#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/39/2213926.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213926_Fobs loop_ _publ_author_name 'How, Fiona N.-F.' 'Watkin, David J.' 'Crouse, Karen A.' 'Tahir, M. Ibrahim M.' _publ_section_title ; Benzyl N'-[1-(3-pyridyl)ethylidene]hydrazinecarbodithioate ; _journal_coeditor_code PK2024 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3023 _journal_page_last o3024 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _audit_creation_date 07-05-15 _audit_creation_method CRYSTALS _cell_angle_alpha 90 _cell_angle_beta 93.2187(7) _cell_angle_gamma 90 _cell_length_a 11.7234(2) _cell_length_b 13.5577(2) _cell_length_c 9.36370(10) _[local]_cod_data_source_file pk2024Isup2.hkl _[local]_cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma _refln_observed_status 0 0 4 40.10 55.03 1.70 o 0 0 6 5327.70 5030.63 102.50 o 0 0 8 3.80 4.93 1.30 o 0 0 10 442.60 448.54 10.50 o 0 0 12 229.10 225.19 11.40 o 0 -1 3 146.70 178.15 3.06 o 0 -1 4 1999.65 2013.15 35.97 o 0 -1 5 1604.75 1616.33 29.91 o 0 -1 6 224.45 182.51 4.98 o 0 -1 7 1042.35 970.58 22.65 o 0 -1 8 14.10 10.45 1.73 o 0 -1 9 6.45 8.47 1.59 o 0 -1 10 293.00 290.11 7.20 o 0 -1 11 39.05 36.46 4.09 o 0 -1 12 105.90 137.07 5.60 o 0 -2 2 9.25 7.96 0.82 o 0 -2 3 7409.70 7725.18 150.88 o 0 -2 4 11.35 11.72 1.26 o 0 -2 5 1971.85 1905.55 35.80 o 0 -2 6 583.20 625.04 11.40 o 0 -2 7 31.30 27.82 2.00 o 0 -2 8 130.25 130.56 3.98 o 0 -2 9 54.80 49.37 2.77 o 0 -2 10 542.50 535.60 15.83 o 0 -2 11 8.85 8.27 2.35 o 0 -2 12 110.90 138.85 9.10 o 0 -3 2 5165.70 5545.29 100.59 o 0 -3 3 563.50 579.70 10.25 o 0 -3 4 2683.05 2714.47 46.71 o 0 -3 5 14.70 19.00 1.20 o 0 -3 6 218.05 209.66 4.76 o 0 -3 7 950.65 970.98 19.96 o 0 -3 8 142.10 140.38 4.20 o 0 -3 9 1560.25 1418.32 36.60 o 0 -3 10 -1.90 0.11 2.02 o 0 -3 11 14.05 20.18 4.70 o 0 -3 12 218.50 224.02 11.10 o 0 -4 0 112.00 58.80 5.40 o 0 -4 1 16.95 26.97 0.96 o 0 -4 2 145.75 156.83 3.21 o 0 -4 3 1316.10 1334.84 22.02 o 0 -4 4 473.30 519.36 8.76 o 0 -4 5 1908.65 1886.22 37.79 o 0 -4 6 453.75 439.70 9.91 o 0 -4 7 1138.35 1087.84 23.90 o 0 -4 8 2258.15 2114.21 51.35 o 0 -4 9 48.60 46.14 2.69 o 0 -4 10 49.45 58.98 3.52 o 0 -4 11 315.75 325.05 18.16 o 0 -5 1 53.50 96.99 2.00 o 0 -5 2 12.00 5.79 0.70 o 0 -5 3 375.80 331.10 6.80 o 0 -5 4 285.75 224.60 5.06 o 0 -5 5 588.45 600.27 10.93 o 0 -5 6 2031.55 2017.04 41.16 o 0 -5 7 383.00 399.74 8.95 o 0 -5 8 206.05 209.74 6.04 o 0 -5 9 6.60 5.11 1.40 o 0 -5 10 834.40 797.07 33.49 o 0 -5 11 4.20 4.19 3.41 o 0 -6 0 45.95 42.62 2.70 o 0 -6 1 429.90 385.96 9.10 o 0 -6 2 21.85 30.59 1.14 o 0 -6 3 1.50 5.86 0.65 o 0 -6 4 1183.15 1101.11 21.82 o 0 -6 5 4143.95 4038.64 80.18 o 0 -6 6 412.65 418.70 9.14 o 0 -6 7 1994.20 1817.74 44.24 o 0 -6 8 19.60 26.39 1.60 o 0 -6 9 621.35 591.89 14.86 o 0 -6 10 11.85 19.48 2.41 o 0 -6 11 1079.65 1063.64 60.62 o 0 -7 1 1486.10 1358.09 30.95 o 0 -7 2 2100.25 1869.40 40.14 o 0 -7 3 264.85 303.39 5.10 o 0 -7 4 737.60 715.61 14.30 o 0 -7 5 199.50 210.61 4.47 o 0 -7 6 1966.20 1897.77 41.25 o 0 -7 7 1175.90 1104.81 29.64 o 0 -7 8 2.80 1.28 1.60 o 0 -7 9 666.25 678.80 20.93 o 0 -7 10 800.10 811.21 44.27 o 0 -7 11 2.30 5.32 4.64 o 0 -8 0 578.10 527.29 20.35 o 0 -8 1 821.45 770.19 15.84 o 0 -8 2 415.35 402.17 8.22 o 0 -8 3 2.95 4.16 1.16 o 0 -8 4 251.85 238.70 5.53 o 0 -8 5 637.85 634.05 12.87 o 0 -8 6 242.55 244.02 6.28 o 0 -8 7 438.05 432.16 12.04 o 0 -8 8 539.15 565.31 14.69 o 0 -8 9 104.00 118.38 4.97 o 0 -8 10 203.65 237.88 12.46 o 0 -8 11 0.50 0.83 6.36 o 0 -9 1 92.20 109.29 2.38 o 0 -9 2 543.20 537.18 11.25 o 0 -9 3 2387.30 2440.12 56.91 o 0 -9 4 156.05 163.47 4.36 o 0 -9 5 9.90 10.69 1.18 o 0 -9 6 15.70 14.87 1.33 o 0 -9 7 1354.20 1280.87 32.09 o 0 -9 8 228.70 227.77 6.97 o 0 -9 9 78.10 76.55 4.89 o 0 -9 10 0.60 0.07 3.38 o 0 -10 0 1313.90 1285.62 32.36 o 0 -10 1 1019.80 1037.88 19.63 o 0 -10 2 1808.45 1782.26 38.44 o 0 -10 3 598.15 610.89 15.46 o 0 -10 4 1504.50 1464.38 42.42 o 0 -10 5 4.60 1.62 1.14 o 0 -10 6 73.05 75.84 2.55 o 0 -10 7 90.55 108.60 3.55 o 0 -10 8 777.15 801.47 29.64 o 0 -10 9 56.50 81.66 4.92 o 0 -10 10 11.40 12.46 3.35 o 0 -11 1 1743.30 1716.90 38.65 o 0 -11 2 42.10 56.33 2.43 o 0 -11 3 538.75 507.85 15.28 o 0 -11 4 867.45 867.49 25.36 o 0 -11 5 349.70 346.74 11.49 o 0 -11 6 268.20 267.08 7.21 o 0 -11 7 59.05 64.31 3.32 o 0 -11 8 69.75 88.83 5.09 o 0 -11 9 111.75 137.26 7.88 o 0 -12 0 342.70 319.30 9.27 o 0 -12 1 1443.40 1449.55 33.63 o 0 -12 2 265.75 258.25 6.85 o 0 -12 3 409.15 364.81 11.72 o 0 -12 4 418.70 401.33 13.63 o 0 -12 5 855.30 832.71 23.97 o 0 -12 6 39.25 38.64 2.55 o 0 -12 7 72.40 80.95 4.14 o 0 -12 8 40.05 45.70 4.48 o 0 -12 9 10.10 16.68 3.00 o 0 -13 1 394.55 406.76 10.57 o 0 -13 2 594.05 568.83 15.56 o 0 -13 3 1265.30 1281.76 34.67 o 0 -13 4 685.75 677.76 21.69 o 0 -13 5 688.00 737.95 23.64 o 0 -13 6 66.65 82.34 3.87 o 0 -13 7 1.75 0.32 5.23 o 0 -13 8 -3.30 0.01 2.80 o 0 -14 0 205.65 238.73 10.50 o 0 -14 1 248.85 241.81 7.17 o 0 -14 2 34.00 28.89 2.16 o 0 -14 3 1157.75 1058.72 37.00 o 0 -14 4 10.80 15.83 2.25 o 0 -14 5 3.45 4.49 2.22 o 0 -14 6 60.15 73.55 5.57 o 0 -14 7 299.20 339.70 11.70 o 0 -15 1 455.90 410.47 13.43 o 0 -15 2 271.45 286.31 11.19 o 0 -15 3 78.35 89.82 4.85 o 0 -15 4 483.20 470.98 28.20 o 0 -15 5 256.65 285.57 18.20 o 0 -15 6 81.80 87.95 6.47 o 0 -16 0 318.90 307.47 13.00 o 0 -16 1 160.10 161.62 5.50 o 0 -16 2 -1.95 1.70 1.71 o 0 -16 3 279.15 287.80 17.86 o 0 -16 4 337.20 327.53 13.20 o 0 -16 5 4.60 9.15 2.50 o 0 -17 1 455.70 431.16 14.80 o 0 -17 2 196.20 206.53 6.50 o 0 -17 3 55.00 63.91 3.20 o 1 0 -12 255.00 257.27 11.50 o 1 0 -10 424.60 409.11 11.80 o 1 0 -8 2.40 0.55 1.60 o 1 0 -6 1727.70 1856.27 35.10 o 1 0 -4 1136.20 1255.42 19.00 o 1 0 4 5.70 5.16 1.00 o 1 0 6 4566.90 4345.64 90.10 o 1 0 8 317.40 284.06 6.90 o 1 0 10 1553.30 1524.29 38.70 o 1 0 12 71.40 62.63 6.80 o 1 -1 -12 81.55 96.52 4.90 o 1 -1 -11 1652.00 1553.58 79.52 o 1 -1 -10 19.50 22.86 1.80 o 1 -1 -9 895.10 901.39 24.90 o 1 -1 -8 560.30 581.64 13.70 o 1 -1 -7 814.10 795.21 17.45 o 1 -1 -6 3.60 11.76 1.33 o 1 -1 -5 2553.70 2723.03 46.97 o 1 -1 -4 210.70 220.10 4.36 o 1 -1 -3 877.10 859.31 16.57 o 1 -1 3 827.00 932.23 15.82 o 1 -1 4 2199.25 2153.63 38.50 o 1 -1 5 557.60 643.10 10.55 o 1 -1 6 13.75 7.33 1.52 o 1 -1 7 176.10 194.69 4.09 o 1 -1 8 857.65 859.25 19.35 o 1 -1 9 2.95 4.22 1.50 o 1 -1 10 309.95 307.22 8.12 o 1 -1 11 687.90 664.77 27.95 o 1 -1 12 32.20 32.08 5.00 o 1 -2 -12 18.45 23.48 4.26 o 1 -2 -11 4.85 4.03 3.04 o 1 -2 -10 733.50 728.06 22.35 o 1 -2 -9 580.55 591.30 14.31 o 1 -2 -8 278.70 295.70 6.98 o 1 -2 -7 1757.25 1726.14 35.64 o 1 -2 -6 225.00 218.50 4.75 o 1 -2 -5 295.30 259.46 6.01 o 1 -2 -4 46.35 55.42 1.46 o 1 -2 -3 563.35 593.03 10.61 o 1 -2 -2 3431.05 3553.51 74.09 o 1 -2 2 2174.25 2233.26 50.83 o 1 -2 3 400.35 461.85 7.79 o 1 -2 4 2642.70 2570.15 53.46 o 1 -2 5 496.10 514.21 9.31 o 1 -2 6 0.50 3.92 1.22 o 1 -2 7 1358.35 1353.78 28.35 o 1 -2 8 61.50 58.19 2.69 o 1 -2 9 775.05 736.11 18.70 o 1 -2 10 245.20 260.11 6.71 o 1 -2 11 81.60 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0.57 3.16 o 1 -9 -9 13.10 14.99 3.23 o 1 -9 -8 244.35 249.28 7.40 o 1 -9 -7 520.25 535.13 15.42 o 1 -9 -6 47.60 51.22 2.07 o 1 -9 -5 433.65 420.37 8.59 o 1 -9 -4 485.10 502.28 10.20 o 1 -9 -3 3584.40 3600.80 73.12 o 1 -9 -2 116.20 109.42 3.06 o 1 -9 -1 1415.00 1395.25 27.23 o 1 -9 0 1276.35 1272.79 32.21 o 1 -9 1 898.85 971.15 20.19 o 1 -9 2 68.90 67.90 2.85 o 1 -9 3 5155.60 5050.61 117.34 o 1 -9 4 907.65 892.32 19.87 o 1 -9 5 168.95 164.85 4.37 o 1 -9 6 1.35 0.05 1.45 o 1 -9 7 1.65 1.89 1.32 o 1 -9 8 152.80 162.93 5.06 o 1 -9 9 104.20 115.13 6.30 o 1 -9 10 50.75 61.35 4.54 o 1 -10 -10 298.90 305.61 14.30 o 1 -10 -9 285.75 305.05 14.91 o 1 -10 -8 161.55 168.60 6.18 o 1 -10 -7 421.60 416.60 11.82 o 1 -10 -6 4.50 7.70 1.30 o 1 -10 -5 829.65 784.10 20.25 o 1 -10 -4 1092.10 1063.88 22.65 o 1 -10 -3 185.20 180.87 4.65 o 1 -10 -2 247.05 276.25 5.65 o 1 -10 -1 5163.50 5198.50 105.25 o 1 -10 0 194.60 196.70 5.35 o 1 -10 1 90.30 108.62 3.06 o 1 -10 2 85.75 89.81 3.06 o 1 -10 3 -0.95 0.77 1.67 o 1 -10 4 48.85 56.14 2.62 o 1 -10 5 153.25 166.92 4.26 o 1 -10 6 453.40 451.57 11.49 o 1 -10 7 50.30 61.56 2.29 o 1 -10 8 6.20 6.11 2.12 o 1 -10 9 58.50 73.96 5.11 o 1 -10 10 173.25 212.19 9.73 o 1 -11 -9 207.50 203.31 9.60 o 1 -11 -8 1.15 5.34 2.77 o 1 -11 -7 325.05 327.80 9.90 o 1 -11 -6 444.60 455.13 11.39 o 1 -11 -5 1596.20 1512.47 39.10 o 1 -11 -4 389.65 420.69 11.40 o 1 -11 -3 288.00 298.09 7.00 o 1 -11 -2 2465.95 2490.79 54.65 o 1 -11 -1 251.50 230.59 6.20 o 1 -11 0 368.15 386.06 8.13 o 1 -11 1 317.55 300.22 9.10 o 1 -11 2 219.15 259.93 5.41 o 1 -11 3 160.15 155.80 4.35 o 1 -11 4 708.55 690.66 20.46 o 1 -11 5 2243.90 2098.90 56.68 o 1 -11 6 -1.30 0.01 1.22 o 1 -11 7 1371.05 1322.99 47.88 o 1 -11 8 4.60 5.15 3.10 o 1 -11 9 3.15 5.29 3.47 o 1 -12 -9 44.50 52.33 4.30 o 1 -12 -8 -7.30 0.92 4.50 o 1 -12 -7 680.75 678.27 31.29 o 1 -12 -6 1451.90 1392.46 40.42 o 1 -12 -5 4.55 6.34 1.46 o 1 -12 -4 350.20 352.96 11.72 o 1 -12 -3 839.65 825.61 23.30 o 1 -12 -2 133.35 126.94 3.70 o 1 -12 -1 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2 -8 -8 1651.45 1584.57 41.36 o 2 -8 -7 22.15 19.50 1.61 o 2 -8 -6 127.05 152.68 3.30 o 2 -8 -5 1387.15 1363.80 26.64 o 2 -8 -4 1291.05 1332.65 23.67 o 2 -8 -3 871.30 859.98 18.27 o 2 -8 -2 16.60 10.65 1.16 o 2 -8 -1 75.55 63.96 2.12 o 2 -8 0 32.70 43.38 1.77 o 2 -8 1 1.30 3.24 1.11 o 2 -8 2 279.80 291.91 6.97 o 2 -8 3 1722.60 1638.16 39.32 o 2 -8 4 2522.60 2398.17 58.00 o 2 -8 5 270.95 263.00 7.60 o 2 -8 6 477.65 463.42 11.52 o 2 -8 7 597.40 591.46 14.98 o 2 -8 8 621.40 621.62 16.89 o 2 -8 9 115.30 121.79 5.26 o 2 -8 10 105.90 117.78 6.72 o 2 -9 -10 22.90 26.37 3.40 o 2 -9 -9 172.00 173.68 10.18 o 2 -9 -8 17.10 24.79 1.97 o 2 -9 -7 9.20 6.53 1.61 o 2 -9 -6 192.75 217.18 4.70 o 2 -9 -5 297.00 291.70 5.98 o 2 -9 -4 228.60 223.24 5.36 o 2 -9 -3 18.45 21.42 1.67 o 2 -9 -2 39.25 33.15 1.86 o 2 -9 -1 198.80 200.48 4.26 o 2 -9 0 203.20 208.02 5.60 o 2 -9 1 1023.35 1040.76 23.79 o 2 -9 2 1109.10 1108.40 25.15 o 2 -9 3 489.05 535.38 11.54 o 2 -9 4 85.60 92.16 4.06 o 2 -9 5 1010.25 989.57 21.50 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10 339.75 342.03 12.28 o 4 -4 11 6.60 9.35 3.50 o 4 -5 -11 -0.80 10.17 8.59 o 4 -5 -10 564.20 549.37 23.17 o 4 -5 -9 463.05 500.10 12.40 o 4 -5 -8 11.25 7.16 1.66 o 4 -5 -7 328.35 357.47 7.65 o 4 -5 -6 223.80 241.88 5.05 o 4 -5 -5 943.50 907.05 18.31 o 4 -5 -4 422.80 441.70 9.25 o 4 -5 -3 365.30 386.20 7.28 o 4 -5 -2 5334.95 4978.77 115.41 o 4 -5 -1 14.25 17.16 0.85 o 4 -5 0 1997.00 1978.91 56.96 o 4 -5 1 8.50 22.74 0.70 o 4 -5 2 14.90 5.44 1.55 o 4 -5 3 1229.30 1202.24 23.27 o 4 -5 4 2215.00 2146.93 48.67 o 4 -5 5 411.10 393.49 9.90 o 4 -5 6 5177.75 4756.13 175.01 o 4 -5 7 631.15 612.06 18.43 o 4 -5 8 116.80 113.15 3.86 o 4 -5 9 156.50 154.60 5.68 o 4 -5 10 5.90 7.12 1.46 o 4 -5 11 -3.60 1.20 3.80 o 4 -6 -11 94.00 91.21 9.60 o 4 -6 -10 18.00 25.64 3.05 o 4 -6 -9 1238.35 1128.38 33.26 o 4 -6 -8 7.95 6.77 1.87 o 4 -6 -7 179.65 171.50 4.96 o 4 -6 -6 422.90 419.66 9.35 o 4 -6 -5 175.15 215.10 4.26 o 4 -6 -4 347.05 380.46 7.20 o 4 -6 -3 910.70 955.40 19.29 o 4 -6 -2 3.30 2.52 1.36 o 4 -6 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15.44 6.65 o 12 -2 -8 363.40 392.93 26.05 o 12 -2 -7 214.75 217.36 9.45 o 12 -2 -6 6.10 7.60 2.26 o 12 -2 -5 1025.70 951.31 31.70 o 12 -2 -4 26.60 30.88 2.15 o 12 -2 -3 59.40 61.03 2.55 o 12 -2 -2 309.75 329.48 8.70 o 12 -2 -1 659.45 623.30 20.33 o 12 -2 0 662.95 653.29 20.23 o 12 -2 1 6.75 9.31 1.36 o 12 -2 2 1.45 0.03 2.05 o 12 -2 3 623.55 632.63 25.17 o 12 -2 4 18.90 26.22 1.80 o 12 -2 5 101.30 127.82 9.40 o 12 -2 6 626.10 569.21 34.90 o 12 -3 -7 1.20 1.27 3.01 o 12 -3 -6 1326.75 1239.94 54.12 o 12 -3 -5 23.25 28.30 2.45 o 12 -3 -4 744.80 726.49 21.40 o 12 -3 -3 304.35 318.32 8.70 o 12 -3 -2 170.60 178.04 5.40 o 12 -3 -1 2460.05 2330.92 85.36 o 12 -3 0 54.65 60.70 2.75 o 12 -3 1 140.90 145.53 5.26 o 12 -3 2 155.00 164.60 4.98 o 12 -3 3 17.50 20.98 1.46 o 12 -3 4 68.10 67.43 3.00 o 12 -3 5 876.50 848.43 53.10 o 12 -3 6 278.40 258.92 18.50 o 12 -4 -7 181.00 177.17 11.46 o 12 -4 -6 -2.80 0.10 3.68 o 12 -4 -5 268.75 266.25 9.95 o 12 -4 -4 600.40 591.08 15.79 o 12 -4 -3 6.15 9.32 1.39 o 12 -4 -2 331.80 325.33 12.61 o 12 -4 -1 488.05 471.69 17.06 o 12 -4 0 335.15 333.64 10.03 o 12 -4 1 529.65 523.94 17.98 o 12 -4 2 40.55 46.64 2.14 o 12 -4 3 126.50 135.15 5.72 o 12 -4 4 142.10 132.15 5.40 o 12 -4 5 176.30 178.52 11.80 o 12 -4 6 298.30 322.37 19.90 o 12 -5 -7 21.35 34.31 4.79 o 12 -5 -6 20.75 43.60 3.61 o 12 -5 -5 15.55 11.68 4.06 o 12 -5 -4 141.45 147.88 5.99 o 12 -5 -3 84.40 94.10 5.77 o 12 -5 -2 161.75 170.23 7.25 o 12 -5 -1 144.10 163.20 5.41 o 12 -5 0 4.80 9.23 1.63 o 12 -5 1 573.85 569.18 17.49 o 12 -5 2 462.60 452.41 14.80 o 12 -5 3 94.70 108.68 4.53 o 12 -5 4 75.90 78.15 3.40 o 12 -5 5 50.20 56.77 4.00 o 12 -5 6 14.10 7.47 7.10 o 12 -6 -7 119.85 114.08 10.65 o 12 -6 -6 9.85 8.17 3.46 o 12 -6 -5 7.00 7.50 3.04 o 12 -6 -4 -0.50 0.15 4.59 o 12 -6 -3 637.75 622.15 25.62 o 12 -6 -2 99.90 105.02 5.15 o 12 -6 -1 28.25 33.74 2.60 o 12 -6 0 115.10 129.53 4.47 o 12 -6 1 89.30 79.20 3.85 o 12 -6 2 461.40 466.75 21.07 o 12 -6 3 624.90 599.12 17.30 o 12 -6 4 3.00 0.13 1.80 o 12 -6 5 79.40 99.56 5.00 o 12 -6 6 -0.70 0.08 4.52 o 12 -7 -6 50.40 55.75 6.40 o 12 -7 -5 108.75 121.87 7.51 o 12 -7 -4 75.55 70.57 6.75 o 12 -7 -3 -1.85 0.39 3.61 o 12 -7 -2 748.10 756.69 27.25 o 12 -7 -1 100.10 106.46 4.02 o 12 -7 0 86.10 92.80 3.49 o 12 -7 1 223.75 214.37 7.10 o 12 -7 2 362.70 347.48 13.59 o 12 -7 3 235.20 226.86 8.10 o 12 -7 4 223.00 229.38 9.10 o 12 -7 5 119.90 123.66 6.10 o 12 -8 -5 14.65 20.94 4.91 o 12 -8 -4 56.25 51.76 6.39 o 12 -8 -3 77.05 84.46 5.97 o 12 -8 -2 28.95 32.03 2.73 o 12 -8 -1 89.75 94.53 4.18 o 12 -8 0 475.60 434.78 16.17 o 12 -8 1 138.85 144.27 5.98 o 12 -8 2 15.45 12.42 2.02 o 12 -8 3 1.70 3.09 1.60 o 12 -8 4 328.20 312.84 15.80 o 12 -9 -5 47.25 56.23 5.96 o 12 -9 -4 248.55 243.81 15.46 o 12 -9 -3 32.90 33.09 4.43 o 12 -9 -2 138.40 153.24 8.42 o 12 -9 -1 462.30 469.06 18.84 o 12 -9 0 68.30 71.99 3.97 o 12 -9 1 1079.10 1036.09 44.53 o 12 -9 2 256.20 264.90 13.76 o 12 -9 3 49.10 56.29 4.10 o 12 -9 4 60.40 83.28 5.30 o 12 -10 -4 3.30 0.37 4.17 o 12 -10 -3 243.30 261.14 15.73 o 12 -10 -2 210.35 229.39 14.47 o 12 -10 -1 144.60 157.84 8.10 o 12 -10 0 27.45 21.98 2.96 o 12 -10 1 28.65 29.52 2.80 o 12 -10 2 5.20 1.93 2.82 o 12 -11 -2 51.00 49.06 6.85 o 12 -11 -1 47.65 55.20 5.34 o 12 -11 0 159.35 156.35 10.22 o 12 -11 1 17.60 23.42 4.50 o 13 0 -6 6.00 2.02 4.30 o 13 0 -4 943.10 951.54 30.40 o 13 0 -2 142.80 134.73 4.80 o 13 0 0 4.50 5.59 1.90 o 13 0 2 399.10 398.39 20.20 o 13 0 6 224.40 186.72 13.70 o 13 -1 -7 106.55 100.28 10.39 o 13 -1 -6 9.70 13.98 4.30 o 13 -1 -5 9.75 6.17 3.29 o 13 -1 -4 350.50 353.82 16.06 o 13 -1 -3 422.40 424.97 17.36 o 13 -1 -2 0.05 2.37 1.91 o 13 -1 -1 1.80 5.92 1.50 o 13 -1 0 109.95 119.28 4.95 o 13 -1 1 158.45 144.11 7.67 o 13 -1 2 6.80 7.20 1.61 o 13 -1 3 324.20 302.60 17.87 o 13 -1 4 32.30 30.71 3.50 o 13 -1 5 33.20 42.05 7.30 o 13 -1 6 66.40 67.84 7.50 o 13 -2 -7 4.85 2.52 5.52 o 13 -2 -6 116.30 114.91 8.08 o 13 -2 -5 49.45 49.29 5.31 o 13 -2 -4 125.50 130.03 7.20 o 13 -2 -3 678.70 686.88 23.54 o 13 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4.83 o 13 -9 -2 44.15 42.20 5.54 o 13 -9 -1 98.20 111.28 6.39 o 13 -9 0 43.15 57.81 3.73 o 13 -9 1 250.75 268.40 14.86 o 14 0 -4 200.30 185.37 13.00 o 14 0 -2 329.80 343.24 20.50 o 14 0 0 259.90 280.35 11.40 o 14 0 2 19.00 27.71 4.00 o 14 0 4 34.10 31.71 5.30 o 14 -1 -5 4.15 1.77 4.17 o 14 -1 -4 155.85 163.72 10.26 o 14 -1 -3 238.45 233.72 14.18 o 14 -1 -2 23.45 28.43 3.20 o 14 -1 -1 9.80 11.96 3.89 o 14 -1 0 160.50 158.63 8.55 o 14 -1 1 377.65 390.02 23.18 o 14 -1 2 -1.15 3.65 4.50 o 14 -1 3 152.60 160.00 10.26 o 14 -1 4 19.90 13.59 5.50 o 14 -2 -5 416.20 439.25 23.99 o 14 -2 -4 35.10 45.68 4.30 o 14 -2 -3 21.35 23.86 4.67 o 14 -2 -2 465.90 480.61 22.93 o 14 -2 -1 85.50 76.31 5.20 o 14 -2 0 246.45 245.75 12.89 o 14 -2 1 -4.55 5.36 4.39 o 14 -2 2 331.95 342.36 21.16 o 14 -2 3 7.10 9.41 3.13 o 14 -2 4 15.40 10.96 3.49 o 14 -3 -5 79.05 94.57 8.15 o 14 -3 -4 296.60 295.83 17.18 o 14 -3 -3 143.70 161.13 10.30 o 14 -3 -2 22.15 22.53 3.98 o 14 -3 -1 69.65 90.10 5.79 o 14 -3 0 45.45 48.43 4.14 o 14 -3 1 757.35 734.37 39.36 o 14 -3 2 10.45 11.58 3.07 o 14 -3 3 16.35 11.48 4.33 o 14 -3 4 56.00 60.51 5.40 o 14 -4 -4 520.60 559.49 33.60 o 14 -4 -3 112.75 107.61 9.60 o 14 -4 -2 47.80 60.20 4.81 o 14 -4 -1 14.85 16.64 4.02 o 14 -4 0 208.55 218.48 11.06 o 14 -4 1 114.50 120.84 6.75 o 14 -4 2 300.80 311.16 16.19 o 14 -4 3 24.80 29.62 4.14 o 14 -5 -4 223.10 226.28 16.86 o 14 -5 -3 40.70 46.65 5.90 o 14 -5 -2 1657.75 1555.14 101.67 o 14 -5 -1 378.25 397.19 21.42 o 14 -5 0 125.65 135.28 6.50 o 14 -5 1 237.25 262.74 12.97 o 14 -5 2 402.55 406.95 23.32 o 14 -5 3 3.75 9.35 3.67 o 14 -6 -3 372.85 355.20 24.01 o 14 -6 -2 77.95 90.55 7.51 o 14 -6 -1 456.35 441.40 21.55 o 14 -6 0 81.00 93.90 5.89 o 14 -6 1 379.75 393.06 22.25 o 14 -6 2 -0.25 8.10 4.64 o 14 -7 -2 7.50 3.51 3.35 o 14 -7 -1 45.55 53.02 5.53 o 14 -7 0 116.05 132.58 7.71 o 14 -7 1 194.30 206.32 13.51 o 15 0 -2 1064.00 977.17 70.50 o 15 0 0 123.00 126.12 9.20 o 15 0 2 264.00 253.23 18.90 o 15 -1 -3 288.30 287.64 21.25 o 15 -1 -2 54.60 60.37 6.75 o 15 -1 -1 540.90 546.60 35.33 o 15 -1 0 98.10 97.63 7.85 o 15 -1 1 155.55 156.67 10.81 o 15 -1 2 72.45 76.29 7.34 o 15 -2 -3 120.60 133.73 10.76 o 15 -2 -2 61.35 69.37 7.19 o 15 -2 -1 8.05 9.42 4.79 o 15 -2 0 28.50 29.71 4.76 o 15 -2 1 194.85 188.30 14.11 o 15 -3 -2 99.30 125.40 9.18 o 15 -3 -1 142.15 157.36 10.60 o 15 -3 0 969.80 949.46 67.71 o 15 -3 1 223.40 259.29 16.90 o 15 -4 -1 2.10 4.98 3.97 o 15 -4 0 27.75 33.19 6.09 o