.37 o -6 7 0 2392.82 2393.56 70.00 o -5 7 0 1028.78 1011.39 36.63 o -4 7 0 5658.93 5840.91 89.73 o -3 7 0 1648.75 1553.33 60.03 o -2 7 0 225.24 216.38 18.12 o -1 7 0 5489.83 5544.89 112.23 o 0 7 0 1788.09 1817.27 46.96 o 1 7 0 3839.08 3862.16 82.33 o 2 7 0 2162.64 2205.02 59.65 o 3 7 0 36.64 48.67 16.46 o 4 7 0 2633.49 2756.69 78.52 o 5 7 0 2004.79 1926.17 110.25 o 6 7 0 747.78 688.60 62.86 o 7 7 0 1292.75 1209.37 254.71 o -12 8 0 502.56 543.66 98.53 o -11 8 0 544.62 418.35 100.53 o -10 8 0 1742.33 1664.78 148.58 o -9 8 0 885.43 1023.89 63.57 o -8 8 0 1712.89 1678.39 69.83 o -7 8 0 2530.26 2515.61 90.53 o -6 8 0 53.04 40.21 27.18 o -5 8 0 1728.34 1711.36 55.21 o -4 8 0 3426.81 3523.43 79.17 o -3 8 0 1225.26 1275.80 56.72 o -2 8 0 5857.45 5945.28 130.02 o -1 8 0 556.52 621.53 36.07 o 0 8 0 1571.17 1612.51 50.25 o 1 8 0 2612.55 2806.41 74.64 o 2 8 0 917.67 868.04 38.72 o 3 8 0 1459.21 1500.94 60.14 o 4 8 0 1902.91 2022.64 93.70 o 5 8 0 1842.30 1733.24 157.24 o 6 8 0 1225.37 1254.39 207.56 o -11 9 0 394.41 163.41 108.36 o -10 9 0 472.98 497.16 68.08 o -9 9 0 541.22 533.25 53.23 o -8 9 0 1382.92 1381.64 55.57 o -7 9 0 294.55 408.88 36.12 o -6 9 0 289.77 336.70 30.70 o -5 9 0 3825.49 3971.29 100.81 o -4 9 0 2532.10 2763.61 67.97 o -3 9 0 124.64 137.72 36.99 o -2 9 0 438.37 412.41 45.42 o -1 9 0 279.91 341.11 25.45 o 0 9 0 2122.27 2116.75 70.22 o 1 9 0 3628.06 3689.00 121.85 o 2 9 0 226.78 202.37 29.15 o 3 9 0 1930.69 1929.98 99.83 o 4 9 0 2392.43 2432.54 164.46 o 5 9 0 452.45 385.16 84.40 o 6 9 0 241.35 388.05 133.53 o -11 10 0 383.08 388.07 106.72 o -10 10 0 86.81 103.05 96.14 o -9 10 0 1219.12 1337.32 89.39 o -8 10 0 2112.61 1941.02 93.48 o -7 10 0 532.31 567.14 60.31 o -6 10 0 152.08 235.49 36.11 o -5 10 0 134.03 177.91 37.24 o -4 10 0 891.25 915.85 42.51 o -3 10 0 1139.11 1006.64 42.50 o -2 10 0 220.66 229.66 26.14 o -1 10 0 2137.92 2246.16 85.82 o 0 10 0 2130.99 2179.27 76.41 o 1 10 0 2513.10 2534.74 109.99 o 2 10 0 566.11 659.44 43.99 o 3 10 0 101.93 134.89 44.82 o 4 10 0 371.65 353.79 64.27 o 5 10 0 170.65 195.19 64.96 o -11 11 0 57.58 224.72 88.26 o -10 11 0 609.34 603.02 77.05 o -9 11 0 723.47 751.15 83.40 o -8 11 0 695.45 703.00 73.72 o -7 11 0 488.64 553.97 50.14 o -6 11 0 647.87 549.83 48.13 o -5 11 0 1599.70 1530.53 83.91 o -4 11 0 2219.24 2257.95 86.64 o -3 11 0 1601.10 1648.66 67.52 o -2 11 0 1973.16 2035.11 68.87 o -1 11 0 1511.20 1389.04 70.30 o 0 11 0 1198.08 1039.34 62.34 o 1 11 0 211.37 168.68 88.99 o 2 11 0 23.97 82.10 45.12 o 3 11 0 39.43 112.46 63.79 o -10 12 0 447.86 493.44 78.26 o -9 12 0 187.38 318.57 356.88 o -8 12 0 1919.27 1888.22 206.29 o -7 12 0 418.44 397.68 58.94 o -6 12 0 1357.55 1161.30 89.21 o -5 12 0 3780.03 3953.41 191.44 o -4 12 0 1899.97 1829.95 94.91 o -3 12 0 1384.81 1333.55 70.82 o -2 12 0 539.76 591.32 47.12 o -1 12 0 25.87 69.20 34.86 o 0 12 0 34.85 34.64 36.25 o 1 12 0 234.51 275.52 82.50 o 2 12 0 552.48 572.21 155.82 o -9 13 0 1080.78 955.81 124.79 o -8 13 0 943.41 1168.87 107.50 o -7 13 0 1060.24 961.50 84.99 o -6 13 0 705.59 534.84 93.65 o -5 13 0 50.56 100.51 46.85 o -4 13 0 535.59 535.95 61.94 o -3 13 0 142.15 117.76 45.00 o -2 13 0 202.51 237.13 43.96 o -1 13 0 447.68 462.97 65.16 o 0 13 0 1256.88 1167.68 123.76 o -7 14 0 210.36 167.70 55.51 o -6 14 0 26.47 6.60 96.61 o -5 14 0 61.07 -0.03 74.17 o -4 14 0 245.71 270.59 85.63 o -3 14 0 482.58 390.90 86.93 o -2 14 0 1133.70 947.85 116.72 o 2 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390.31 53.22 o -1 -11 1 557.15 486.70 65.88 o 0 -11 1 28.84 99.13 39.52 o 1 -11 1 411.74 542.78 35.54 o 2 -11 1 1859.22 1912.10 73.45 o 3 -11 1 819.85 847.37 42.93 o 4 -11 1 2856.03 2991.74 114.92 o 5 -11 1 758.68 752.03 46.64 o 6 -11 1 1125.77 1058.31 64.53 o 7 -11 1 392.92 373.20 45.51 o 8 -11 1 64.15 147.16 38.11 o 9 -11 1 606.20 511.55 163.78 o 10 -11 1 72.01 74.06 152.12 o -5 -10 1 769.66 928.27 287.71 o -4 -10 1 137.41 216.49 54.70 o -3 -10 1 167.51 216.88 45.89 o -2 -10 1 479.06 474.74 43.88 o -1 -10 1 2030.02 2033.23 81.80 o 0 -10 1 2071.12 2042.05 83.59 o 1 -10 1 2571.25 2751.40 82.60 o 2 -10 1 2933.14 3009.25 94.09 o 3 -10 1 3435.57 3770.36 100.65 o 4 -10 1 1569.76 1573.79 60.92 o 5 -10 1 293.99 347.08 34.35 o 6 -10 1 28.26 34.96 28.83 o 7 -10 1 456.20 372.97 38.92 o 8 -10 1 1425.92 1523.88 73.99 o 9 -10 1 434.54 470.75 64.93 o 10 -10 1 527.41 458.26 88.48 o 11 -10 1 726.17 578.18 117.32 o -6 -9 1 127.44 165.31 71.83 o -5 -9 1 798.73 765.42 72.75 o -4 -9 1 859.70 802.59 69.74 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63.94 54.56 51.16 o 11 -8 1 1265.99 1192.21 141.79 o -8 -7 1 415.33 465.49 69.39 o -7 -7 1 616.75 693.84 146.93 o -6 -7 1 1732.75 1855.09 127.45 o -5 -7 1 2735.33 2784.61 125.20 o -4 -7 1 699.31 731.22 35.16 o -3 -7 1 41.99 20.58 14.11 o -2 -7 1 43.02 64.06 16.69 o -1 -7 1 713.65 789.14 29.60 o 0 -7 1 941.02 963.54 35.89 o 1 -7 1 321.32 354.08 30.65 o 2 -7 1 3131.37 3207.97 61.48 o 3 -7 1 9789.10 9979.39 179.95 o 4 -7 1 4108.19 4097.91 73.41 o 5 -7 1 3844.36 4107.81 78.04 o 6 -7 1 419.91 456.21 22.48 o 7 -7 1 1562.12 1615.11 61.12 o 8 -7 1 2481.31 2333.14 97.08 o 9 -7 1 396.84 339.15 47.88 o 10 -7 1 433.15 522.84 45.90 o 11 -7 1 616.72 771.61 103.33 o 12 -7 1 773.45 729.75 151.19 o -8 -6 1 1969.17 1831.46 261.76 o -7 -6 1 446.26 511.81 67.36 o -6 -6 1 743.09 647.16 70.21 o -5 -6 1 1262.20 1121.78 53.84 o -4 -6 1 45.11 59.39 23.91 o -3 -6 1 398.95 388.80 27.08 o -2 -6 1 870.10 859.69 32.99 o -1 -6 1 3579.48 3481.43 70.14 o 0 -6 1 10781.07 10840.29 209.76 o 1 -6 1 2321.35 2458.01 48.43 o 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