#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2213688.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213688_Fobs loop_ _publ_author_name 'Schuchmann, Daniella' 'Schulz, Stephan' 'Fl\"orke, Ulrich' _publ_section_title ; Tri-tert-butylgallane--(tert-butyl)diethylstibine adduct ; _journal_coeditor_code BT2352 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1606 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.479 _cell_angle_gamma 90.000 _cell_length_a 9.1138 _cell_length_b 23.6975 _cell_length_c 11.0267 _exptl_crystal_F_000 992.00 _reflns_d_resolution_high 0.7600 _[local]_cod_data_source_file bt2352Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C20 H46 Ga Sb in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 319.77 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 67035.75 73479.19 503.75 o 4 0 0 46545.61 51543.15 1634.06 o 6 0 0 236.46 320.25 46.98 o 8 0 0 131.38 198.35 83.65 o 10 0 0 3284.87 3448.69 281.18 o 1 1 0 5.82 9.48 6.88 o 2 1 0 3033.19 2571.02 369.92 o 3 1 0 269.36 327.35 24.60 o 4 1 0 2365.16 2471.73 73.32 o 5 1 0 211.97 246.12 26.86 o 6 1 0 4292.74 4752.13 107.97 o 7 1 0 19.93 37.88 37.76 o 8 1 0 1390.53 1334.84 90.25 o 9 1 0 14.31 -11.94 50.97 o 10 1 0 326.66 229.15 66.69 o 11 1 0 7.84 -8.37 65.00 o 0 2 0 258.52 271.06 28.31 o 1 2 0 102251.63 46691.86 22102.04 o 2 2 0 1138.52 634.68 388.09 o 3 2 0 53034.09 35851.97 20097.74 o 4 2 0 150.32 161.50 26.67 o 5 2 0 1892.82 1931.41 48.99 o 6 2 0 752.64 747.69 50.38 o 7 2 0 6.86 31.31 38.27 o 8 2 0 155.46 211.50 58.18 o 9 2 0 1184.30 1356.58 97.30 o 10 2 0 198.68 200.41 62.20 o 11 2 0 2010.24 2003.80 145.72 o 1 3 0 1270.27 1086.27 46.95 o 2 3 0 755.71 551.57 165.68 o 3 3 0 15995.18 16711.48 242.95 o 4 3 0 3425.45 2459.30 846.91 o 5 3 0 9606.40 7779.71 1543.92 o 6 3 0 1525.86 1289.81 258.80 o 7 3 0 7214.45 6676.89 996.00 o 8 3 0 965.70 680.99 202.43 o 9 3 0 4975.10 3427.20 932.96 o 10 3 0 388.25 300.08 98.37 o 11 3 0 394.68 322.35 84.43 o 0 4 0 45471.28 43344.52 2735.93 o 1 4 0 5117.61 4951.93 264.80 o 2 4 0 2888.75 2827.65 66.94 o 3 4 0 2948.73 3203.52 122.66 o 4 4 0 6632.89 6725.08 116.65 o 5 4 0 519.24 528.75 59.54 o 6 4 0 67.47 59.19 31.74 o 7 4 0 215.33 151.53 43.37 o 8 4 0 1.34 39.00 44.96 o 9 4 0 508.56 518.84 75.36 o 10 4 0 1221.63 1195.20 116.37 o 11 4 0 231.22 255.57 104.59 o 1 5 0 3568.99 3598.98 133.91 o 2 5 0 1639.37 1491.49 53.89 o 3 5 0 7043.21 6656.03 298.07 o 4 5 0 16012.54 16293.42 233.88 o 5 5 0 8402.63 8607.63 148.91 o 6 5 0 16018.45 16377.26 275.86 o 7 5 0 7588.99 7677.00 152.99 o 8 5 0 7799.74 7813.97 276.83 o 9 5 0 2711.74 2728.27 130.62 o 10 5 0 2552.74 2560.12 157.76 o 11 5 0 640.78 551.26 96.45 o 0 6 0 13075.54 13699.59 184.20 o 1 6 0 11378.15 11644.07 194.61 o 2 6 0 1957.24 2040.65 45.82 o 3 6 0 811.32 777.71 50.15 o 4 6 0 3786.29 4069.75 96.72 o 5 6 0 19.12 58.68 33.37 o 6 6 0 32.59 18.53 38.50 o 7 6 0 2.89 27.45 41.09 o 8 6 0 307.35 293.13 55.39 o 9 6 0 205.81 179.17 65.42 o 10 6 0 558.68 541.89 93.15 o 11 6 0 109.37 151.19 80.85 o 1 7 0 10714.13 7823.54 2110.41 o 2 7 0 3522.84 3467.35 63.47 o 3 7 0 3631.37 3559.99 62.51 o 4 7 0 9626.52 9013.40 157.57 o 5 7 0 21161.87 21510.72 550.02 o 6 7 0 14584.00 14621.62 772.04 o 7 7 0 10373.90 10829.25 228.77 o 8 7 0 7269.78 7098.69 163.16 o 9 7 0 6262.54 6464.09 232.10 o 10 7 0 2105.78 2073.91 148.53 o 11 7 0 863.17 773.75 111.06 o 0 8 0 1893.72 2014.18 81.98 o 1 8 0 1358.98 1032.13 198.41 o 2 8 0 1610.04 1641.23 48.82 o 3 8 0 1571.08 1811.84 48.39 o 4 8 0 136.18 222.26 35.39 o 5 8 0 2.59 31.37 35.75 o 6 8 0 984.51 972.51 69.72 o 7 8 0 698.00 660.24 68.39 o 8 8 0 5.95 16.50 47.37 o 9 8 0 1151.35 1202.35 117.78 o 10 8 0 80.05 150.35 89.61 o 11 8 0 754.92 801.15 113.10 o 1 9 0 206.13 180.65 22.28 o 2 9 0 5969.50 5965.96 105.06 o 3 9 0 7679.98 7269.85 110.20 o 4 9 0 12506.21 12282.40 247.64 o 5 9 0 8990.97 8716.59 199.65 o 6 9 0 9880.49 9734.35 185.84 o 7 9 0 5962.69 6263.28 277.37 o 8 9 0 5333.10 5536.32 202.25 o 9 9 0 4383.91 4433.70 200.96 o 10 9 0 1819.84 1720.58 140.03 o 11 9 0 613.94 527.61 99.19 o 0 10 0 1325.99 1216.27 61.75 o 1 10 0 20517.52 19835.66 469.35 o 2 10 0 871.90 857.06 39.87 o 3 10 0 16392.99 16948.59 157.04 o 4 10 0 60.94 58.77 23.82 o 5 10 0 1827.61 1848.00 81.41 o 6 10 0 174.73 81.87 52.02 o 7 10 0 69.89 57.66 47.49 o 8 10 0 804.19 942.06 122.20 o 9 10 0 422.93 536.90 91.29 o 10 10 0 681.87 816.30 109.45 o 11 10 0 740.28 742.34 110.08 o 1 11 0 2418.56 2527.42 63.79 o 2 11 0 4718.54 4440.17 82.99 o 3 11 0 272.16 303.94 30.65 o 4 11 0 3365.35 3297.47 75.91 o 5 11 0 6221.59 5992.38 141.47 o 6 11 0 6426.59 6317.67 164.27 o 7 11 0 509.09 737.41 122.87 o 8 11 0 2907.89 2922.17 151.91 o 9 11 0 1168.29 1241.37 101.07 o 10 11 0 613.96 743.50 109.36 o 11 11 0 79.85 115.98 84.23 o 0 12 0 58227.54 59275.45 460.62 o 1 12 0 591.30 486.86 36.03 o 2 12 0 22520.33 22589.76 444.28 o 3 12 0 1370.92 1338.46 51.44 o 4 12 0 9600.10 9826.36 241.65 o 5 12 0 0.29 16.94 35.14 o 6 12 0 927.22 982.14 72.09 o 7 12 0 2.49 -23.70 50.96 o 8 12 0 394.49 399.22 78.70 o 9 12 0 252.42 213.31 72.83 o 10 12 0 936.35 1136.16 160.05 o 11 12 0 272.60 344.75 102.97 o 1 13 0 166.08 200.66 29.92 o 2 13 0 0.57 8.22 24.09 o 3 13 0 1541.83 1608.17 58.38 o 4 13 0 66.15 59.79 27.82 o 5 13 0 3500.36 3404.82 113.70 o 6 13 0 292.58 246.97 50.13 o 7 13 0 1217.12 1214.93 127.27 o 8 13 0 2.96 12.16 59.17 o 9 13 0 798.45 831.04 102.07 o 10 13 0 5.22 122.51 80.08 o 0 14 0 1921.66 1667.64 90.15 o 1 14 0 32135.03 31677.74 747.00 o 2 14 0 450.71 426.89 37.80 o 3 14 0 17854.32 16864.93 562.52 o 4 14 0 600.29 585.24 42.66 o 5 14 0 2976.11 2819.92 106.55 o 6 14 0 133.10 102.47 45.43 o 7 14 0 69.33 101.70 58.92 o 8 14 0 79.57 145.16 65.37 o 9 14 0 1305.89 1297.74 120.54 o 10 14 0 86.08 154.44 85.11 o 1 15 0 246.20 278.72 34.40 o 2 15 0 103.40 119.43 34.29 o 3 15 0 2032.41 1915.75 68.42 o 4 15 0 7.78 32.50 30.57 o 5 15 0 335.88 352.42 52.60 o 6 15 0 187.03 200.29 63.41 o 7 15 0 2360.22 2041.49 132.65 o 8 15 0 14.86 60.75 62.82 o 9 15 0 398.49 358.95 82.37 o 10 15 0 30.32 28.29 76.44 o 0 16 0 22149.81 20983.05 1525.89 o 1 16 0 511.85 466.90 42.30 o 2 16 0 16714.54 16097.96 333.64 o 3 16 0 306.79 296.52 42.38 o 4 16 0 7320.88 7166.70 128.63 o 5 16 0 74.01 57.57 41.99 o 6 16 0 322.07 269.38 69.00 o 7 16 0 51.01 82.16 65.48 o 8 16 0 255.60 315.88 76.91 o 9 16 0 0.15 6.45 65.45 o 10 16 0 1122.39 1060.24 161.14 o 1 17 0 29.16 40.26 31.35 o 2 17 0 211.36 176.58 35.42 o 3 17 0 338.18 306.82 42.04 o 4 17 0 2037.55 2225.08 78.55 o 5 17 0 366.65 491.46 67.15 o 6 17 0 3808.25 3740.12 170.57 o 7 17 0 415.65 499.03 82.08 o 8 17 0 2787.35 2600.30 160.52 o 9 17 0 97.62 131.10 71.24 o 10 17 0 896.13 884.48 161.21 o 0 18 0 73.93 86.92 46.85 o 1 18 0 7752.23 7463.93 137.03 o 2 18 0 56.02 81.84 31.47 o 3 18 0 3948.61 3898.57 102.27 o 4 18 0 26.25 39.66 37.67 o 5 18 0 847.09 710.84 74.89 o 6 18 0 1.35 -21.08 47.09 o 7 18 0 49.28 35.51 60.93 o 8 18 0 239.14 290.03 89.76 o 9 18 0 504.75 612.79 94.84 o 1 19 0 142.99 189.91 39.24 o 2 19 0 266.32 233.62 40.29 o 3 19 0 2950.21 2911.91 92.15 o 4 19 0 376.83 386.61 51.09 o 5 19 0 5622.17 5255.48 174.86 o 6 19 0 1105.07 1021.84 102.95 o 7 19 0 6447.98 6547.54 244.15 o 8 19 0 799.87 791.64 103.85 o 9 19 0 2115.09 2255.65 165.43 o 0 20 0 1513.22 1371.22 97.21 o 1 20 0 563.14 651.23 53.05 o 2 20 0 775.40 643.96 52.89 o 3 20 0 449.96 478.17 48.55 o 4 20 0 690.20 646.36 67.45 o 5 20 0 2.63 -5.07 43.92 o 6 20 0 23.81 84.46 59.82 o 7 20 0 167.03 253.28 73.64 o 8 20 0 50.04 111.50 69.72 o 9 20 0 146.57 225.28 85.15 o 1 21 0 0.98 -8.33 32.11 o 2 21 0 2072.42 2068.67 83.60 o 3 21 0 1132.66 1060.00 63.87 o 4 21 0 4476.87 4464.34 162.89 o 5 21 0 1374.96 1216.95 96.32 o 6 21 0 6309.00 6307.58 236.93 o 7 21 0 942.01 794.74 103.52 o 8 21 0 3608.63 3586.20 197.36 o 0 22 0 665.23 765.80 82.34 o 1 22 0 95.22 104.74 38.32 o 2 22 0 974.42 992.10 63.77 o 3 22 0 32.95 48.79 37.24 o 4 22 0 0.16 13.89 46.33 o 5 22 0 3.26 -12.99 53.72 o 6 22 0 1.65 46.32 61.30 o 7 22 0 85.17 36.69 64.44 o 8 22 0 526.91 705.70 103.20 o 1 23 0 46.44 98.12 36.97 o 2 23 0 729.51 727.96 58.18 o 3 23 0 1693.49 1762.93 82.04 o 4 23 0 966.32 995.10 91.05 o 5 23 0 3320.07 3324.62 153.92 o 6 23 0 1150.57 994.14 107.89 o 7 23 0 2375.64 2478.65 165.69 o 8 23 0 510.23 491.58 101.71 o 0 24 0 3843.48 3914.60 182.47 o 1 24 0 1118.79 1085.14 68.58 o 2 24 0 2812.84 2762.98 101.22 o 3 24 0 617.05 532.85 69.31 o 4 24 0 880.93 781.79 82.91 o 5 24 0 9.74 10.56 48.78 o 6 24 0 172.21 188.40 70.51 o 7 24 0 64.00 94.27 68.77 o 1 25 0 94.94 222.48 45.33 o 2 25 0 157.46 222.10 45.81 o 3 25 0 524.77 526.91 73.72 o 4 25 0 569.93 693.47 79.37 o 5 25 0 490.77 531.53 75.13 o 6 25 0 739.93 781.78 118.01 o 7 25 0 414.22 427.73 100.20 o 0 26 0 1237.81 1235.96 105.05 o 1 26 0 5959.58 6051.08 151.79 o 2 26 0 1182.57 1192.45 90.19 o 3 26 0 2592.81 2394.18 132.81 o 4 26 0 195.69 215.83 60.25 o 5 26 0 523.85 498.73 76.51 o 6 26 0 52.83 73.62 67.67 o 1 27 0 20.32 77.41 38.04 o 2 27 0 239.34 316.64 55.50 o 3 27 0 4.61 11.49 46.60 o 4 27 0 317.91 493.46 72.89 o 5 27 0 45.01 127.94 56.34 o 0 28 0 3449.58 3370.65 171.20 o 1 28 0 716.26 860.23 67.31 o 2 28 0 2964.13 2735.03 142.43 o 3 28 0 311.01 321.34 66.35 o 4 28 0 891.13 816.28 90.76 o 5 28 0 80.94 83.90 64.83 o 1 29 0 13.97 81.10 52.87 o 2 29 0 38.64 71.86 53.39 o 3 29 0 251.12 343.30 68.06 o 4 29 0 66.70 102.09 60.79 o 0 30 0 157.27 297.68 70.82 o 1 30 0 2229.81 2172.94 115.21 o 2 30 0 350.79 474.42 75.07 o 3 30 0 1470.21 1525.99 122.88 o 1 31 0 12.01 31.78 53.51 o -11 0 1 3389.72 3180.75 324.87 o -9 0 1 6495.31 4735.51 1050.79 o -7 0 1 6711.44 5393.31 687.03 o -5 0 1 2048.59 1492.89 526.89 o -3 0 1 17007.32 19597.97 220.04 o -1 0 1 34417.51 29507.66 528.55 o 1 0 1 62047.09 64749.41 4434.79 o 3 0 1 61268.77 72711.85 1689.57 o 5 0 1 29997.20 33686.25 763.82 o 7 0 1 11973.18 11627.43 305.01 o 9 0 1 1399.09 1356.67 136.05 o 11 0 1 71.69 30.33 83.59 o -11 1 1 984.47 929.47 142.51 o -10 1 1 1731.50 1790.96 134.25 o -9 1 1 696.20 472.91 125.05 o -8 1 1 1466.65 931.91 269.59 o -7 1 1 715.04 578.52 115.36 o -6 1 1 24.75 19.21 20.99 o -5 1 1 2986.80 3136.82 163.59 o -4 1 1 72.04 114.10 20.76 o -3 1 1 17593.03 18083.85 383.69 o -2 1 1 15031.37 13218.22 1512.63 o -1 1 1 20326.14 18016.14 364.44 o 0 1 1 7133.64 7086.81 255.82 o 1 1 1 16456.02 13653.35 3031.81 o 2 1 1 578.52 433.47 109.83 o 3 1 1 4267.00 4573.30 163.19 o 4 1 1 6023.00 6575.77 121.40 o 5 1 1 264.27 340.51 45.41 o 6 1 1 411.06 459.22 40.74 o 7 1 1 344.37 350.80 46.36 o 8 1 1 297.39 303.30 61.14 o 9 1 1 910.73 944.80 84.68 o 10 1 1 13.64 21.90 52.93 o 11 1 1 538.33 619.08 81.94 o -11 2 1 31.43 -33.28 85.32 o -10 2 1 3585.32 3331.85 175.28 o -9 2 1 829.80 780.80 81.69 o -8 2 1 6693.51 6792.22 207.73 o -7 2 1 1075.22 1224.53 66.36 o -6 2 1 5417.57 5332.36 145.55 o -5 2 1 2357.23 2272.24 52.11 o -4 2 1 154.25 286.19 26.05 o -3 2 1 11552.49 12018.25 101.44 o -2 2 1 4226.86 4398.58 77.85 o -1 2 1 4512.05 3982.76 141.25 o 0 2 1 45474.87 41715.14 828.68 o 1 2 1 2260.94 1739.78 353.01 o 2 2 1 3399.91 3542.25 51.83 o 3 2 1 125.30 121.13 21.88 o 4 2 1 35294.61 40003.81 667.88 o 5 2 1 526.04 555.18 50.91 o 6 2 1 16502.76 17376.18 256.45 o 7 2 1 347.26 375.03 48.11 o 8 2 1 5568.17 5711.78 167.35 o 9 2 1 49.46 3.16 53.13 o 10 2 1 39.70 83.81 56.42 o 11 2 1 57.81 93.77 62.09 o -11 3 1 501.74 410.68 115.63 o -10 3 1 692.50 742.91 102.80 o -9 3 1 1702.33 1606.97 102.00 o -8 3 1 43.93 -0.05 51.64 o -7 3 1 3096.90 3293.61 115.61 o -6 3 1 1846.78 2133.55 125.42 o -5 3 1 1142.92 1186.62 53.30 o -4 3 1 16845.27 18205.43 228.20 o -3 3 1 75.55 89.66 21.58 o -2 3 1 20027.30 19233.32 620.71 o -1 3 1 5308.66 5200.75 172.60 o 0 3 1 29320.26 27592.25 724.29 o 1 3 1 314.73 236.14 44.26 o 2 3 1 1484.67 1581.08 66.75 o 3 3 1 494.55 442.65 28.54 o 4 3 1 8.12 28.33 37.06 o 5 3 1 3990.18 4328.31 112.97 o 6 3 1 1494.61 1544.72 81.58 o 7 3 1 2075.69 2100.96 84.46 o 8 3 1 1654.31 1712.67 100.36 o 9 3 1 1079.43 1125.06 92.62 o 10 3 1 2801.36 2802.96 135.36 o 11 3 1 136.41 155.41 74.99 o -11 4 1 1050.08 929.22 113.23 o -10 4 1 346.43 292.16 83.48 o -9 4 1 3159.52 3171.96 165.38 o -8 4 1 2115.49 1919.26 104.25 o -7 4 1 2073.06 2010.20 82.66 o -6 4 1 5831.30 6157.67 169.47 o -5 4 1 2786.83 2890.89 86.03 o -4 4 1 7406.20 7432.73 120.47 o -3 4 1 2631.01 2740.40 74.61 o -2 4 1 3631.45 3165.43 120.61 o -1 4 1 168.94 175.37 13.24 o 0 4 1 5675.72 5632.81 135.12 o 1 4 1 1266.65 934.41 184.04 o 2 4 1 463.55 497.78 24.42 o 3 4 1 11115.03 11214.56 235.92 o 4 4 1 1156.94 1237.88 88.65 o 5 4 1 9227.06 10065.62 694.36 o 6 4 1 2509.31 2718.77 103.33 o 7 4 1 7294.85 7735.24 152.51 o 8 4 1 850.36 942.12 81.75 o 9 4 1 1085.16 1054.61 91.53 o 10 4 1 642.04 680.90 82.19 o 11 4 1 0.20 14.99 71.15 o -11 5 1 507.46 693.76 107.35 o -10 5 1 836.66 778.13 104.54 o -9 5 1 63.72 29.83 60.04 o -8 5 1 3227.79 3242.00 118.54 o -7 5 1 1914.46 2071.68 85.56 o -6 5 1 8192.13 7937.56 608.00 o -5 5 1 11991.82 12284.22 174.84 o -4 5 1 8034.85 8173.29 128.51 o -3 5 1 22344.52 22443.29 743.30 o -2 5 1 5349.33 5209.15 144.13 o -1 5 1 28775.91 28350.55 352.42 o 0 5 1 15959.29 16717.36 277.61 o 1 5 1 4455.37 3414.45 846.03 o 2 5 1 277.78 345.75 25.54 o 3 5 1 1441.25 1591.13 46.98 o 4 5 1 1526.08 1565.42 78.58 o 5 5 1 580.03 665.62 63.27 o 6 5 1 5924.28 5915.79 147.45 o 7 5 1 2600.52 2620.98 95.48 o 8 5 1 2038.46 2239.42 95.34 o 9 5 1 5071.39 5086.56 172.52 o 10 5 1 1682.31 1682.27 113.14 o 11 5 1 1958.53 1977.94 148.18 o -11 6 1 538.69 466.30 126.29 o -10 6 1 407.52 548.52 92.33 o -9 6 1 2863.56 2718.46 155.31 o -8 6 1 373.20 488.51 59.05 o -7 6 1 5303.68 5670.93 149.22 o -6 6 1 1090.18 1124.38 101.55 o -5 6 1 4026.83 3774.31 100.13 o -4 6 1 503.18 573.84 43.04 o -3 6 1 12906.01 12438.00 296.24 o -2 6 1 986.99 1141.73 37.39 o -1 6 1 699.03 829.24 33.30 o 0 6 1 7599.35 7485.18 303.03 o 1 6 1 124.81 80.88 47.60 o 2 6 1 3454.67 3437.94 62.28 o 3 6 1 4147.17 4133.63 150.19 o 4 6 1 3939.87 4057.93 119.67 o 5 6 1 2828.86 2971.33 114.46 o 6 6 1 1098.56 1103.07 86.12 o 7 6 1 3553.74 3885.39 114.81 o 8 6 1 1064.97 1107.02 75.12 o 9 6 1 1258.19 980.32 155.67 o 10 6 1 80.32 34.44 70.59 o 11 6 1 182.03 183.17 82.11 o -11 7 1 0.36 -21.83 72.62 o -10 7 1 46.58 1.17 67.92 o -9 7 1 1262.54 1255.01 116.54 o -8 7 1 1139.86 1085.65 84.69 o -7 7 1 2461.85 2404.25 93.31 o -6 7 1 7577.49 7484.77 304.17 o -5 7 1 12217.00 12507.49 181.49 o -4 7 1 20688.75 20316.68 658.07 o -3 7 1 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195.88 185.05 35.74 o -4 6 2 23046.25 22557.62 711.66 o -3 6 2 1233.85 1117.65 64.83 o -2 6 2 44714.68 45206.12 1117.79 o -1 6 2 4.70 8.57 14.08 o 0 6 2 37840.68 39442.53 1036.54 o 1 6 2 487.42 462.14 26.28 o 2 6 2 25667.16 26494.40 895.14 o 3 6 2 409.85 350.68 34.41 o 4 6 2 2920.67 2981.28 78.33 o 5 6 2 206.93 229.13 44.71 o 6 6 2 785.66 788.04 79.96 o 7 6 2 1284.86 1262.97 86.88 o 8 6 2 977.36 1003.97 72.60 o 9 6 2 276.22 278.99 68.48 o 10 6 2 4096.09 4033.68 164.60 o 11 6 2 147.28 177.33 81.87 o -11 7 2 602.84 471.19 98.31 o -10 7 2 231.38 191.93 77.66 o -9 7 2 416.23 425.58 82.38 o -8 7 2 136.05 144.05 52.20 o -7 7 2 46.43 -1.61 48.32 o -6 7 2 90.92 74.92 41.23 o -5 7 2 1445.52 1504.73 80.24 o -4 7 2 1154.94 1019.55 49.57 o -3 7 2 10486.91 10427.57 274.25 o -2 7 2 14594.48 15685.48 273.00 o -1 7 2 23049.36 23812.47 413.60 o 0 7 2 7434.06 7825.83 191.87 o 1 7 2 18167.60 19272.44 492.85 o 2 7 2 1667.48 1752.70 52.85 o 3 7 2 7728.17 7608.60 382.15 o 4 7 2 2605.64 2724.62 103.06 o 5 7 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4019.14 4107.69 163.05 o -6 9 2 1945.48 1834.35 108.33 o -5 9 2 380.63 351.63 39.09 o -4 9 2 5575.48 5606.41 105.50 o -3 9 2 341.40 360.93 31.83 o -2 9 2 10850.00 10984.47 208.16 o -1 9 2 3349.57 3444.36 73.89 o 0 9 2 10703.57 11409.56 232.64 o 1 9 2 16916.44 18233.35 525.08 o 2 9 2 3434.84 3176.71 76.11 o 3 9 2 13419.10 13645.41 392.85 o 4 9 2 625.84 622.28 42.52 o 5 9 2 4413.99 4368.54 170.75 o 6 9 2 360.95 404.56 70.53 o 7 9 2 2255.10 2313.52 191.62 o 8 9 2 1040.42 1030.19 76.97 o 9 9 2 10.58 100.35 64.31 o 10 9 2 1269.44 1339.39 128.40 o 11 9 2 84.00 187.48 87.66 o -11 10 2 122.54 187.02 87.67 o -10 10 2 234.39 225.03 81.40 o -9 10 2 290.23 342.75 145.92 o -8 10 2 734.32 604.64 82.18 o -7 10 2 202.67 179.67 63.21 o -6 10 2 3074.51 3137.58 137.96 o -5 10 2 1862.51 1883.07 72.18 o -4 10 2 21553.18 22009.76 220.79 o -3 10 2 174.06 250.54 28.76 o -2 10 2 25309.90 25034.14 409.23 o -1 10 2 1691.96 1726.13 57.78 o 0 10 2 22552.19 24316.11 495.80 o 1 10 2 1426.02 1257.27 52.74 o 2 10 2 5117.76 5216.48 119.84 o 3 10 2 1390.85 1441.34 57.08 o 4 10 2 672.73 763.37 45.78 o 5 10 2 2923.59 2834.00 84.17 o 6 10 2 1555.25 1459.32 105.02 o 7 10 2 1112.39 1130.06 102.97 o 8 10 2 1873.52 1968.32 111.78 o 9 10 2 842.02 844.61 88.20 o 10 10 2 1897.37 1955.26 151.13 o 11 10 2 349.15 359.03 99.25 o -11 11 2 98.47 103.76 87.15 o -10 11 2 3119.11 3097.37 184.87 o -9 11 2 690.47 663.41 82.98 o -8 11 2 4051.51 3913.88 174.09 o -7 11 2 988.57 1078.30 96.53 o -6 11 2 3630.01 3513.34 148.76 o -5 11 2 1416.09 1470.90 67.07 o -4 11 2 1782.89 1736.22 65.90 o -3 11 2 4087.34 3843.56 85.22 o -2 11 2 2485.17 2670.01 72.01 o -1 11 2 315.97 266.50 32.75 o 0 11 2 9264.78 9271.71 150.69 o 1 11 2 14.11 18.13 26.93 o 2 11 2 15418.74 15554.70 415.11 o 3 11 2 652.67 688.25 45.43 o 4 11 2 12459.37 12323.29 239.55 o 5 11 2 897.05 896.59 80.84 o 6 11 2 6215.55 6351.53 197.72 o 7 11 2 1022.18 1146.91 137.13 o 8 11 2 1607.64 1568.89 122.23 o 9 11 2 1298.81 1035.18 206.97 o 10 11 2 48.03 89.40 76.32 o 11 11 2 507.77 394.02 127.21 o -10 12 2 204.68 131.24 78.68 o -9 12 2 13.57 20.08 54.67 o -8 12 2 1243.23 1120.21 104.81 o -7 12 2 1359.82 1400.27 109.37 o -6 12 2 2618.79 2362.68 129.05 o -5 12 2 2867.23 2788.90 131.12 o -4 12 2 3822.95 3775.47 97.39 o -3 12 2 7308.79 7384.89 123.08 o -2 12 2 6897.85 7192.40 155.68 o -1 12 2 5742.54 5674.95 107.88 o 0 12 2 8.77 5.03 26.24 o 1 12 2 7098.59 7120.95 122.60 o 2 12 2 1295.23 1207.48 205.87 o 3 12 2 41.37 20.36 29.06 o 4 12 2 8871.57 8375.16 138.85 o 5 12 2 116.55 91.63 54.13 o 6 12 2 4136.61 3883.91 159.14 o 7 12 2 1288.53 1297.50 107.60 o 8 12 2 2119.83 2256.16 120.71 o 9 12 2 597.90 667.89 83.04 o 10 12 2 930.08 1069.75 123.06 o -10 13 2 625.35 652.22 107.32 o -9 13 2 2832.51 3145.35 168.88 o -8 13 2 1977.80 1912.43 131.87 o -7 13 2 4815.82 4901.93 189.57 o -6 13 2 1907.11 1838.21 118.56 o -5 13 2 1623.53 1635.94 108.12 o -4 13 2 1666.13 1731.85 71.82 o -3 13 2 88.05 78.63 28.37 o -2 13 2 143.84 135.46 29.88 o -1 13 2 4239.03 4218.36 97.61 o 0 13 2 107.93 121.56 31.13 o 1 13 2 10675.06 10923.07 187.77 o 2 13 2 1958.24 1733.09 395.23 o 3 13 2 11575.16 11468.89 166.00 o 4 13 2 2659.76 2614.14 83.61 o 5 13 2 9604.52 9505.41 232.80 o 6 13 2 1904.80 1917.21 120.30 o 7 13 2 3161.62 3184.33 133.31 o 8 13 2 1642.93 1541.40 104.24 o 9 13 2 1078.91 1150.57 116.29 o 10 13 2 342.80 350.09 91.29 o -10 14 2 20.39 61.25 79.56 o -9 14 2 729.25 723.61 98.19 o -8 14 2 406.13 438.37 83.33 o -7 14 2 2067.57 1891.44 126.15 o -6 14 2 1.27 67.96 55.28 o -5 14 2 5517.62 5384.94 184.80 o -4 14 2 121.95 132.60 36.94 o -3 14 2 5050.85 5064.13 162.17 o -2 14 2 42.58 82.61 28.93 o -1 14 2 3216.93 3182.39 88.82 o 0 14 2 17.13 8.86 27.88 o 1 14 2 1694.83 1629.02 81.57 o 2 14 2 30.47 34.04 23.97 o 3 14 2 5681.44 5633.97 180.63 o 4 14 2 6.64 -26.12 32.77 o 5 14 2 7779.72 7828.86 250.95 o 6 14 2 367.06 414.30 72.87 o 7 14 2 4656.53 4665.00 160.98 o 8 14 2 88.07 76.18 62.52 o 9 14 2 2340.70 2341.74 156.24 o 10 14 2 46.53 112.72 82.09 o -10 15 2 2167.45 2143.11 170.29 o -9 15 2 1759.79 1804.89 137.74 o -8 15 2 3972.74 4168.62 192.29 o -7 15 2 2093.38 1936.22 129.73 o -6 15 2 3725.09 3772.15 167.01 o -5 15 2 1777.41 1534.04 108.95 o -4 15 2 2384.85 2332.62 87.87 o -3 15 2 150.30 175.15 35.20 o -2 15 2 58.76 68.85 31.84 o -1 15 2 66.25 68.48 30.72 o 0 15 2 1333.32 1284.73 62.89 o 1 15 2 3174.85 3226.81 93.55 o 2 15 2 6746.26 5409.32 994.69 o 3 15 2 3315.63 3276.25 144.85 o 4 15 2 6363.98 6235.27 133.61 o 5 15 2 4481.72 4117.35 160.88 o 6 15 2 3471.34 3639.90 175.40 o 7 15 2 2325.24 2193.13 115.83 o 8 15 2 2101.27 2264.73 148.36 o 9 15 2 270.55 197.85 74.54 o 10 15 2 318.93 368.43 99.83 o -10 16 2 206.01 245.48 94.10 o -9 16 2 24.47 89.76 67.39 o -8 16 2 672.82 791.42 99.94 o -7 16 2 74.09 162.00 65.54 o -6 16 2 2908.52 2985.72 154.24 o -5 16 2 1502.43 1422.64 109.28 o -4 16 2 3694.33 3537.45 108.48 o -3 16 2 2237.31 2171.92 81.93 o -2 16 2 2321.90 2215.37 82.21 o -1 16 2 4844.91 4555.32 112.74 o 0 16 2 4.22 10.90 31.04 o 1 16 2 2520.44 2291.48 125.25 o 2 16 2 1000.27 857.42 85.60 o 3 16 2 2194.40 2134.51 84.67 o 4 16 2 5639.61 5286.74 193.14 o 5 16 2 676.74 681.82 71.07 o 6 16 2 3184.05 3389.78 135.38 o 7 16 2 66.57 107.00 52.73 o 8 16 2 3640.28 3598.61 187.03 o 9 16 2 65.38 191.73 85.38 o 10 16 2 1657.56 1885.70 208.82 o -9 17 2 1617.62 1803.63 142.65 o -8 17 2 1458.11 1433.85 123.99 o -7 17 2 2808.93 2754.92 155.93 o -6 17 2 481.54 539.26 81.93 o -5 17 2 4341.16 4263.38 176.47 o -4 17 2 14.45 -7.63 40.23 o -3 17 2 2146.45 2166.74 75.32 o -2 17 2 1388.63 1335.35 68.78 o -1 17 2 433.85 607.71 52.13 o 0 17 2 3965.35 3721.53 121.80 o 1 17 2 681.18 675.69 54.16 o 2 17 2 5666.25 5164.28 198.41 o 3 17 2 752.47 809.69 59.59 o 4 17 2 5832.65 5564.32 133.76 o 5 17 2 2488.55 2468.00 151.87 o 6 17 2 2300.77 2094.11 110.65 o 7 17 2 1180.04 1407.61 119.09 o 8 17 2 609.18 585.09 94.01 o 9 17 2 686.43 706.53 103.39 o -9 18 2 120.95 181.41 72.58 o -8 18 2 81.45 72.26 63.88 o -7 18 2 579.35 525.03 84.13 o -6 18 2 1302.17 1143.18 106.77 o -5 18 2 2416.28 2322.39 137.50 o -4 18 2 3574.49 3244.91 150.42 o -3 18 2 3045.28 3028.49 90.24 o -2 18 2 9264.07 9056.92 168.02 o -1 18 2 1720.43 1672.72 78.13 o 0 18 2 4463.37 4373.78 118.52 o 1 18 2 16.08 39.86 36.69 o 2 18 2 5745.00 5689.89 134.66 o 3 18 2 852.76 886.71 63.33 o 4 18 2 1562.97 1610.85 93.80 o 5 18 2 1240.95 1281.18 80.37 o 6 18 2 54.08 38.16 46.58 o 7 18 2 2065.65 2234.95 147.74 o 8 18 2 113.79 106.37 71.69 o 9 18 2 1256.98 1406.59 135.08 o -9 19 2 456.86 515.60 95.34 o -8 19 2 459.06 496.28 87.85 o -7 19 2 207.80 281.01 72.00 o -6 19 2 972.85 942.16 101.36 o -5 19 2 88.41 84.50 54.85 o -4 19 2 1118.25 1129.43 88.93 o -3 19 2 1934.62 1755.97 87.50 o -2 19 2 783.28 852.90 57.11 o -1 19 2 4043.98 3912.36 131.25 o 0 19 2 276.37 291.47 47.14 o 1 19 2 5809.73 5830.85 199.85 o 2 19 2 105.59 96.22 40.39 o 3 19 2 3919.27 3887.53 117.14 o 4 19 2 2.44 66.74 44.49 o 5 19 2 2454.99 2493.39 106.96 o 6 19 2 179.34 217.16 55.00 o 7 19 2 394.28 388.99 80.31 o 8 19 2 224.74 330.17 82.85 o 9 19 2 45.27 82.56 75.25 o -9 20 2 3.93 -70.68 70.68 o -8 20 2 1.23 6.52 63.15 o -7 20 2 905.26 845.12 101.59 o -6 20 2 722.70 823.27 97.74 o -5 20 2 5322.16 5324.83 207.35 o -4 20 2 1347.62 1300.79 94.75 o -3 20 2 7061.00 6934.42 163.55 o -2 20 2 2981.57 2854.51 93.31 o -1 20 2 8555.19 8310.81 154.01 o 0 20 2 141.60 212.68 43.94 o 1 20 2 4468.11 4418.97 125.37 o 2 20 2 18.23 16.42 37.37 o 3 20 2 808.25 700.25 59.72 o 4 20 2 371.87 398.16 53.95 o 5 20 2 12.44 2.61 39.37 o 6 20 2 399.50 491.60 83.48 o 7 20 2 427.30 509.74 88.11 o 8 20 2 434.26 448.37 92.19 o 9 20 2 1057.64 1109.61 131.50 o -8 21 2 135.79 110.56 70.00 o -7 21 2 49.45 77.83 59.30 o -6 21 2 29.96 -15.91 57.74 o -5 21 2 192.34 142.31 60.11 o -4 21 2 474.60 461.17 66.35 o -3 21 2 166.86 132.53 48.45 o -2 21 2 2411.50 2373.54 88.65 o -1 21 2 259.22 196.36 46.51 o 0 21 2 3978.17 3952.45 111.52 o 1 21 2 400.19 410.66 48.17 o 2 21 2 1704.01 1717.68 77.97 o 3 21 2 714.94 679.05 56.35 o 4 21 2 1652.19 1689.00 89.80 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