#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2213532.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213532_Fobs loop_ _publ_author_name 'Mizuguchi, Jin' 'Uta, Kazuya' 'Sato, Yohei' _publ_section_title ; Ammonium bis{3-anilinocarbonyl-1-[(5-chloro-2-oxidophenyl)diazenyl]-2-naphtholato}ferrate(III) acetone solvate ; _journal_coeditor_code SA2047 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1329 _journal_page_last m1330 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.747 _cell_angle_gamma 90.000 _cell_length_a 11.3199 _cell_length_b 13.7962 _cell_length_c 27.7573 _exptl_crystal_F_000 1988.00 _reflns_d_resolution_high 0.8101 _[local]_cod_data_source_file sa2047Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' YNU' _shelx_refln_list_code 4 _shelx_f_calc_maximum 410.01 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 196.80 211.90 59.93 o 4 0 0 806.68 781.55 93.66 o 6 0 0 535.80 535.88 73.61 o 8 0 0 706.33 691.58 97.30 o 10 0 0 1497.21 1097.07 171.13 o 12 0 0 716.77 1323.88 286.39 o 2 1 0 15903.54 18757.88 1298.54 o 3 1 0 60381.29 74857.39 5751.23 o 4 1 0 16570.27 20077.22 1012.13 o 5 1 0 2436.49 4341.22 262.33 o 6 1 0 8140.52 8215.20 677.59 o 7 1 0 1189.48 1728.31 153.22 o 8 1 0 321.37 457.45 60.95 o 9 1 0 57.05 132.14 46.70 o 10 1 0 161.58 313.14 70.49 o 11 1 0 3.53 433.87 113.39 o 12 1 0 74.73 80.43 60.57 o 13 1 0 0.85 -64.22 172.62 o 1 2 0 550.99 1846.58 131.88 o 2 2 0 1335.30 1517.02 198.94 o 3 2 0 5814.97 7700.21 681.06 o 4 2 0 263.21 770.28 112.99 o 5 2 0 1009.90 2137.89 342.36 o 6 2 0 11709.06 12844.21 825.79 o 7 2 0 1474.03 3030.04 417.83 o 8 2 0 4.80 154.15 42.43 o 9 2 0 138.11 1238.20 140.85 o 10 2 0 186.64 450.59 82.60 o 11 2 0 92.72 226.81 72.72 o 12 2 0 319.01 288.01 149.56 o 13 2 0 17.33 -4.43 41.42 o 1 3 0 73920.88 84610.35 7267.93 o 2 3 0 75785.08 92710.46 9097.77 o 3 3 0 12757.17 17012.56 882.70 o 4 3 0 8393.31 9540.29 463.54 o 5 3 0 650.94 1284.10 141.26 o 6 3 0 7395.24 7072.32 564.80 o 7 3 0 41.41 157.28 45.06 o 8 3 0 1976.88 2098.43 172.14 o 9 3 0 1.66 466.62 119.55 o 10 3 0 920.43 791.75 178.80 o 11 3 0 15.92 283.43 108.34 o 12 3 0 234.96 198.34 85.27 o 13 3 0 138.59 160.20 78.19 o 0 4 0 3155.41 3476.87 287.70 o 1 4 0 28244.81 39901.13 2499.33 o 2 4 0 246.53 197.86 48.52 o 3 4 0 90.03 45.66 27.11 o 4 4 0 2805.13 3228.35 170.15 o 5 4 0 139.73 111.55 37.20 o 6 4 0 4019.23 4305.87 288.73 o 7 4 0 72.69 2494.99 513.58 o 8 4 0 772.77 842.11 148.01 o 9 4 0 469.98 1548.79 213.72 o 10 4 0 823.23 752.01 138.24 o 11 4 0 227.45 138.41 89.42 o 12 4 0 138.42 123.25 63.84 o 13 4 0 106.72 22.70 42.81 o 1 5 0 80.51 237.76 35.75 o 2 5 0 337.49 442.96 81.22 o 3 5 0 221.85 217.62 31.79 o 4 5 0 51.07 19.69 25.41 o 5 5 0 2107.20 2690.95 211.55 o 6 5 0 9197.69 10377.14 573.56 o 7 5 0 1196.67 1691.63 139.71 o 8 5 0 95.54 264.85 71.40 o 9 5 0 364.15 274.11 123.54 o 10 5 0 1064.10 1056.51 247.48 o 11 5 0 110.77 124.46 64.37 o 12 5 0 24.11 2.20 46.78 o 13 5 0 3.02 16.63 58.21 o 0 6 0 22446.21 22497.78 1551.07 o 1 6 0 14823.75 16230.45 733.42 o 2 6 0 3343.06 4186.03 192.57 o 3 6 0 57.51 42.97 26.35 o 4 6 0 832.88 819.92 69.94 o 5 6 0 2101.43 2362.47 182.72 o 6 6 0 2007.69 2482.88 211.26 o 7 6 0 214.10 601.66 184.16 o 8 6 0 128.78 278.49 116.09 o 9 6 0 179.93 420.63 145.00 o 10 6 0 409.69 323.00 92.56 o 11 6 0 662.12 601.86 145.46 o 12 6 0 62.01 -10.27 53.38 o 13 6 0 245.63 96.76 72.63 o 1 7 0 1054.77 3923.88 911.38 o 2 7 0 7505.78 8120.23 419.74 o 3 7 0 675.97 841.69 99.34 o 4 7 0 32.66 313.43 102.58 o 5 7 0 1021.60 766.09 66.40 o 6 7 0 456.46 452.39 58.04 o 7 7 0 121.47 632.84 162.78 o 8 7 0 1401.91 1394.80 321.89 o 9 7 0 933.65 891.35 244.57 o 10 7 0 817.28 692.45 191.15 o 11 7 0 528.90 431.99 174.90 o 12 7 0 293.34 308.93 107.02 o 0 8 0 10286.33 11752.43 728.70 o 1 8 0 1524.72 1643.07 114.20 o 2 8 0 291.69 305.33 31.60 o 3 8 0 2071.67 2331.39 139.04 o 4 8 0 484.77 1273.84 144.77 o 5 8 0 186.17 166.64 33.21 o 6 8 0 1034.49 1816.67 292.95 o 7 8 0 1717.90 1686.35 222.46 o 8 8 0 525.07 1049.97 202.52 o 9 8 0 517.24 622.69 116.50 o 10 8 0 105.75 60.74 54.66 o 11 8 0 18.56 59.08 54.94 o 12 8 0 53.99 -4.23 47.90 o 1 9 0 673.04 903.21 56.11 o 2 9 0 2406.20 3976.25 392.60 o 3 9 0 458.94 467.45 50.64 o 4 9 0 1593.49 1777.93 104.11 o 5 9 0 1084.17 1249.11 102.02 o 6 9 0 644.50 613.52 67.64 o 7 9 0 955.44 865.98 196.70 o 8 9 0 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