#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:30:52 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181059 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/39/2213961.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213961_Fobs loop_ _publ_author_name 'Wilkinson, Hazel S.' 'Harrison, William T. A.' _publ_section_title ; Ethylenediammonium bis(dihydrogenarsenate): R~4~^3^(14) loops built up from O---H···O hydrogen bonds ; _journal_coeditor_code SJ2232 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1610 _journal_page_last m1612 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.381 _cell_angle_gamma 90.000 _cell_length_a 4.8971 _cell_length_b 8.8054 _cell_length_c 11.4894 _exptl_crystal_F_000 412.00 _reflns_d_resolution_high 0.6584 _cod_data_source_file sj2232Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' hw12 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 146.78 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 7215.91 7105.74 53.25 o 2 0 0 10.71 17.91 2.12 o 3 0 0 254.62 260.26 4.78 o 4 0 0 4217.23 4245.42 38.74 o 5 0 0 1679.36 1634.32 23.19 o 6 0 0 997.43 1047.42 31.66 o 7 0 0 522.19 510.79 24.99 o 1 1 0 2748.11 3013.20 38.05 o 2 1 0 11359.22 11152.90 84.54 o 3 1 0 2415.99 2450.36 13.35 o 4 1 0 892.02 892.68 8.36 o 5 1 0 155.91 151.21 7.18 o 6 1 0 214.35 205.55 11.27 o 7 1 0 271.45 288.43 14.39 o 0 2 0 175.97 194.63 6.82 o 1 2 0 239.44 287.89 9.05 o 2 2 0 35.76 50.56 1.74 o 3 2 0 25.66 39.03 3.57 o 4 2 0 83.45 81.35 3.93 o 5 2 0 2.23 4.45 3.89 o 6 2 0 19.11 14.55 5.66 o 7 2 0 4.93 14.83 7.70 o 1 3 0 13.35 17.05 2.23 o 2 3 0 3181.14 3211.27 35.86 o 3 3 0 3568.34 3602.49 52.92 o 4 3 0 1298.74 1318.01 16.08 o 5 3 0 30.65 26.47 4.41 o 6 3 0 296.72 309.80 10.92 o 7 3 0 399.47 388.28 23.63 o 0 4 0 798.24 708.46 15.13 o 1 4 0 5313.81 5287.43 24.51 o 2 4 0 2098.04 2204.86 29.90 o 3 4 0 187.51 211.09 9.64 o 4 4 0 1332.99 1366.06 13.88 o 5 4 0 2137.40 2202.01 34.54 o 6 4 0 989.64 970.59 18.51 o 7 4 0 48.12 48.68 12.71 o 1 5 0 1152.55 1143.83 15.18 o 2 5 0 410.40 405.39 7.86 o 3 5 0 891.45 902.62 13.90 o 4 5 0 208.90 212.09 7.50 o 5 5 0 15.67 18.53 4.86 o 6 5 0 11.31 14.09 6.00 o 0 6 0 451.16 428.56 14.82 o 1 6 0 775.21 804.15 13.88 o 2 6 0 70.12 62.27 4.22 o 3 6 0 126.26 114.60 5.97 o 4 6 0 41.34 46.16 5.54 o 5 6 0 169.04 169.48 7.45 o 6 6 0 174.87 170.63 9.27 o 1 7 0 3510.08 3416.30 31.23 o 2 7 0 1540.40 1463.66 16.62 o 3 7 0 2117.76 2052.81 20.89 o 4 7 0 562.15 560.02 12.05 o 5 7 0 6.79 2.72 5.68 o 6 7 0 17.69 12.47 6.46 o 0 8 0 1769.26 1751.43 32.73 o 1 8 0 1803.05 1723.84 22.73 o 2 8 0 150.48 144.19 8.39 o 3 8 0 172.98 186.19 9.35 o 4 8 0 314.96 290.88 11.60 o 5 8 0 752.22 754.82 16.39 o 1 9 0 2.39 5.12 4.34 o 2 9 0 29.98 28.57 6.50 o 3 9 0 45.98 42.42 7.42 o 4 9 0 4.14 13.38 8.70 o 5 9 0 8.23 6.33 8.34 o 0 10 0 615.98 657.44 17.29 o 1 10 0 488.23 504.76 26.91 o 2 10 0 146.96 165.33 9.72 o 3 10 0 9.37 3.18 8.31 o 4 10 0 228.74 242.43 15.38 o 1 11 0 191.31 206.12 20.13 o 2 11 0 1263.90 1287.48 27.77 o 3 11 0 856.09 875.54 24.92 o 4 11 0 284.16 319.78 14.38 o 1 12 0 271.91 269.80 14.39 o 2 12 0 33.21 47.84 10.24 o 3 12 0 8.71 9.82 16.44 o 1 13 0 4.34 1.11 8.22 o -7 1 1 159.80 190.60 19.76 o -6 1 1 21.71 9.82 6.61 o -5 1 1 702.30 695.34 12.79 o -4 1 1 3206.06 3184.93 15.54 o -3 1 1 4670.37 4703.06 16.60 o -2 1 1 642.32 591.41 4.84 o -1 1 1 129.39 144.53 2.08 o 0 1 1 1274.00 1406.47 21.92 o 1 1 1 8446.62 8064.44 84.79 o 2 1 1 1979.38 1894.45 17.64 o 3 1 1 2405.15 2400.82 20.73 o 4 1 1 856.36 826.18 11.29 o 5 1 1 457.77 440.73 16.05 o 6 1 1 551.13 548.79 16.93 o 7 1 1 450.12 460.84 17.70 o -7 2 1 773.74 770.65 30.91 o -6 2 1 1194.22 1219.64 19.08 o -5 2 1 1430.34 1459.00 22.86 o -4 2 1 334.55 339.62 5.88 o -3 2 1 699.75 728.06 7.02 o -2 2 1 3375.64 3311.46 17.27 o -1 2 1 18039.43 17414.27 144.36 o 0 2 1 13869.78 13900.14 298.56 o 1 2 1 1600.58 1790.81 37.59 o 2 2 1 87.62 100.81 3.15 o 3 2 1 5236.01 5449.24 38.66 o 4 2 1 3647.16 3718.42 26.05 o 5 2 1 1517.33 1569.34 25.08 o 6 2 1 563.25 580.48 35.68 o 7 2 1 3.11 7.08 7.73 o -7 3 1 67.20 69.39 14.44 o -6 3 1 50.15 44.21 6.67 o -5 3 1 508.00 550.72 9.68 o -4 3 1 375.93 387.08 7.44 o -3 3 1 1704.68 1754.32 14.94 o -2 3 1 2721.00 2845.12 28.89 o -1 3 1 114.99 109.21 2.87 o 0 3 1 502.15 565.03 21.45 o 1 3 1 5747.36 6155.13 48.78 o 2 3 1 7288.48 7803.65 60.77 o 3 3 1 270.12 287.17 8.99 o 4 3 1 8.25 5.44 4.18 o 5 3 1 64.28 72.12 5.09 o 6 3 1 356.93 350.62 11.70 o 7 3 1 166.11 162.35 12.54 o -7 4 1 26.82 20.07 11.35 o -6 4 1 62.18 60.78 8.82 o -5 4 1 16.26 12.75 4.31 o -4 4 1 56.98 50.53 4.46 o -3 4 1 205.23 208.61 6.29 o -2 4 1 127.65 127.81 3.69 o -1 4 1 244.66 240.04 5.67 o 0 4 1 29.52 37.75 8.40 o 1 4 1 1118.64 1142.58 20.01 o 2 4 1 1.58 5.49 3.65 o 3 4 1 223.62 226.80 11.45 o 4 4 1 6.04 3.93 4.18 o 5 4 1 61.03 67.14 5.42 o 6 4 1 21.46 25.38 6.75 o -6 5 1 0.05 -1.20 6.12 o -5 5 1 234.88 228.30 8.24 o -4 5 1 1557.43 1556.62 22.09 o -3 5 1 2763.74 2824.19 45.52 o -2 5 1 2368.47 2342.01 35.76 o -1 5 1 226.26 201.70 5.31 o 0 5 1 955.53 969.25 19.41 o 1 5 1 1800.46 1695.83 46.08 o 2 5 1 3774.08 3817.91 68.04 o 3 5 1 1947.64 1910.13 20.56 o 4 5 1 38.11 41.30 5.29 o 5 5 1 40.34 53.77 5.56 o 6 5 1 410.30 424.12 13.68 o -6 6 1 865.26 890.94 17.34 o -5 6 1 1149.23 1132.93 20.19 o -4 6 1 388.77 387.21 8.90 o -3 6 1 156.65 169.82 6.73 o -2 6 1 3196.61 3082.73 37.31 o -1 6 1 2303.31 2239.04 19.87 o 0 6 1 2120.53 2092.06 22.55 o 1 6 1 794.08 803.99 17.93 o 2 6 1 13.37 10.54 4.87 o 3 6 1 69.44 78.55 6.39 o 4 6 1 1762.24 1705.63 39.38 o 5 6 1 1498.61 1456.13 17.70 o 6 6 1 107.26 97.72 7.90 o -6 7 1 4.70 7.88 6.57 o -5 7 1 2.35 3.07 6.08 o -4 7 1 353.05 335.25 10.19 o -3 7 1 214.74 215.62 12.83 o -2 7 1 62.58 57.07 6.14 o -1 7 1 80.48 82.17 6.00 o 0 7 1 196.21 194.15 7.28 o 1 7 1 4.27 22.89 9.63 o 2 7 1 65.08 67.35 8.49 o 3 7 1 333.49 333.30 8.32 o 4 7 1 10.63 9.05 5.14 o 5 7 1 1.20 0.47 5.32 o 6 7 1 27.88 22.29 6.87 o -5 8 1 213.27 197.99 9.80 o -4 8 1 14.30 16.65 7.36 o -3 8 1 192.99 196.14 9.29 o -2 8 1 375.64 353.30 10.93 o -1 8 1 781.10 733.29 19.34 o 0 8 1 1087.33 1062.53 15.12 o 1 8 1 42.11 41.78 5.03 o 2 8 1 62.50 55.02 7.98 o 3 8 1 108.96 118.92 8.73 o 4 8 1 505.59 484.97 12.34 o 5 8 1 275.81 263.87 11.03 o -5 9 1 231.59 231.16 13.03 o -4 9 1 1039.21 1039.50 41.30 o -3 9 1 978.80 993.94 29.57 o -2 9 1 851.86 841.87 40.42 o -1 9 1 199.37 180.16 7.72 o 0 9 1 826.26 816.44 16.95 o 1 9 1 2180.96 2105.89 41.50 o 2 9 1 2277.93 2228.14 178.25 o 3 9 1 823.70 783.24 23.21 o 4 9 1 2.05 12.87 7.13 o 5 9 1 63.00 72.33 10.08 o -4 10 1 23.77 22.21 8.25 o -3 10 1 1.16 -1.67 8.38 o -2 10 1 501.57 533.54 18.00 o -1 10 1 1145.39 1194.70 24.03 o 0 10 1 1103.41 1167.44 27.77 o 1 10 1 535.98 563.05 60.95 o 2 10 1 104.00 108.75 8.94 o 3 10 1 679.95 641.73 33.29 o 4 10 1 351.77 373.03 18.95 o -4 11 1 2.83 7.40 8.21 o -3 11 1 0.90 -3.03 7.13 o -2 11 1 1.38 -0.03 7.57 o -1 11 1 8.93 1.34 8.02 o 0 11 1 0.31 0.91 4.37 o 1 11 1 43.49 48.71 7.74 o 2 11 1 1.49 -1.27 6.58 o 3 11 1 1.64 -7.76 8.69 o 4 11 1 2.99 -4.92 8.68 o -3 12 1 14.57 12.64 7.53 o -2 12 1 299.60 324.64 16.16 o -1 12 1 433.92 485.15 17.86 o 1 12 1 83.44 88.29 8.75 o 2 12 1 0.14 -5.55 8.34 o 3 12 1 156.41 183.75 14.18 o -1 13 1 16.90 13.05 8.67 o 1 13 1 450.10 502.20 19.34 o -7 0 2 786.77 820.41 30.82 o -6 0 2 699.01 729.84 25.73 o -5 0 2 487.65 497.19 12.86 o -4 0 2 1862.32 1837.51 16.55 o -3 0 2 2140.61 2140.72 27.18 o -2 0 2 1340.37 1239.75 10.43 o -1 0 2 21544.04 21216.22 141.26 o 0 0 2 4250.33 4356.04 123.95 o 1 0 2 20.03 36.05 2.87 o 2 0 2 5682.73 5668.61 100.54 o 3 0 2 11205.19 11138.24 47.01 o 4 0 2 3295.18 3225.03 28.39 o 5 0 2 458.37 447.66 19.72 o 6 0 2 10.09 12.81 9.26 o 7 0 2 165.50 157.97 17.17 o -7 1 2 10.79 19.98 11.62 o -6 1 2 419.05 426.50 11.54 o -5 1 2 1001.05 1040.00 11.36 o -4 1 2 1102.39 1109.39 9.11 o -3 1 2 1017.13 1070.47 7.80 o -2 1 2 358.76 416.61 6.29 o -1 1 2 481.23 540.19 6.55 o 0 1 2 2946.18 3095.29 14.86 o 1 1 2 13287.73 12475.26 146.92 o 2 1 2 1662.79 1655.80 50.04 o 3 1 2 17.48 21.34 2.19 o 4 1 2 318.16 324.76 7.17 o 5 1 2 900.85 891.03 14.49 o 6 1 2 442.47 429.24 15.78 o 7 1 2 260.16 256.94 14.19 o -7 2 2 8.03 12.44 10.72 o -6 2 2 7.50 4.84 5.33 o -5 2 2 92.43 83.59 5.38 o -4 2 2 5.23 9.20 3.48 o -3 2 2 7.69 6.00 2.25 o -2 2 2 35.13 23.86 1.85 o -1 2 2 578.69 709.60 9.73 o 0 2 2 1319.62 1459.27 13.37 o 1 2 2 20.63 38.88 2.15 o 2 2 2 89.77 112.73 4.75 o 3 2 2 0.73 -0.07 3.00 o 4 2 2 250.74 256.33 7.13 o 5 2 2 16.55 13.06 5.21 o 6 2 2 8.96 5.66 7.19 o 7 2 2 14.15 9.47 7.99 o -7 3 2 32.23 29.52 11.17 o -6 3 2 148.11 157.20 10.98 o -5 3 2 902.61 880.49 18.37 o -4 3 2 3240.05 3394.67 31.61 o -3 3 2 4807.49 4927.08 32.78 o -2 3 2 236.16 214.67 3.81 o -1 3 2 2416.63 2565.79 20.08 o 0 3 2 5332.24 5458.72 66.02 o 1 3 2 2333.76 2234.90 24.76 o 2 3 2 2380.83 2385.24 22.79 o 3 3 2 1039.84 1037.17 13.90 o 4 3 2 3.77 10.94 4.73 o 5 3 2 427.79 443.81 9.15 o 6 3 2 909.69 920.76 40.97 o 7 3 2 455.28 487.00 18.76 o -7 4 2 590.89 579.74 23.77 o -6 4 2 1035.03 1079.59 43.79 o -5 4 2 421.76 438.07 12.58 o -4 4 2 25.43 21.03 3.86 o -3 4 2 2283.97 2256.97 20.44 o -2 4 2 10483.82 10939.31 71.10 o -1 4 2 5048.75 4950.04 32.23 o 0 4 2 1180.31 1143.63 11.22 o 1 4 2 2.79 3.49 2.29 o 2 4 2 1202.89 1260.59 14.62 o 3 4 2 2215.56 2200.31 21.27 o 4 4 2 2211.58 2159.07 23.68 o 5 4 2 1074.24 1088.95 14.10 o 6 4 2 55.55 51.64 7.47 o -6 5 2 12.49 10.39 6.73 o -5 5 2 302.65 284.62 9.32 o -4 5 2 553.70 551.88 9.53 o -3 5 2 240.56 258.28 8.67 o -2 5 2 332.40 319.58 9.00 o -1 5 2 86.80 92.41 4.90 o 0 5 2 1139.82 1107.59 12.23 o 1 5 2 1145.71 1118.75 13.40 o 2 5 2 721.67 739.43 12.07 o 3 5 2 117.37 127.64 9.46 o 4 5 2 18.77 12.93 4.77 o 5 5 2 272.08 280.74 9.56 o 6 5 2 137.22 150.77 10.08 o -6 6 2 153.72 153.03 10.11 o -5 6 2 5.67 3.62 5.48 o -4 6 2 3.36 7.31 5.01 o -3 6 2 160.30 153.88 5.84 o -2 6 2 775.24 749.23 13.39 o -1 6 2 313.82 306.50 8.18 o 0 6 2 385.47 391.30 8.55 o 1 6 2 92.78 90.18 4.75 o 2 6 2 586.37 580.46 11.77 o 3 6 2 295.85 291.95 9.54 o 4 6 2 198.28 192.11 8.98 o 5 6 2 125.97 119.32 7.83 o 6 6 2 1.29 -0.54 5.39 o -6 7 2 82.04 87.03 9.26 o -5 7 2 1079.75 1072.70 18.21 o -4 7 2 1597.78 1591.67 24.11 o -3 7 2 317.04 325.26 11.07 o -2 7 2 742.71 709.26 10.81 o -1 7 2 37.37 43.88 5.22 o 0 7 2 3031.23 2943.96 24.10 o 1 7 2 3710.19 3640.55 40.29 o 2 7 2 3053.22 2957.05 80.93 o 3 7 2 238.06 225.87 9.18 o 4 7 2 227.20 228.39 8.84 o 5 7 2 503.91 500.52 16.63 o 6 7 2 473.88 443.73 13.60 o -5 8 2 98.09 99.19 9.71 o -4 8 2 3.16 1.32 6.82 o -3 8 2 816.19 804.90 16.85 o -2 8 2 1716.33 1615.33 21.44 o -1 8 2 1542.70 1564.48 21.88 o 0 8 2 1610.73 1640.26 19.20 o 1 8 2 3.82 1.90 6.81 o 2 8 2 543.51 521.73 24.91 o 3 8 2 929.74 944.91 28.15 o 4 8 2 1257.86 1241.64 18.94 o 5 8 2 198.40 187.55 9.71 o -5 9 2 21.64 23.50 8.54 o -4 9 2 69.25 76.99 9.44 o -3 9 2 101.41 85.55 8.39 o -2 9 2 26.96 24.17 7.62 o -1 9 2 42.58 40.92 6.09 o 0 9 2 23.21 17.99 5.42 o 1 9 2 27.12 26.97 8.00 o 2 9 2 137.18 127.56 10.66 o 3 9 2 1.95 3.14 5.37 o 4 9 2 0.92 5.08 7.20 o 5 9 2 5.32 4.91 7.54 o -4 10 2 5.95 -1.08 7.58 o -3 10 2 339.67 363.08 13.17 o -2 10 2 530.59 532.82 18.09 o -1 10 2 481.29 476.18 12.34 o 0 10 2 62.13 62.49 6.73 o 1 10 2 45.60 40.87 8.44 o 2 10 2 86.93 81.69 12.99 o 3 10 2 387.97 387.70 18.35 o 4 10 2 257.85 269.09 16.14 o -4 11 2 489.94 539.80 17.64 o -3 11 2 623.44 657.73 21.80 o -2 11 2 4.06 13.61 7.05 o -1 11 2 409.27 445.93 16.76 o 0 11 2 668.01 627.96 24.00 o 1 11 2 1155.21 1223.73 139.30 o 2 11 2 530.33 559.59 16.46 o 3 11 2 34.98 39.41 8.30 o -3 12 2 99.09 113.42 10.01 o -2 12 2 255.07 295.02 12.77 o -1 12 2 453.87 510.32 18.64 o 0 12 2 84.21 78.38 13.35 o 1 12 2 0.11 -0.14 6.66 o 2 12 2 179.68 195.68 11.69 o 3 12 2 361.55 386.17 26.71 o 1 13 2 0.14 -1.05 6.89 o -6 1 3 262.54 272.38 9.73 o -5 1 3 1218.37 1209.68 12.31 o -4 1 3 2929.66 2979.15 18.37 o -3 1 3 46.56 39.89 2.82 o -2 1 3 315.57 310.16 3.85 o -1 1 3 3273.27 3385.26 15.77 o 0 1 3 18107.37 17203.83 133.44 o 1 1 3 484.54 437.50 4.83 o 2 1 3 57.60 39.45 2.82 o 3 1 3 22.16 26.25 4.15 o 4 1 3 983.44 1059.84 12.14 o 5 1 3 756.86 747.10 17.91 o 6 1 3 504.25 501.13 16.92 o 7 1 3 235.73 245.49 14.29 o -7 2 3 580.80 602.36 26.90 o -6 2 3 459.92 488.32 16.15 o -5 2 3 87.66 86.49 4.80 o -4 2 3 1581.83 1599.11 12.00 o -3 2 3 3228.57 3199.09 24.53 o -2 2 3 7025.70 6976.28 30.30 o -1 2 3 1710.09 1578.92 11.80 o 0 2 3 41.55 57.93 2.54 o 1 2 3 627.73 613.03 8.40 o 2 2 3 7994.81 8197.73 172.43 o 3 2 3 4806.14 4757.41 30.65 o 4 2 3 1229.39 1225.11 12.40 o 5 2 3 83.39 92.93 6.99 o 6 2 3 264.79 287.59 14.16 o 7 2 3 373.80 376.29 17.19 o -7 3 3 20.35 14.80 10.81 o -6 3 3 637.91 630.19 18.02 o -5 3 3 403.27 404.03 10.88 o -4 3 3 161.76 174.75 5.27 o -3 3 3 119.98 113.84 3.96 o -2 3 3 970.40 1027.84 7.62 o -1 3 3 268.60 228.16 3.70 o 0 3 3 257.22 223.73 6.98 o 1 3 3 4217.80 4511.23 37.16 o 2 3 3 310.24 318.46 7.42 o 3 3 3 163.00 156.66 6.75 o 4 3 3 604.50 628.24 21.71 o 5 3 3 690.79 718.87 14.87 o 6 3 3 160.83 154.10 11.72 o -7 4 3 123.41 122.01 11.53 o -6 4 3 38.57 38.40 6.92 o -5 4 3 47.21 43.26 6.14 o -4 4 3 0.92 7.73 3.71 o -3 4 3 463.01 464.45 8.35 o -2 4 3 1110.23 1155.26 22.05 o -1 4 3 121.39 128.90 4.24 o 0 4 3 1136.01 1170.82 17.06 o 1 4 3 37.47 32.88 2.43 o 2 4 3 761.60 737.73 11.32 o 3 4 3 339.78 314.32 8.92 o 4 4 3 332.02 306.87 9.70 o 5 4 3 8.14 9.35 5.15 o 6 4 3 10.68 14.50 6.49 o -6 5 3 711.02 714.08 17.31 o -5 5 3 1652.52 1602.40 22.72 o -4 5 3 1238.46 1246.12 22.96 o -3 5 3 940.59 914.02 9.12 o -2 5 3 74.02 84.22 5.67 o -1 5 3 4992.35 5091.34 31.89 o 0 5 3 3797.17 3675.23 30.29 o 1 5 3 5478.70 5404.59 43.23 o 2 5 3 1901.53 1890.52 19.47 o 3 5 3 135.78 133.37 7.21 o 4 5 3 477.46 485.60 12.40 o 5 5 3 1147.61 1083.08 18.82 o 6 5 3 841.75 857.46 29.40 o -6 6 3 166.44 170.91 10.66 o -5 6 3 122.74 123.11 7.70 o -4 6 3 516.93 501.22 11.48 o -3 6 3 4110.21 3940.38 32.79 o -2 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