#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2213565.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213565_Fobs loop_ _publ_author_name 'Du, Zhong-Xiang' 'Han, Min-Le' 'Hou, Hong-Wei' _publ_section_title ; Bis(4-aminobenzenesulfonato-\kN)diaquabis(dimethylformamide-\kO)copper(II) ; _journal_coeditor_code SJ2280 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1354 _journal_page_last m1355 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.973 _cell_angle_gamma 90.000 _cell_length_a 7.1780 _cell_length_b 11.8969 _cell_length_c 14.6493 _exptl_crystal_F_000 614.00 _reflns_d_resolution_high 0.8255 _[local]_cod_data_source_file sj2280Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' B in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 149.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5739.16 6050.68 61.32 o 4 0 0 2258.09 2235.25 23.84 o 6 0 0 2975.19 2986.08 40.02 o 8 0 0 817.22 822.94 20.67 o 1 1 0 10616.94 10834.27 167.11 o 2 1 0 4595.07 5124.89 49.19 o 3 1 0 20.21 8.35 0.88 o 4 1 0 361.15 377.20 4.17 o 5 1 0 2909.97 2918.74 24.23 o 6 1 0 151.12 140.79 3.29 o 7 1 0 122.73 120.54 3.04 o 8 1 0 2.03 0.39 1.47 o 0 2 0 3256.65 2628.27 68.37 o 1 2 0 515.13 525.65 5.14 o 2 2 0 6908.32 7362.35 85.24 o 3 2 0 471.99 543.56 5.81 o 4 2 0 8.93 4.30 1.00 o 5 2 0 1.22 -1.00 0.67 o 6 2 0 11.67 11.65 1.62 o 7 2 0 5.01 3.29 1.38 o 8 2 0 4.31 3.47 1.54 o 1 3 0 40.20 42.04 0.80 o 2 3 0 12.06 9.57 1.11 o 3 3 0 1180.68 1226.60 11.86 o 4 3 0 0.16 -0.62 0.57 o 5 3 0 298.21 312.04 3.93 o 6 3 0 2.23 -0.26 0.92 o 7 3 0 26.26 25.26 2.01 o 8 3 0 5.92 2.42 2.10 o 0 4 0 16080.48 11784.30 278.38 o 1 4 0 4.96 3.39 0.37 o 2 4 0 814.02 688.89 7.12 o 3 4 0 242.44 282.37 3.89 o 4 4 0 1880.83 1864.18 15.91 o 5 4 0 53.40 53.06 1.90 o 6 4 0 588.52 609.88 8.26 o 7 4 0 3.89 6.93 1.54 o 8 4 0 625.83 613.86 10.05 o 1 5 0 13077.22 11362.54 138.64 o 2 5 0 6.40 3.22 0.48 o 3 5 0 1932.25 1852.83 17.67 o 4 5 0 144.37 159.17 2.95 o 5 5 0 2281.84 2271.24 22.00 o 6 5 0 17.32 17.43 1.42 o 7 5 0 686.97 682.22 11.04 o 8 5 0 2.22 1.54 1.60 o 0 6 0 18292.11 15089.47 378.23 o 1 6 0 346.23 381.79 3.54 o 2 6 0 901.40 915.70 8.28 o 3 6 0 182.12 203.71 4.26 o 4 6 0 633.32 586.14 7.11 o 5 6 0 2.30 4.84 1.04 o 6 6 0 468.32 473.35 8.51 o 7 6 0 95.65 91.98 2.97 o 1 7 0 264.94 289.03 3.42 o 2 7 0 295.15 342.40 3.91 o 3 7 0 129.14 121.86 2.58 o 4 7 0 2.16 3.50 1.66 o 5 7 0 3.20 3.78 2.14 o 6 7 0 77.77 72.06 3.40 o 7 7 0 31.07 31.92 2.05 o 0 8 0 41.85 57.01 1.79 o 1 8 0 36.30 32.55 1.46 o 2 8 0 33.03 27.03 1.11 o 3 8 0 15.18 17.33 2.46 o 4 8 0 86.01 82.66 2.47 o 5 8 0 120.66 113.27 3.71 o 6 8 0 57.87 56.99 2.35 o 7 8 0 41.55 41.48 2.33 o 1 9 0 2117.30 2025.07 21.36 o 2 9 0 0.85 0.64 0.79 o 3 9 0 2919.00 2857.54 27.16 o 4 9 0 123.46 129.43 3.60 o 5 9 0 581.85 577.51 7.83 o 6 9 0 4.79 5.51 1.41 o 0 10 0 734.48 798.28 12.69 o 1 10 0 5.38 2.35 0.91 o 2 10 0 1213.08 1208.68 15.42 o 3 10 0 19.22 15.58 1.39 o 4 10 0 1089.51 1064.39 12.14 o 5 10 0 212.61 202.60 4.25 o 6 10 0 623.49 649.28 9.03 o 1 11 0 109.60 118.54 3.34 o 2 11 0 4.93 3.00 1.32 o 3 11 0 2.53 1.38 1.18 o 4 11 0 13.15 13.84 1.55 o 5 11 0 50.39 54.82 2.72 o 0 12 0 18.77 17.95 2.05 o 1 12 0 5.40 4.29 1.37 o 2 12 0 14.79 10.94 2.09 o 3 12 0 46.99 40.23 3.50 o 4 12 0 10.43 10.17 1.55 o 1 13 0 96.13 84.45 3.17 o 2 13 0 0.77 0.85 2.01 o 3 13 0 3.47 1.26 1.46 o 0 14 0 256.90 258.47 10.03 o 1 14 0 2.31 0.40 1.46 o 2 14 0 498.21 521.15 9.76 o -7 0 1 32.26 37.73 3.56 o -5 0 1 377.41 368.31 6.94 o -3 0 1 1015.36 1118.89 12.34 o -1 0 1 211.39 265.96 3.96 o 1 0 1 42.39 58.13 2.01 o 3 0 1 1140.81 1273.76 13.92 o 5 0 1 118.55 119.33 3.63 o 7 0 1 18.19 16.32 2.82 o -8 1 1 74.43 85.06 3.34 o -7 1 1 33.02 26.76 1.69 o -6 1 1 1328.33 1335.70 13.93 o -5 1 1 1.41 -1.15 1.11 o -4 1 1 3906.33 4056.15 29.68 o -3 1 1 398.09 470.28 4.07 o -2 1 1 7689.06 8492.91 76.01 o -1 1 1 2967.17 3182.58 32.15 o 1 1 1 1608.40 1736.51 15.42 o 2 1 1 10141.31 10836.48 84.63 o 3 1 1 399.79 426.44 3.79 o 4 1 1 3995.65 4095.82 34.42 o 5 1 1 24.76 24.00 1.22 o 6 1 1 70.41 66.88 2.39 o 7 1 1 8.63 4.46 1.18 o 8 1 1 211.45 207.78 5.12 o -8 2 1 19.76 18.61 1.94 o -7 2 1 349.55 347.95 6.41 o -6 2 1 0.01 0.63 0.89 o -5 2 1 4608.97 4837.68 39.10 o -4 2 1 1239.36 1327.05 11.59 o -3 2 1 1120.94 983.05 8.62 o -2 2 1 0.76 -0.09 0.32 o -1 2 1 21605.36 18815.54 279.97 o 0 2 1 5409.68 4874.45 78.78 o 1 2 1 6911.95 6836.19 59.46 o 2 2 1 36.46 30.80 1.17 o 3 2 1 1050.93 894.99 8.04 o 4 2 1 1.08 0.61 0.70 o 5 2 1 3276.36 3353.56 27.69 o 6 2 1 22.79 22.27 1.40 o 7 2 1 736.98 772.45 11.07 o 8 2 1 28.96 24.13 2.20 o -8 3 1 27.72 28.71 2.44 o -7 3 1 6.47 7.66 1.47 o -6 3 1 1341.41 1366.12 14.22 o -5 3 1 21.29 23.30 1.48 o -4 3 1 3020.55 3031.39 24.86 o -3 3 1 250.81 272.09 3.18 o -2 3 1 454.32 589.78 7.09 o -1 3 1 46.49 42.33 0.82 o 0 3 1 14010.04 10794.18 189.55 o 1 3 1 113.03 105.53 1.20 o 2 3 1 19.15 46.90 0.95 o 3 3 1 14.83 18.22 1.16 o 4 3 1 787.17 692.91 6.75 o 5 3 1 41.25 44.60 1.52 o 6 3 1 418.69 407.74 5.74 o 7 3 1 55.83 58.46 2.73 o 8 3 1 216.12 224.24 5.46 o -8 4 1 4.40 1.38 1.53 o -7 4 1 67.63 63.54 2.82 o -6 4 1 19.36 19.24 1.42 o -5 4 1 1008.87 981.97 10.63 o -4 4 1 190.61 188.23 2.94 o -3 4 1 167.67 197.09 3.15 o -2 4 1 63.48 61.64 1.67 o -1 4 1 3840.08 3768.18 29.82 o 0 4 1 119.56 101.07 1.32 o 1 4 1 3193.64 3151.17 25.07 o 2 4 1 443.54 504.24 6.43 o 3 4 1 615.10 611.03 5.87 o 4 4 1 24.32 31.35 1.12 o 5 4 1 680.07 641.00 8.04 o 6 4 1 142.63 134.81 3.18 o 7 4 1 1.86 1.23 1.33 o 8 4 1 66.70 65.28 3.20 o -8 5 1 22.62 20.39 2.16 o -7 5 1 72.41 71.66 3.10 o -6 5 1 178.95 186.46 3.70 o -5 5 1 1.12 -0.77 1.88 o -4 5 1 929.22 909.69 9.82 o -3 5 1 48.00 51.89 1.57 o -2 5 1 209.71 266.29 3.01 o -1 5 1 124.73 111.94 1.68 o 0 5 1 833.49 805.95 6.46 o 1 5 1 576.55 568.10 4.81 o 2 5 1 2616.07 2784.83 22.56 o 3 5 1 162.25 165.60 3.94 o 4 5 1 928.94 912.96 9.87 o 5 5 1 26.11 24.42 1.48 o 6 5 1 18.78 18.88 1.45 o 7 5 1 32.85 31.98 2.26 o -7 6 1 72.11 78.81 3.28 o -6 6 1 82.72 80.11 3.05 o -5 6 1 400.91 407.79 5.76 o -4 6 1 7.06 11.39 1.13 o -3 6 1 1031.02 937.49 9.89 o -2 6 1 146.73 155.85 2.21 o -1 6 1 406.93 340.70 3.24 o 0 6 1 897.32 1019.75 8.11 o 1 6 1 15.46 7.17 0.82 o 2 6 1 23.48 34.27 1.06 o 3 6 1 1656.81 1679.62 16.37 o 4 6 1 36.53 32.25 1.52 o 5 6 1 234.46 245.47 4.24 o 6 6 1 110.75 116.22 3.07 o 7 6 1 163.27 185.44 4.23 o -7 7 1 6.63 9.70 1.51 o -6 7 1 597.41 629.87 8.29 o -5 7 1 27.45 20.92 1.46 o -4 7 1 1955.25 1949.21 19.20 o -3 7 1 251.32 261.66 3.98 o -2 7 1 1847.68 1698.20 14.54 o -1 7 1 154.36 190.73 2.60 o 0 7 1 1858.85 1754.15 13.47 o 1 7 1 199.29 232.86 3.60 o 2 7 1 3418.19 3309.36 26.97 o 3 7 1 84.09 77.76 2.77 o 4 7 1 2604.94 2557.62 24.50 o 5 7 1 0.00 0.60 0.96 o 6 7 1 541.69 554.17 7.64 o 7 7 1 48.51 47.24 2.31 o -7 8 1 170.27 166.57 4.12 o -6 8 1 0.48 1.12 1.17 o -5 8 1 516.99 501.10 6.94 o -4 8 1 258.22 259.97 4.36 o -3 8 1 654.53 671.92 7.95 o -2 8 1 138.58 132.35 2.25 o -1 8 1 2186.37 2215.29 18.60 o 0 8 1 97.76 121.80 2.69 o 1 8 1 1054.85 1041.05 9.52 o 2 8 1 38.71 35.94 1.99 o 3 8 1 680.09 674.60 10.14 o 4 8 1 7.70 6.88 1.12 o 5 8 1 560.12 552.14 7.48 o 6 8 1 21.82 22.52 1.74 o -6 9 1 1.22 1.76 1.17 o -5 9 1 0.54 0.17 1.10 o -4 9 1 2.21 2.35 1.04 o -3 9 1 8.82 9.11 1.47 o -2 9 1 15.40 18.18 2.08 o -1 9 1 9.48 12.20 1.03 o 0 9 1 189.07 197.03 3.43 o 1 9 1 9.33 11.64 0.92 o 2 9 1 20.12 15.98 1.95 o 3 9 1 92.76 85.70 4.21 o 4 9 1 13.64 12.24 1.34 o 5 9 1 4.51 5.57 1.29 o 6 9 1 2.95 3.78 1.58 o -6 10 1 6.70 5.53 1.51 o -5 10 1 134.05 127.75 3.37 o -4 10 1 24.32 23.34 1.70 o -3 10 1 54.08 52.08 2.08 o -2 10 1 41.11 38.94 2.30 o -1 10 1 177.79 166.58 3.62 o 0 10 1 107.31 103.10 2.52 o 1 10 1 410.79 383.14 5.26 o 2 10 1 103.40 92.81 2.54 o 3 10 1 92.82 100.81 3.23 o 4 10 1 1.39 -0.02 1.12 o 5 10 1 5.65 5.78 1.91 o 6 10 1 1.39 1.33 2.00 o -5 11 1 17.66 11.95 1.57 o -4 11 1 900.07 877.04 10.68 o -3 11 1 12.71 13.29 1.43 o -2 11 1 1242.47 1154.59 14.55 o -1 11 1 5.75 2.98 0.99 o 0 11 1 724.08 667.49 8.05 o 1 11 1 1.80 3.60 1.22 o 2 11 1 793.77 777.28 10.76 o 3 11 1 27.80 23.68 2.01 o 4 11 1 68.28 68.27 2.65 o 5 11 1 17.80 18.79 1.77 o -4 12 1 5.97 5.91 1.37 o -3 12 1 603.16 617.68 9.58 o -2 12 1 27.49 27.51 2.02 o -1 12 1 161.40 170.19 4.19 o 0 12 1 87.37 74.26 2.42 o 1 12 1 562.16 527.19 8.26 o 2 12 1 21.42 18.27 1.84 o 3 12 1 566.04 576.47 9.66 o 4 12 1 7.91 8.85 1.52 o -3 13 1 12.74 11.98 1.82 o -2 13 1 77.82 83.71 3.35 o -1 13 1 0.01 -1.54 1.20 o 0 13 1 60.58 66.75 2.47 o 1 13 1 54.80 45.40 2.50 o 2 13 1 365.04 380.21 7.05 o 3 13 1 12.67 13.98 1.89 o -2 14 1 4.75 3.96 1.62 o -1 14 1 10.69 8.87 1.80 o 0 14 1 0.01 -2.43 1.62 o 1 14 1 34.54 30.82 2.35 o -8 0 2 178.90 198.27 8.46 o -6 0 2 4291.69 4399.09 66.70 o -4 0 2 18473.85 19872.76 448.47 o -2 0 2 15598.41 16112.44 429.60 o 0 0 2 5940.84 7100.52 129.02 o 2 0 2 4647.16 4634.95 47.20 o 4 0 2 7824.21 7861.37 89.17 o 6 0 2 3169.14 3222.41 43.10 o 8 0 2 1026.44 964.56 23.40 o -8 1 2 1.76 2.72 1.46 o -7 1 2 198.81 220.23 4.37 o -6 1 2 104.64 93.87 2.53 o -5 1 2 3589.04 3736.17 30.53 o -4 1 2 1514.70 1524.86 11.83 o -3 1 2 826.93 729.60 5.95 o -2 1 2 12622.18 13364.62 117.01 o -1 1 2 5280.78 5353.61 88.29 o 0 1 2 2373.21 2552.26 47.22 o 1 1 2 6614.50 6765.38 63.07 o 2 1 2 572.30 634.20 5.11 o 3 1 2 994.38 916.07 7.35 o 4 1 2 751.70 790.07 9.02 o 5 1 2 470.03 436.61 4.94 o 6 1 2 0.91 0.14 0.92 o 7 1 2 414.00 408.22 6.12 o 8 1 2 94.35 104.52 3.80 o -8 2 2 55.89 49.20 3.70 o -7 2 2 7.77 8.86 2.25 o -6 2 2 372.30 373.22 6.03 o -5 2 2 30.92 31.68 1.73 o -4 2 2 212.65 202.60 2.32 o -3 2 2 140.77 177.91 3.44 o -2 2 2 1457.57 1453.22 10.85 o -1 2 2 589.48 580.46 5.01 o 0 2 2 4634.71 4851.68 107.99 o 1 2 2 26.44 7.98 0.48 o 2 2 2 384.10 393.19 4.29 o 3 2 2 1290.03 1362.98 13.09 o 4 2 2 268.83 288.00 3.49 o 5 2 2 109.49 109.05 2.16 o 6 2 2 67.46 58.07 2.03 o 7 2 2 42.74 38.37 2.32 o 8 2 2 3.89 3.48 1.55 o -8 3 2 2.54 0.67 1.44 o -7 3 2 1.99 1.89 1.27 o -6 3 2 231.46 222.73 3.91 o -5 3 2 62.40 53.40 1.53 o -4 3 2 528.34 565.26 5.68 o -3 3 2 693.65 687.38 5.78 o -2 3 2 6.93 11.15 0.47 o -1 3 2 86.92 100.93 1.28 o 0 3 2 2445.03 2404.24 19.23 o 1 3 2 218.91 225.55 2.39 o 2 3 2 102.03 100.95 1.50 o 3 3 2 2250.04 2190.06 18.15 o 4 3 2 47.97 53.47 1.43 o 5 3 2 230.88 217.62 3.19 o 6 3 2 218.19 226.27 4.80 o 7 3 2 42.54 45.61 2.44 o 8 3 2 27.62 31.10 2.43 o -8 4 2 151.98 163.58 4.68 o -7 4 2 1.44 0.14 1.31 o -6 4 2 292.42 304.84 6.89 o -5 4 2 597.80 620.22 7.42 o -4 4 2 3076.02 3095.64 25.96 o -3 4 2 0.42 -0.25 0.36 o -2 4 2 6513.53 6263.29 45.48 o -1 4 2 246.58 256.95 2.26 o 0 4 2 800.14 667.16 5.49 o 1 4 2 42.07 42.24 1.27 o 2 4 2 2864.16 2870.10 23.22 o 3 4 2 126.44 122.34 1.90 o 4 4 2 3152.90 3296.97 27.09 o 5 4 2 689.04 685.46 8.08 o 6 4 2 575.51 595.29 7.65 o 7 4 2 31.84 27.38 2.13 o -8 5 2 130.79 137.43 8.60 o -7 5 2 739.49 766.95 10.94 o -6 5 2 103.49 95.85 2.68 o -5 5 2 4065.14 4096.21 37.68 o -4 5 2 42.47 46.59 2.24 o -3 5 2 2170.15 2065.21 22.62 o -2 5 2 109.04 120.26 1.81 o -1 5 2 6791.47 6281.38 41.46 o 0 5 2 1205.34 1346.75 9.48 o 1 5 2 6119.57 5684.21 40.83 o 2 5 2 24.27 29.36 0.69 o 3 5 2 2597.59 2535.32 23.60 o 4 5 2 30.94 32.19 1.43 o 5 5 2 2316.68 2296.43 22.30 o 6 5 2 20.74 21.05 1.54 o 7 5 2 660.44 668.36 10.31 o -7 6 2 24.08 25.45 1.83 o -6 6 2 800.32 794.44 9.61 o -5 6 2 7.41 8.73 1.13 o -4 6 2 1779.53 1716.74 16.96 o -3 6 2 1847.97 1914.23 21.34 o -2 6 2 1414.92 1447.85 12.44 o -1 6 2 585.55 543.70 4.75 o 0 6 2 3224.02 2899.71 31.68 o 1 6 2 365.95 337.15 3.41 o 2 6 2 833.42 777.86 7.28 o 3 6 2 505.83 469.27 5.82 o 4 6 2 960.59 919.45 10.12 o 5 6 2 105.11 99.95 2.68 o 6 6 2 479.78 471.31 6.76 o 7 6 2 312.98 290.24 6.21 o -7 7 2 14.66 13.29 1.58 o -6 7 2 0.08 0.79 1.11 o -5 7 2 3.10 2.83 1.03 o -4 7 2 26.32 24.50 1.44 o -3 7 2 187.95 189.92 3.28 o -2 7 2 1201.94 1323.62 11.64 o -1 7 2 226.93 236.26 3.00 o 0 7 2 15.25 12.73 0.66 o 1 7 2 2.66 3.06 0.57 o 2 7 2 290.61 288.11 3.52 o 3 7 2 293.29 283.70 4.40 o 4 7 2 190.61 185.07 3.53 o 5 7 2 17.79 20.29 1.51 o 6 7 2 8.62 10.78 1.51 o 7 7 2 77.64 79.21 3.00 o -7 8 2 15.57 17.25 1.76 o -6 8 2 5.96 5.68 1.31 o -5 8 2 366.44 362.70 5.62 o -4 8 2 53.00 43.55 1.83 o -3 8 2 301.61 288.12 5.30 o -2 8 2 247.88 246.38 3.30 o -1 8 2 278.15 269.69 3.43 o 0 8 2 104.96 123.69 1.86 o 1 8 2 81.63 79.44 1.74 o 2 8 2 2.95 4.91 1.49 o 3 8 2 9.61 11.80 1.17 o 4 8 2 98.78 105.61 4.17 o 5 8 2 779.45 763.87 9.45 o 6 8 2 39.76 48.11 2.33 o -6 9 2 96.23 89.83 2.97 o -5 9 2 598.76 577.63 7.80 o -4 9 2 123.86 119.39 3.24 o -3 9 2 2248.30 2176.58 21.26 o -2 9 2 30.40 24.49 1.38 o -1 9 2 1474.93 1453.95 12.94 o 0 9 2 60.28 70.40 1.97 o 1 9 2 1123.74 1072.28 9.99 o 2 9 2 104.18 103.14 2.54 o 3 9 2 2707.23 2658.15 25.54 o 4 9 2 324.89 320.54 6.23 o 5 9 2 1218.15 1196.28 13.52 o 6 9 2 24.84 25.75 1.94 o -6 10 2 197.44 197.72 4.46 o -5 10 2 21.09 17.57 1.62 o -4 10 2 633.87 626.46 8.16 o -3 10 2 157.52 153.84 3.72 o -2 10 2 1214.75 1217.33 12.90 o -1 10 2 124.33 116.12 2.63 o 0 10 2 1139.49 1060.55 11.30 o 1 10 2 381.90 352.76 5.04 o 2 10 2 2564.60 2533.72 24.38 o 3 10 2 1.49 2.71 1.05 o 4 10 2 970.85 969.41 11.37 o 5 10 2 61.48 61.02 3.63 o -5 11 2 39.21 41.65 2.23 o -4 11 2 51.64 47.90 2.20 o -3 11 2 50.21 48.64 2.09 o -2 11 2 15.03 15.65 1.88 o -1 11 2 17.54 21.04 1.55 o 0 11 2 25.46 26.61 1.82 o 1 11 2 318.49 299.18 5.73 o 2 11 2 98.15 93.29 4.03 o 3 11 2 245.36 236.28 4.44 o 4 11 2 0.23 -0.94 1.16 o 5 11 2 16.54 23.02 2.13 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