#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/37/2213746.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2213746_Fobs
loop_
_publ_author_name
'Ali, Basem Fares'
'Al-Far, Rawhi'
'Haddad, Salim'
_publ_section_title
;
 A lead--halide ladder complex:
 <i>catena</i>-poly[bis(2,3-dimethylquinoxalinium)
 [[di-\m~2~-bromido-bis[dibromoplumbate(II)]]-di-\m~2~-bromido]]
;
_journal_coeditor_code           DN2167
_journal_issue                   6
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m1569
_journal_volume                  63
_journal_year                    2007
_space_group_IT_number           12
_symmetry_space_group_name_Hall  '-C 2y'
_symmetry_space_group_name_H-M   'C 1 2/m 1'
_cell_angle_alpha                90.000
_cell_angle_beta                 101.830
_cell_angle_gamma                90.000
_cell_length_a                   9.4180
_cell_length_b                   28.1410
_cell_length_c                   6.0290
_exptl_crystal_F_000             1232.00
_reflns_d_resolution_high        0.8333
_[local]_cod_data_source_file    dn2167Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' rawhi in C2/m'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            564.14
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x, -y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 39911.02 44914.46 3322.07 o
4 0 0 317307.31 352463.13 15667.18 o
6 0 0 1045.03 1163.75 744.49 o
8 0 0 67216.30 72207.25 7192.53 o
10 0 0 4715.79 4409.61 2508.57 o
3 1 0 59744.64 70465.87 3538.24 o
5 1 0 139367.17 157246.02 7784.19 o
7 1 0 11827.57 12401.17 1767.15 o
9 1 0 45331.32 29637.21 6488.14 o
11 1 0 1134.44 880.91 957.47 o
2 2 0 14005.87 15886.84 969.69 o
4 2 0 35235.73 41513.64 2362.86 o
6 2 0 20583.12 22697.65 2434.26 o
8 2 0 10936.15 10060.56 2143.74 o
10 2 0 7343.20 6793.14 2234.21 o
1 3 0 7664.78 7987.67 487.29 o
3 3 0 1150.99 2564.49 901.87 o
5 3 0 193.13 399.23 266.79 o
7 3 0 48.34 655.55 1140.23 o
9 3 0 122.36 509.53 578.84 o
11 3 0 320.52 442.08 634.56 o
2 4 0 12806.25 14260.03 1006.66 o
4 4 0 36009.67 39339.78 2461.99 o
6 4 0 2759.91 3133.10 763.70 o
8 4 0 12784.71 13273.70 2602.99 o
10 4 0 339.76 441.42 412.16 o
1 5 0 79112.60 78301.22 4150.46 o
3 5 0 109683.29 126665.63 6470.46 o
5 5 0 23776.94 26116.52 2138.45 o
7 5 0 54174.97 51994.95 4755.53 o
9 5 0 4021.05 4425.37 1408.21 o
4 6 0 5668.30 7357.77 817.83 o
6 6 0 140599.22 146440.53 13693.17 o
8 6 0 6928.56 6925.35 1709.51 o
10 6 0 25602.17 24251.82 5345.56 o
1 7 0 101611.34 89486.30 5513.99 o
3 7 0 158318.11 182221.27 9487.02 o
5 7 0 19319.84 25254.30 2621.73 o
7 7 0 79484.05 66601.29 9628.00 o
9 7 0 1588.01 995.40 799.00 o
0 8 0 7919.28 4680.48 1040.94 o
2 8 0 115271.84 125017.12 6087.46 o
4 8 0 6683.56 6917.00 584.87 o
6 8 0 42285.41 41763.09 3960.57 o
8 8 0 5121.85 4228.69 1069.02 o
10 8 0 7942.31 7575.57 2555.60 o
1 9 0 580.44 528.06 504.20 o
3 9 0 3178.67 3560.33 462.73 o
5 9 0 2646.70 2596.66 440.57 o
7 9 0 1227.78 2078.32 821.41 o
9 9 0 479.76 592.70 933.79 o
2 10 0 42787.87 43646.18 2540.62 o
4 10 0 3347.92 3593.84 500.09 o
6 10 0 22169.76 23390.06 2649.22 o
8 10 0 158.32 1176.45 3991.35 o
10 10 0 2162.76 1060.12 907.23 o
3 11 0 24486.36 23642.08 1740.28 o
5 11 0 33348.26 35860.15 3723.64 o
7 11 0 7672.29 6899.36 1207.23 o
9 11 0 16625.86 16834.99 3585.72 o
0 12 0 237238.11 236175.08 25457.30 o
2 12 0 7093.19 6570.88 713.26 o
4 12 0 117941.02 119655.09 9233.81 o
6 12 0 7537.44 6023.33 1456.07 o
8 12 0 35954.45 34149.29 4393.74 o
10 12 0 8877.50 8567.19 2511.25 o
1 13 0 85109.02 72220.81 4392.26 o
3 13 0 44357.62 45463.29 2670.07 o
5 13 0 108360.66 96900.49 10014.55 o
7 13 0 4130.92 4212.84 1354.01 o
9 13 0 30084.78 28406.71 7547.20 o
0 14 0 156473.53 142997.84 12481.70 o
2 14 0 484.30 320.69 462.66 o
4 14 0 74725.61 70524.71 6055.09 o
6 14 0 636.56 816.62 1091.74 o
8 14 0 24904.41 24514.82 4823.19 o
10 14 0 2577.33 2375.42 1425.05 o
1 15 0 4100.77 2535.89 612.27 o
3 15 0 1993.85 1921.44 554.90 o
5 15 0 4509.96 4015.64 1298.45 o
7 15 0 1000.81 1054.29 875.57 o
9 15 0 2779.21 1709.42 1349.14 o
0 16 0 11498.67 10791.63 1902.08 o
2 16 0 14.65 244.78 328.33 o
4 16 0 7347.57 7042.56 1583.99 o
6 16 0 195.35 262.91 439.74 o
8 16 0 2727.37 2553.27 1442.85 o
1 17 0 22589.76 16717.73 2118.91 o
3 17 0 21190.70 24679.68 3787.27 o
5 17 0 8160.81 7274.23 1774.90 o
7 17 0 8874.58 8639.59 2062.83 o
9 17 0 2306.88 1773.98 1333.52 o
0 18 0 10732.82 10779.62 2257.57 o
2 18 0 62255.97 57195.82 4720.37 o
4 18 0 10540.79 10335.06 1607.90 o
6 18 0 25358.96 24466.57 4876.17 o
8 18 0 7952.29 6818.17 2604.74 o
1 19 0 30033.48 28666.14 3225.96 o
3 19 0 51946.67 51452.10 4481.91 o
5 19 0 5954.79 5494.48 1526.44 o
7 19 0 34749.39 36976.09 6848.94 o
9 19 0 584.64 822.36 1183.57 o
0 20 0 669.70 11352.76 3946.64 o
2 20 0 77525.44 74831.50 5649.32 o
4 20 0 131.58 274.69 446.12 o
6 20 0 37748.81 38161.27 5143.51 o
8 20 0 924.46 1348.04 1348.82 o
1 21 0 5962.26 5997.52 1672.27 o
3 21 0 7739.62 7777.60 1439.00 o
5 21 0 913.13 1236.23 1307.01 o
7 21 0 4858.73 4327.64 1843.87 o
0 22 0 382.01 508.45 1318.90 o
2 22 0 28.98 450.61 635.56 o
4 22 0 6.36 417.34 1155.12 o
6 22 0 354.59 773.47 1583.96 o
8 22 0 67.13 1097.07 2323.66 o
1 23 0 15467.80 16583.05 2748.11 o
3 23 0 5206.83 5029.04 1204.52 o
5 23 0 1765.52 1009.67 1142.13 o
7 23 0 504.48 492.69 1368.98 o
0 24 0 11515.02 13390.34 2941.23 o
2 24 0 6158.65 6124.41 1483.88 o
4 24 0 12891.47 11624.75 2023.86 o
6 24 0 8696.20 8088.62 2913.32 o
1 25 0 12702.13 15457.92 3349.40 o
3 25 0 5244.10 3868.09 1093.16 o
5 25 0 20862.31 20861.86 4949.72 o
7 25 0 1654.57 1460.42 2799.11 o
0 26 0 57460.60 73773.41 8051.40 o
2 26 0 322.82 249.70 1270.62 o
4 26 0 27104.36 25499.55 5099.98 o
6 26 0 84.48 292.57 814.55 o
1 27 0 3693.21 4949.13 1524.24 o
3 27 0 1632.98 1307.71 983.46 o
5 27 0 6959.69 6024.41 2539.70 o
0 28 0 1240.67 876.84 1494.67 o
2 28 0 73.66 131.01 827.05 o
4 28 0 919.92 378.08 916.45 o
6 28 0 14.33 528.69 1245.58 o
1 29 0 830.60 947.24 1560.55 o
3 29 0 742.74 545.71 1211.81 o
5 29 0 345.08 312.95 958.51 o
0 30 0 3852.43 4232.23 2829.02 o
2 30 0 3485.62 3603.40 2163.13 o
4 30 0 3278.50 3630.64 2441.59 o
1 31 0 3533.78 4621.74 2188.71 o
3 31 0 6714.51 6470.37 2923.35 o
2 32 0 14041.76 16446.82 4705.53 o
1 33 0 2184.14 2763.56 1876.76 o
-10 0 1 6033.22 7948.76 2825.82 o
-8 0 1 30094.38 31988.11 4817.27 o
-6 0 1 3762.80 3932.64 965.46 o
-4 0 1 191136.13 202055.92 15683.71 o
-2 0 1 9488.80 12940.09 1633.79 o
0 0 1 110861.80 63337.68 19988.01 o
2 0 1 155028.75 149188.84 17267.55 o
4 0 1 116434.52 126127.93 9177.09 o
6 0 1 2744.12 2724.41 1061.20 o
8 0 1 63251.04 65875.86 8601.24 o
10 0 1 378.94 350.69 796.34 o
-11 1 1 92.14 281.01 528.81 o
-9 1 1 34100.11 34037.75 3477.50 o
-7 1 1 463.52 555.57 417.88 o
-5 1 1 61143.71 63438.38 3547.45 o
-3 1 1 4246.50 5213.69 684.71 o
1 1 1 30509.21 33099.86 2406.06 o
3 1 1 42664.36 41562.41 3126.14 o
5 1 1 18731.91 19614.60 1667.43 o
7 1 1 1700.34 1915.65 637.54 o
9 1 1 13243.78 11566.36 2417.98 o
-10 2 1 5508.99 5641.89 1862.86 o
-8 2 1 696.15 831.01 510.28 o
-6 2 1 7020.52 7031.56 860.60 o
-4 2 1 3818.22 3849.24 558.62 o
-2 2 1 12685.07 13764.80 1022.45 o
0 2 1 38848.02 37951.78 5072.19 o
2 2 1 21474.46 21115.45 1331.86 o
4 2 1 22434.58 23671.02 1446.56 o
6 2 1 2541.50 2903.28 754.07 o
8 2 1 3413.19 3051.72 825.29 o
10 2 1 1004.55 707.13 595.26 o
-11 3 1 1627.96 1347.31 930.11 o
-9 3 1 337.42 443.06 471.84 o
-7 3 1 4095.36 3914.76 960.89 o
-5 3 1 340.09 486.52 239.35 o
-3 3 1 5797.05 6032.86 483.58 o
-1 3 1 10.78 386.79 165.29 o
1 3 1 844.44 1282.27 232.23 o
3 3 1 307.35 389.22 212.11 o
5 3 1 339.13 574.20 281.73 o
7 3 1 1060.45 962.60 660.35 o
9 3 1 478.87 331.72 536.27 o
-10 4 1 200.02 334.12 461.23 o
-8 4 1 8478.37 8814.09 1456.21 o
-6 4 1 589.16 788.99 422.98 o
-4 4 1 14754.04 15842.35 1302.72 o
-2 4 1 1341.11 1509.94 275.71 o
0 4 1 10874.18 9877.52 1397.74 o
2 4 1 406.91 566.69 229.30 o
4 4 1 6287.58 10063.75 2899.59 o
6 4 1 119.72 317.00 408.50 o
8 4 1 3418.71 3569.02 974.73 o
10 4 1 79.12 320.97 671.91 o
-11 5 1 8183.90 6906.61 2206.51 o
-9 5 1 255.83 530.57 457.06 o
-7 5 1 26047.24 26585.82 2591.14 o
-5 5 1 126.25 1069.03 1546.11 o
-3 5 1 43536.09 45569.90 2761.12 o
-1 5 1 1877.46 1828.68 333.75 o
1 5 1 34351.45 32982.70 2136.29 o
3 5 1 12525.39 13914.05 1028.03 o
5 5 1 5197.04 5552.54 900.91 o
7 5 1 12904.76 12088.99 1729.84 o
9 5 1 702.19 728.26 721.49 o
-10 6 1 8684.45 7647.31 2243.75 o
-8 6 1 3925.68 4219.03 998.84 o
-6 6 1 48454.70 50071.32 4467.75 o
-4 6 1 343.31 819.71 573.51 o
-2 6 1 170343.14 207543.56 14374.69 o
0 6 1 23231.18 21495.59 2252.25 o
2 6 1 156599.64 151224.95 11119.04 o
4 6 1 9839.49 10054.22 1057.20 o
6 6 1 77217.82 85322.16 8825.25 o
8 6 1 285.31 389.49 329.71 o
10 6 1 18271.21 18585.04 4476.08 o
-11 7 1 21266.27 19746.25 4071.65 o
-9 7 1 221.14 488.82 574.51 o
-7 7 1 72339.94 75934.03 7249.17 o
-5 7 1 632.54 1808.56 3000.21 o
-3 7 1 102481.76 106141.09 5044.70 o
-1 7 1 300.15 701.88 332.96 o
1 7 1 61530.01 60481.30 3782.23 o
3 7 1 14597.57 15935.15 1350.74 o
5 7 1 10641.86 10570.89 1657.13 o
7 7 1 22781.13 22239.77 3053.24 o
9 7 1 1199.37 1367.64 874.70 o
-10 8 1 4235.95 3497.83 1534.33 o
-8 8 1 6100.80 6100.57 1353.90 o
-6 8 1 17264.64 15863.53 1960.06 o
-4 8 1 4701.81 4648.37 527.83 o
-2 8 1 56368.77 56520.43 2926.26 o
0 8 1 769.00 674.85 313.72 o
2 8 1 65599.13 62237.82 3512.79 o
4 8 1 564.81 575.09 391.70 o
6 8 1 28965.18 30837.48 3926.62 o
8 8 1 482.24 606.31 614.48 o
10 8 1 7213.60 6504.21 2356.51 o
-9 9 1 3730.59 4177.46 1150.79 o
-7 9 1 2211.12 2452.67 750.85 o
-5 9 1 3711.40 3529.68 563.47 o
-3 9 1 3849.28 3973.03 491.55 o
-1 9 1 6209.76 5538.89 608.83 o
1 9 1 15233.46 15027.64 1304.97 o
3 9 1 5497.75 6690.84 773.67 o
5 9 1 3272.03 3761.50 932.82 o
7 9 1 1407.50 2749.69 1157.33 o
9 9 1 1162.51 1373.81 1047.46 o
-10 10 1 5927.88 5205.41 1897.80 o
-8 10 1 636.78 357.33 375.68 o
-6 10 1 6801.38 6401.55 1248.53 o
-4 10 1 17943.96 18350.03 1319.81 o
-2 10 1 704.99 6463.21 5685.63 o
0 10 1 12667.46 10405.51 1048.51 o
2 10 1 6642.46 6147.12 667.88 o
4 10 1 6510.16 6326.60 1121.71 o
6 10 1 535.55 963.71 895.38 o
8 10 1 1569.02 1624.20 834.41 o
10 10 1 1748.46 961.37 884.48 o
-9 11 1 2481.82 1863.53 1155.47 o
-7 11 1 220.95 229.14 223.04 o
-5 11 1 12817.01 11793.43 1465.93 o
-3 11 1 3749.60 4094.77 536.03 o
-1 11 1 15793.06 13918.81 1209.35 o
1 11 1 2297.64 2423.18 461.76 o
3 11 1 3490.37 3156.29 512.83 o
5 11 1 8743.55 10104.39 1809.27 o
7 11 1 1401.24 2372.85 1203.93 o
9 11 1 4669.37 5129.03 2009.32 o
-10 12 1 3946.92 3775.76 1601.23 o
-8 12 1 6581.26 6246.79 1418.01 o
-6 12 1 2812.49 2578.64 822.27 o
-4 12 1 51701.56 51183.47 3740.68 o
-2 12 1 668.60 608.17 372.42 o
0 12 1 98321.61 83655.83 4808.30 o
2 12 1 2058.36 1648.08 503.70 o
4 12 1 69746.63 73507.06 6719.02 o
6 12 1 107.60 208.52 542.74 o
8 12 1 22666.33 21665.46 4342.01 o
-9 13 1 50741.84 44238.36 10748.11 o
-7 13 1 146.05 322.96 318.01 o
-5 13 1 71256.49 70312.91 5394.75 o
-3 13 1 2667.29 2274.31 479.84 o
-1 13 1 54686.84 48562.73 3080.20 o
1 13 1 9676.75 9869.66 1039.85 o
3 13 1 25230.40 23896.02 2396.86 o
5 13 1 14344.24 18178.24 2472.44 o
7 13 1 1359.09 1400.13 902.44 o
9 13 1 16435.45 15765.98 4364.55 o
-10 14 1 2762.74 2485.92 1789.51 o
-8 14 1 11188.51 11076.47 2251.84 o
-6 14 1 3138.30 3048.97 976.27 o
-4 14 1 59708.25 53222.82 4832.97 o
-2 14 1 1487.75 1370.40 614.89 o
0 14 1 88161.41 80231.74 4668.85 o
2 14 1 1134.00 583.91 392.19 o
4 14 1 66713.82 72347.59 6286.08 o
6 14 1 126.64 435.08 707.80 o
8 14 1 24329.44 21783.70 5030.25 o
-9 15 1 2897.72 3050.62 1999.19 o
-7 15 1 1957.76 2662.02 1413.21 o
-5 15 1 12865.39 12064.57 1840.91 o
-3 15 1 5471.13 4806.24 722.11 o
-1 15 1 23255.71 20923.21 1831.73 o
1 15 1 8245.15 7091.86 866.21 o
3 15 1 14070.46 14860.67 2076.79 o
5 15 1 5777.02 6458.12 1774.60 o
7 15 1 3875.38 3157.90 1291.58 o
9 15 1 2310.54 1777.25 1441.38 o
-8 16 1 560.13 696.21 1018.84 o
-6 16 1 5764.18 4550.95 1318.80 o
-4 16 1 739.42 516.71 523.51 o
-2 16 1 10855.73 9872.00 1308.83 o
0 16 1 153.88 45.37 119.57 o
2 16 1 8223.86 8786.84 1139.90 o
4 16 1 68.23 340.64 543.56 o
6 16 1 2589.16 2953.06 1240.68 o
8 16 1 105.37 219.27 531.58 o
-9 17 1 1080.72 1049.29 898.17 o
-7 17 1 1049.55 1186.17 963.28 o
-5 17 1 617.06 832.16 1103.09 o
-3 17 1 1941.55 1666.38 636.94 o
-1 17 1 478.02 481.60 606.69 o
1 17 1 595.80 384.14 550.13 o
3 17 1 887.38 645.97 592.24 o
5 17 1 241.22 378.32 678.57 o
7 17 1 1776.27 2217.79 1204.85 o
9 17 1 166.81 358.83 967.36 o
-8 18 1 5472.62 5325.30 2230.48 o
-6 18 1 6160.75 5401.47 1817.48 o
-4 18 1 3429.86 3039.50 1050.54 o
-2 18 1 22462.91 19321.97 2492.40 o
0 18 1 1132.96 1624.70 1264.23 o
2 18 1 28639.78 28240.71 2534.67 o
4 18 1 621.34 559.48 831.65 o
6 18 1 13911.26 13706.07 3307.75 o
8 18 1 1049.96 689.18 1000.74 o
-9 19 1 75.19 376.62 827.15 o
-7 19 1 35458.38 35835.43 6652.41 o
-5 19 1 205.21 348.52 505.90 o
-3 19 1 49041.51 49665.78 4735.08 o
-1 19 1 2493.54 2476.25 981.04 o
1 19 1 27933.08 27791.19 2596.75 o
3 19 1 12613.38 13689.61 1734.80 o
5 19 1 6172.89 7411.99 2265.26 o
7 19 1 14819.53 15996.84 4213.12 o
-8 20 1 2960.82 2538.40 1772.82 o
-6 20 1 22876.69 20019.90 3444.05 o
-4 20 1 639.59 841.61 937.76 o
-2 20 1 60859.43 61278.97 5725.86 o
0 20 1 105.30 321.23 864.89 o
2 20 1 74751.73 75414.81 5619.02 o
4 20 1 135.87 361.43 591.61 o
6 20 1 33664.80 38304.27 7008.76 o
8 20 1 51.04 200.08 602.97 o
-7 21 1 11898.22 11569.14 3392.73 o
-5 21 1 2083.95 1929.40 1224.94 o
-3 21 1 22658.49 20386.55 2809.99 o
-1 21 1 3317.31 3719.60 1593.65 o
1 21 1 15177.36 14743.41 2203.94 o
3 21 1 4215.64 4819.98 1240.58 o
5 21 1 6473.51 6618.44 1996.65 o
7 21 1 4727.50 4708.37 2280.40 o
-8 22 1 1825.79 1777.14 1734.72 o
-6 22 1 379.56 333.10 818.23 o
-4 22 1 5779.15 4598.70 901.93 o
-2 22 1 1450.83 1959.83 1320.69 o
0 22 1 2916.35 4043.81 1738.00 o
2 22 1 524.47 196.70 431.22 o
4 22 1 1678.55 1776.40 874.12 o
6 22 1 1160.52 1145.51 1467.44 o
-7 23 1 557.02 773.49 2021.48 o
-5 23 1 916.76 959.94 2403.86 o
-1 23 1 64.65 366.88 1554.52 o
1 23 1 2012.63 1728.42 967.50 o
3 23 1 1132.06 878.75 785.28 o
5 23 1 88.66 557.32 1325.27 o
7 23 1 392.29 706.64 1222.85 o
-6 24 1 3307.92 3237.56 2044.40 o
-4 24 1 1171.40 2102.68 2087.75 o
-2 24 1 2175.29 2347.26 1211.38 o
0 24 1 8335.55 9542.00 2584.20 o
2 24 1 4028.33 4773.06 1248.70 o
4 24 1 6086.64 8744.36 1880.37 o
6 24 1 851.15 1479.47 1787.80 o
-7 25 1 114.87 532.89 1343.65 o
-5 25 1 17141.20 15826.72 4159.10 o
-3 25 1 1021.04 1047.50 1314.56 o
-1 25 1 21080.16 27560.29 5145.51 o
1 25 1 8758.14 9702.52 1950.38 o
3 25 1 10047.95 10745.73 2370.45 o
5 25 1 9896.35 10539.16 3517.92 o
-6 26 1 3185.23 2468.84 1933.67 o
-4 26 1 27762.16 23343.80 4818.00 o
-2 26 1 604.77 417.42 1974.96 o
0 26 1 30353.68 46583.17 5331.88 o
4 26 1 24912.72 26317.20 5359.16 o
6 26 1 149.96 398.31 1008.10 o
-5 27 1 12121.63 12194.99 3921.60 o
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