#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/39/2213931.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213931_Fobs loop_ _publ_author_name 'Hamed, Khemiri' 'Samah, Akriche' 'Mohamed, Rzaigui' _publ_section_title ; 3-Amino-2-chloropyridinium dihydrogenphosphate ; _journal_coeditor_code PV2010 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2896 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.726 _cell_angle_gamma 90.000 _cell_length_a 7.3907 _cell_length_b 16.2300 _cell_length_c 7.5038 _exptl_crystal_F_000 464.00 _reflns_d_resolution_high 0.8419 _[local]_cod_data_source_file pv2010Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' cad4 in P 21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 147.22 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 654.08 634.55 4.63 o 2 0 0 180.39 127.66 0.72 o 3 0 0 3815.23 3570.10 4.50 o 4 0 0 924.20 889.70 3.31 o 5 0 0 0.21 0.73 0.39 o 6 0 0 1.74 2.72 0.64 o 7 0 0 20.80 17.01 1.08 o 8 0 0 126.29 119.15 1.16 o 1 1 0 1371.92 1260.62 1.70 o 2 1 0 1166.81 1083.90 8.29 o 3 1 0 272.48 235.58 1.19 o 4 1 0 4172.39 3906.57 10.15 o 5 1 0 624.05 565.64 2.94 o 6 1 0 58.80 51.45 0.67 o 7 1 0 90.01 86.92 0.93 o 8 1 0 68.70 79.29 0.99 o 0 2 0 7.09 34.37 0.34 o 1 2 0 13284.02 11110.35 240.87 o 2 2 0 1490.16 1289.36 2.29 o 3 2 0 0.61 13.41 6.21 o 4 2 0 12.72 13.07 0.59 o 5 2 0 893.88 842.81 3.10 o 6 2 0 1710.96 1618.75 12.60 o 7 2 0 298.73 295.46 1.96 o 8 2 0 75.61 83.71 2.94 o 1 3 0 280.80 252.44 0.90 o 2 3 0 1276.49 1189.68 5.71 o 3 3 0 1018.78 1076.38 17.01 o 4 3 0 66.27 66.38 1.21 o 5 3 0 26.69 19.17 0.42 o 6 3 0 568.28 541.65 2.78 o 7 3 0 27.74 25.51 0.99 o 8 3 0 191.47 211.62 1.52 o 0 4 0 8979.23 8347.08 7.41 o 1 4 0 5642.92 5156.37 18.01 o 2 4 0 4283.15 4376.46 16.53 o 3 4 0 665.52 589.35 2.42 o 4 4 0 797.20 793.94 5.25 o 5 4 0 47.75 48.98 0.81 o 6 4 0 1.95 2.68 0.39 o 7 4 0 90.17 80.98 0.91 o 8 4 0 1.85 2.79 0.77 o 1 5 0 2099.36 2099.59 4.03 o 2 5 0 572.39 549.72 1.89 o 3 5 0 61.23 63.47 0.53 o 4 5 0 1545.38 1516.25 3.77 o 5 5 0 732.95 716.76 2.92 o 6 5 0 15.96 17.69 1.08 o 7 5 0 0.02 0.30 0.57 o 8 5 0 17.22 21.20 0.68 o 0 6 0 37.18 62.98 0.66 o 1 6 0 640.59 688.83 7.07 o 2 6 0 25.43 34.49 0.38 o 3 6 0 84.16 104.02 0.74 o 4 6 0 3.10 3.78 0.28 o 5 6 0 449.54 440.88 7.15 o 6 6 0 821.64 770.09 5.75 o 7 6 0 9.77 11.67 0.51 o 8 6 0 81.74 88.59 1.11 o 1 7 0 104.48 110.94 1.30 o 2 7 0 220.14 213.79 1.55 o 3 7 0 43.01 40.59 0.47 o 4 7 0 111.83 96.31 1.27 o 5 7 0 34.46 35.37 0.58 o 6 7 0 4.96 4.00 0.67 o 7 7 0 119.62 115.43 1.13 o 8 7 0 22.38 20.35 0.69 o 0 8 0 129.22 170.18 1.61 o 1 8 0 21.98 23.82 0.92 o 2 8 0 382.50 434.50 1.90 o 3 8 0 79.10 73.48 0.64 o 4 8 0 262.90 257.59 1.77 o 5 8 0 0.04 0.64 0.70 o 6 8 0 185.90 190.35 1.31 o 7 8 0 13.54 13.31 0.60 o 1 9 0 652.44 683.08 3.74 o 2 9 0 320.88 301.11 1.69 o 3 9 0 179.22 182.41 1.24 o 4 9 0 930.97 868.85 3.30 o 5 9 0 13.59 14.64 0.50 o 6 9 0 4.81 5.41 0.80 o 7 9 0 31.19 29.97 0.75 o 0 10 0 663.56 653.15 3.46 o 1 10 0 0.42 2.04 0.50 o 2 10 0 70.19 63.13 0.63 o 3 10 0 118.98 115.63 1.48 o 4 10 0 78.96 77.07 1.31 o 5 10 0 454.06 437.74 2.66 o 6 10 0 1.09 0.78 0.69 o 7 10 0 4.91 3.13 0.51 o 1 11 0 29.07 31.10 0.49 o 2 11 0 1323.01 1268.74 4.92 o 3 11 0 895.44 874.16 3.33 o 4 11 0 86.81 75.09 1.06 o 5 11 0 190.49 187.24 1.30 o 6 11 0 6.82 8.35 0.52 o 7 11 0 22.48 19.33 0.68 o 0 12 0 426.76 440.51 3.20 o 1 12 0 12.58 9.39 0.41 o 2 12 0 352.15 339.62 2.31 o 3 12 0 0.03 2.30 1.27 o 4 12 0 10.22 10.62 0.48 o 5 12 0 8.26 10.42 1.23 o 6 12 0 266.84 277.44 1.91 o 1 13 0 297.36 287.39 1.98 o 2 13 0 65.82 60.96 1.42 o 3 13 0 1076.01 1015.27 3.92 o 4 13 0 456.07 458.55 4.78 o 5 13 0 200.58 189.53 1.44 o 6 13 0 79.30 87.73 1.43 o 0 14 0 915.77 878.05 4.96 o 1 14 0 1053.40 1023.08 3.84 o 2 14 0 268.60 250.99 1.86 o 3 14 0 4.87 5.19 0.65 o 4 14 0 30.94 29.45 0.67 o 5 14 0 0.86 0.43 0.67 o 1 15 0 78.94 83.23 1.64 o 2 15 0 1394.63 1368.91 4.76 o 3 15 0 37.08 36.82 1.02 o 4 15 0 8.26 7.17 0.52 o 5 15 0 42.86 51.35 0.87 o 0 16 0 38.10 31.35 0.92 o 1 16 0 15.74 19.43 0.57 o 2 16 0 43.21 34.09 1.62 o 3 16 0 6.44 8.23 0.50 o 4 16 0 10.46 12.15 0.59 o 1 17 0 14.47 10.84 0.53 o 2 17 0 12.61 14.95 0.97 o 3 17 0 74.24 70.44 0.97 o 4 17 0 186.66 198.68 1.58 o 0 18 0 153.26 136.83 1.77 o 1 18 0 19.10 21.13 0.66 o 2 18 0 64.62 67.60 1.04 o 3 18 0 159.06 167.68 2.97 o 1 19 0 249.06 271.05 1.98 o -8 1 1 69.43 71.32 0.92 o -7 1 1 400.26 403.56 4.77 o -6 1 1 0.97 3.02 0.34 o -5 1 1 30.85 35.06 1.42 o -4 1 1 713.73 724.76 12.22 o -3 1 1 19.11 31.72 0.65 o -2 1 1 2194.69 2093.22 27.40 o -1 1 1 1029.77 1166.32 29.57 o 0 1 1 73.65 81.68 1.62 o 1 1 1 3482.54 3487.47 49.58 o 2 1 1 2660.62 2537.69 27.50 o 3 1 1 469.22 376.12 7.87 o 4 1 1 14.23 17.25 0.85 o 5 1 1 71.45 71.26 0.91 o 6 1 1 3.28 2.75 16.15 o 7 1 1 10.59 10.45 0.80 o 8 1 1 124.86 138.35 1.47 o -8 2 1 33.98 34.31 1.38 o -7 2 1 3.83 4.37 1.20 o -6 2 1 174.85 185.24 1.91 o -5 2 1 10.40 6.90 0.32 o -4 2 1 213.75 225.36 1.38 o -3 2 1 41.51 46.01 1.04 o -2 2 1 186.32 140.01 3.02 o -1 2 1 28.64 41.05 2.74 o 0 2 1 243.24 278.68 8.84 o 1 2 1 163.91 142.28 4.42 o 2 2 1 451.15 515.08 8.34 o 3 2 1 14.50 13.73 1.71 o 4 2 1 727.87 726.76 5.64 o 5 2 1 7.59 10.91 0.42 o 6 2 1 207.60 205.11 4.22 o 7 2 1 74.21 75.37 8.45 o 8 2 1 0.20 1.00 0.70 o -8 3 1 46.08 48.42 0.81 o -7 3 1 111.51 106.49 1.00 o -6 3 1 1297.71 1255.31 4.12 o -5 3 1 211.86 202.93 1.32 o -4 3 1 42.24 29.59 0.41 o -3 3 1 1693.25 1620.55 32.07 o -2 3 1 1467.89 1377.40 20.75 o -1 3 1 835.76 999.10 22.09 o 0 3 1 14.16 17.13 0.40 o 1 3 1 4510.42 4394.32 57.10 o 2 3 1 1621.49 1626.83 23.57 o 3 3 1 174.66 175.61 2.90 o 4 3 1 1.36 1.41 0.26 o 5 3 1 0.31 0.35 0.38 o 6 3 1 315.37 313.70 2.18 o 7 3 1 278.93 290.09 2.05 o 8 3 1 62.96 72.54 0.99 o -8 4 1 116.14 113.40 1.18 o -7 4 1 23.32 18.12 1.52 o -6 4 1 17.29 14.92 0.65 o -5 4 1 1593.59 1546.05 4.16 o -4 4 1 1375.84 1263.28 12.75 o -3 4 1 1228.84 1335.22 5.48 o -2 4 1 2431.53 2487.52 52.47 o -1 4 1 4373.56 4442.72 79.82 o 0 4 1 264.97 315.01 7.50 o 1 4 1 324.36 377.72 6.67 o 2 4 1 4040.94 3993.61 37.16 o 3 4 1 59.78 54.77 2.01 o 4 4 1 0.69 14.26 7.69 o 5 4 1 4.14 6.60 0.69 o 6 4 1 0.64 0.60 0.47 o 7 4 1 359.46 347.50 4.36 o 8 4 1 29.21 29.70 0.74 o -8 5 1 465.44 493.95 7.77 o -7 5 1 353.74 345.58 2.18 o -6 5 1 216.03 204.07 1.38 o -5 5 1 476.81 471.11 6.42 o -4 5 1 1.50 1.14 0.25 o -3 5 1 0.03 0.76 0.20 o -2 5 1 491.17 560.33 5.85 o -1 5 1 4755.37 4740.04 68.43 o 0 5 1 2245.70 2392.96 29.98 o 1 5 1 1.18 0.62 0.22 o 2 5 1 2083.73 2004.65 24.17 o 3 5 1 2911.96 2908.15 38.40 o 4 5 1 27.99 20.81 1.43 o 5 5 1 54.44 59.77 3.47 o 6 5 1 782.34 773.81 3.48 o 7 5 1 51.75 63.15 1.47 o 8 5 1 192.70 201.01 1.58 o -8 6 1 122.88 119.86 1.24 o -7 6 1 95.88 97.20 1.03 o -6 6 1 425.91 398.74 2.48 o -5 6 1 2.22 4.78 1.05 o -4 6 1 0.93 2.98 0.53 o -3 6 1 44.11 59.59 0.53 o -2 6 1 689.15 689.78 5.59 o -1 6 1 291.32 336.54 6.38 o 0 6 1 816.40 828.07 18.16 o 1 6 1 1513.21 1405.28 20.96 o 2 6 1 529.55 488.91 8.90 o 3 6 1 905.07 939.15 9.52 o 4 6 1 289.85 260.34 1.70 o 5 6 1 828.08 785.88 3.23 o 6 6 1 116.93 113.82 1.04 o 7 6 1 34.75 36.73 0.74 o 8 6 1 72.26 86.54 1.15 o -8 7 1 7.99 6.86 0.70 o -7 7 1 432.44 450.44 5.69 o -6 7 1 520.29 519.68 6.48 o -5 7 1 4.86 7.34 2.19 o -4 7 1 1074.75 1023.00 9.26 o -3 7 1 638.63 575.70 6.74 o -2 7 1 692.86 680.02 2.60 o -1 7 1 1409.08 1489.95 6.96 o 0 7 1 751.83 652.78 6.12 o 1 7 1 223.35 218.28 4.56 o 2 7 1 1482.41 1535.79 24.12 o 3 7 1 55.44 56.51 0.57 o 4 7 1 70.39 69.02 0.68 o 5 7 1 84.88 82.63 0.83 o 6 7 1 2.97 2.13 0.40 o 7 7 1 126.22 138.18 6.50 o -7 8 1 77.77 80.72 1.00 o -6 8 1 100.67 93.37 1.58 o -5 8 1 247.73 239.42 1.62 o -4 8 1 1630.33 1646.83 9.05 o -3 8 1 0.34 0.95 0.26 o -2 8 1 1868.87 1832.01 18.06 o -1 8 1 2033.30 2000.62 16.20 o 0 8 1 2773.47 2841.74 17.51 o 1 8 1 481.62 481.59 8.86 o 2 8 1 6.44 5.02 0.38 o 3 8 1 86.14 93.68 0.97 o 4 8 1 43.06 45.16 1.70 o 5 8 1 1.76 2.27 0.39 o 6 8 1 79.94 68.17 0.87 o 7 8 1 215.18 210.67 1.56 o -7 9 1 60.82 59.94 0.91 o -6 9 1 144.90 147.58 1.31 o -5 9 1 656.49 622.21 3.19 o -4 9 1 168.54 166.01 1.33 o -3 9 1 344.11 344.33 2.05 o -2 9 1 19.65 25.91 1.87 o -1 9 1 270.56 234.27 3.28 o 0 9 1 3998.20 4153.22 59.62 o 1 9 1 235.84 266.64 1.57 o 2 9 1 1757.17 1692.84 22.07 o 3 9 1 1753.05 1709.87 11.53 o 4 9 1 552.95 563.84 9.84 o 5 9 1 578.32 572.42 3.41 o 6 9 1 227.33 241.40 1.69 o 7 9 1 286.67 307.72 2.19 o -7 10 1 231.28 232.11 2.27 o -6 10 1 108.60 102.65 2.35 o -5 10 1 30.03 35.31 0.64 o -4 10 1 894.95 870.66 10.02 o -3 10 1 17.60 18.89 0.53 o -2 10 1 6.34 6.24 0.32 o -1 10 1 55.74 43.72 0.57 o 0 10 1 403.33 367.28 6.77 o 1 10 1 2799.08 2819.77 20.24 o 2 10 1 832.49 796.71 8.35 o 3 10 1 8.54 8.53 0.42 o 4 10 1 833.14 791.30 3.37 o 5 10 1 523.91 512.88 4.67 o 6 10 1 54.20 54.02 0.84 o 7 10 1 13.52 15.75 0.71 o -7 11 1 290.11 305.84 2.10 o -6 11 1 84.15 96.18 1.04 o -5 11 1 1.61 1.22 1.18 o -4 11 1 527.98 503.97 2.74 o -3 11 1 502.97 478.20 2.97 o -2 11 1 670.70 656.49 2.75 o -1 11 1 3.29 10.42 2.86 o 0 11 1 156.83 170.05 1.20 o 1 11 1 1274.60 1211.53 3.64 o 2 11 1 114.30 122.90 1.31 o 3 11 1 121.03 122.06 1.07 o 4 11 1 191.37 190.25 1.38 o 5 11 1 136.47 131.69 1.31 o 6 11 1 27.08 24.91 0.68 o -6 12 1 9.93 11.69 0.55 o -5 12 1 278.76 281.02 3.70 o -4 12 1 461.13 467.30 2.74 o -3 12 1 99.40 88.69 1.38 o -2 12 1 14.75 13.33 1.00 o -1 12 1 994.49 989.06 3.44 o 0 12 1 148.93 164.32 2.70 o 1 12 1 221.31 215.74 1.46 o 2 12 1 30.35 30.12 1.14 o 3 12 1 2.44 2.71 0.40 o 4 12 1 1.52 1.76 0.40 o 5 12 1 2.34 1.22 0.53 o 6 12 1 119.37 109.94 2.14 o -6 13 1 1.60 2.61 1.01 o -5 13 1 177.99 166.31 1.33 o -4 13 1 14.91 16.49 0.59 o -3 13 1 2.33 3.47 0.44 o -2 13 1 49.71 55.94 0.77 o -1 13 1 469.86 459.85 2.51 o 0 13 1 28.31 26.00 0.53 o 1 13 1 10.34 8.25 0.44 o 2 13 1 1185.90 1194.60 9.89 o 3 13 1 68.00 63.39 0.86 o 4 13 1 73.78 72.80 0.91 o 5 13 1 24.05 21.66 0.64 o 6 13 1 46.66 51.95 1.05 o -6 14 1 164.04 165.27 1.46 o -5 14 1 13.80 14.31 0.84 o -4 14 1 0.18 -0.22 0.47 o -3 14 1 33.14 37.99 0.67 o -2 14 1 3.01 1.40 0.78 o -1 14 1 34.98 42.82 0.70 o 0 14 1 161.64 166.88 2.92 o 1 14 1 394.05 396.19 6.21 o 2 14 1 267.36 263.57 2.32 o 3 14 1 24.06 24.00 1.18 o 4 14 1 333.76 341.55 2.27 o 5 14 1 188.21 190.50 1.50 o -5 15 1 7.60 9.09 0.57 o -4 15 1 0.12 0.95 0.51 o -3 15 1 92.24 92.82 0.99 o -2 15 1 64.03 65.20 0.85 o -1 15 1 3.99 5.48 0.43 o 0 15 1 118.44 114.22 1.10 o 1 15 1 107.26 111.81 1.03 o 2 15 1 12.97 9.48 0.53 o 3 15 1 25.34 21.95 0.63 o 4 15 1 23.85 22.68 1.29 o 5 15 1 0.21 0.33 0.68 o -4 16 1 85.87 79.30 2.06 o -3 16 1 71.61 75.24 1.36 o -2 16 1 38.69 34.54 0.83 o -1 16 1 41.96 45.66 0.92 o 0 16 1 249.51 251.60 1.87 o 1 16 1 27.36 28.72 0.63 o 2 16 1 11.65 11.12 0.54 o 3 16 1 42.77 44.56 0.80 o 4 16 1 33.98 39.80 0.91 o -4 17 1 13.24 13.91 0.76 o -3 17 1 19.29 16.30 1.16 o -2 17 1 6.46 7.07 0.64 o -1 17 1 17.12 16.73 0.60 o 0 17 1 25.81 26.81 0.79 o 1 17 1 31.82 34.54 1.31 o 2 17 1 4.90 5.20 0.52 o 3 17 1 2.17 2.56 0.50 o -3 18 1 0.12 -0.76 0.76 o -2 18 1 0.10 0.75 0.55 o -1 18 1 157.25 161.68 1.39 o 0 18 1 126.76 126.97 1.23 o 1 18 1 45.84 50.06 0.85 o 2 18 1 2.19 1.74 1.29 o -1 19 1 1.08 2.21 0.53 o 0 19 1 13.12 14.10 1.24 o -8 0 2 166.24 167.01 4.98 o -7 0 2 62.92 74.09 2.52 o -6 0 2 1588.92 1535.04 23.44 o -5 0 2 3104.52 2908.86 40.87 o -4 0 2 75.49 61.98 1.86 o -3 0 2 14905.38 13118.54 268.24 o -2 0 2 6961.15 6931.63 203.21 o -1 0 2 3855.97 3821.85 114.07 o 0 0 2 178.56 172.27 6.83 o 1 0 2 3199.10 3218.27 119.85 o 2 0 2 2.54 2.70 0.20 o 3 0 2 114.43 111.86 2.78 o 4 0 2 22.97 22.31 0.43 o 5 0 2 1850.22 1769.35 25.46 o 6 0 2 1233.23 1173.13 6.79 o 7 0 2 140.01 147.76 3.18 o 8 0 2 23.63 28.11 0.76 o -8 1 2 123.45 138.54 1.92 o -7 1 2 629.69 625.67 7.31 o -6 1 2 210.75 200.91 3.34 o -5 1 2 257.02 223.63 5.55 o -4 1 2 1268.98 1258.81 24.89 o -3 1 2 1.93 6.64 1.60 o -2 1 2 380.43 381.60 9.15 o -1 1 2 11.51 55.78 43.04 o 0 1 2 11564.82 12225.74 352.86 o 1 1 2 21672.28 18916.61 633.79 o 2 1 2 422.73 410.18 4.83 o 3 1 2 276.93 286.88 13.02 o 4 1 2 353.17 319.93 11.34 o 5 1 2 272.59 259.51 1.99 o 6 1 2 0.36 -0.11 0.54 o 7 1 2 81.60 81.17 2.76 o 8 1 2 112.82 123.47 1.28 o -8 2 2 20.22 23.58 0.64 o -7 2 2 18.96 21.39 0.57 o -6 2 2 325.44 325.76 3.80 o -5 2 2 57.50 60.67 1.36 o -4 2 2 44.91 20.86 0.37 o -3 2 2 246.03 210.44 3.12 o -2 2 2 1425.18 1587.98 35.93 o -1 2 2 5076.13 5179.54 102.64 o 0 2 2 10801.61 11041.56 294.56 o 1 2 2 1938.44 2110.58 44.90 o 2 2 2 0.74 0.85 0.37 o 3 2 2 1831.70 1735.95 9.34 o 4 2 2 3243.35 3185.45 57.56 o 5 2 2 21.25 23.27 0.78 o 6 2 2 46.77 47.76 0.71 o 7 2 2 103.64 93.28 1.04 o 8 2 2 0.41 1.13 1.02 o -8 3 2 35.51 36.97 0.76 o -7 3 2 4.71 3.86 0.42 o -6 3 2 7.91 9.91 0.61 o -5 3 2 1071.01 1035.07 6.68 o -4 3 2 594.20 601.34 10.76 o -3 3 2 788.19 860.00 15.08 o -2 3 2 97.88 75.40 1.20 o -1 3 2 3983.53 4194.83 138.45 o 0 3 2 1392.54 1607.99 49.35 o 1 3 2 7.96 8.90 1.06 o 2 3 2 8.12 3.70 1.01 o 3 3 2 1258.12 1311.42 18.01 o 4 3 2 280.78 261.24 3.41 o 5 3 2 180.16 177.31 2.40 o 6 3 2 0.04 0.00 0.74 o 7 3 2 51.07 51.34 0.83 o 8 3 2 16.41 19.50 0.66 o -8 4 2 199.15 216.84 1.88 o -7 4 2 184.78 202.22 4.69 o -6 4 2 693.99 664.18 4.72 o -5 4 2 3110.11 3006.67 6.29 o -4 4 2 83.71 92.66 2.50 o -3 4 2 1310.78 1381.72 20.73 o -2 4 2 913.31 890.93 19.82 o -1 4 2 117.00 155.27 3.78 o 0 4 2 51.49 48.79 1.52 o 1 4 2 549.54 642.79 18.41 o 2 4 2 498.07 521.63 10.98 o 3 4 2 84.43 105.33 1.67 o 4 4 2 37.14 31.59 0.49 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