#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/38/2213814.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213814_Fobs loop_ _publ_author_name 'Wisser, Barbara' 'Janiak, Christoph' _publ_section_title ; 5,5'-Diamino-2,2'-bipyridin-1,1'-diium bis(5,5'-diamino-2,2'-bipyridin-1-ium) tetrakis(rac-1,1'-binaphthalene-2,2'-diyl phosphate) hexahydrate: a two-dimensional supramolecular hydrogen-bonded network ; _journal_coeditor_code HG2222 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2871 _journal_page_last o2872 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 82.940 _cell_angle_beta 76.232 _cell_angle_gamma 85.571 _cell_length_a 9.7001 _cell_length_b 14.1020 _cell_length_c 18.2440 _exptl_crystal_F_000 1073.83 _reflns_d_resolution_high 0.8331 _[local]_cod_data_source_file hg2222Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' barbp.ins in P-1 P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 201.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 36.61 9.28 6.89 o 6 0 0 10.49 15.30 22.32 o 7 0 0 126.96 28.69 30.44 o 8 0 0 249.65 264.10 66.73 o 9 0 0 314.09 317.86 36.14 o 10 0 0 8.22 21.89 21.62 o 11 0 0 138.38 204.70 37.11 o -11 1 0 169.17 137.41 33.30 o -10 1 0 333.95 361.34 45.46 o -9 1 0 386.21 473.96 48.99 o -8 1 0 92.00 120.96 23.24 o -7 1 0 241.54 227.03 32.20 o -6 1 0 4.53 0.91 10.37 o -4 1 0 204.65 223.06 22.44 o 0 1 0 402.07 339.30 20.13 o 1 1 0 6212.23 6018.99 395.39 o 2 1 0 5476.56 5406.02 361.15 o 5 1 0 0.60 17.62 18.36 o 6 1 0 3.65 6.99 27.76 o 7 1 0 11.93 5.12 24.69 o 8 1 0 53.06 -15.14 35.40 o 9 1 0 111.65 63.47 51.48 o 11 1 0 225.12 196.39 35.44 o -11 2 0 3.96 1.38 26.28 o -10 2 0 43.32 -3.55 28.86 o -9 2 0 345.29 277.53 40.76 o -8 2 0 1116.40 1129.11 70.71 o -7 2 0 888.64 835.61 65.72 o -6 2 0 19.18 23.91 14.74 o -5 2 0 87.83 71.33 51.15 o -4 2 0 3593.09 3830.68 229.58 o -3 2 0 166.14 154.86 37.64 o -2 2 0 1784.30 1663.30 124.61 o -1 2 0 613.61 531.75 34.79 o 0 2 0 12506.75 11923.55 549.35 o 1 2 0 6166.75 5941.15 278.22 o 3 2 0 4098.14 4055.80 282.77 o 4 2 0 599.57 600.40 67.97 o 5 2 0 237.43 163.90 41.03 o 6 2 0 14.50 -13.20 26.40 o 7 2 0 127.56 160.76 46.55 o -11 3 0 1.78 8.63 48.66 o -10 3 0 69.00 113.71 65.88 o -9 3 0 4.60 10.22 22.38 o -8 3 0 48.07 55.69 46.35 o -7 3 0 53.22 17.26 17.52 o -6 3 0 5.99 -7.70 15.40 o -5 3 0 11.12 26.36 15.90 o -4 3 0 2080.08 2107.78 87.89 o -3 3 0 7430.47 7306.49 340.87 o -2 3 0 1366.71 1064.36 62.57 o -1 3 0 3064.96 2952.60 206.99 o 0 3 0 4140.20 3805.33 260.37 o 1 3 0 8193.28 7997.01 530.36 o 2 3 0 40.71 49.34 22.44 o 3 3 0 86.85 111.84 30.01 o 4 3 0 1353.00 1469.39 112.23 o 6 3 0 1842.00 1940.44 167.67 o 7 3 0 207.22 266.85 63.90 o -10 4 0 17.87 83.35 31.97 o -9 4 0 27.00 2.65 26.98 o -8 4 0 83.91 -15.14 30.27 o -7 4 0 77.51 76.05 33.10 o -6 4 0 18.89 19.32 25.49 o -5 4 0 1036.80 1072.85 79.77 o -4 4 0 8.36 14.78 14.51 o -3 4 0 41.91 74.25 15.67 o -2 4 0 733.95 672.98 51.59 o -1 4 0 278.46 256.46 28.68 o 0 4 0 366.18 323.72 45.26 o 1 4 0 6923.58 6594.47 444.46 o 2 4 0 1003.92 995.31 55.65 o 3 4 0 755.79 889.62 42.11 o 4 4 0 2056.23 1958.59 79.27 o 5 4 0 601.32 583.01 78.38 o -10 5 0 75.13 74.80 32.05 o -9 5 0 5.22 16.18 26.90 o -8 5 0 109.41 91.76 24.94 o -7 5 0 52.06 32.49 20.16 o -6 5 0 324.49 336.91 33.92 o -5 5 0 9.43 -1.97 14.77 o -4 5 0 628.78 631.19 41.33 o -3 5 0 269.26 220.71 23.66 o -2 5 0 1184.83 1162.01 44.18 o -1 5 0 405.73 556.58 43.13 o 0 5 0 102.16 112.25 15.26 o 1 5 0 33.90 34.39 9.00 o 2 5 0 53.94 63.01 13.81 o 3 5 0 478.67 481.13 31.27 o 4 5 0 60.67 63.24 14.17 o 5 5 0 41.45 39.14 10.58 o 6 5 0 664.04 714.87 47.25 o 7 5 0 1096.91 1098.81 125.04 o 8 5 0 5.96 0.23 48.33 o 9 5 0 32.73 5.71 49.69 o -10 6 0 200.43 248.90 42.77 o -9 6 0 91.10 140.72 38.22 o -8 6 0 40.40 18.24 21.93 o -7 6 0 9.77 4.70 29.22 o -6 6 0 397.50 349.38 35.18 o -5 6 0 158.22 168.69 24.73 o -4 6 0 0.52 -3.27 13.94 o -3 6 0 1155.40 1087.26 39.52 o -2 6 0 53.56 79.86 11.24 o -1 6 0 851.18 816.54 44.82 o 0 6 0 848.15 880.93 38.44 o 1 6 0 53.56 56.28 15.12 o 2 6 0 212.29 207.71 24.19 o 3 6 0 320.42 286.22 25.90 o 4 6 0 207.79 192.07 22.16 o 5 6 0 2172.56 2312.60 97.26 o 6 6 0 10.19 -5.71 11.41 o 7 6 0 447.20 420.29 89.27 o 8 6 0 129.37 141.09 36.82 o 9 6 0 616.32 684.44 111.45 o -10 7 0 6.25 -5.48 27.89 o -9 7 0 1.41 -17.02 34.05 o -8 7 0 180.00 154.52 32.54 o -7 7 0 51.52 59.64 23.61 o -6 7 0 79.22 52.57 41.31 o -5 7 0 1821.46 1663.06 111.15 o -4 7 0 69.50 36.35 17.25 o -3 7 0 4.54 16.39 13.26 o -2 7 0 69.06 58.07 11.13 o -1 7 0 145.68 190.97 19.29 o 0 7 0 734.42 833.38 39.96 o 1 7 0 8387.94 9322.42 253.58 o 2 7 0 3.10 4.29 12.95 o 3 7 0 4.78 0.41 12.65 o 4 7 0 39.49 23.77 15.10 o 5 7 0 690.00 651.17 43.46 o 6 7 0 978.91 1010.79 57.17 o 7 7 0 3.04 -8.45 22.05 o 8 7 0 54.87 47.70 28.90 o 9 7 0 93.43 63.78 34.78 o 10 7 0 21.37 -2.87 25.47 o -9 8 0 103.31 131.41 35.96 o -8 8 0 664.65 720.42 95.01 o -7 8 0 145.28 145.02 32.03 o -6 8 0 53.20 24.39 22.47 o -5 8 0 2.83 -1.96 15.69 o -4 8 0 175.77 186.02 22.98 o -3 8 0 80.20 72.80 12.78 o -2 8 0 33.55 21.10 10.01 o -1 8 0 13.86 18.23 11.85 o 0 8 0 810.86 905.86 43.66 o 1 8 0 89.47 84.72 13.62 o 2 8 0 3.79 -6.79 13.58 o 3 8 0 36.72 75.09 18.37 o 4 8 0 54.09 15.38 16.10 o 5 8 0 465.17 465.47 39.38 o 6 8 0 125.22 174.03 27.28 o 7 8 0 183.42 215.28 31.08 o 8 8 0 158.65 195.16 36.83 o 9 8 0 7.21 27.44 64.25 o 10 8 0 6.57 -15.39 30.78 o -9 9 0 10.73 72.71 33.94 o -8 9 0 6.93 -13.87 27.73 o -7 9 0 431.61 523.43 51.63 o -6 9 0 964.42 1063.56 82.78 o -5 9 0 845.63 843.40 50.27 o -4 9 0 279.39 279.93 23.62 o -3 9 0 11.96 8.71 11.84 o -2 9 0 345.01 346.85 24.94 o -1 9 0 37.06 46.44 13.76 o 0 9 0 374.65 355.48 27.93 o 1 9 0 113.15 118.96 16.38 o 2 9 0 123.21 128.86 22.93 o 3 9 0 593.03 663.85 48.30 o 4 9 0 379.99 378.09 36.72 o 5 9 0 1234.70 1264.12 70.95 o 6 9 0 1092.09 1176.74 69.56 o 7 9 0 355.50 281.42 44.13 o 8 9 0 201.93 138.72 48.10 o 9 9 0 215.06 205.96 42.14 o -8 10 0 213.37 186.83 44.27 o -7 10 0 339.74 441.93 49.10 o -6 10 0 119.89 84.84 29.98 o -5 10 0 1.99 -4.59 18.93 o -4 10 0 616.08 672.05 39.70 o -3 10 0 239.45 262.67 22.40 o -2 10 0 411.68 420.89 27.10 o -1 10 0 1021.64 1102.11 50.51 o 0 10 0 14.46 26.58 15.17 o 1 10 0 11.45 9.54 12.40 o 2 10 0 284.48 385.33 29.28 o 3 10 0 62.05 47.58 22.28 o 4 10 0 2.08 7.94 19.52 o 5 10 0 594.99 706.59 54.19 o 6 10 0 354.22 344.40 39.52 o 7 10 0 309.75 255.88 46.98 o 8 10 0 165.62 75.21 36.84 o 9 10 0 3.03 -13.19 41.44 o -8 11 0 52.50 36.45 36.36 o -7 11 0 0.01 7.86 28.26 o -6 11 0 73.63 74.28 26.83 o -5 11 0 604.93 653.09 76.50 o -4 11 0 0.50 28.03 24.78 o -3 11 0 805.55 775.71 39.70 o -2 11 0 11.68 -5.02 11.69 o -1 11 0 201.84 167.41 24.45 o 0 11 0 81.98 104.52 19.94 o 1 11 0 57.39 32.16 17.39 o 2 11 0 324.55 382.53 59.54 o 3 11 0 194.24 142.84 28.11 o 4 11 0 632.85 724.01 138.00 o 5 11 0 924.89 1001.92 68.26 o 6 11 0 571.00 513.43 50.06 o 7 11 0 1398.98 1480.55 108.71 o 8 11 0 223.73 231.10 50.94 o -7 12 0 21.53 48.00 50.79 o -6 12 0 22.56 44.23 26.08 o -5 12 0 25.15 90.13 30.29 o -4 12 0 143.55 106.11 18.46 o -3 12 0 24.20 32.13 17.26 o -2 12 0 6.19 23.91 16.03 o -1 12 0 17.33 23.12 14.89 o 0 12 0 16.48 11.67 19.84 o 1 12 0 15.05 -3.48 13.90 o 2 12 0 0.12 -2.04 18.97 o 3 12 0 97.21 97.02 27.64 o 4 12 0 168.48 104.88 41.11 o 5 12 0 6.32 13.42 25.09 o 6 12 0 0.01 -7.93 61.08 o 7 12 0 903.94 867.95 86.61 o 8 12 0 90.91 129.11 45.16 o -6 13 0 171.66 50.87 47.46 o -5 13 0 209.23 202.16 55.97 o -4 13 0 242.41 205.43 24.34 o 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0 19.83 -17.94 35.88 o 2 16 0 5.89 -16.20 32.40 o 3 16 0 31.24 30.66 34.19 o -3 -16 1 0.09 -14.38 28.77 o -2 -16 1 109.91 79.88 39.41 o -1 -16 1 3.27 -5.98 31.74 o 0 -16 1 24.22 26.44 18.58 o 1 -16 1 6.36 -8.63 17.27 o 2 -16 1 0.11 -9.00 18.01 o -5 -15 1 34.83 58.15 60.72 o -4 -15 1 30.00 -14.88 29.77 o -3 -15 1 243.58 331.32 50.97 o -2 -15 1 195.40 134.57 39.34 o -1 -15 1 3.58 -9.17 29.50 o 0 -15 1 138.27 97.27 42.35 o 1 -15 1 72.04 32.06 19.89 o 2 -15 1 13.85 7.12 18.61 o 3 -15 1 4.61 -6.13 17.84 o 4 -15 1 140.54 122.05 30.68 o -6 -14 1 4.66 29.65 40.70 o -5 -14 1 22.32 38.57 33.39 o -4 -14 1 152.95 141.79 37.08 o -3 -14 1 9.70 -2.09 29.40 o -2 -14 1 52.48 55.29 31.43 o -1 -14 1 149.55 106.39 36.98 o 0 -14 1 426.98 417.76 42.36 o 1 -14 1 0.02 -6.56 17.72 o 2 -14 1 10.82 -1.62 17.74 o 3 -14 1 100.50 92.57 22.43 o 4 -14 1 141.21 141.69 25.88 o 5 -14 1 7.07 -10.64 30.15 o -7 -13 1 35.12 70.47 45.61 o -6 -13 1 6.20 -8.89 26.67 o -5 -13 1 48.54 79.35 43.15 o -4 -13 1 114.88 93.33 31.88 o 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