#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:30:52 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181059 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/39/2213945.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213945_Fobs loop_ _publ_author_name 'Bahadur, S. Asath' 'Kannan, R. Sayee' 'Sridhar, B.' _publ_section_title ; Creatininium hydrogen oxalate monohydrate ; _journal_coeditor_code RZ2133 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2387 _journal_page_last o2389 _journal_volume 63 _journal_year 2007 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.1728 _cell_length_b 6.3520 _cell_length_c 16.6567 _exptl_crystal_F_000 464.00 _reflns_d_resolution_high 0.8414 _cod_data_source_file rz2133Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' AA28 in Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 107.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 604.01 648.79 8.09 o 4 0 0 256.69 247.19 3.09 o 6 0 0 1003.08 1034.40 15.64 o 8 0 0 243.86 238.43 3.88 o 10 0 0 83.35 80.47 1.61 o 2 1 0 369.12 390.27 5.02 o 4 1 0 320.69 316.62 2.80 o 6 1 0 3631.25 4109.14 43.45 o 8 1 0 30.23 30.00 0.52 o 10 1 0 14.23 11.86 0.36 o 2 2 0 330.32 316.13 3.18 o 4 2 0 119.76 118.76 1.11 o 6 2 0 619.26 644.01 6.23 o 8 2 0 153.29 150.47 1.83 o 10 2 0 55.33 54.17 0.87 o 2 3 0 48.23 47.21 0.49 o 4 3 0 30.95 30.11 0.37 o 6 3 0 1273.56 1316.70 14.14 o 8 3 0 16.70 17.06 0.40 o 10 3 0 1.70 1.84 0.22 o 0 4 0 11591.77 11039.81 162.20 o 2 4 0 59.04 51.60 0.71 o 4 4 0 6.75 8.17 0.22 o 6 4 0 168.81 176.79 2.40 o 8 4 0 50.82 52.86 0.96 o 2 5 0 1.14 1.39 0.17 o 4 5 0 5.34 5.33 0.25 o 6 5 0 180.10 182.14 3.65 o 8 5 0 5.03 5.10 0.43 o 0 6 0 1416.30 1420.64 23.02 o 2 6 0 3.99 3.56 0.23 o 4 6 0 0.62 0.36 0.17 o 6 6 0 31.01 29.16 0.66 o 2 7 0 0.12 0.44 0.24 o 4 7 0 1.30 0.94 0.22 o 1 0 1 26.67 17.97 0.30 o 3 0 1 981.48 1121.86 10.67 o 4 0 1 18.52 20.97 0.27 o 5 0 1 1073.46 1261.56 12.00 o 6 0 1 552.05 562.25 5.42 o 7 0 1 230.49 207.69 2.38 o 8 0 1 760.87 728.64 7.92 o 9 0 1 0.19 -0.03 0.14 o 10 0 1 0.72 1.58 0.22 o 0 1 1 1173.83 1216.43 17.72 o 1 1 1 4336.47 3314.03 37.98 o 2 1 1 140.95 119.11 0.83 o 3 1 1 821.87 826.69 5.32 o 4 1 1 448.60 480.06 2.98 o 5 1 1 50.47 57.37 0.44 o 6 1 1 135.19 151.67 1.41 o 7 1 1 3.00 1.58 0.12 o 8 1 1 6.13 6.39 0.17 o 9 1 1 13.67 7.40 0.20 o 10 1 1 0.22 0.31 0.12 o 1 2 1 0.14 0.40 0.06 o 2 2 1 0.10 0.50 0.05 o 3 2 1 449.85 467.29 3.06 o 4 2 1 0.28 0.74 0.08 o 5 2 1 574.50 630.52 3.90 o 6 2 1 251.13 248.82 3.67 o 7 2 1 135.55 121.87 1.07 o 8 2 1 524.28 513.11 4.01 o 9 2 1 0.02 -0.08 0.09 o 10 2 1 0.03 0.24 0.12 o 0 3 1 426.64 382.82 4.11 o 1 3 1 1120.05 1070.70 7.87 o 2 3 1 29.84 36.22 0.28 o 3 3 1 305.51 296.57 1.87 o 4 3 1 134.26 139.07 0.96 o 5 3 1 32.19 34.22 0.29 o 6 3 1 38.31 35.96 0.49 o 7 3 1 1.09 1.16 0.14 o 8 3 1 4.70 4.34 0.17 o 9 3 1 10.38 7.35 0.22 o 1 4 1 0.00 0.33 0.18 o 2 4 1 0.03 0.10 0.11 o 3 4 1 75.28 76.28 0.69 o 4 4 1 1.73 1.88 0.11 o 5 4 1 122.86 124.56 0.95 o 6 4 1 34.53 33.07 0.40 o 7 4 1 35.54 34.75 0.53 o 8 4 1 189.56 193.76 1.90 o 9 4 1 0.11 0.31 0.24 o 0 5 1 8.14 6.98 0.51 o 1 5 1 213.07 195.81 1.59 o 2 5 1 20.28 19.31 0.28 o 3 5 1 47.64 43.32 0.50 o 4 5 1 28.72 27.48 0.36 o 5 5 1 19.31 18.97 0.29 o 6 5 1 4.15 4.11 0.20 o 7 5 1 0.00 0.11 0.17 o 8 5 1 4.01 4.23 0.28 o 1 6 1 0.94 1.24 0.17 o 2 6 1 0.02 0.06 0.14 o 3 6 1 9.66 9.56 0.23 o 4 6 1 0.05 0.17 0.12 o 5 6 1 16.49 17.38 0.32 o 6 6 1 2.40 2.13 0.18 o 0 7 1 2.48 3.04 0.26 o 1 7 1 42.29 37.00 0.48 o 2 7 1 9.51 7.53 0.24 o 3 7 1 5.35 5.18 0.20 o 4 7 1 6.31 6.05 0.22 o 0 0 2 419.76 421.58 9.54 o 2 0 2 1052.59 1099.13 10.46 o 3 0 2 28.53 22.04 0.41 o 4 0 2 547.80 606.92 5.81 o 5 0 2 799.18 898.47 8.58 o 6 0 2 19.15 21.53 0.38 o 7 0 2 322.23 323.73 3.60 o 8 0 2 0.24 0.03 0.12 o 9 0 2 45.14 42.75 0.69 o 10 0 2 171.99 160.57 1.98 o 1 1 2 1911.14 1829.18 11.40 o 2 1 2 8.09 7.44 0.10 o 3 1 2 1.85 0.88 0.04 o 4 1 2 2575.28 2943.66 18.77 o 5 1 2 57.04 65.65 0.52 o 6 1 2 23.20 20.75 0.38 o 7 1 2 121.22 127.38 1.17 o 8 1 2 8.18 7.44 0.18 o 9 1 2 65.10 64.97 0.66 o 10 1 2 0.02 0.58 0.14 o 0 2 2 46.71 54.63 0.67 o 1 2 2 1940.41 1872.48 13.77 o 2 2 2 619.25 622.04 4.88 o 3 2 2 0.05 0.25 0.04 o 4 2 2 295.82 318.39 2.00 o 5 2 2 475.21 513.06 3.20 o 6 2 2 9.44 10.47 0.18 o 7 2 2 187.49 191.70 1.58 o 8 2 2 1.96 0.74 0.15 o 9 2 2 28.59 26.91 0.38 o 10 2 2 112.32 105.89 1.00 o 1 3 2 310.27 303.81 2.18 o 2 3 2 7.43 7.97 0.12 o 3 3 2 8.68 8.77 0.20 o 4 3 2 627.15 643.50 3.99 o 5 3 2 25.92 22.33 0.22 o 6 3 2 17.94 16.82 0.27 o 7 3 2 58.16 55.81 0.64 o 8 3 2 3.54 3.51 0.22 o 9 3 2 24.81 24.74 0.36 o 0 4 2 0.10 0.81 0.22 o 1 4 2 398.71 393.90 3.02 o 2 4 2 141.20 136.39 2.39 o 3 4 2 0.00 0.11 0.09 o 4 4 2 82.03 83.87 0.72 o 5 4 2 153.62 159.62 1.18 o 6 4 2 1.51 1.91 0.12 o 7 4 2 51.78 55.48 0.75 o 8 4 2 4.00 3.33 0.25 o 9 4 2 8.18 7.24 0.25 o 1 5 2 59.00 59.20 0.59 o 2 5 2 2.47 2.20 0.12 o 3 5 2 5.14 5.25 0.16 o 4 5 2 81.07 82.46 0.76 o 5 5 2 8.95 7.68 0.22 o 6 5 2 14.91 15.22 0.32 o 7 5 2 21.80 21.13 0.47 o 8 5 2 0.47 1.21 0.36 o 0 6 2 0.02 0.50 0.25 o 1 6 2 75.80 71.44 0.71 o 2 6 2 21.09 20.70 0.32 o 3 6 2 1.25 1.40 0.14 o 4 6 2 20.90 19.74 0.32 o 5 6 2 39.64 39.73 0.51 o 6 6 2 0.07 0.00 0.14 o 1 7 2 12.49 13.03 0.28 o 2 7 2 0.76 0.67 0.15 o 3 7 2 1.48 1.78 0.16 o 1 0 3 2008.63 1863.26 29.10 o 2 0 3 286.22 285.51 2.51 o 3 0 3 605.86 641.98 6.13 o 4 0 3 281.51 272.00 2.66 o 5 0 3 155.68 170.17 1.71 o 6 0 3 6.70 8.63 0.45 o 7 0 3 100.67 107.07 1.33 o 8 0 3 1.58 2.00 0.19 o 9 0 3 6.24 7.34 0.29 o 10 0 3 3.88 4.18 0.25 o 0 1 3 2159.91 2058.63 19.45 o 1 1 3 622.20 654.87 4.04 o 2 1 3 195.60 176.17 1.11 o 3 1 3 1036.87 1159.91 7.11 o 4 1 3 842.86 888.40 5.71 o 5 1 3 207.57 246.63 1.72 o 6 1 3 85.86 97.85 0.83 o 7 1 3 12.00 9.75 0.18 o 8 1 3 14.78 10.84 0.22 o 9 1 3 89.55 87.10 0.89 o 10 1 3 182.66 189.92 1.63 o 1 2 3 1173.58 1140.04 7.31 o 2 2 3 231.79 234.85 1.48 o 3 2 3 343.73 351.26 2.20 o 4 2 3 150.19 140.34 1.07 o 5 2 3 74.11 77.45 0.58 o 6 2 3 2.69 3.13 0.11 o 7 2 3 71.67 69.54 0.67 o 8 2 3 1.00 1.10 0.13 o 9 2 3 2.35 3.19 0.18 o 10 2 3 2.82 3.23 0.16 o 0 3 3 717.14 692.23 6.06 o 1 3 3 124.01 134.03 1.06 o 2 3 3 15.16 14.25 0.23 o 3 3 3 160.52 158.07 1.04 o 4 3 3 228.31 213.41 2.10 o 5 3 3 73.49 81.01 0.61 o 6 3 3 66.05 72.07 0.60 o 7 3 3 11.62 11.95 0.23 o 8 3 3 7.49 6.22 0.19 o 9 3 3 38.99 39.00 0.48 o 1 4 3 240.78 229.58 1.80 o 2 4 3 56.68 54.60 0.52 o 3 4 3 59.47 57.24 0.68 o 4 4 3 16.02 14.77 0.21 o 5 4 3 8.54 8.03 0.17 o 6 4 3 1.00 1.30 0.19 o 7 4 3 38.22 36.40 0.52 o 8 4 3 0.74 0.62 0.15 o 9 4 3 0.01 0.05 0.14 o 0 5 3 168.60 157.26 1.84 o 1 5 3 16.34 17.18 0.27 o 2 5 3 1.72 1.89 0.12 o 3 5 3 13.18 13.82 0.25 o 4 5 3 33.10 30.50 0.38 o 5 5 3 9.83 9.80 0.24 o 6 5 3 29.32 28.57 0.50 o 7 5 3 5.27 6.29 0.26 o 8 5 3 1.44 2.17 0.23 o 1 6 3 28.93 24.23 0.38 o 2 6 3 5.52 5.59 0.20 o 3 6 3 4.49 4.29 0.18 o 4 6 3 0.01 -0.14 0.12 o 5 6 3 0.12 0.27 0.13 o 6 6 3 0.63 0.71 0.18 o 0 7 3 38.35 35.73 0.67 o 1 7 3 2.38 2.41 0.17 o 2 7 3 0.36 0.33 0.13 o 3 7 3 0.71 0.89 0.16 o 0 0 4 1785.30 1831.99 37.30 o 1 0 4 519.83 528.25 8.30 o 2 0 4 112.97 110.77 1.10 o 3 0 4 2211.79 2404.10 31.73 o 4 0 4 21.17 22.77 0.42 o 5 0 4 250.08 236.08 2.34 o 6 0 4 208.68 216.16 2.18 o 7 0 4 53.07 47.85 0.69 o 8 0 4 35.15 40.12 0.64 o 9 0 4 644.26 653.88 7.16 o 10 0 4 7.88 6.72 0.34 o 1 1 4 29.11 41.76 0.30 o 2 1 4 3045.49 2944.31 18.78 o 3 1 4 6487.33 5959.55 79.39 o 4 1 4 23.71 26.63 0.24 o 5 1 4 212.57 248.02 1.74 o 6 1 4 117.21 127.46 0.95 o 7 1 4 536.70 520.78 4.03 o 8 1 4 68.46 62.34 0.63 o 9 1 4 37.28 31.07 0.40 o 10 1 4 0.12 -0.20 0.14 o 0 2 4 804.25 812.75 7.07 o 1 2 4 324.09 321.91 2.21 o 2 2 4 28.34 25.71 0.21 o 3 2 4 1209.57 1220.74 8.21 o 4 2 4 11.16 11.06 0.14 o 5 2 4 160.56 151.02 1.16 o 6 2 4 125.77 121.56 0.92 o 7 2 4 21.46 20.25 0.28 o 8 2 4 29.33 31.07 0.44 o 9 2 4 426.18 429.98 3.41 o 10 2 4 3.38 2.90 0.19 o 1 3 4 13.84 13.47 0.15 o 2 3 4 653.31 614.81 3.80 o 3 3 4 1563.36 1549.79 9.49 o 4 3 4 1.01 1.76 0.09 o 5 3 4 77.56 77.26 0.59 o 6 3 4 40.53 44.23 0.48 o 7 3 4 219.29 215.40 1.67 o 8 3 4 52.67 49.42 0.55 o 9 3 4 21.62 19.63 0.39 o 0 4 4 157.69 160.00 1.92 o 1 4 4 70.68 64.96 0.89 o 2 4 4 4.41 4.58 0.16 o 3 4 4 192.90 182.77 2.27 o 4 4 4 0.14 0.20 0.08 o 5 4 4 48.60 43.53 0.43 o 6 4 4 46.80 43.19 0.52 o 7 4 4 1.16 1.60 0.20 o 8 4 4 14.45 13.76 0.33 o 1 5 4 0.07 0.06 0.09 o 2 5 4 110.44 102.48 0.91 o 3 5 4 149.01 147.45 1.57 o 4 5 4 0.54 0.55 0.11 o 5 5 4 21.27 20.12 0.35 o 6 5 4 9.03 10.39 0.27 o 7 5 4 54.30 57.61 0.90 o 0 6 4 25.45 25.78 0.50 o 1 6 4 8.41 7.65 0.23 o 2 6 4 1.49 1.98 0.16 o 3 6 4 10.44 9.97 0.24 o 4 6 4 3.84 3.25 0.16 o 5 6 4 10.10 8.62 0.25 o 6 6 4 14.26 13.79 0.37 o 1 7 4 0.87 0.92 0.16 o 2 7 4 17.93 15.15 0.30 o 3 7 4 6.16 6.87 0.24 o 1 0 5 35.53 37.70 0.47 o 2 0 5 147.83 130.71 1.32 o 3 0 5 415.51 448.38 3.93 o 4 0 5 187.02 207.94 2.06 o 5 0 5 90.46 104.19 1.10 o 6 0 5 49.70 53.24 0.64 o 7 0 5 20.47 22.20 0.36 o 8 0 5 707.75 692.46 7.54 o 9 0 5 15.67 12.34 0.42 o 10 0 5 4.77 5.06 0.33 o 0 1 5 5065.73 4687.18 104.23 o 1 1 5 2.02 3.39 0.08 o 2 1 5 3302.15 3512.31 22.40 o 3 1 5 644.21 633.31 3.91 o 4 1 5 148.22 143.74 1.03 o 5 1 5 26.89 30.01 0.29 o 6 1 5 85.73 72.58 0.59 o 7 1 5 97.56 95.22 0.80 o 8 1 5 132.89 133.48 1.16 o 9 1 5 171.11 177.76 1.79 o 10 1 5 0.82 0.09 0.14 o 1 2 5 6.77 6.02 0.12 o 2 2 5 115.05 101.89 0.68 o 3 2 5 213.40 211.02 1.35 o 4 2 5 74.39 67.61 0.49 o 5 2 5 37.35 36.16 0.31 o 6 2 5 21.75 20.88 0.24 o 7 2 5 11.71 12.66 0.28 o 8 2 5 495.98 496.81 3.88 o 9 2 5 9.61 8.45 0.26 o 10 2 5 3.12 3.26 0.20 o 0 3 5 1286.87 1200.82 10.42 o 1 3 5 15.78 16.85 0.19 o 2 3 5 814.12 792.72 4.89 o 3 3 5 169.81 166.50 1.10 o 4 3 5 62.71 62.86 0.65 o 5 3 5 15.82 15.08 0.22 o 6 3 5 30.40 29.35 0.32 o 7 3 5 35.45 33.82 0.39 o 8 3 5 71.24 71.57 0.72 o 9 3 5 73.11 75.25 0.90 o 1 4 5 0.77 1.05 0.12 o 2 4 5 20.77 19.34 0.27 o 3 4 5 13.05 10.53 0.20 o 4 4 5 2.92 1.49 0.10 o 5 4 5 7.71 6.30 0.16 o 6 4 5 1.35 1.53 0.14 o 7 4 5 3.91 5.61 0.38 o 8 4 5 180.14 187.37 2.04 o 0 5 5 163.58 154.70 2.11 o 1 5 5 1.71 1.89 0.12 o 2 5 5 118.22 109.56 0.96 o 3 5 5 28.06 26.57 0.35 o 4 5 5 11.53 11.50 0.24 o 5 5 5 4.99 5.11 0.18 o 6 5 5 2.34 2.92 0.19 o 7 5 5 4.57 5.40 0.26 o 1 6 5 1.63 1.97 0.16 o 2 6 5 0.45 0.65 0.12 o 3 6 5 1.97 1.90 0.16 o 4 6 5 0.98 1.22 0.14 o 5 6 5 2.22 2.23 0.17 o 6 6 5 0.16 0.32 0.15 o 0 7 5 14.12 13.79 0.40 o 1 7 5 0.02 0.06 0.13 o 2 7 5 15.33 14.43 0.34 o 3 7 5 4.69 4.26 0.20 o 0 0 6 253.97 239.09 3.03 o 1 0 6 4269.13 3969.66 48.42 o 2 0 6 22.06 25.69 0.31 o 3 0 6 151.16 188.20 1.70 o 4 0 6 43.41 39.45 0.76 o 5 0 6 122.38 123.10 1.40 o 6 0 6 457.86 484.48 4.71 o 7 0 6 1377.39 1379.03 17.40 o 8 0 6 29.43 28.08 0.62 o 9 0 6 1.89 2.17 0.26 o 10 0 6 6.30 8.08 0.36 o 1 1 6 1088.85 1095.78 6.73 o 2 1 6 65.04 56.42 0.39 o 3 1 6 207.00 192.54 1.29 o 4 1 6 184.85 197.30 1.26 o 5 1 6 230.64 260.80 1.83 o 6 1 6 14.98 15.13 0.22 o 7 1 6 1345.87 1363.57 9.20 o 8 1 6 23.99 18.61 0.35 o 9 1 6 22.52 19.96 0.39 o 10 1 6 3.31 4.43 0.22 o 0 2 6 112.47 110.85 1.05 o 1 2 6 1846.47 1835.77 11.41 o 2 2 6 17.18 17.55 0.17 o 3 2 6 86.65 96.66 0.69 o 4 2 6 23.21 22.25 0.21 o 5 2 6 75.16 76.82 0.62 o 6 2 6 274.99 290.28 2.16 o 7 2 6 908.93 934.25 6.72 o 8 2 6 19.83 18.73 0.36 o 9 2 6 1.29 1.48 0.16 o 1 3 6 284.99 263.89 1.68 o 2 3 6 9.87 10.75 0.18 o 3 3 6 45.07 44.48 0.35 o 4 3 6 91.23 90.83 0.67 o 5 3 6 104.33 110.48 0.84 o 6 3 6 1.87 3.31 0.19 o 7 3 6 643.72 660.34 5.11 o 8 3 6 19.60 17.34 0.36 o 9 3 6 11.66 10.99 0.30 o 0 4 6 23.44 25.42 0.44 o 1 4 6 306.31 293.67 3.26 o 2 4 6 3.72 3.68 0.14 o 3 4 6 21.24 21.98 0.27 o 4 4 6 7.35 7.35 0.15 o 5 4 6 23.45 24.91 0.33 o 6 4 6 78.47 82.27 0.78 o 7 4 6 305.48 336.55 4.64 o 8 4 6 6.49 6.58 0.34 o 1 5 6 32.30 29.84 0.37 o 2 5 6 2.43 2.52 0.15 o 3 5 6 10.79 10.48 0.24 o 4 5 6 29.64 31.25 0.38 o 5 5 6 48.20 50.27 0.58 o 6 5 6 0.02 0.39 0.16 o 7 5 6 172.84 187.00 4.58 o 0 6 6 4.08 4.33 0.25 o 1 6 6 44.38 42.73 0.50 o 2 6 6 0.35 0.31 0.12 o 3 6 6 4.42 5.14 0.20 o 4 6 6 1.96 1.93 0.17 o 5 6 6 4.83 5.41 0.21 o 1 7 6 1.52 2.27 0.16 o 2 7 6 0.72 0.39 0.14 o 1 0 7 41.58 44.67 0.50 o 2 0 7 73.24 81.30 0.87 o 3 0 7 281.81 278.77 2.75 o 4 0 7 864.69 927.04 8.07 o 5 0 7 108.20 109.58 1.17 o 6 0 7 192.63 185.73 2.48 o 7 0 7 469.05 463.35 7.37 o 9 0 7 23.16 20.33 0.55 o 10 0 7 0.05 -0.15 0.19 o 0 1 7 0.80 2.96 0.18 o 1 1 7 2276.72 2427.16 14.84 o 2 1 7 12.79 7.53 0.10 o 3 1 7 486.11 516.34 3.37 o 4 1 7 489.23 518.01 3.22 o 5 1 7 15.54 14.21 0.34 o 6 1 7 501.09 518.87 4.03 o 7 1 7 13.47 12.05 0.25 o 8 1 7 1.66 2.83 0.20 o 9 1 7 9.10 9.34 0.38 o 10 1 7 9.72 8.61 0.28 o 1 2 7 27.43 27.14 0.23 o 2 2 7 34.39 35.00 0.28 o 3 2 7 137.20 139.75 0.92 o 4 2 7 509.66 522.06 3.40 o 5 2 7 34.99 31.25 0.32 o 6 2 7 128.89 126.88 1.11 o 7 2 7 267.94 278.10 2.25 o 8 2 7 0.51 0.59 0.20 o 9 2 7 19.50 18.27 0.38 o 0 3 7 0.19 0.83 0.17 o 1 3 7 743.04 773.93 4.79 o 2 3 7 0.07 0.68 0.10 o 3 3 7 183.83 186.76 1.33 o 4 3 7 197.68 194.32 1.28 o 5 3 7 4.63 5.21 0.15 o 6 3 7 249.52 262.13 2.12 o 7 3 7 1.82 2.59 0.16 o 8 3 7 2.30 2.41 0.18 o 9 3 7 5.04 4.95 0.24 o 1 4 7 14.15 12.73 0.21 o 2 4 7 3.53 3.26 0.13 o 3 4 7 41.77 43.58 0.51 o 4 4 7 133.59 129.56 1.04 o 5 4 7 1.71 1.52 0.12 o 6 4 7 43.50 45.89 0.67 o 7 4 7 55.51 59.93 0.81 o 8 4 7 2.93 3.51 0.29 o 0 5 7 2.04 1.67 0.18 o 1 5 7 80.00 83.43 0.77 o 2 5 7 5.31 5.41 0.26 o 3 5 7 43.62 43.18 0.48 o 4 5 7 45.24 43.66 0.53 o 5 5 7 0.57 0.96 0.15 o 6 5 7 75.64 80.90 2.00 o 7 5 7 0.28 1.33 0.29 o 1 6 7 4.22 4.88 0.20 o 2 6 7 0.00 0.18 0.12 o 3 6 7 15.58 14.96 0.29 o 4 6 7 24.19 22.77 0.38 o 5 6 7 0.00 0.01 0.15 o 0 7 7 1.82 1.12 0.22 o 1 7 7 4.28 5.25 0.25 o 0 0 8 966.10 1014.52 19.25 o 1 0 8 810.41 831.26 7.97 o 2 0 8 733.11 810.03 7.77 o 3 0 8 397.39 436.97 4.26 o 4 0 8 667.62 686.69 6.61 o 5 0 8 96.70 93.90 1.43 o 6 0 8 830.57 818.82 8.88 o 7 0 8 15.74 11.39 0.35 o 8 0 8 60.31 60.74 1.07 o 9 0 8 19.80 22.06 0.57 o 1 1 8 876.80 897.38 5.53 o 2 1 8 16.47 22.06 0.21 o 3 1 8 56.67 58.63 0.43 o 4 1 8 38.44 43.47 0.38 o 5 1 8 4.35 2.93 0.20 o 6 1 8 66.48 69.70 0.67 o 7 1 8 680.15 697.14 5.39 o 8 1 8 36.34 35.65 0.53 o 9 1 8 51.50 60.51 0.77 o 0 2 8 490.07 473.81 4.17 o 1 2 8 305.33 298.85 1.97 o 2 2 8 455.66 464.78 2.91 o 3 2 8 261.15 285.00 1.82 o 4 2 8 397.12 397.62 3.57 o 5 2 8 70.21 70.63 0.67 o 6 2 8 544.21 538.36 4.19 o 7 2 8 15.58 13.41 0.26 o 8 2 8 44.15 46.32 0.74 o 9 2 8 11.95 14.38 0.35 o 1 3 8 297.85 290.56 2.02 o 2 3 8 2.74 3.08 0.12 o 3 3 8 35.74 36.54 0.40 o 4 3 8 14.95 17.60 0.24 o 5 3 8 0.98 1.41 0.21 o 6 3 8 18.85 21.07 0.32 o 7 3 8 294.18 305.83 2.77 o 8 3 8 23.85 24.81 0.44 o 0 4 8 68.42 68.77 1.28 o 1 4 8 27.83 25.96 0.28 o 2 4 8 162.63 154.27 1.20 o 3 4 8 91.98 93.67 0.79 o 4 4 8 109.43 107.66 1.16 o 5 4 8 34.00 37.44 0.64 o 6 4 8 181.37 186.05 1.99 o 7 4 8 10.28 10.31 0.31 o 8 4 8 19.20 21.00 0.62 o 1 5 8 51.67 49.86 0.53 o 2 5 8 0.74 0.50 0.12 o 3 5 8 8.87 8.25 0.22 o 4 5 8 4.19 5.44 0.21 o 5 5 8 1.30 2.18 0.35 o 6 5 8 1.37 2.18 0.31 o 0 6 8 3.62 4.83 0.28 o 1 6 8 0.74 0.54 0.13 o 2 6 8 43.93 41.31 0.51 o 3 6 8 20.95 21.72 0.36 o 4 6 8 19.51 20.11 0.38 o 1 0 9 694.45 742.09 7.13 o 2 0 9 74.87 67.34 0.77 o 3 0 9 493.02 477.64 4.66 o 4 0 9 146.86 132.36 1.59 o 5 0 9 49.76 46.58 0.69 o 6 0 9 63.53 68.02 0.94 o 7 0 9 254.91 283.00 3.24 o 8 0 9 40.72 35.60 0.75 o 9 0 9 7.54 9.50 0.40 o 0 1 9 448.15 485.13 4.28 o 1 1 9 764.74 847.50 5.47 o 2 1 9 513.63 498.90 3.43 o 3 1 9 12.61 10.48 0.15 o 4 1 9 9.58 10.98 0.18 o 5 1 9 76.67 72.27 0.68 o 6 1 9 504.32 521.39 4.07 o 7 1 9 735.35 768.36 5.93 o 8 1 9 25.34 25.99 0.44 o 9 1 9 83.01 88.57 1.03 o 1 2 9 353.50 360.66 2.27 o 2 2 9 37.87 31.21 0.28 o 3 2 9 304.05 308.39 2.16 o 4 2 9 74.73 71.10 0.62 o 5 2 9 58.69 54.86 0.56 o 6 2 9 39.65 41.44 0.47 o 7 2 9 171.68 192.67 1.63 o 8 2 9 27.10 24.96 0.44 o 9 2 9 4.75 5.90 0.26 o 0 3 9 159.18 181.36 1.70 o 1 3 9 332.51 357.35 2.27 o 2 3 9 136.28 131.75 0.94 o 3 3 9 0.78 0.96 0.07 o 4 3 9 1.31 1.99 0.11 o 5 3 9 24.21 23.80 0.33 o 6 3 9 226.62 242.87 2.00 o 7 3 9 372.25 400.96 3.19 o 8 3 9 11.24 12.03 0.39 o 1 4 9 58.33 56.71 0.50 o 2 4 9 12.94 10.39 0.19 o 3 4 9 65.96 67.07 0.78 o 4 4 9 10.22 10.64 0.25 o 5 4 9 43.31 41.58 0.61 o 6 4 9 11.57 12.34 0.31 o 7 4 9 62.86 68.30 0.90 o 0 5 9 30.36 31.77 0.55 o 1 5 9 70.43 70.07 0.72 o 2 5 9 16.39 17.72 0.28 o 3 5 9 0.20 0.32 0.13 o 4 5 9 0.40 0.36 0.15 o 5 5 9 2.64 2.38 0.22 o 6 5 9 52.68 58.23 0.90 o 1 6 9 3.93 4.01 0.18 o 2 6 9 3.76 3.51 0.19 o 3 6 9 5.35 5.99 0.23 o 4 6 9 0.14 0.33 0.18 o 0 0 10 808.67 782.59 16.49 o 1 0 10 0.34 0.15 0.08 o 2 0 10 563.41 576.35 5.58 o 3 0 10 45.97 60.54 1.24 o 4 0 10 28.26 27.26 0.48 o 5 0 10 53.46 57.73 0.81 o 6 0 10 6.60 7.35 0.26 o 7 0 10 5.34 4.79 0.25 o 8 0 10 155.29 148.50 2.17 o 9 0 10 176.37 201.01 2.90 o 1 1 10 27.61 22.11 0.25 o 2 1 10 1018.26 1018.26 6.90 o 3 1 10 25.10 23.57 0.29 o 4 1 10 290.53 255.12 2.05 o 5 1 10 2.21 2.64 0.21 o 6 1 10 134.29 130.81 1.14 o 7 1 10 0.98 1.40 0.14 o 8 1 10 85.15 94.42 0.98 o 9 1 10 54.85 55.83 0.75 o 0 2 10 522.77 535.83 4.72 o 1 2 10 3.96 3.48 0.17 o 2 2 10 335.45 356.48 2.48 o 3 2 10 34.67 40.37 0.38 o 4 2 10 13.53 11.99 0.21 o 5 2 10 40.28 43.68 0.48 o 6 2 10 8.51 9.20 0.21 o 7 2 10 2.10 2.19 0.14 o 8 2 10 113.83 111.43 1.13 o 1 3 10 23.94 24.26 0.26 o 2 3 10 372.02 357.43 2.64 o 3 3 10 0.12 0.04 0.08 o 4 3 10 79.54 70.76 0.64 o 5 3 10 1.60 1.32 0.12 o 6 3 10 58.89 56.94 0.61 o 7 3 10 0.34 0.77 0.13 o 8 3 10 39.32 46.77 0.90 o 0 4 10 179.26 184.83 2.43 o 1 4 10 4.96 4.33 0.15 o 2 4 10 74.28 82.22 0.98 o 3 4 10 11.49 10.82 0.23 o 4 4 10 0.41 0.47 0.15 o 5 4 10 18.75 19.67 0.40 o 6 4 10 7.95 7.92 0.26 o 7 4 10 0.13 0.11 0.16 o 1 5 10 16.69 17.59 0.31 o 2 5 10 80.44 78.49 0.87 o 3 5 10 3.24 4.42 0.20 o 4 5 10 6.69 7.85 0.39 o 5 5 10 0.23 0.38 0.23 o 6 5 10 14.94 15.88 0.53 o 0 6 10 42.77 41.92 0.71 o 1 6 10 1.02 1.37 0.17 o 2 6 10 8.99 10.31 0.30 o 3 6 10 2.54 2.58 0.21 o 1 0 11 43.97 41.22 0.82 o 2 0 11 141.15 135.92 1.43 o 3 0 11 346.51 366.96 3.62 o 4 0 11 280.98 259.15 2.95 o 5 0 11 4.03 1.94 0.17 o 6 0 11 2.96 4.55 0.22 o 7 0 11 0.07 0.16 0.15 o 8 0 11 44.55 39.23 0.70 o 9 0 11 8.75 8.98 0.42 o 0 1 11 21.42 23.34 0.78 o 1 1 11 12.53 14.46 0.31 o 2 1 11 217.64 193.79 1.41 o 3 1 11 3.39 5.77 0.13 o 4 1 11 32.87 27.87 0.38 o 5 1 11 307.09 323.76 2.59 o 6 1 11 100.46 89.80 0.85 o 7 1 11 57.88 65.03 0.67 o 8 1 11 4.10 3.58 0.16 o 1 2 11 14.80 14.97 0.20 o 2 2 11 90.65 90.87 0.73 o 3 2 11 216.06 222.00 1.61 o 4 2 11 157.40 153.85 1.31 o 5 2 11 6.62 4.69 0.16 o 6 2 11 1.38 2.54 0.19 o 7 2 11 0.11 0.39 0.12 o 8 2 11 27.12 24.79 0.41 o 0 3 11 12.54 14.80 0.31 o 1 3 11 7.58 10.00 0.22 o 2 3 11 47.99 40.66 0.39 o 3 3 11 0.00 0.10 0.08 o 4 3 11 7.22 7.20 0.17 o 5 3 11 163.76 174.32 1.48 o 6 3 11 58.66 56.28 0.62 o 7 3 11 24.24 27.19 0.39 o 1 4 11 0.26 0.47 0.12 o 2 4 11 20.91 22.17 0.33 o 3 4 11 51.46 49.55 0.61 o 4 4 11 26.15 27.31 0.45 o 5 4 11 8.17 7.58 0.26 o 6 4 11 0.27 0.52 0.16 o 0 5 11 2.62 3.27 0.26 o 1 5 11 6.17 7.50 0.23 o 2 5 11 2.95 3.00 0.18 o 3 5 11 0.37 0.72 0.16 o 4 5 11 0.22 0.27 0.16 o 5 5 11 56.52 59.64 0.91 o 1 6 11 0.43 0.58 0.18 o 2 6 11 1.54 2.16 0.19 o 0 0 12 544.34 483.29 19.25 o 1 0 12 79.11 82.41 1.08 o 2 0 12 9.43 8.23 0.25 o 3 0 12 1.81 2.56 0.26 o 4 0 12 491.02 474.31 8.28 o 5 0 12 168.27 141.61 1.76 o 6 0 12 0.86 0.58 0.17 o 7 0 12 56.49 59.73 0.91 o 8 0 12 38.97 40.88 0.71 o 1 1 12 103.13 92.30 0.84 o 2 1 12 149.15 151.40 1.13 o 3 1 12 232.75 202.57 1.48 o 4 1 12 34.30 29.43 0.37 o 5 1 12 95.57 93.36 0.87 o 6 1 12 22.67 18.26 0.30 o 7 1 12 1.81 2.14 0.15 o 8 1 12 11.20 9.35 0.24 o 0 2 12 360.34 345.21 3.88 o 1 2 12 49.96 51.67 0.54 o 2 2 12 3.28 2.53 0.12 o 3 2 12 1.19 1.30 0.11 o 4 2 12 323.91 331.12 2.65 o 5 2 12 121.88 110.33 1.01 o 6 2 12 0.96 0.70 0.12 o 7 2 12 41.01 43.84 0.52 o 8 2 12 25.25 28.89 0.42 o 1 3 12 45.12 48.41 0.52 o 2 3 12 51.43 48.30 0.46 o 3 3 12 141.08 131.56 1.03 o 4 3 12 7.71 6.64 0.19 o 5 3 12 53.00 50.49 0.56 o 6 3 12 14.35 14.13 0.28 o 7 3 12 1.76 1.59 0.15 o 0 4 12 150.04 157.32 2.20 o 1 4 12 16.73 17.13 0.33 o 2 4 12 0.20 0.65 0.14 o 3 4 12 0.02 0.01 0.12 o 4 4 12 103.91 109.16 1.27 o 5 4 12 51.34 52.44 0.75 o 6 4 12 1.19 1.57 0.21 o 1 5 12 13.79 16.64 0.50 o 2 5 12 10.08 9.56 0.31 o 3 5 12 50.73 53.35 0.73 o 4 5 12 0.71 0.89 0.26 o 0 6 12 48.65 56.45 1.29 o 1 0 13 1077.65 1070.91 11.63 o 2 0 13 3.50 3.54 0.20 o 3 0 13 14.04 11.61 0.26 o 4 0 13 312.36 308.70 3.51 o 5 0 13 112.55 111.29 1.42 o 6 0 13 12.39 11.84 0.36 o 7 0 13 3.28 3.64 0.22 o 8 0 13 38.06 42.44 0.76 o 0 1 13 62.93 56.19 0.83 o 1 1 13 0.91 1.34 0.14 o 2 1 13 31.74 27.16 0.40 o 3 1 13 11.75 11.30 0.22 o 4 1 13 157.67 125.26 1.11 o 5 1 13 67.61 56.09 0.60 o 6 1 13 8.04 6.66 0.21 o 7 1 13 11.89 7.79 0.21 o 8 1 13 2.88 3.47 0.18 o 1 2 13 721.75 735.56 5.70 o 2 2 13 0.76 0.80 0.15 o 3 2 13 6.10 6.17 0.17 o 4 2 13 216.67 214.61 1.79 o 5 2 13 69.49 68.89 0.70 o 6 2 13 3.65 3.97 0.17 o 7 2 13 2.23 2.80 0.16 o 0 3 13 12.56 12.47 0.36 o 1 3 13 5.22 4.35 0.18 o 2 3 13 12.01 11.23 0.30 o 3 3 13 3.03 3.19 0.16 o 4 3 13 88.66 82.70 0.81 o 5 3 13 29.89 29.16 0.40 o 6 3 13 1.69 2.08 0.16 o 1 4 13 243.13 265.39 2.77 o 2 4 13 0.14 0.06 0.14 o 3 4 13 0.35 0.76 0.14 o 4 4 13 70.14 71.07 1.20 o 5 4 13 17.79 19.04 0.42 o 0 5 13 0.42 0.30 0.27 o 1 5 13 6.15 5.66 0.29 o 2 5 13 3.95 4.52 0.36 o 3 5 13 0.44 0.55 0.22 o 0 0 14 875.57 829.74 12.82 o 1 0 14 873.59 834.66 9.13 o 2 0 14 98.76 93.43 1.40 o 3 0 14 14.46 16.03 0.38 o 4 0 14 38.56 30.48 0.65 o 5 0 14 98.52 95.21 1.28 o 6 0 14 125.00 118.53 1.55 o 7 0 14 0.39 0.51 0.18 o 1 1 14 19.77 18.64 0.30 o 2 1 14 348.53 329.00 2.82 o 3 1 14 1.31 2.71 0.16 o 4 1 14 8.46 7.16 0.25 o 5 1 14 375.31 368.78 2.97 o 6 1 14 136.50 135.65 1.23 o 7 1 14 1.23 0.19 0.12 o 0 2 14 505.40 506.00 5.63 o 1 2 14 584.14 574.20 4.51 o 2 2 14 76.09 74.76 0.73 o 3 2 14 8.01 9.02 0.23 o 4 2 14 24.06 20.53 0.39 o 5 2 14 77.56 75.39 0.77 o 6 2 14 83.70 79.84 0.81 o 7 2 14 0.34 0.23 0.12 o 1 3 14 12.24 11.41 0.25 o 2 3 14 191.61 194.79 1.66 o 3 3 14 0.01 0.00 0.13 o 4 3 14 0.90 1.00 0.16 o 5 3 14 175.04 184.21 1.72 o 6 3 14 59.01 59.03 0.66 o 0 4 14 125.50 132.57 1.96 o 1 4 14 197.34 212.73 2.06 o 2 4 14 32.79 33.90 0.50 o 3 4 14 1.39 1.79 0.22 o 4 4 14 6.46 6.63 0.38 o 5 4 14 38.76 39.14 0.72 o 1 5 14 4.62 4.72 0.30 o 2 5 14 64.19 68.32 1.73 o 1 0 15 16.60 17.53 0.66 o 2 0 15 117.67 116.95 1.50 o 3 0 15 145.66 140.96 2.11 o 4 0 15 56.20 51.41 0.98 o 5 0 15 44.08 51.01 0.98 o 6 0 15 142.90 129.89 2.00 o 7 0 15 37.80 38.57 0.71 o 0 1 15 2060.95 2084.64 22.44 o 1 1 15 41.18 40.91 0.48 o 2 1 15 40.90 40.69 0.48 o 3 1 15 3.42 3.04 0.18 o 4 1 15 0.02 0.31 0.14 o 5 1 15 40.25 38.23 0.57 o 6 1 15 10.80 9.07 0.28 o 1 2 15 9.20 10.82 0.25 o 2 2 15 93.26 93.30 0.97 o 3 2 15 110.25 114.42 1.21 o 4 2 15 42.89 41.50 0.60 o 5 2 15 28.68 32.09 0.52 o 6 2 15 88.56 82.96 1.00 o 0 3 15 1014.79 1084.12 11.82 o 1 3 15 11.29 13.95 0.33 o 2 3 15 13.70 14.81 0.29 o 3 3 15 1.35 2.21 0.17 o 4 3 15 0.19 -0.07 0.14 o 5 3 15 20.65 21.65 0.43 o 1 4 15 1.96 3.44 0.20 o 2 4 15 45.39 48.54 0.65 o 3 4 15 49.91 58.01 1.21 o 4 4 15 16.70 17.90 0.53 o 0 0 16 33.70 36.45 0.93 o 1 0 16 93.50 97.26 1.30 o 2 0 16 154.98 158.48 2.14 o 3 0 16 48.40 44.77 0.91 o 4 0 16 43.50 33.31 0.89 o 5 0 16 74.01 79.02 1.36 o 6 0 16 6.01 5.45 0.36 o 1 1 16 3.71 4.02 0.17 o 2 1 16 7.44 6.53 0.20 o 3 1 16 62.49 59.56 0.83 o 4 1 16 27.33 23.10 0.43 o 5 1 16 35.68 31.11 0.51 o 6 1 16 22.64 22.30 0.44 o 0 2 16 12.20 14.12 0.39 o 1 2 16 71.62 79.12 0.80 o 2 2 16 117.31 118.92 1.10 o 3 2 16 35.57 33.85 0.58 o 4 2 16 29.88 24.33 0.45 o 5 2 16 52.62 57.72 0.77 o 1 3 16 0.26 0.71 0.13 o 2 3 16 3.53 3.89 0.17 o 3 3 16 39.98 38.22 0.59 o 4 3 16 10.44 9.08 0.31 o 0 4 16 0.05 0.29 0.28 o 1 4 16 33.71 40.06 0.59 o 2 4 16 49.49 51.49 0.75 o 1 0 17 39.94 44.52 0.75 o 2 0 17 34.13 27.72 0.56 o 3 0 17 112.01 124.56 1.93 o 4 0 17 0.45 0.62 0.21 o 5 0 17 8.15 8.30 0.40 o 0 1 17 23.04 20.88 0.48 o 1 1 17 9.47 7.10 0.21 o 2 1 17 13.86 11.29 0.25 o 3 1 17 1.91 1.22 0.16 o 4 1 17 2.30 1.55 0.17 o 5 1 17 12.18 9.14 0.30 o 1 2 17 30.81 33.20 0.44 o 2 2 17 24.27 22.00 0.35 o 3 2 17 76.88 88.06 1.05 o 4 2 17 0.30 0.32 0.15 o 0 3 17 13.17 12.73 0.39 o 1 3 17 8.27 7.39 0.23 o 2 3 17 4.02 3.57 0.18 o 3 3 17 0.02 0.18 0.16 o 0 0 18 31.39 34.99 0.93 o 1 0 18 10.84 11.31 0.37 o 2 0 18 31.05 32.66 0.61 o 3 0 18 68.55 67.64 1.23 o 4 0 18 13.04 15.29 0.52 o 1 1 18 4.35 5.22 0.20 o 2 1 18 7.90 8.53 0.24 o 3 1 18 185.76 195.63 2.02 o 4 1 18 27.01 27.56 0.54 o 0 2 18 21.42 23.45 0.55 o 1 2 18 8.23 8.67 0.25 o 2 2 18 19.34 21.97 0.40 o 3 2 18 44.11 45.89 0.69 o 1 3 18 1.63 2.80 0.17 o 1 0 19 1.12 1.72 0.19 o 2 0 19 3.53 3.68 0.29 o 3 0 19 70.53 75.90 1.38 o 0 1 19 1.55 0.94 0.19 o 1 1 19 7.55 7.70 0.23 o 2 1 19 0.75 1.46 0.18 o 1 2 19 1.21 1.67 0.15 o