#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:29:44 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181056 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/36/2213608.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213608_Fobs loop_ _publ_author_name 'Yan, Guo-Bing' 'Ng, Seik Weng' _publ_section_title ; catena-Poly[bis[silver(I)-\m-1,2-di-4-pyridylethane-\k^2^N:N'] fumarate nonahydrate] ; _journal_coeditor_code XU2221 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1368 _journal_page_last m1369 _journal_volume 63 _journal_year 2007 _space_group_IT_number 70 _symmetry_space_group_name_Hall '-F 2uv 2vw' _symmetry_space_group_name_H-M 'F d d d :2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.5567 _cell_length_b 15.2839 _cell_length_c 33.4135 _exptl_crystal_F_000 3504.00 _reflns_d_resolution_high 0.7699 _cod_data_source_file xu2221Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Fddd' _shelx_refln_list_code 4 _shelx_f_calc_maximum 1461.59 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+3/4, -y+3/4, z' '-x+3/4, y, -z+3/4' 'x, -y+3/4, -z+3/4' 'x, y+1/2, z+1/2' '-x+3/4, -y+5/4, z+1/2' '-x+3/4, y+1/2, -z+5/4' 'x, -y+5/4, -z+5/4' 'x+1/2, y, z+1/2' '-x+5/4, -y+3/4, z+1/2' '-x+5/4, y, -z+5/4' 'x+1/2, -y+3/4, -z+5/4' 'x+1/2, y+1/2, z' '-x+5/4, -y+5/4, z' '-x+5/4, y+1/2, -z+3/4' 'x+1/2, -y+5/4, -z+3/4' '-x, -y, -z' 'x-3/4, y-3/4, -z' 'x-3/4, -y, z-3/4' '-x, y-3/4, z-3/4' '-x, -y+1/2, -z+1/2' 'x-3/4, y-1/4, -z+1/2' 'x-3/4, -y+1/2, z-1/4' '-x, y-1/4, z-1/4' '-x+1/2, -y, -z+1/2' 'x-1/4, y-3/4, -z+1/2' 'x-1/4, -y, z-1/4' '-x+1/2, y-3/4, z-1/4' '-x+1/2, -y+1/2, -z' 'x-1/4, y-1/4, -z' 'x-1/4, -y+1/2, z-3/4' '-x+1/2, y-1/4, z-3/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 947198.75 1049053.63 12602.56 o 8 0 0 134681.36 137967.13 1332.01 o 12 0 0 51519.58 53736.50 1591.61 o 16 0 0 25770.55 26711.99 1348.40 o 2 2 0 24229.12 23558.40 228.07 o 6 2 0 64823.79 67500.04 507.90 o 10 2 0 2778.45 2910.85 251.42 o 14 2 0 11.97 183.00 186.39 o 0 4 0 1646106.75 1486109.75 15721.21 o 4 4 0 292116.31 297682.09 1729.85 o 8 4 0 85121.91 79843.48 654.20 o 12 4 0 53144.10 48586.84 1346.99 o 16 4 0 24395.94 28126.32 1487.38 o 2 6 0 37945.22 39479.93 525.80 o 6 6 0 422.79 398.08 69.46 o 10 6 0 356.57 640.56 228.76 o 14 6 0 1522.28 1291.60 239.82 o 0 8 0 340800.75 332741.63 4239.21 o 4 8 0 153028.92 146271.38 1165.91 o 8 8 0 100835.30 97963.38 1135.09 o 12 8 0 34228.77 32830.61 937.57 o 16 8 0 10008.42 11004.38 817.02 o 2 10 0 320.30 263.00 271.12 o 6 10 0 1242.74 942.30 116.46 o 10 10 0 1271.69 1889.45 408.39 o 14 10 0 21.73 225.90 164.24 o 0 12 0 13992.30 14218.73 774.95 o 4 12 0 28757.54 31239.32 678.45 o 8 12 0 17643.18 20435.41 1088.69 o 12 12 0 15845.47 16315.68 1152.08 o 2 14 0 841.58 914.25 211.82 o 6 14 0 203.91 100.27 103.90 o 10 14 0 591.48 1096.35 381.27 o 0 16 0 4732.88 5345.42 637.25 o 4 16 0 8208.96 8202.40 535.70 o 8 16 0 3446.83 2819.26 304.52 o 2 18 0 85.93 -122.29 120.08 o 6 18 0 85.66 -75.50 157.59 o 1 1 1 90873.16 93620.51 451.04 o 3 1 1 33217.88 34944.40 204.96 o 5 1 1 133857.58 140216.48 589.81 o 7 1 1 47077.80 40019.79 271.16 o 9 1 1 69881.21 65012.66 477.53 o 11 1 1 22901.77 22783.63 345.00 o 13 1 1 20813.16 19376.80 664.64 o 15 1 1 10352.78 10132.94 399.39 o 17 1 1 6917.54 6232.97 378.91 o 1 3 1 33833.69 33625.14 220.97 o 3 3 1 138037.58 134982.81 612.14 o 5 3 1 104777.26 98867.55 662.42 o 7 3 1 77486.48 79913.24 431.99 o 9 3 1 22563.00 23628.16 265.63 o 11 3 1 37787.08 36787.65 597.91 o 13 3 1 27390.26 25338.71 532.42 o 15 3 1 8590.76 9034.58 847.52 o 17 3 1 2649.99 1736.13 259.29 o 1 5 1 361108.38 360525.91 1694.79 o 3 5 1 104225.14 100771.82 548.73 o 5 5 1 109948.12 110415.95 602.06 o 7 5 1 27598.99 27435.96 270.77 o 9 5 1 27814.85 27251.78 305.79 o 11 5 1 23999.73 23787.99 509.31 o 13 5 1 13146.48 13896.33 536.12 o 15 5 1 4675.58 4756.08 359.63 o 1 7 1 44107.44 40763.12 441.10 o 3 7 1 52215.28 51897.36 403.03 o 5 7 1 49880.63 49720.44 402.43 o 7 7 1 39699.05 40997.79 373.92 o 9 7 1 15748.11 17290.72 306.92 o 11 7 1 7303.59 7460.65 301.10 o 13 7 1 13664.07 12875.18 417.11 o 15 7 1 6389.97 5776.13 329.44 o 1 9 1 101356.23 93779.61 918.16 o 3 9 1 30726.00 30541.74 365.96 o 5 9 1 5176.74 4925.59 231.92 o 7 9 1 15794.34 15975.46 275.35 o 9 9 1 7681.33 7456.23 244.02 o 11 9 1 5822.94 5497.70 292.58 o 13 9 1 4236.81 4115.87 372.06 o 15 9 1 2556.41 2686.02 328.25 o 1 11 1 5251.09 5077.09 237.30 o 3 11 1 12881.37 11583.15 297.46 o 5 11 1 15056.12 16086.65 286.14 o 7 11 1 15476.82 14612.25 323.25 o 9 11 1 2720.36 2706.95 185.26 o 11 11 1 4792.40 4884.19 339.05 o 13 11 1 3492.58 3020.67 271.91 o 1 13 1 21991.95 22653.95 505.61 o 3 13 1 13922.79 13229.09 500.49 o 5 13 1 4699.68 5033.11 221.68 o 7 13 1 5197.85 5479.47 236.17 o 9 13 1 2800.11 2847.54 238.04 o 11 13 1 2275.99 2423.66 290.27 o 13 13 1 1032.26 707.38 267.11 o 1 15 1 4630.13 4875.30 296.53 o 3 15 1 891.54 1009.20 156.97 o 5 15 1 4591.85 5508.77 308.61 o 7 15 1 2595.55 2738.49 199.33 o 9 15 1 1371.15 2001.45 268.31 o 11 15 1 436.44 50.60 198.45 o 1 17 1 2001.39 1761.83 273.46 o 3 17 1 662.53 821.12 161.64 o 5 17 1 219.59 42.26 102.53 o 7 17 1 1413.68 1347.11 197.48 o 9 17 1 506.27 182.50 133.85 o 1 19 1 173.21 214.44 125.30 o 3 19 1 405.58 3.37 205.20 o 5 19 1 474.05 348.23 268.58 o 2 0 2 101.12 -47.02 31.35 o 6 0 2 27063.66 31344.23 313.55 o 10 0 2 0.50 86.81 62.61 o 14 0 2 9.80 -108.14 72.09 o 0 2 2 11714.11 15931.59 265.04 o 2 2 2 140620.44 145313.72 644.36 o 4 2 2 25913.38 23336.16 172.77 o 6 2 2 747817.00 834731.38 2724.86 o 8 2 2 211.75 187.87 29.96 o 10 2 2 152874.33 156021.66 1024.04 o 12 2 2 162.88 93.67 58.72 o 14 2 2 63633.10 62443.30 935.91 o 16 2 2 17.76 -104.18 69.45 o 2 4 2 47117.22 50093.49 317.11 o 4 4 2 1562.14 1392.43 56.78 o 6 4 2 8233.45 8008.28 124.73 o 8 4 2 8478.70 8781.08 136.38 o 10 4 2 1766.61 1873.32 133.97 o 12 4 2 3876.56 3751.88 227.50 o 14 4 2 88.23 40.61 73.65 o 16 4 2 430.25 259.54 196.11 o 0 6 2 35829.45 37100.53 506.66 o 2 6 2 116529.10 106973.38 651.92 o 4 6 2 13746.55 14091.02 186.05 o 6 6 2 250660.28 252406.25 1163.07 o 8 6 2 1432.81 1402.81 82.88 o 10 6 2 76333.80 76711.92 932.20 o 12 6 2 0.30 24.97 66.04 o 14 6 2 40589.76 40078.96 761.83 o 16 6 2 94.97 175.09 133.56 o 2 8 2 6195.54 7071.81 162.01 o 4 8 2 1988.84 2346.67 97.60 o 6 8 2 874.42 706.93 65.36 o 8 8 2 3514.39 3816.99 144.15 o 10 8 2 48.99 -29.76 72.93 o 12 8 2 2519.71 2791.70 231.64 o 14 8 2 582.79 362.37 112.37 o 16 8 2 468.09 -154.20 203.34 o 0 10 2 768.74 992.77 162.36 o 2 10 2 63403.24 62833.73 764.87 o 4 10 2 0.04 8.50 40.87 o 6 10 2 54995.10 56564.28 556.84 o 8 10 2 1459.24 1449.29 125.89 o 10 10 2 26873.13 27533.05 581.70 o 12 10 2 73.54 8.95 85.33 o 14 10 2 15572.63 16128.89 523.62 o 2 12 2 51.95 16.86 55.70 o 4 12 2 1027.13 987.93 98.93 o 6 12 2 94.30 142.03 65.50 o 8 12 2 100.30 128.82 70.83 o 10 12 2 162.13 192.57 94.50 o 12 12 2 315.62 625.82 152.13 o 14 12 2 19.96 89.98 164.45 o 0 14 2 319.55 516.66 164.81 o 2 14 2 14448.86 14129.29 419.49 o 4 14 2 213.11 54.04 75.55 o 6 14 2 9766.11 10042.64 305.02 o 8 14 2 34.44 157.60 80.70 o 10 14 2 8016.32 9466.46 629.06 o 12 14 2 63.61 61.54 149.64 o 2 16 2 25.64 57.20 88.40 o 4 16 2 109.70 113.73 94.87 o 6 16 2 32.78 -63.19 91.35 o 8 16 2 165.48 137.19 96.43 o 10 16 2 66.22 -40.60 212.47 o 0 18 2 110.84 159.30 221.98 o 2 18 2 2655.33 2551.61 282.51 o 4 18 2 90.09 219.41 115.91 o 6 18 2 1688.43 1863.39 236.36 o 1 1 3 120591.62 127715.83 557.22 o 3 1 3 105653.15 113504.67 535.67 o 5 1 3 58761.78 52397.57 299.49 o 7 1 3 12435.70 14095.30 144.99 o 9 1 3 28841.00 31503.09 318.64 o 11 1 3 14381.74 13857.37 303.03 o 13 1 3 41061.12 38986.62 691.62 o 15 1 3 4982.30 4698.50 307.32 o 17 1 3 5036.80 4232.75 556.76 o 1 3 3 3521.78 3672.20 124.48 o 3 3 3 21169.26 22025.35 186.96 o 5 3 3 126489.16 135584.36 613.79 o 7 3 3 56397.03 52948.52 345.78 o 9 3 3 49368.32 49252.26 406.04 o 11 3 3 18102.85 18458.63 524.33 o 13 3 3 25040.84 23014.25 888.35 o 15 3 3 8265.41 8033.91 367.72 o 17 3 3 6206.98 5002.51 1283.00 o 1 5 3 112592.27 97509.88 577.00 o 3 5 3 23736.24 20777.42 207.91 o 5 5 3 17629.39 16185.82 190.47 o 7 5 3 10724.94 9791.43 155.48 o 9 5 3 36720.19 36217.00 427.44 o 11 5 3 3040.27 3649.41 221.21 o 13 5 3 19138.60 18622.78 480.16 o 15 5 3 4009.32 4155.76 344.65 o 1 7 3 748.74 513.77 63.74 o 3 7 3 10097.36 10173.02 185.69 o 5 7 3 86655.59 89404.00 628.85 o 7 7 3 60494.62 60078.01 513.73 o 9 7 3 16749.62 17226.79 309.31 o 11 7 3 30935.91 30876.60 603.89 o 13 7 3 12473.11 10812.18 443.89 o 15 7 3 5247.26 4912.50 312.84 o 1 9 3 48029.08 50089.05 562.49 o 3 9 3 5191.53 4738.31 160.39 o 5 9 3 34395.65 33821.91 380.44 o 7 9 3 8147.40 7837.88 195.49 o 9 9 3 18704.78 19263.71 398.76 o 11 9 3 6862.88 7504.47 396.11 o 13 9 3 4685.87 4837.62 494.09 o 15 9 3 1526.20 1072.14 169.75 o 1 11 3 9764.02 10097.47 306.72 o 3 11 3 7077.31 7415.70 215.39 o 5 11 3 24274.76 24263.90 367.97 o 7 11 3 18473.19 18421.39 341.23 o 9 11 3 8049.74 8893.46 293.06 o 11 11 3 4019.54 3624.44 315.06 o 13 11 3 4928.00 4539.69 318.25 o 1 13 3 6942.49 6548.98 290.59 o 3 13 3 71.50 172.21 82.86 o 5 13 3 2018.21 1862.53 137.21 o 7 13 3 5209.70 5421.74 234.64 o 9 13 3 3689.21 3795.96 233.08 o 11 13 3 3420.37 3928.61 348.46 o 13 13 3 987.16 501.87 190.98 o 1 15 3 1466.31 1520.79 180.05 o 3 15 3 4413.56 4443.02 280.70 o 5 15 3 2810.72 2830.71 238.21 o 7 15 3 3802.38 4247.02 238.83 o 9 15 3 1549.69 1605.28 213.30 o 11 15 3 462.28 239.51 215.67 o 1 17 3 1137.89 805.52 192.56 o 3 17 3 1066.08 1285.64 184.22 o 5 17 3 640.63 506.13 145.58 o 7 17 3 817.53 767.69 233.33 o 9 17 3 620.82 660.24 247.48 o 1 19 3 946.47 1162.12 199.38 o 3 19 3 303.40 442.44 235.53 o 0 0 4 618009.94 604609.56 6956.92 o 4 0 4 112230.77 110286.72 895.22 o 8 0 4 127978.77 123579.48 963.13 o 12 0 4 49320.46 53701.67 1316.27 o 16 0 4 19723.33 20125.46 840.33 o 2 2 4 291.37 197.70 24.85 o 4 2 4 2718.97 2371.66 55.87 o 6 2 4 48691.08 49562.94 313.84 o 8 2 4 2035.15 1875.02 81.22 o 10 2 4 416.28 433.97 72.42 o 12 2 4 920.38 996.09 108.56 o 14 2 4 119.32 98.01 79.17 o 16 2 4 460.75 241.26 131.51 o 0 4 4 1612794.75 1595573.63 12402.36 o 2 4 4 16894.50 16546.53 238.75 o 4 4 4 199905.06 192319.06 815.33 o 6 4 4 52.68 27.86 30.32 o 8 4 4 124425.20 126450.27 706.56 o 10 4 4 96.48 140.30 53.18 o 12 4 4 40038.41 41888.32 684.64 o 14 4 4 1.09 24.41 83.67 o 16 4 4 13880.45 13677.70 584.13 o 2 6 4 557.02 650.09 56.31 o 4 6 4 965.10 1016.20 60.40 o 6 6 4 763.36 762.03 57.10 o 8 6 4 2028.77 2380.66 112.71 o 10 6 4 6067.95 6791.68 228.82 o 12 6 4 978.77 1121.17 147.07 o 14 6 4 38.35 55.07 78.79 o 16 6 4 106.55 148.28 128.79 o 0 8 4 110245.42 106406.52 1088.86 o 2 8 4 9281.20 8615.88 274.63 o 4 8 4 51029.59 48519.37 457.03 o 6 8 4 1405.20 1592.83 100.06 o 8 8 4 24724.55 25491.70 360.56 o 10 8 4 18.14 80.34 68.22 o 12 8 4 31033.59 31092.94 738.59 o 14 8 4 0.27 102.21 85.00 o 16 8 4 11841.33 12332.40 878.10 o 2 10 4 24.68 155.18 73.95 o 4 10 4 1.30 -15.95 41.84 o 6 10 4 1722.16 1625.88 115.33 o 8 10 4 383.21 330.63 70.32 o 10 10 4 254.87 384.58 104.81 o 12 10 4 385.77 375.09 119.74 o 14 10 4 1138.81 931.64 167.08 o 0 12 4 31765.63 29949.74 789.70 o 2 12 4 125.47 158.07 71.89 o 4 12 4 26926.57 25818.34 394.22 o 6 12 4 599.90 384.70 72.14 o 8 12 4 15732.20 15332.85 349.86 o 10 12 4 57.56 131.14 90.49 o 12 12 4 12039.38 12205.48 733.56 o 2 14 4 0.87 161.38 97.83 o 4 14 4 44.78 166.72 81.64 o 6 14 4 184.88 185.23 81.24 o 8 14 4 88.28 50.12 83.00 o 10 14 4 0.98 159.93 115.24 o 12 14 4 70.89 130.53 195.90 o 0 16 4 2206.02 2941.09 564.31 o 2 16 4 2.87 82.65 73.31 o 4 16 4 5537.87 5511.51 496.11 o 6 16 4 163.70 168.04 101.99 o 8 16 4 2789.52 3104.87 274.43 o 10 16 4 74.22 47.83 167.46 o 2 18 4 266.32 275.71 113.32 o 4 18 4 10.02 131.01 115.34 o 6 18 4 0.94 61.19 101.88 o 1 1 5 126586.19 127367.34 510.48 o 3 1 5 99477.35 95228.73 478.41 o 5 1 5 14454.66 11663.45 183.66 o 7 1 5 15120.50 15317.34 197.64 o 9 1 5 8493.73 9825.99 177.03 o 11 1 5 16800.65 16544.19 503.23 o 13 1 5 23565.12 22759.91 454.76 o 15 1 5 5063.20 4723.81 457.08 o 17 1 5 5241.12 4769.28 741.84 o 1 3 5 5654.30 5322.83 100.23 o 3 3 5 7053.90 6891.36 107.70 o 5 3 5 45803.16 47575.86 294.67 o 7 3 5 23917.91 22089.33 225.63 o 9 3 5 25500.23 26341.27 324.30 o 11 3 5 9616.95 10097.14 442.31 o 13 3 5 13955.76 14649.77 497.07 o 15 3 5 8554.18 9144.11 383.18 o 17 3 5 4681.99 3836.93 633.84 o 1 5 5 121005.95 118453.49 665.31 o 3 5 5 13252.63 15130.01 186.24 o 5 5 5 2173.43 2298.06 72.51 o 7 5 5 4275.64 3722.33 113.69 o 9 5 5 13496.78 12734.13 326.69 o 11 5 5 4621.62 4942.87 212.77 o 13 5 5 11347.79 11228.81 454.61 o 15 5 5 4255.14 4344.31 349.03 o 1 7 5 10494.32 8078.40 193.80 o 3 7 5 18183.23 15781.47 233.77 o 5 7 5 44705.48 43360.96 369.62 o 7 7 5 31901.15 30277.80 333.64 o 9 7 5 2377.77 2435.97 141.34 o 11 7 5 17419.20 17890.96 651.57 o 13 7 5 4610.37 4250.86 272.79 o 15 7 5 6290.74 7116.99 512.08 o 1 9 5 85068.91 84432.53 771.06 o 3 9 5 19544.77 17973.06 281.15 o 5 9 5 20031.13 21634.49 320.23 o 7 9 5 5576.94 5298.41 169.86 o 9 9 5 6727.90 6427.56 244.55 o 11 9 5 6392.52 6395.47 378.57 o 13 9 5 3168.72 3600.67 269.94 o 15 9 5 1564.45 1287.06 200.54 o 1 11 5 21817.99 20452.19 439.93 o 3 11 5 6825.18 7215.27 252.93 o 5 11 5 15263.89 16067.91 301.51 o 7 11 5 8236.79 8163.82 220.91 o 9 11 5 839.51 831.97 196.06 o 11 11 5 1587.76 1209.40 212.95 o 13 11 5 1426.86 1353.20 197.68 o 1 13 5 13634.79 12710.45 383.80 o 3 13 5 2628.79 2584.43 177.84 o 5 13 5 1499.94 1657.45 129.61 o 7 13 5 4310.97 4495.95 218.51 o 9 13 5 1884.27 1871.34 182.69 o 11 13 5 2059.03 1324.78 419.30 o 13 13 5 1018.63 939.39 259.25 o 1 15 5 2164.08 1984.63 233.53 o 3 15 5 4102.60 3601.23 257.16 o 5 15 5 1989.33 2321.44 223.15 o 7 15 5 2479.00 2203.20 200.43 o 9 15 5 120.70 56.53 105.41 o 11 15 5 330.64 64.39 296.54 o 1 17 5 1897.28 1594.92 209.80 o 3 17 5 2076.75 2110.93 229.78 o 5 17 5 932.54 1020.44 202.27 o 7 17 5 795.15 688.95 158.70 o 1 19 5 731.11 944.13 221.43 o 3 19 5 302.06 235.85 139.29 o 2 0 6 2763.14 2944.34 76.42 o 6 0 6 4531.91 5170.66 145.82 o 10 0 6 7587.79 7798.11 227.08 o 14 0 6 363.26 453.01 422.78 o 0 2 6 33475.01 35546.02 315.56 o 2 2 6 105065.05 103319.18 567.42 o 4 2 6 19993.26 19070.61 182.97 o 6 2 6 279173.56 290314.34 1484.94 o 8 2 6 3717.53 4071.34 151.84 o 10 2 6 52979.33 56508.84 510.94 o 12 2 6 8.90 -9.26 48.70 o 14 2 6 44794.17 44459.92 790.18 o 16 2 6 64.50 29.52 113.22 o 2 4 6 15258.92 16783.53 169.33 o 4 4 6 959.02 1183.63 59.98 o 6 4 6 757.88 634.86 46.84 o 8 4 6 1071.58 1126.85 91.09 o 10 4 6 62.25 15.39 40.80 o 12 4 6 508.26 534.80 94.16 o 14 4 6 11.41 60.23 93.53 o 16 4 6 231.53 -35.12 91.24 o 0 6 6 33182.86 35618.63 512.50 o 2 6 6 88023.53 85618.62 809.77 o 4 6 6 6850.16 9211.75 178.02 o 6 6 6 125343.23 127980.32 742.55 o 8 6 6 11968.26 11198.70 219.88 o 10 6 6 35425.95 35698.10 472.27 o 12 6 6 210.09 238.68 88.47 o 14 6 6 29064.38 30446.17 968.65 o 16 6 6 184.40 19.30 124.27 o 2 8 6 9241.34 9698.96 204.84 o 4 8 6 1434.17 1593.48 97.61 o 6 8 6 902.09 738.34 104.89 o 8 8 6 648.95 851.70 97.80 o 10 8 6 621.48 744.93 179.82 o 12 8 6 350.48 171.63 89.27 o 14 8 6 702.01 413.79 120.99 o 0 10 6 1021.73 778.03 154.52 o 2 10 6 35279.56 33731.55 483.72 o 4 10 6 60.65 63.98 48.40 o 6 10 6 33615.78 32961.95 423.23 o 8 10 6 198.90 235.33 64.72 o 10 10 6 17334.15 16592.90 400.21 o 12 10 6 5.22 107.16 114.34 o 14 10 6 11929.11 11980.71 462.05 o 2 12 6 0.00 7.61 51.04 o 4 12 6 163.86 173.58 64.73 o 6 12 6 1.56 52.67 51.00 o 8 12 6 277.15 401.25 90.70 o 10 12 6 1539.62 1163.36 172.13 o 12 12 6 0.17 93.10 136.55 o 0 14 6 1369.12 1556.75 248.98 o 2 14 6 13246.55 13163.91 426.26 o 4 14 6 29.12 -27.15 52.44 o 6 14 6 7765.98 7740.74 254.08 o 8 14 6 168.60 252.25 104.57 o 10 14 6 6115.13 5769.62 509.32 o 12 14 6 86.44 53.48 194.69 o 2 16 6 231.59 226.80 101.02 o 4 16 6 105.20 213.46 102.85 o 6 16 6 173.79 -17.79 98.43 o 8 16 6 273.55 287.94 128.48 o 10 16 6 10.05 94.14 166.00 o 0 18 6 162.13 78.08 146.69 o 2 18 6 2335.73 1850.59 275.62 o 4 18 6 6.28 38.34 111.52 o 6 18 6 1308.30 1482.76 214.94 o 1 1 7 6690.82 5641.59 105.40 o 3 1 7 6267.12 4768.64 75.78 o 5 1 7 58126.68 58798.95 397.64 o 7 1 7 50859.50 46160.84 384.54 o 9 1 7 25118.41 23859.57 301.09 o 11 1 7 24573.69 25166.60 560.52 o 13 1 7 11874.08 10942.70 319.46 o 15 1 7 8182.66 8237.38 385.82 o 17 1 7 5280.17 5364.41 517.29 o 1 3 7 333.73 190.82 26.57 o 3 3 7 32403.49 32683.65 266.55 o 5 3 7 26922.87 26057.97 235.33 o 7 3 7 49247.06 51965.09 367.21 o 9 3 7 1439.21 1704.67 109.65 o 11 3 7 39818.13 39310.54 547.68 o 13 3 7 15583.31 15392.26 460.23 o 15 3 7 7345.33 7387.74 359.93 o 17 3 7 2986.66 2862.27 549.07 o 1 5 7 61158.67 66394.28 450.68 o 3 5 7 11666.36 12123.49 169.25 o 5 5 7 79876.18 76152.11 503.53 o 7 5 7 24641.56 24529.84 271.45 o 9 5 7 29881.68 29928.82 409.67 o 11 5 7 20957.69 20892.88 472.69 o 13 5 7 11714.33 12226.71 475.25 o 15 5 7 3118.01 2896.94 257.16 o 1 7 7 5709.50 4831.13 140.93 o 3 7 7 27162.00 27356.32 315.85 o 5 7 7 16376.59 16494.81 275.13 o 7 7 7 34945.75 36568.18 373.08 o 9 7 7 3452.07 3673.01 166.30 o 11 7 7 10190.04 10028.18 416.72 o 13 7 7 8442.06 8035.90 638.56 o 15 7 7 5057.57 4725.75 517.07 o 1 9 7 28391.88 25008.20 394.86 o 3 9 7 4646.21 4300.63 149.49 o 5 9 7 6047.85 5475.84 168.39 o 7 9 7 17006.35 16745.88 272.19 o 9 9 7 16964.07 16189.46 333.40 o 11 9 7 6042.90 5900.32 295.99 o 13 9 7 5233.70 4334.28 293.03 o 15 9 7 1694.77 893.37 249.13 o 1 11 7 16.43 171.09 61.21 o 3 11 7 6248.20 6294.90 201.26 o 5 11 7 6878.36 7616.98 211.99 o 7 11 7 13467.80 14389.20 310.33 o 9 11 7 2314.48 2023.25 178.26 o 11 11 7 4743.31 5128.15 309.45 o 13 11 7 3488.91 3659.27 290.95 o 1 13 7 8998.66 9289.56 331.85 o 3 13 7 3857.63 4137.10 217.22 o 5 13 7 4304.64 4436.77 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8 111.33 217.84 40.19 o 8 4 8 101141.20 99150.44 776.73 o 10 4 8 2782.00 2204.43 131.96 o 12 4 8 57017.67 56594.25 823.35 o 14 4 8 41.37 16.55 77.11 o 16 4 8 15597.47 14960.80 507.65 o 2 6 8 8969.39 10586.20 168.45 o 4 6 8 2042.54 2101.83 88.26 o 6 6 8 779.75 897.23 69.71 o 8 6 8 282.35 386.28 65.91 o 10 6 8 173.12 214.93 62.07 o 12 6 8 0.67 75.26 71.78 o 14 6 8 920.62 936.60 183.73 o 16 6 8 14.25 -53.61 99.79 o 0 8 8 106340.51 106348.41 1117.33 o 2 8 8 14.52 31.99 37.27 o 4 8 8 63499.41 60968.31 531.73 o 6 8 8 234.01 241.03 53.80 o 8 8 8 79825.98 80235.64 893.60 o 10 8 8 1463.23 1258.33 151.44 o 12 8 8 31757.24 33603.71 1786.65 o 14 8 8 33.00 -31.91 81.30 o 2 10 8 67.21 160.53 62.72 o 4 10 8 19.13 24.58 43.83 o 6 10 8 371.82 379.31 64.74 o 8 10 8 86.20 103.43 59.49 o 10 10 8 1773.22 1910.50 170.61 o 12 10 8 242.91 296.32 150.22 o 14 10 8 6.58 140.34 115.39 o 0 12 8 6700.03 6210.61 806.85 o 2 12 8 423.48 407.74 86.57 o 4 12 8 17800.74 18201.37 355.19 o 6 12 8 61.05 130.17 59.26 o 8 12 8 12765.13 13874.37 308.80 o 10 12 8 83.33 57.19 87.14 o 12 12 8 13089.54 13294.45 560.03 o 2 14 8 1014.74 1026.58 151.27 o 4 14 8 2.29 -39.36 51.75 o 6 14 8 372.71 355.29 93.64 o 8 14 8 0.87 -6.04 84.57 o 10 14 8 382.12 67.49 110.63 o 0 16 8 3320.78 3173.29 362.95 o 2 16 8 817.79 568.47 138.86 o 4 16 8 6222.73 6468.23 346.52 o 6 16 8 0.39 27.98 91.83 o 8 16 8 2789.63 3046.11 276.73 o 2 18 8 134.25 56.28 109.80 o 4 18 8 35.17 95.86 103.50 o 6 18 8 20.96 185.12 155.80 o 1 1 9 27400.23 29807.34 187.54 o 3 1 9 2716.97 2493.74 52.69 o 5 1 9 94688.31 92584.04 545.45 o 7 1 9 25116.28 22451.50 259.24 o 9 1 9 47236.01 45451.92 476.53 o 11 1 9 20737.97 19473.12 379.15 o 13 1 9 12534.09 12293.11 378.83 o 15 1 9 4263.29 4441.44 292.88 o 17 1 9 9100.89 10570.23 683.02 o 1 3 9 140908.48 139790.50 638.31 o 3 3 9 102370.86 102508.71 516.59 o 5 3 9 76155.81 73268.15 480.58 o 7 3 9 39842.14 39738.57 469.47 o 9 3 9 10542.14 11661.13 368.98 o 11 3 9 20817.91 20738.12 368.25 o 13 3 9 15634.32 15213.02 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96.99 o 11 11 9 1245.22 1304.70 172.22 o 13 11 9 1926.42 1686.85 261.45 o 1 13 9 11010.28 11823.26 373.34 o 3 13 9 8264.59 8800.07 284.91 o 5 13 9 1732.88 1784.56 163.26 o 7 13 9 2101.54 2074.41 163.63 o 9 13 9 1304.78 1480.27 188.17 o 11 13 9 1007.52 914.24 332.51 o 1 15 9 5731.87 5712.72 355.21 o 3 15 9 1684.17 1707.43 196.10 o 5 15 9 4317.31 4431.73 250.97 o 7 15 9 1879.03 1850.82 209.50 o 9 15 9 560.11 539.16 153.34 o 1 17 9 1232.39 723.31 161.92 o 3 17 9 492.17 339.35 124.72 o 5 17 9 95.31 54.11 106.64 o 7 17 9 720.47 829.53 163.67 o 1 19 9 142.02 258.00 138.96 o 3 19 9 431.58 228.76 291.45 o 2 0 10 866.98 874.69 52.51 o 6 0 10 3937.61 3653.59 209.92 o 10 0 10 716.37 508.18 120.58 o 14 0 10 63.83 117.27 171.14 o 0 2 10 2313.97 1591.62 81.91 o 2 2 10 701788.88 739532.25 2748.53 o 4 2 10 16750.41 18169.14 184.02 o 6 2 10 291469.81 301773.81 1375.84 o 8 2 10 151.79 105.80 47.46 o 10 2 10 31261.63 30344.84 418.98 o 12 2 10 99.41 158.49 65.50 o 14 2 10 35343.44 36828.90 1225.82 o 16 2 10 11.81 105.29 93.87 o 2 4 10 11614.80 13651.17 136.00 o 4 4 10 4225.85 4125.11 111.00 o 6 4 10 153.23 51.35 30.81 o 8 4 10 753.27 866.52 89.50 o 10 4 10 704.12 810.82 118.98 o 12 4 10 217.41 125.50 66.51 o 14 4 10 109.20 94.94 84.01 o 16 4 10 619.67 656.69 146.17 o 0 6 10 1574.23 1395.59 99.82 o 2 6 10 206501.83 208805.98 955.83 o 4 6 10 1.04 -25.41 27.45 o 6 6 10 127416.97 126926.13 756.95 o 8 6 10 217.99 177.07 53.84 o 10 6 10 22654.04 22278.99 386.38 o 12 6 10 6.51 89.36 92.30 o 14 6 10 22689.52 24315.34 719.74 o 16 6 10 6.79 -10.74 104.05 o 2 8 10 5245.13 5867.33 170.17 o 4 8 10 2131.31 2385.83 108.19 o 6 8 10 1609.24 1565.29 98.31 o 8 8 10 1.61 191.20 61.38 o 10 8 10 413.11 348.12 119.12 o 12 8 10 14.15 125.06 122.29 o 14 8 10 32.03 102.66 114.59 o 0 10 10 89.37 85.09 63.91 o 2 10 10 63522.88 65915.01 718.93 o 4 10 10 2394.97 2539.52 192.38 o 6 10 10 39203.44 39397.40 726.14 o 8 10 10 696.70 414.22 95.09 o 10 10 10 13525.56 14057.80 336.23 o 12 10 10 0.24 41.16 116.97 o 14 10 10 8818.33 9715.40 423.97 o 2 12 10 243.69 143.59 68.67 o 4 12 10 1449.85 1586.88 147.78 o 6 12 10 411.09 235.59 71.75 o 8 12 10 0.04 117.61 69.66 o 10 12 10 164.63 214.81 106.57 o 12 12 10 28.10 241.62 169.20 o 0 14 10 33.81 46.50 154.20 o 2 14 10 8796.17 8860.93 420.95 o 4 14 10 109.98 50.57 65.49 o 6 14 10 6633.21 7164.82 266.05 o 8 14 10 73.74 37.37 100.72 o 10 14 10 5264.79 5245.14 382.02 o 2 16 10 21.52 9.73 86.17 o 4 16 10 86.34 120.49 103.71 o 6 16 10 0.12 69.40 80.50 o 8 16 10 152.77 232.46 135.82 o 0 18 10 40.88 133.45 153.02 o 2 18 10 2110.43 1998.05 232.25 o 4 18 10 0.12 20.94 124.98 o 6 18 10 1184.30 1251.95 240.11 o 1 1 11 148423.03 149434.25 823.50 o 3 1 11 119756.36 129295.70 550.74 o 5 1 11 52184.72 51470.50 436.98 o 7 1 11 35433.66 36310.88 342.35 o 9 1 11 4185.31 4467.48 166.27 o 11 1 11 24507.05 23779.48 388.24 o 13 1 11 17181.22 16974.47 578.73 o 15 1 11 4974.15 5086.66 379.35 o 17 1 11 4345.23 3777.56 633.83 o 1 3 11 112120.52 106422.23 531.76 o 3 3 11 74004.59 74041.70 379.41 o 5 3 11 80418.70 81626.71 497.06 o 7 3 11 44797.94 43360.40 462.91 o 9 3 11 2893.01 2725.45 136.94 o 11 3 11 20382.78 21284.96 393.50 o 13 3 11 8220.10 7278.58 285.06 o 15 3 11 6549.65 6209.32 345.92 o 1 5 11 67270.49 58318.00 364.36 o 3 5 11 49309.66 45829.96 305.83 o 5 5 11 15516.75 15450.68 211.97 o 7 5 11 43856.00 42679.84 483.35 o 9 5 11 24414.37 24356.52 386.68 o 11 5 11 9050.92 9362.09 256.93 o 13 5 11 10589.98 10048.60 329.45 o 15 5 11 3371.22 2939.10 368.38 o 1 7 11 9929.09 9996.38 230.04 o 3 7 11 16485.84 16867.82 234.74 o 5 7 11 48416.09 50745.64 445.35 o 7 7 11 25404.11 27707.95 364.02 o 9 7 11 1944.68 1928.51 138.79 o 11 7 11 17444.26 19147.35 425.95 o 13 7 11 6104.19 5639.16 393.96 o 15 7 11 2979.53 2490.38 300.54 o 1 9 11 19872.00 20141.76 332.69 o 3 9 11 6619.14 5703.35 162.71 o 5 9 11 19948.38 19184.33 545.53 o 7 9 11 16348.07 16457.93 299.05 o 9 9 11 19666.90 19099.38 392.73 o 11 9 11 7779.87 8156.88 263.86 o 13 9 11 3736.01 3673.74 339.89 o 15 9 11 1298.11 1730.14 513.45 o 1 11 11 8141.81 8937.26 435.85 o 3 11 11 4768.29 5802.47 227.93 o 5 11 11 12884.65 13898.30 314.05 o 7 11 11 8282.83 8578.76 257.20 o 9 11 11 3840.58 4170.71 231.01 o 11 11 11 1181.47 910.97 158.49 o 13 11 11 3254.69 2822.14 403.67 o 1 13 11 4436.42 4257.40 235.41 o 3 13 11 155.50 267.06 80.55 o 5 13 11 1398.19 1316.94 128.37 o 7 13 11 4928.19 5347.67 238.40 o 9 13 11 4367.57 4074.36 338.80 o 11 13 11 2681.63 2650.50 300.89 o 1 15 11 855.15 908.76 147.91 o 3 15 11 2040.27 1980.08 215.82 o 5 15 11 1780.62 1856.32 164.47 o 7 15 11 1617.37 1514.89 171.17 o 9 15 11 1335.29 1261.20 196.57 o 1 17 11 864.09 1144.38 176.85 o 3 17 11 784.36 611.48 148.36 o 5 17 11 384.23 394.15 124.48 o 7 17 11 563.19 700.51 162.54 o 0 0 12 17420.32 12118.94 290.41 o 4 0 12 87213.53 71129.23 662.65 o 8 0 12 267765.34 263824.81 2136.66 o 12 0 12 79990.53 76247.02 1381.33 o 16 0 12 10048.93 9697.63 483.24 o 2 2 12 436.67 623.28 36.59 o 4 2 12 4658.56 5107.55 140.99 o 6 2 12 15285.25 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51.79 o 4 10 12 20.32 80.45 50.52 o 6 10 12 117.13 229.81 63.19 o 8 10 12 11.48 24.01 56.65 o 10 10 12 2503.45 2622.81 177.92 o 12 10 12 187.57 220.43 123.82 o 14 10 12 172.37 115.24 167.08 o 0 12 12 26830.20 24614.46 681.71 o 2 12 12 56.86 61.33 56.61 o 4 12 12 19172.44 19347.63 409.57 o 6 12 12 244.81 64.93 58.81 o 8 12 12 10591.03 10731.44 340.98 o 10 12 12 67.58 97.62 97.59 o 12 12 12 8423.40 8557.66 611.70 o 2 14 12 0.27 106.43 73.69 o 4 14 12 42.69 101.49 64.60 o 6 14 12 427.73 360.05 93.59 o 8 14 12 29.92 123.66 92.79 o 10 14 12 96.21 37.17 106.06 o 0 16 12 1776.83 1646.70 654.96 o 2 16 12 0.02 34.43 91.64 o 4 16 12 3671.58 3886.35 236.84 o 6 16 12 118.76 217.22 96.39 o 8 16 12 1686.09 1591.12 249.01 o 2 18 12 154.44 58.53 115.44 o 4 18 12 5.76 14.90 100.06 o 1 1 13 74221.14 73672.34 429.70 o 3 1 13 65058.32 62567.30 344.10 o 5 1 13 17526.48 19177.25 201.69 o 7 1 13 55622.88 57303.61 548.48 o 9 1 13 7883.00 8083.60 213.80 o 11 1 13 38802.10 38991.37 513.81 o 13 1 13 9493.39 9462.41 393.21 o 15 1 13 2706.37 2241.96 201.56 o 1 3 13 31175.01 28931.81 221.75 o 3 3 13 13989.93 12444.18 135.62 o 5 3 13 28031.40 27660.57 311.53 o 7 3 13 30319.91 30068.89 445.77 o 9 3 13 14015.65 14635.77 289.44 o 11 3 13 11325.80 11456.85 260.85 o 13 3 13 6709.19 7699.79 352.01 o 15 3 13 4240.54 4099.51 257.70 o 1 5 13 21039.06 19633.15 200.88 o 3 5 13 3940.34 3793.55 111.09 o 5 5 13 6134.45 6159.77 204.03 o 7 5 13 24959.01 23959.14 363.64 o 9 5 13 15510.41 15509.49 313.25 o 11 5 13 20759.23 21293.47 627.37 o 13 5 13 6353.09 6634.55 312.47 o 15 5 13 2607.82 2337.35 244.38 o 1 7 13 23474.76 23664.21 273.42 o 3 7 13 28512.66 27336.19 333.90 o 5 7 13 25289.92 23469.72 306.39 o 7 7 13 21918.57 22266.97 369.21 o 9 7 13 1028.91 1159.06 119.99 o 11 7 13 6911.89 7543.71 257.05 o 13 7 13 2521.45 2836.93 293.92 o 15 7 13 3088.39 3330.46 433.89 o 1 9 13 20557.58 22592.65 293.23 o 3 9 13 10544.15 9461.75 231.49 o 5 9 13 10673.52 10536.51 234.85 o 7 9 13 13656.54 14123.03 311.83 o 9 9 13 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42 5.35 -177.92 247.39 o 2 4 42 21.36 132.88 119.36 o 1 1 43 332.12 384.17 169.16 o