#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2213922.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213922_Fobs loop_ _publ_author_name 'Xiao, Zhu-Ping' 'Zheng, Da-Gui' 'Xie, Guo-Hao' 'Ye, Hong-De' _publ_section_title ; 2,4,6-Trihydroxyanisole ; _journal_coeditor_code OM2124 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2941 _journal_volume 63 _journal_year 2007 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.2310 _cell_length_b 9.4010 _cell_length_c 15.0950 _exptl_crystal_F_000 328.00 _reflns_d_resolution_high 0.8121 _[local]_cod_data_source_file om2124Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' X in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 96.51 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 678.84 651.52 8.17 o 4 0 0 209.83 199.43 6.84 o 6 0 0 12.01 14.37 3.08 o 1 1 0 1112.70 940.32 7.47 o 2 1 0 1492.26 1292.25 11.91 o 3 1 0 318.17 335.24 7.43 o 4 1 0 76.69 70.78 4.20 o 5 1 0 16.81 12.10 2.73 o 6 1 0 0.85 2.59 1.85 o 0 2 0 1978.67 2265.08 12.09 o 1 2 0 313.45 284.66 4.65 o 2 2 0 8.29 6.92 1.15 o 3 2 0 8.46 9.19 1.57 o 4 2 0 28.53 24.06 2.69 o 5 2 0 2.82 0.87 1.99 o 6 2 0 2.36 3.43 2.38 o 1 3 0 0.35 0.10 0.84 o 2 3 0 492.14 432.07 7.76 o 3 3 0 15.04 17.17 2.06 o 4 3 0 69.67 77.06 4.76 o 5 3 0 6.03 4.93 1.96 o 6 3 0 0.46 0.38 1.96 o 0 4 0 845.93 946.01 10.85 o 1 4 0 1137.82 1256.09 12.87 o 2 4 0 60.71 55.76 3.19 o 3 4 0 31.77 29.13 2.55 o 4 4 0 4.55 1.54 1.96 o 5 4 0 15.40 15.28 2.62 o 6 4 0 4.47 7.38 2.24 o 1 5 0 112.82 117.53 4.45 o 2 5 0 57.24 58.41 3.46 o 3 5 0 260.20 243.85 7.66 o 4 5 0 0.65 -0.56 1.96 o 5 5 0 0.39 0.70 1.96 o 0 6 0 10.25 7.73 1.64 o 1 6 0 27.06 21.44 2.31 o 2 6 0 109.25 110.90 5.18 o 3 6 0 17.48 19.26 2.66 o 4 6 0 4.78 5.49 2.10 o 5 6 0 17.19 25.80 4.16 o 1 7 0 1190.72 1164.65 16.65 o 2 7 0 18.49 16.36 2.55 o 3 7 0 162.31 144.55 7.01 o 4 7 0 2.05 2.03 1.64 o 5 7 0 0.96 -2.34 2.34 o 0 8 0 239.38 267.26 8.67 o 1 8 0 1490.37 1421.28 20.06 o 2 8 0 36.17 31.48 3.57 o 3 8 0 0.80 1.29 1.85 o 4 8 0 43.29 51.97 5.00 o 1 9 0 31.46 38.01 3.71 o 2 9 0 1.25 1.61 1.71 o 3 9 0 71.50 69.24 5.84 o 4 9 0 0.03 -2.20 2.20 o 0 10 0 0.21 -0.98 1.68 o 1 10 0 5.15 2.10 2.55 o 2 10 0 1.19 -1.78 2.17 o 3 10 0 3.34 4.82 2.20 o 1 11 0 0.16 3.98 2.31 o 2 11 0 5.40 6.64 3.01 o 1 0 1 9313.42 8819.15 109.76 o 2 0 1 92.59 82.73 2.98 o 3 0 1 1.39 0.63 1.05 o 4 0 1 1.49 1.50 1.50 o 5 0 1 19.00 22.90 2.76 o 6 0 1 0.21 3.32 1.68 o 0 1 1 9.88 10.64 0.70 o 1 1 1 891.68 745.61 6.78 o 2 1 1 89.26 79.45 3.05 o 3 1 1 220.42 197.66 5.73 o 4 1 1 9.62 7.41 1.47 o 5 1 1 20.78 22.24 3.08 o 6 1 1 7.79 7.06 2.45 o 0 2 1 476.89 518.16 5.51 o 1 2 1 66.34 60.80 2.21 o 2 2 1 323.26 284.87 5.83 o 3 2 1 91.48 85.57 3.92 o 4 2 1 49.00 47.82 3.67 o 5 2 1 33.25 33.19 3.81 o 6 2 1 4.88 9.47 2.66 o 0 3 1 233.37 270.93 4.87 o 1 3 1 1483.57 1420.14 12.16 o 2 3 1 61.81 61.69 3.08 o 3 3 1 691.19 639.77 11.10 o 4 3 1 9.00 9.30 1.99 o 5 3 1 13.02 14.51 2.24 o 6 3 1 3.44 2.34 2.34 o 0 4 1 3193.72 3833.04 22.31 o 1 4 1 608.41 694.64 9.47 o 2 4 1 624.34 644.07 10.29 o 3 4 1 20.24 21.43 2.45 o 4 4 1 120.87 119.36 5.78 o 5 4 1 5.83 4.86 2.31 o 6 4 1 2.67 2.87 2.48 o 0 5 1 180.34 199.34 5.62 o 1 5 1 284.14 321.57 7.18 o 2 5 1 413.57 414.82 8.99 o 3 5 1 27.25 27.73 2.76 o 4 5 1 26.36 25.56 3.29 o 5 5 1 2.19 2.10 2.24 o 0 6 1 30.54 23.05 2.24 o 1 6 1 169.82 182.03 6.14 o 2 6 1 19.41 19.48 2.27 o 3 6 1 12.44 9.47 2.55 o 4 6 1 3.08 4.58 1.57 o 5 6 1 10.06 10.07 2.97 o 0 7 1 4.29 1.75 1.71 o 1 7 1 69.17 67.79 4.09 o 2 7 1 437.92 424.01 10.64 o 3 7 1 27.82 23.11 3.29 o 4 7 1 26.24 24.20 3.85 o 5 7 1 1.23 2.41 1.99 o 0 8 1 1378.01 1394.99 19.68 o 1 8 1 11.77 11.89 2.27 o 2 8 1 264.03 250.71 8.84 o 3 8 1 6.06 1.92 2.20 o 4 8 1 15.83 20.45 3.67 o 0 9 1 6.34 6.33 2.38 o 1 9 1 21.10 15.91 2.83 o 2 9 1 39.12 41.83 4.23 o 3 9 1 1.35 2.52 2.20 o 4 9 1 22.38 25.07 4.06 o 0 10 1 6.44 4.51 1.92 o 1 10 1 17.77 16.92 3.08 o 2 10 1 3.26 1.08 2.27 o 3 10 1 33.36 35.84 4.62 o 0 11 1 90.15 88.43 6.40 o 1 11 1 13.16 10.66 2.83 o 0 0 2 49.28 41.18 1.34 o 1 0 2 41.89 42.05 1.79 o 2 0 2 1790.32 1679.82 13.91 o 3 0 2 0.38 -0.31 1.05 o 4 0 2 184.92 165.90 6.59 o 5 0 2 4.75 3.18 1.99 o 6 0 2 0.20 -2.17 2.17 o 0 1 2 1548.71 1648.02 9.25 o 1 1 2 6531.10 6136.65 96.37 o 2 1 2 672.49 583.52 8.18 o 3 1 2 198.61 185.50 5.72 o 4 1 2 64.87 71.95 4.27 o 5 1 2 6.35 6.43 2.10 o 6 1 2 7.02 4.51 2.59 o 0 2 2 21.32 26.11 1.36 o 1 2 2 352.52 334.13 5.25 o 2 2 2 122.67 121.99 3.96 o 3 2 2 79.37 71.29 3.68 o 4 2 2 34.98 32.46 3.11 o 5 2 2 0.69 4.47 1.36 o 6 2 2 4.88 4.96 2.69 o 0 3 2 1116.43 1336.67 11.21 o 1 3 2 140.35 161.27 4.15 o 2 3 2 249.73 225.13 5.63 o 3 3 2 4.97 2.94 1.40 o 4 3 2 80.90 82.46 4.69 o 5 3 2 2.73 -0.31 1.82 o 6 3 2 4.87 6.71 2.34 o 0 4 2 698.35 756.51 9.57 o 1 4 2 671.73 754.56 9.98 o 2 4 2 216.12 214.93 6.01 o 3 4 2 59.82 54.38 3.64 o 4 4 2 25.92 19.90 2.94 o 5 4 2 2.58 0.31 1.82 o 6 4 2 1.13 -2.20 2.20 o 0 5 2 422.55 497.96 8.76 o 1 5 2 85.59 84.94 3.71 o 2 5 2 72.66 76.53 3.85 o 3 5 2 80.74 78.86 4.52 o 4 5 2 1.67 1.12 1.64 o 5 5 2 29.50 26.85 3.71 o 0 6 2 298.23 305.24 7.63 o 1 6 2 34.52 36.69 2.90 o 2 6 2 125.75 109.25 5.05 o 3 6 2 8.68 9.58 2.24 o 4 6 2 3.02 1.54 2.10 o 5 6 2 7.87 9.02 2.41 o 0 7 2 131.21 133.64 5.64 o 1 7 2 70.18 68.74 4.13 o 2 7 2 165.19 165.94 6.66 o 3 7 2 219.37 240.35 8.77 o 4 7 2 7.22 11.47 1.96 o 5 7 2 28.04 26.36 4.09 o 0 8 2 543.93 556.59 12.35 o 1 8 2 116.50 111.86 5.85 o 2 8 2 71.61 66.97 4.97 o 3 8 2 17.86 19.79 3.08 o 4 8 2 5.66 4.86 2.62 o 0 9 2 17.66 16.08 3.11 o 1 9 2 122.91 112.20 6.13 o 2 9 2 40.91 40.29 4.09 o 3 9 2 45.37 47.11 4.37 o 0 10 2 26.92 22.34 3.46 o 1 10 2 6.06 6.92 2.45 o 2 10 2 34.42 30.14 4.48 o 3 10 2 3.62 4.05 2.55 o 0 11 2 3.61 5.14 2.59 o 1 11 2 83.05 86.95 6.26 o 1 0 3 3613.86 3261.26 69.96 o 2 0 3 45.55 41.55 2.31 o 3 0 3 30.32 26.51 2.41 o 4 0 3 32.93 31.20 3.22 o 5 0 3 0.05 -0.87 1.68 o 6 0 3 0.01 -1.12 2.31 o 0 1 3 40.30 41.14 1.72 o 1 1 3 1089.75 1037.60 9.29 o 2 1 3 1232.39 1098.79 11.73 o 3 1 3 254.27 243.79 6.72 o 4 1 3 47.86 41.94 3.60 o 5 1 3 4.12 5.35 2.17 o 6 1 3 3.44 5.31 2.34 o 0 2 3 391.97 420.46 5.88 o 1 2 3 53.45 51.56 2.28 o 2 2 3 150.35 145.17 4.42 o 3 2 3 73.02 63.44 3.71 o 4 2 3 12.33 17.31 2.24 o 5 2 3 20.54 21.57 3.22 o 6 2 3 7.44 10.84 2.80 o 0 3 3 58.08 72.93 2.87 o 1 3 3 597.93 604.47 8.31 o 2 3 3 48.62 44.83 2.73 o 3 3 3 72.26 59.96 3.68 o 4 3 3 29.34 31.96 3.11 o 5 3 3 13.66 7.87 2.69 o 6 3 3 0.94 2.80 1.99 o 0 4 3 345.89 367.40 6.92 o 1 4 3 116.23 143.56 4.45 o 2 4 3 24.91 26.54 2.38 o 3 4 3 21.34 21.68 2.41 o 4 4 3 34.76 36.27 3.39 o 5 4 3 0.87 1.33 1.92 o 0 5 3 163.04 200.19 5.69 o 1 5 3 231.44 232.03 6.29 o 2 5 3 3.33 1.33 1.33 o 3 5 3 173.96 168.90 6.63 o 4 5 3 52.81 61.18 4.65 o 5 5 3 15.40 15.91 3.50 o 0 6 3 31.88 29.80 2.66 o 1 6 3 4.49 3.25 1.47 o 2 6 3 9.36 11.64 2.17 o 3 6 3 72.31 70.23 4.69 o 4 6 3 13.93 12.10 3.53 o 5 6 3 15.58 12.48 3.15 o 0 7 3 112.20 117.20 5.32 o 1 7 3 159.55 161.22 6.27 o 2 7 3 125.82 121.23 5.88 o 3 7 3 140.11 135.03 6.73 o 4 7 3 71.02 59.02 5.14 o 5 7 3 10.02 9.82 3.46 o 0 8 3 225.00 196.05 7.51 o 1 8 3 90.50 90.98 5.25 o 2 8 3 16.83 13.63 2.59 o 3 8 3 7.94 8.39 2.13 o 4 8 3 11.66 12.41 3.39 o 0 9 3 177.49 173.52 7.89 o 1 9 3 76.70 80.80 5.18 o 2 9 3 68.50 68.19 5.14 o 3 9 3 40.76 39.17 4.16 o 0 10 3 9.12 4.82 2.45 o 1 10 3 3.83 2.80 2.31 o 2 10 3 15.64 10.70 2.97 o 3 10 3 10.13 6.12 3.22 o 0 11 3 0.25 1.19 2.27 o 1 11 3 0.98 0.38 2.20 o 0 0 4 25.64 23.45 1.43 o 1 0 4 361.14 339.61 5.61 o 2 0 4 1893.93 1705.51 15.25 o 3 0 4 0.38 1.05 1.19 o 4 0 4 11.62 10.91 2.10 o 5 0 4 0.05 -0.87 1.36 o 6 0 4 14.64 22.27 3.50 o 0 1 4 538.20 509.40 6.53 o 1 1 4 71.18 68.67 2.59 o 2 1 4 1213.17 1169.52 12.56 o 3 1 4 697.94 682.29 11.43 o 4 1 4 35.76 43.05 3.60 o 5 1 4 27.88 31.30 3.67 o 6 1 4 9.96 10.03 3.32 o 0 2 4 2465.44 2667.79 16.69 o 1 2 4 168.86 176.71 4.36 o 2 2 4 116.54 121.82 4.17 o 3 2 4 83.44 85.26 4.13 o 4 2 4 109.68 111.08 5.78 o 5 2 4 15.56 22.37 3.39 o 6 2 4 43.61 61.69 6.02 o 0 3 4 1871.86 2308.04 16.82 o 1 3 4 521.38 539.80 8.24 o 2 3 4 18.62 20.70 2.03 o 3 3 4 143.45 147.48 5.57 o 4 3 4 5.68 8.60 1.92 o 5 3 4 21.73 27.38 3.36 o 6 3 4 5.51 6.08 2.10 o 0 4 4 3.30 0.66 1.15 o 1 4 4 447.87 505.65 8.77 o 2 4 4 8.45 7.87 1.54 o 3 4 4 3.94 3.22 1.33 o 4 4 4 9.41 11.05 2.38 o 5 4 4 2.43 2.03 1.85 o 0 5 4 691.25 889.57 12.33 o 1 5 4 298.73 310.26 7.50 o 2 5 4 60.49 63.62 3.67 o 3 5 4 14.20 13.46 2.41 o 4 5 4 0.86 1.75 1.43 o 5 5 4 13.46 10.07 3.36 o 0 6 4 21.01 20.04 2.48 o 1 6 4 117.12 115.55 5.05 o 2 6 4 20.26 22.73 2.73 o 3 6 4 78.15 66.77 4.79 o 4 6 4 63.41 67.80 5.42 o 5 6 4 99.55 94.74 7.00 o 0 7 4 87.63 91.48 4.69 o 1 7 4 43.71 42.40 3.32 o 2 7 4 50.81 53.70 3.95 o 3 7 4 146.43 139.63 6.90 o 4 7 4 4.91 10.77 2.59 o 0 8 4 0.62 -0.24 1.89 o 1 8 4 341.87 333.08 9.81 o 2 8 4 133.17 146.93 7.00 o 3 8 4 22.29 18.74 3.29 o 4 8 4 19.26 15.63 3.46 o 0 9 4 54.96 53.07 4.44 o 1 9 4 358.09 341.15 10.65 o 2 9 4 52.80 56.04 4.79 o 3 9 4 25.93 28.67 3.71 o 0 10 4 10.76 7.94 2.90 o 1 10 4 3.18 -1.05 2.90 o 2 10 4 62.24 72.10 5.74 o 0 11 4 3.54 2.38 2.73 o 1 11 4 35.63 41.19 4.62 o 1 0 5 1128.11 1114.51 11.13 o 2 0 5 0.15 -0.28 0.94 o 3 0 5 285.34 268.06 7.28 o 4 0 5 42.91 43.51 3.78 o 5 0 5 3.41 2.17 1.12 o 6 0 5 0.02 2.76 1.96 o 0 1 5 5.20 5.84 0.87 o 1 1 5 802.59 768.74 9.34 o 2 1 5 137.58 114.59 4.21 o 3 1 5 745.23 736.33 12.25 o 4 1 5 45.13 45.05 3.67 o 5 1 5 10.22 12.51 2.62 o 6 1 5 3.31 4.33 2.52 o 0 2 5 1251.20 1298.25 12.44 o 1 2 5 894.24 899.96 10.61 o 2 2 5 167.54 173.10 5.27 o 3 2 5 198.50 191.98 6.49 o 4 2 5 0.63 -0.49 1.57 o 5 2 5 109.16 106.18 6.65 o 6 2 5 5.22 8.04 2.83 o 0 3 5 475.47 554.07 8.58 o 1 3 5 289.82 304.17 6.52 o 2 3 5 264.03 261.34 6.72 o 3 3 5 2.17 3.91 1.26 o 4 3 5 2.68 4.96 1.82 o 5 3 5 34.08 40.70 3.92 o 0 4 5 9.91 9.68 1.40 o 1 4 5 150.86 199.14 5.68 o 2 4 5 53.78 64.32 3.53 o 3 4 5 5.43 5.35 1.64 o 4 4 5 46.32 48.20 3.99 o 5 4 5 5.13 6.57 1.75 o 0 5 5 191.80 250.24 6.85 o 1 5 5 365.77 417.37 8.88 o 2 5 5 118.42 120.41 5.19 o 3 5 5 28.86 31.65 3.15 o 4 5 5 109.91 119.35 6.65 o 5 5 5 2.52 5.87 1.96 o 0 6 5 1022.52 1165.57 15.66 o 1 6 5 60.85 66.28 3.99 o 2 6 5 22.66 21.12 2.69 o 3 6 5 68.78 60.85 4.58 o 4 6 5 405.40 447.43 12.87 o 5 6 5 7.70 5.49 3.25 o 0 7 5 4.23 4.40 1.82 o 1 7 5 35.77 32.32 3.25 o 2 7 5 67.72 61.37 4.65 o 3 7 5 4.29 3.01 2.41 o 4 7 5 63.56 64.58 5.53 o 0 8 5 186.39 157.41 6.91 o 1 8 5 7.20 9.33 2.41 o 2 8 5 107.94 102.09 5.99 o 3 8 5 40.64 41.69 4.27 o 4 8 5 17.45 15.56 3.25 o 0 9 5 1.77 3.36 1.82 o 1 9 5 9.75 8.46 2.83 o 2 9 5 187.68 191.55 8.52 o 3 9 5 21.85 20.63 4.13 o 0 10 5 74.49 69.66 5.88 o 1 10 5 51.84 51.84 4.30 o 2 10 5 4.77 2.27 2.48 o 0 11 5 23.37 31.85 3.81 o 1 11 5 11.49 7.69 2.83 o 0 0 6 127.81 147.64 4.21 o 1 0 6 8.56 10.07 1.36 o 2 0 6 0.09 0.77 1.05 o 3 0 6 331.88 332.04 8.48 o 4 0 6 251.86 241.26 8.21 o 5 0 6 3.36 3.53 1.75 o 6 0 6 0.00 0.00 2.17 o 0 1 6 35.14 30.31 1.99 o 1 1 6 317.56 325.17 6.53 o 2 1 6 528.58 530.60 9.28 o 3 1 6 67.72 67.69 3.85 o 4 1 6 56.95 57.66 4.23 o 5 1 6 32.69 37.24 4.30 o 6 1 6 1.96 2.45 2.45 o 0 2 6 2520.98 2698.36 19.61 o 1 2 6 199.55 194.41 5.24 o 2 2 6 229.42 238.93 6.47 o 3 2 6 56.06 49.86 3.67 o 4 2 6 456.50 463.57 11.80 o 5 2 6 33.04 37.66 4.06 o 0 3 6 87.57 99.51 3.89 o 1 3 6 286.32 312.74 7.01 o 2 3 6 331.74 319.63 7.82 o 3 3 6 65.79 59.77 4.06 o 4 3 6 21.52 21.29 3.01 o 5 3 6 14.63 19.47 2.97 o 0 4 6 403.56 520.51 9.57 o 1 4 6 297.54 320.81 7.57 o 2 4 6 45.31 49.57 3.25 o 3 4 6 30.13 31.23 3.04 o 4 4 6 39.90 40.22 3.85 o 5 4 6 1.84 4.65 1.57 o 0 5 6 4.62 3.78 1.47 o 1 5 6 69.97 69.90 3.82 o 2 5 6 177.14 176.09 6.42 o 3 5 6 221.79 230.74 8.28 o 4 5 6 26.60 26.05 3.22 o 5 5 6 23.01 23.04 4.37 o 0 6 6 0.47 -0.63 1.40 o 1 6 6 348.11 386.71 9.43 o 2 6 6 65.83 60.64 4.16 o 3 6 6 99.41 103.10 5.92 o 4 6 6 35.46 34.55 4.13 o 5 6 6 34.77 34.20 4.44 o 0 7 6 17.91 16.89 2.27 o 1 7 6 74.33 77.06 4.69 o 2 7 6 59.83 50.69 4.06 o 3 7 6 51.93 48.41 4.44 o 4 7 6 16.21 17.13 3.08 o 0 8 6 74.62 66.07 4.90 o 1 8 6 85.23 80.92 5.46 o 2 8 6 77.18 76.88 5.42 o 3 8 6 39.75 40.53 4.93 o 4 8 6 20.62 19.54 3.81 o 0 9 6 31.20 24.69 3.71 o 1 9 6 68.15 61.65 4.83 o 2 9 6 53.34 58.69 4.90 o 3 9 6 119.26 112.06 7.53 o 0 10 6 194.66 197.37 9.15 o 1 10 6 61.91 46.63 4.86 o 2 10 6 11.06 14.02 3.18 o 1 0 7 6.00 5.14 1.26 o 2 0 7 300.26 329.92 7.67 o 3 0 7 13.29 12.03 1.96 o 4 0 7 12.52 11.99 2.41 o 5 0 7 3.79 1.68 1.99 o 0 1 7 45.42 53.20 2.87 o 1 1 7 583.97 592.56 9.45 o 2 1 7 1.63 1.19 1.19 o 3 1 7 23.57 22.80 2.69 o 4 1 7 5.96 5.38 2.20 o 5 1 7 14.54 14.47 2.62 o 0 2 7 460.12 443.13 8.32 o 1 2 7 381.95 373.98 7.73 o 2 2 7 77.27 74.09 3.92 o 3 2 7 67.14 68.31 4.27 o 4 2 7 353.57 378.62 10.93 o 5 2 7 18.01 20.91 3.39 o 0 3 7 6.30 7.17 1.22 o 1 3 7 123.70 140.40 4.98 o 2 3 7 73.70 81.08 4.13 o 3 3 7 21.25 26.92 3.01 o 4 3 7 58.25 63.01 4.90 o 5 3 7 3.65 3.53 2.06 o 0 4 7 17.04 22.38 2.10 o 1 4 7 171.52 203.77 6.32 o 2 4 7 155.08 158.89 6.00 o 3 4 7 202.49 222.02 7.82 o 4 4 7 28.62 25.07 3.22 o 5 4 7 2.11 4.79 2.24 o 0 5 7 56.80 60.26 3.57 o 1 5 7 117.70 126.65 5.36 o 2 5 7 150.49 144.43 6.17 o 3 5 7 297.06 310.58 9.62 o 4 5 7 7.18 1.92 2.38 o 5 5 7 10.05 11.29 4.02 o 0 6 7 374.87 424.30 10.17 o 1 6 7 10.50 9.40 2.62 o 2 6 7 3.36 3.60 1.71 o 3 6 7 41.61 39.80 4.30 o 4 6 7 1.53 4.51 2.27 o 0 7 7 44.96 43.27 3.88 o 1 7 7 39.89 35.78 3.39 o 2 7 7 64.86 70.88 4.86 o 3 7 7 26.24 26.61 3.36 o 4 7 7 7.64 9.79 2.97 o 0 8 7 3.76 4.12 2.06 o 1 8 7 28.98 34.65 3.46 o 2 8 7 0.48 -0.63 1.85 o 3 8 7 73.07 77.15 6.09 o 0 9 7 106.15 87.97 6.34 o 1 9 7 8.26 5.73 2.45 o 2 9 7 38.84 36.30 4.20 o 3 9 7 37.03 35.28 4.65 o 0 10 7 27.33 21.54 3.50 o 1 10 7 14.25 13.63 3.46 o 2 10 7 12.82 14.86 3.15 o 0 0 8 1015.18 1073.51 13.39 o 1 0 8 610.41 629.08 10.43 o 2 0 8 2.62 2.45 1.40 o 3 0 8 5.43 6.15 1.64 o 4 0 8 0.02 -0.28 1.75 o 5 0 8 5.05 9.05 2.17 o 0 1 8 346.94 378.33 8.01 o 1 1 8 55.70 49.74 3.01 o 2 1 8 5.15 4.16 1.36 o 3 1 8 193.77 178.37 6.73 o 4 1 8 17.15 18.98 3.18 o 5 1 8 44.31 39.28 4.90 o 0 2 8 233.23 237.20 6.54 o 1 2 8 98.82 110.08 4.45 o 2 2 8 29.73 24.27 2.52 o 3 2 8 73.47 79.83 4.79 o 4 2 8 4.45 4.65 2.10 o 5 2 8 33.16 39.30 4.58 o 0 3 8 11.98 14.23 1.68 o 1 3 8 30.02 24.80 2.41 o 2 3 8 136.07 137.24 5.54 o 3 3 8 285.16 268.54 8.78 o 4 3 8 6.84 9.61 2.48 o 5 3 8 21.51 26.15 3.92 o 0 4 8 3.66 3.22 1.05 o 1 4 8 62.26 57.60 3.71 o 2 4 8 236.14 240.20 7.65 o 3 4 8 52.15 49.12 4.37 o 4 4 8 2.53 0.63 2.24 o 5 4 8 0.66 0.77 2.17 o 0 5 8 3.86 4.23 1.64 o 1 5 8 166.12 163.84 6.31 o 2 5 8 242.13 240.01 8.11 o 3 5 8 39.89 34.45 3.71 o 4 5 8 9.15 10.80 2.06 o 5 5 8 0.65 5.24 1.75 o 0 6 8 0.12 -1.61 1.61 o 1 6 8 2.94 4.26 1.92 o 2 6 8 146.58 149.32 6.90 o 3 6 8 24.13 25.07 3.18 o 4 6 8 0.96 -0.70 2.06 o 0 7 8 75.00 87.03 5.28 o 1 7 8 56.37 52.86 4.55 o 2 7 8 62.74 57.10 4.86 o 3 7 8 1.40 -1.99 2.31 o 4 7 8 1.15 2.34 2.34 o 0 8 8 3.34 -0.91 2.62 o 1 8 8 67.42 60.39 4.86 o 2 8 8 12.79 15.45 2.69 o 3 8 8 7.99 6.71 2.87 o 0 9 8 22.83 19.79 3.36 o 1 9 8 39.98 43.64 4.55 o 2 9 8 15.40 14.19 3.22 o 0 10 8 0.51 -1.92 2.69 o 1 10 8 3.65 8.67 2.83 o 1 0 9 394.43 423.53 9.13 o 2 0 9 39.40 33.58 2.90 o 3 0 9 5.47 7.38 2.17 o 4 0 9 41.11 38.26 3.81 o 5 0 9 0.01 -1.92 1.92 o 0 1 9 123.42 111.58 4.80 o 1 1 9 20.87 20.81 2.45 o 2 1 9 89.06 76.54 4.20 o 3 1 9 3.78 3.22 1.61 o 4 1 9 82.36 80.53 5.42 o 5 1 9 19.56 23.84 3.92 o 0 2 9 5.09 5.66 1.22 o 1 2 9 33.24 32.46 2.69 o 2 2 9 48.09 47.51 3.39 o 3 2 9 58.64 52.48 4.27 o 4 2 9 2.71 4.89 1.96 o 5 2 9 7.12 6.33 2.87 o 0 3 9 0.69 0.59 1.15 o 1 3 9 190.28 181.52 6.32 o 2 3 9 152.61 154.44 6.31 o 3 3 9 250.00 262.25 8.77 o 4 3 9 87.48 85.50 5.81 o 5 3 9 14.53 11.92 3.53 o 0 4 9 119.48 116.84 5.47 o 1 4 9 12.13 13.32 1.82 o 2 4 9 11.95 7.80 1.99 o 3 4 9 27.35 24.16 3.18 o 4 4 9 19.71 17.34 3.11 o 5 4 9 2.67 0.42 2.41 o 0 5 9 16.08 17.24 2.52 o 1 5 9 183.32 195.74 7.22 o 2 5 9 184.28 180.42 7.29 o 3 5 9 50.67 42.57 4.16 o 4 5 9 0.85 0.35 1.96 o 0 6 9 4.93 3.74 1.99 o 1 6 9 67.10 60.64 4.83 o 2 6 9 53.25 55.13 4.30 o 3 6 9 29.01 27.73 3.50 o 4 6 9 2.45 2.27 1.61 o 0 7 9 18.35 22.83 3.08 o 1 7 9 73.18 82.30 5.32 o 2 7 9 49.53 55.26 4.83 o 3 7 9 11.24 16.36 2.97 o 4 7 9 5.30 2.45 2.62 o 0 8 9 85.91 83.43 5.84 o 1 8 9 10.00 11.96 2.94 o 2 8 9 29.80 26.78 3.92 o 3 8 9 35.28 37.31 4.37 o 0 9 9 0.25 1.08 2.27 o 1 9 9 7.68 9.61 2.27 o 2 9 9 6.12 3.88 2.80 o 0 10 9 18.53 24.75 4.47 o 0 0 10 895.42 812.08 13.40 o 1 0 10 307.37 309.56 8.27 o 2 0 10 139.45 138.18 5.89 o 3 0 10 45.67 38.83 3.64 o 4 0 10 64.37 61.71 5.25 o 5 0 10 2.44 3.84 1.54 o 0 1 10 781.17 783.71 13.15 o 1 1 10 287.89 281.92 7.98 o 2 1 10 33.60 34.20 3.18 o 3 1 10 55.05 54.47 4.13 o 4 1 10 36.82 43.40 4.27 o 5 1 10 11.73 15.00 3.04 o 0 2 10 48.01 54.72 3.43 o 1 2 10 27.78 31.44 2.94 o 2 2 10 64.32 59.66 4.13 o 3 2 10 58.06 63.08 4.72 o 4 2 10 2.41 0.31 1.82 o 5 2 10 15.16 15.63 3.53 o 0 3 10 0.22 0.21 1.12 o 1 3 10 133.89 154.29 6.10 o 2 3 10 218.54 220.88 7.75 o 3 3 10 88.82 74.45 5.29 o 4 3 10 41.71 36.27 4.51 o 5 3 10 5.08 4.40 2.38 o 0 4 10 40.78 38.23 3.71 o 1 4 10 279.49 284.05 8.61 o 2 4 10 343.97 342.13 9.95 o 3 4 10 8.64 8.70 2.41 o 4 4 10 11.91 21.43 3.36 o 0 5 10 229.80 234.97 8.25 o 1 5 10 266.00 261.32 8.71 o 2 5 10 42.91 41.17 4.30 o 3 5 10 10.07 11.85 2.73 o 4 5 10 12.66 10.77 3.25 o 0 6 10 102.71 109.34 6.16 o 1 6 10 13.60 14.72 2.69 o 2 6 10 27.70 26.26 3.50 o 3 6 10 7.42 8.63 2.55 o 4 6 10 6.42 10.31 2.80 o 0 7 10 117.45 129.41 6.93 o 1 7 10 100.43 93.36 6.23 o 2 7 10 14.15 11.50 3.50 o 3 7 10 50.84 49.70 5.11 o 0 8 10 14.12 17.13 3.53 o 1 8 10 127.80 127.17 7.07 o 2 8 10 74.89 71.72 5.77 o 3 8 10 4.39 4.05 3.11 o 0 9 10 0.01 1.15 2.41 o 1 9 10 16.17 9.72 3.32 o 2 9 10 52.51 60.02 5.42 o 1 0 11 246.85 215.73 7.52 o 2 0 11 185.82 171.27 7.26 o 3 0 11 0.01 -1.36 1.64 o 4 0 11 0.16 0.35 1.89 o 5 0 11 5.74 4.05 2.73 o 0 1 11 135.77 124.10 5.68 o 1 1 11 92.18 94.50 4.97 o 2 1 11 45.98 43.17 3.95 o 3 1 11 59.93 62.03 5.00 o 4 1 11 8.54 7.83 2.62 o 5 1 11 0.11 -2.31 2.31 o 0 2 11 6.63 6.78 2.06 o 1 2 11 14.84 15.49 2.24 o 2 2 11 67.98 65.61 4.30 o 3 2 11 68.41 59.80 4.79 o 4 2 11 9.69 9.33 2.73 o 5 2 11 8.25 9.86 2.83 o 0 3 11 0.58 1.96 1.26 o 1 3 11 171.45 150.30 6.63 o 2 3 11 201.32 209.40 7.79 o 3 3 11 50.97 52.78 4.34 o 4 3 11 2.99 1.43 2.55 o 0 4 11 986.57 993.02 16.92 o 1 4 11 647.46 630.89 13.53 o 2 4 11 90.97 82.64 5.11 o 3 4 11 0.16 -2.20 2.20 o 4 4 11 32.55 38.25 4.76 o 0 5 11 182.68 173.92 7.64 o 1 5 11 77.83 71.92 4.93 o 2 5 11 21.59 17.97 3.08 o 3 5 11 4.90 5.10 2.27 o 4 5 11 33.74 42.63 5.18 o 0 6 11 37.31 42.98 4.16 o 1 6 11 5.81 4.05 2.03 o 2 6 11 1.14 2.97 2.20 o 3 6 11 14.61 11.33 2.97 o 0 7 11 80.98 83.07 5.81 o 1 7 11 43.43 51.94 4.58 o 2 7 11 10.78 12.55 2.31 o 3 7 11 24.17 37.41 4.62 o 0 8 11 129.26 129.66 7.53 o 1 8 11 63.93 63.74 5.81 o 2 8 11 36.91 38.82 4.65 o 0 9 11 20.99 20.38 3.92 o 1 9 11 21.28 22.55 4.16 o 0 0 12 381.88 345.11 9.86 o 1 0 12 56.39 58.78 4.20 o 2 0 12 2.61 0.00 1.75 o 3 0 12 16.42 15.87 2.80 o 4 0 12 19.37 24.58 3.22 o 0 1 12 0.99 0.24 1.75 o 1 1 12 51.99 50.80 4.09 o 2 1 12 50.88 46.49 4.20 o 3 1 12 84.11 75.21 5.14 o 4 1 12 2.20 -0.70 1.61 o 0 2 12 174.38 187.72 7.40 o 1 2 12 60.05 52.24 4.34 o 2 2 12 53.36 43.48 4.37 o 3 2 12 71.76 75.89 5.25 o 4 2 12 2.31 1.12 2.10 o 0 3 12 248.11 252.17 8.88 o 1 3 12 246.01 255.86 8.70 o 2 3 12 18.91 21.68 2.90 o 3 3 12 3.94 3.60 2.10 o 4 3 12 8.49 7.55 2.69 o 0 4 12 1284.95 1352.29 20.95 o 1 4 12 286.26 309.49 10.04 o 2 4 12 1.49 0.94 2.06 o 3 4 12 2.34 4.12 1.68 o 4 4 12 0.95 2.38 2.38 o 0 5 12 0.06 3.08 1.96 o 1 5 12 120.12 117.80 6.62 o 2 5 12 14.44 15.73 2.90 o 3 5 12 32.19 38.08 4.30 o 4 5 12 12.42 11.96 3.88 o 0 6 12 17.98 20.10 2.83 o 1 6 12 1.62 3.36 1.33 o 2 6 12 25.53 22.20 3.81 o 3 6 12 6.82 6.57 2.10 o 0 7 12 0.37 0.35 1.82 o 1 7 12 8.67 8.70 3.22 o 2 7 12 10.38 11.82 3.11 o 0 8 12 92.87 96.80 6.79 o 1 8 12 45.57 49.42 5.46 o 2 8 12 7.32 6.61 2.97 o 1 0 13 32.18 23.15 3.04 o 2 0 13 212.90 207.44 8.45 o 3 0 13 4.37 4.72 2.52 o 4 0 13 0.01 0.00 1.78 o 0 1 13 15.32 11.08 2.10 o 1 1 13 33.93 25.28 3.22 o 2 1 13 47.38 33.79 3.81 o 3 1 13 23.83 24.27 3.71 o 4 1 13 6.45 8.11 2.41 o 0 2 13 53.94 56.67 4.55 o 1 2 13 60.06 56.15 4.44 o 2 2 13 54.79 45.62 4.27 o 3 2 13 2.95 4.44 1.92 o 4 2 13 4.26 3.91 2.48 o 0 3 13 8.68 9.79 2.66 o 1 3 13 120.60 110.14 6.58 o 2 3 13 39.50 45.53 4.27 o 3 3 13 28.45 28.22 3.71 o 4 3 13 0.92 0.80 2.27 o 0 4 13 100.69 105.58 6.62 o 1 4 13 38.43 46.79 4.41 o 2 4 13 31.03 35.35 3.64 o 3 4 13 2.74 6.26 2.17 o 4 4 13 5.99 12.09 3.36 o 0 5 13 89.32 82.91 5.88 o 1 5 13 50.51 50.75 4.90 o 2 5 13 18.30 14.82 3.46 o 3 5 13 14.88 14.33 3.43 o 0 6 13 1.19 -0.66 2.24 o 1 6 13 19.43 20.52 3.46 o 2 6 13 20.24 29.02 3.78 o 3 6 13 41.43 44.38 4.93 o 0 7 13 18.98 18.32 3.81 o 1 7 13 11.31 14.37 3.57 o 2 7 13 4.16 3.25 2.69 o 0 8 13 28.18 39.72 4.83 o 1 8 13 38.96 41.61 5.21 o 0 0 14 54.09 49.40 4.58 o 1 0 14 107.37 108.22 6.27 o 2 0 14 0.27 -2.17 2.17 o 3 0 14 57.20 58.70 5.74 o 4 0 14 20.13 30.10 3.81 o 0 1 14 3.93 7.90 1.71 o 1 1 14 19.69 14.47 3.01 o 2 1 14 14.39 18.39 2.94 o 3 1 14 10.33 16.71 2.62 o 4 1 14 0.94 -2.90 2.90 o 0 2 14 2.90 2.17 1.75 o 1 2 14 25.15 21.71 3.39 o 2 2 14 12.77 13.04 3.22 o 3 2 14 7.77 5.52 2.62 o 4 2 14 15.20 17.16 3.22 o 0 3 14 43.58 42.08 4.51 o 1 3 14 264.87 246.97 9.83 o 2 3 14 46.44 48.02 4.72 o 3 3 14 19.02 25.42 3.85 o 0 4 14 363.96 364.29 11.95 o 1 4 14 19.74 25.35 3.18 o 2 4 14 25.21 21.99 3.53 o 3 4 14 1.31 -0.38 1.78 o 0 5 14 42.82 46.16 4.69 o 1 5 14 90.51 103.66 6.58 o 2 5 14 79.51 83.24 6.12 o 3 5 14 10.32 13.21 2.94 o 0 6 14 11.14 10.42 2.90 o 1 6 14 4.76 5.80 2.76 o 2 6 14 11.20 12.90 3.18 o 0 7 14 30.34 31.22 4.72 o 1 7 14 5.88 9.96 3.04 o 1 0 15 0.11 -0.31 1.96 o 2 0 15 1.06 2.13 1.75 o 3 0 15 0.01 -0.73 1.71 o 0 1 15 0.00 0.00 1.78 o 1 1 15 87.86 84.20 5.63 o 2 1 15 3.41 5.00 2.20 o 3 1 15 11.99 8.98 2.69 o 0 2 15 1.50 1.71 2.17 o 1 2 15 5.16 3.43 2.17 o 2 2 15 6.60 6.54 1.78 o 3 2 15 9.20 2.80 3.39 o 0 3 15 151.39 155.14 8.02 o 1 3 15 2.60 2.13 2.45 o 2 3 15 105.90 102.10 6.69 o 3 3 15 15.41 17.93 3.78 o 0 4 15 56.02 55.23 5.18 o 1 4 15 163.47 180.97 8.97 o 2 4 15 45.44 47.88 5.00 o 3 4 15 18.99 21.08 3.15 o 0 5 15 23.37 19.82 4.20 o 1 5 15 74.41 74.42 6.12 o 2 5 15 14.08 11.01 3.25 o 0 6 15 13.78 23.18 3.71 o 1 6 15 0.22 0.00 2.13 o 0 0 16 10.42 9.30 2.94 o 1 0 16 1.34 2.90 2.24 o 2 0 16 0.47 0.38 1.92 o 3 0 16 8.96 13.81 2.80 o 0 1 16 275.96 257.28 10.39 o 1 1 16 17.35 13.95 3.64 o 2 1 16 17.44 18.91 3.43 o 3 1 16 2.55 4.19 2.24 o 0 2 16 89.29 85.99 6.12 o 1 2 16 6.87 5.59 2.83 o 2 2 16 11.82 9.40 3.04 o 3 2 16 15.28 20.07 3.43 o 0 3 16 11.89 7.24 2.97 o 1 3 16 30.21 35.00 4.23 o 2 3 16 15.25 12.48 3.57 o 0 4 16 2.39 5.98 2.48 o 1 4 16 57.37 70.13 5.67 o 2 4 16 124.98 127.82 8.58 o 0 5 16 9.12 8.77 3.15 o 1 5 16 54.31 60.23 5.63 o 1 0 17 31.57 26.09 3.88 o 2 0 17 11.81 10.80 2.76 o 0 1 17 23.50 19.19 3.74 o 1 1 17 37.05 46.58 5.04 o 2 1 17 4.11 5.00 2.27 o 0 2 17 8.34 13.56 3.04 o 1 2 17 14.42 19.02 2.94 o 2 2 17 5.64 9.72 2.52 o 0 3 17 26.20 26.36 3.99 o 1 3 17 19.64 22.06 3.64 o 2 3 17 1.60 0.87 2.69 o 0 4 17 0.11 6.43 1.68 o 1 4 17 19.05 15.56 3.95 o 0 0 18 13.75 6.75 2.66 o 1 0 18 60.53 52.61 5.49 o 0 1 18 0.33 0.42 2.13 o 1 1 18 12.92 13.35 3.18 o 0 2 18 5.83 9.47 3.29 o 1 2 18 2.35 1.33 2.52 o