#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:30:52 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181059 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/39/2213972.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2213972_Fobs loop_ _publ_author_name 'Nayak, Susanta K.' 'Jena, Anirudha' 'Neelgund, Gururaj M.' 'Shivashankar, S. A.' 'Guru Row, T. N.' _publ_section_title ; Bis(tert-butyl-3-oxobutanoato)dipyridinenickel(II) benzene solvate ; _journal_coeditor_code SJ2312 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1604 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 99.205 _cell_angle_beta 93.504 _cell_angle_gamma 117.338 _cell_length_a 8.3748 _cell_length_b 8.8057 _cell_length_c 12.5949 _exptl_crystal_F_000 324.00 _reflns_d_resolution_high 0.8201 _cod_data_source_file sj2312Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' nitm in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 109.53 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 5626.53 4822.47 173.39 o 2 0 0 2626.78 2550.62 27.62 o 3 0 0 176.26 139.47 2.12 o 4 0 0 304.64 275.07 3.46 o 5 0 0 363.07 364.55 5.38 o 6 0 0 3.10 2.84 1.39 o 7 0 0 102.58 103.28 2.42 o 8 0 0 42.55 39.69 1.89 o -9 1 0 52.14 54.52 2.79 o -8 1 0 67.69 74.36 2.11 o -7 1 0 42.41 43.28 1.46 o -6 1 0 50.78 51.51 1.44 o -5 1 0 164.95 145.57 3.09 o -4 1 0 428.43 486.44 6.61 o -3 1 0 81.19 85.73 1.52 o -2 1 0 954.62 959.79 21.10 o -1 1 0 1536.81 1566.32 57.56 o 0 1 0 2322.25 2077.31 25.62 o 1 1 0 483.57 513.44 6.51 o 2 1 0 11.52 11.03 0.36 o 3 1 0 126.89 128.56 2.51 o 4 1 0 321.70 325.61 4.11 o 5 1 0 108.80 113.77 2.29 o 6 1 0 90.41 84.16 3.53 o 7 1 0 74.88 85.76 2.78 o 8 1 0 70.83 68.68 2.63 o -9 2 0 70.02 74.43 2.21 o -8 2 0 101.51 98.59 2.43 o -7 2 0 105.05 96.28 2.22 o -6 2 0 462.04 461.52 6.67 o -5 2 0 0.84 2.55 0.49 o -4 2 0 145.78 193.51 3.03 o -3 2 0 25.97 30.73 0.60 o -2 2 0 2836.64 2822.30 79.70 o -1 2 0 11995.90 8494.03 517.47 o 0 2 0 766.28 751.45 8.22 o 1 2 0 694.98 684.69 7.60 o 2 2 0 412.60 401.65 4.73 o 3 2 0 187.98 172.81 2.41 o 4 2 0 38.23 34.21 1.11 o 5 2 0 297.84 286.59 5.73 o 6 2 0 310.75 288.84 6.03 o 7 2 0 141.27 127.41 3.69 o -9 3 0 22.32 28.05 1.36 o -8 3 0 4.24 5.17 0.66 o -7 3 0 432.74 419.92 6.36 o -6 3 0 205.96 203.53 3.46 o -5 3 0 6.20 8.78 0.77 o -4 3 0 78.59 76.74 1.25 o -3 3 0 667.77 724.17 8.11 o -2 3 0 6177.75 5615.23 229.27 o -1 3 0 1278.22 1343.98 14.57 o 0 3 0 279.48 296.78 3.53 o 1 3 0 17.11 19.99 0.53 o 2 3 0 283.76 293.68 4.36 o 3 3 0 3.76 6.04 0.83 o 4 3 0 8.52 9.68 0.66 o 5 3 0 55.60 58.20 2.13 o 6 3 0 93.60 95.74 3.04 o 7 3 0 67.60 67.26 2.68 o -10 4 0 25.33 26.32 1.40 o -9 4 0 10.53 13.39 1.33 o -8 4 0 26.49 27.13 1.21 o -7 4 0 420.80 411.45 6.25 o -6 4 0 25.35 21.03 0.97 o -5 4 0 29.42 22.08 0.66 o -4 4 0 2.51 1.48 0.32 o -3 4 0 2392.79 2446.29 26.38 o -2 4 0 2983.08 2919.54 51.77 o -1 4 0 840.16 806.60 9.01 o 0 4 0 262.95 222.40 2.84 o 1 4 0 177.35 157.77 2.19 o 2 4 0 18.86 12.26 0.67 o 3 4 0 9.57 11.30 0.72 o 4 4 0 165.23 165.33 3.22 o 5 4 0 59.84 56.19 3.26 o 6 4 0 86.76 88.86 7.47 o -10 5 0 11.79 13.04 1.31 o -9 5 0 21.21 25.48 1.28 o -8 5 0 101.15 105.42 2.49 o -7 5 0 0.81 -0.48 0.70 o -6 5 0 25.15 19.41 2.42 o -5 5 0 83.77 89.64 1.59 o -4 5 0 258.72 250.19 3.30 o -3 5 0 540.82 557.37 6.54 o -2 5 0 521.07 542.84 6.35 o -1 5 0 374.05 372.98 4.54 o 0 5 0 349.38 383.96 5.59 o 1 5 0 334.31 372.40 5.58 o 2 5 0 2.11 2.96 0.79 o 3 5 0 112.04 111.70 2.50 o 4 5 0 133.81 136.53 6.20 o 5 5 0 78.24 74.90 2.74 o -10 6 0 0.94 1.59 0.66 o -9 6 0 51.40 51.82 3.29 o -8 6 0 164.58 159.69 3.25 o -7 6 0 1.65 0.96 0.43 o -6 6 0 63.22 61.90 1.60 o -5 6 0 120.75 121.89 2.37 o -4 6 0 359.72 363.14 4.61 o -3 6 0 340.71 343.88 4.38 o -2 6 0 277.12 266.45 3.52 o -1 6 0 459.94 468.29 6.74 o 0 6 0 678.95 693.47 9.63 o 1 6 0 13.69 12.95 0.82 o 2 6 0 17.21 14.84 0.92 o 3 6 0 124.42 116.03 2.91 o 4 6 0 112.11 104.27 3.46 o -9 7 0 59.50 59.87 4.87 o -8 7 0 51.76 54.56 3.48 o -7 7 0 29.94 33.01 1.37 o -6 7 0 45.16 45.10 1.80 o -5 7 0 192.28 187.98 3.43 o -4 7 0 48.47 40.49 1.05 o -3 7 0 186.97 176.43 3.14 o -2 7 0 0.74 0.63 0.33 o -1 7 0 44.25 42.95 1.50 o 0 7 0 17.12 16.93 0.92 o 1 7 0 4.10 3.08 0.55 o 2 7 0 34.77 39.84 1.53 o 3 7 0 36.48 43.43 1.76 o -9 8 0 30.62 31.25 1.85 o -8 8 0 7.57 10.01 1.29 o -7 8 0 7.39 7.59 0.99 o -6 8 0 107.31 107.64 2.50 o -5 8 0 23.48 26.74 1.21 o -4 8 0 14.05 17.47 1.32 o -3 8 0 206.36 216.22 4.99 o -2 8 0 240.23 236.96 5.43 o -1 8 0 166.78 163.88 4.28 o 0 8 0 0.28 0.17 0.62 o 1 8 0 34.36 37.69 2.01 o 2 8 0 67.89 64.74 2.77 o -8 9 0 1.35 1.70 0.70 o -7 9 0 36.57 36.02 2.79 o -6 9 0 84.86 70.81 2.57 o -5 9 0 37.96 34.70 1.85 o -4 9 0 68.47 63.35 2.44 o -3 9 0 93.86 89.25 3.01 o -2 9 0 134.63 127.00 3.81 o -1 9 0 28.30 25.93 1.71 o 0 9 0 0.88 -0.61 0.63 o -7 10 0 15.69 21.08 2.26 o -6 10 0 0.21 1.24 0.77 o -5 10 0 1.29 2.53 0.85 o -4 10 0 37.80 35.26 1.99 o -3 10 0 80.52 80.56 3.08 o -2 10 0 34.79 37.18 5.23 o 2 -10 1 25.50 26.39 1.85 o 3 -10 1 69.34 69.87 7.05 o 4 -10 1 28.58 29.01 1.82 o 5 -10 1 0.32 0.24 0.66 o 6 -10 1 6.87 7.96 2.05 o 7 -10 1 13.53 13.70 1.89 o 0 -9 1 28.09 26.56 3.28 o 1 -9 1 48.53 50.33 2.56 o 2 -9 1 171.66 169.09 4.49 o 3 -9 1 95.21 96.25 6.93 o 4 -9 1 6.03 7.44 1.02 o 5 -9 1 0.54 1.12 0.70 o 6 -9 1 47.52 47.23 2.59 o 7 -9 1 66.64 63.03 4.05 o 8 -9 1 27.85 27.29 1.66 o -2 -8 1 40.38 41.76 2.18 o -1 -8 1 46.35 51.54 3.45 o 0 -8 1 16.82 18.08 1.62 o 1 -8 1 62.22 57.22 2.28 o 2 -8 1 211.93 211.19 4.92 o 3 -8 1 117.44 114.91 3.24 o 4 -8 1 46.68 45.21 2.01 o 5 -8 1 0.60 0.77 0.39 o 6 -8 1 56.62 56.39 1.70 o 7 -8 1 67.58 66.48 4.77 o 8 -8 1 30.80 31.71 2.28 o 9 -8 1 27.61 36.28 2.96 o -3 -7 1 17.52 19.49 1.19 o -2 -7 1 18.05 18.46 1.07 o -1 -7 1 12.64 10.53 0.82 o 0 -7 1 176.69 167.03 3.23 o 1 -7 1 80.11 76.45 1.90 o 2 -7 1 76.39 77.35 1.86 o 3 -7 1 13.18 11.34 0.89 o 4 -7 1 9.15 7.38 0.50 o 5 -7 1 115.89 117.51 2.06 o 6 -7 1 58.62 59.73 2.41 o 7 -7 1 250.53 248.63 4.31 o 8 -7 1 68.10 67.87 2.57 o 9 -7 1 71.47 72.53 2.16 o -4 -6 1 85.25 83.16 6.64 o -3 -6 1 115.85 117.31 3.15 o -2 -6 1 36.32 36.68 1.34 o -1 -6 1 184.95 190.63 3.48 o 0 -6 1 815.20 831.32 11.30 o 1 -6 1 762.85 787.42 10.64 o 2 -6 1 248.60 249.11 3.69 o 3 -6 1 165.88 161.83 2.39 o 4 -6 1 170.62 176.71 2.61 o 5 -6 1 64.76 69.22 1.43 o 6 -6 1 6.17 6.33 0.82 o 7 -6 1 10.56 10.14 0.75 o 8 -6 1 55.02 55.37 1.74 o 9 -6 1 97.21 100.72 2.67 o 10 -6 1 0.30 -0.51 0.64 o -5 -5 1 42.58 40.92 2.94 o -4 -5 1 100.19 103.34 3.06 o -3 -5 1 29.29 26.62 1.14 o -2 -5 1 64.72 61.47 1.64 o -1 -5 1 745.97 729.62 9.95 o 0 -5 1 706.79 716.28 9.67 o 1 -5 1 518.68 511.71 6.01 o 2 -5 1 37.31 49.11 1.00 o 3 -5 1 109.95 140.09 2.10 o 4 -5 1 167.69 148.12 2.36 o 5 -5 1 118.48 102.33 2.21 o 6 -5 1 148.78 134.90 4.00 o 7 -5 1 47.56 48.37 1.49 o 8 -5 1 79.79 77.03 2.08 o 9 -5 1 55.62 60.61 1.96 o 10 -5 1 2.60 3.51 0.74 o -6 -4 1 40.03 37.99 1.98 o -5 -4 1 86.10 79.61 2.66 o -4 -4 1 55.39 55.41 1.62 o -3 -4 1 0.76 1.37 0.43 o -2 -4 1 246.82 254.85 4.04 o -1 -4 1 545.36 556.95 7.63 o 0 -4 1 1331.22 1427.29 24.97 o 1 -4 1 309.65 349.81 4.17 o 2 -4 1 283.66 303.67 3.72 o 3 -4 1 1153.78 1258.05 13.84 o 4 -4 1 318.68 334.14 4.13 o 5 -4 1 97.34 97.39 1.61 o 6 -4 1 363.90 364.02 5.47 o 7 -4 1 406.67 422.13 6.38 o 8 -4 1 40.44 40.92 1.47 o 9 -4 1 6.16 5.73 0.77 o 10 -4 1 4.19 6.05 0.83 o -7 -3 1 47.80 44.83 2.50 o -6 -3 1 97.99 99.29 3.08 o -5 -3 1 76.53 71.84 2.37 o -4 -3 1 34.46 38.45 1.46 o -3 -3 1 85.20 78.24 1.72 o -2 -3 1 1239.50 1248.45 13.76 o -1 -3 1 383.26 354.19 4.97 o 0 -3 1 500.26 467.88 6.24 o 1 -3 1 490.58 556.65 6.25 o 2 -3 1 155.65 146.25 2.23 o 3 -3 1 81.30 69.82 1.13 o 4 -3 1 71.84 70.18 3.05 o 5 -3 1 129.86 136.92 2.45 o 6 -3 1 519.87 524.77 7.44 o 7 -3 1 301.86 296.71 4.85 o 8 -3 1 13.62 13.19 0.90 o 9 -3 1 3.59 6.31 1.44 o -7 -2 1 141.60 131.63 8.82 o -6 -2 1 378.59 356.62 7.06 o -5 -2 1 384.82 383.41 7.19 o -4 -2 1 11.27 13.70 0.56 o -3 -2 1 969.05 1052.98 11.73 o -2 -2 1 1652.38 1790.75 19.38 o -1 -2 1 1227.87 1259.29 19.23 o 0 -2 1 54.75 40.38 1.45 o 1 -2 1 201.32 228.63 2.68 o 2 -2 1 966.20 937.80 10.24 o 3 -2 1 259.93 303.29 3.60 o 4 -2 1 119.51 147.15 2.01 o 5 -2 1 86.57 76.85 2.39 o 6 -2 1 438.18 442.56 6.46 o 7 -2 1 51.97 55.22 1.62 o 8 -2 1 38.45 37.96 2.46 o 9 -2 1 29.09 33.43 1.50 o -8 -1 1 73.90 70.36 2.99 o -7 -1 1 76.99 72.36 2.50 o -6 -1 1 48.23 42.00 2.48 o -5 -1 1 19.02 20.11 0.86 o -4 -1 1 130.36 123.68 1.88 o -3 -1 1 1981.73 2161.05 23.32 o -2 -1 1 368.84 355.87 4.80 o -1 -1 1 5126.70 4731.66 57.92 o 0 -1 1 3165.91 2835.22 95.48 o 1 -1 1 262.87 330.50 3.69 o 2 -1 1 1721.13 1673.38 40.76 o 3 -1 1 141.29 145.85 1.91 o 4 -1 1 727.81 720.77 8.16 o 5 -1 1 839.21 847.84 11.22 o 6 -1 1 150.53 133.65 2.64 o 7 -1 1 13.22 16.34 1.13 o 8 -1 1 12.58 13.43 0.94 o 9 -1 1 29.73 31.06 1.79 o -9 0 1 16.94 13.67 1.29 o -8 0 1 87.07 84.41 3.12 o -7 0 1 94.07 86.22 2.69 o -6 0 1 26.65 29.35 1.15 o -5 0 1 1.20 1.49 0.76 o -4 0 1 781.95 884.98 9.92 o -3 0 1 1028.03 1077.75 11.82 o -2 0 1 210.62 228.22 3.12 o -1 0 1 2796.18 2660.05 28.39 o 1 0 1 1577.12 1539.48 16.48 o 2 0 1 211.47 221.56 2.93 o 3 0 1 528.54 550.67 6.28 o 4 0 1 891.08 1007.52 11.27 o 5 0 1 109.18 123.31 2.38 o 6 0 1 6.44 5.16 0.58 o 7 0 1 0.39 0.46 0.65 o 8 0 1 19.09 19.92 1.42 o -9 1 1 109.88 109.44 3.43 o -8 1 1 137.41 134.86 3.00 o -7 1 1 133.41 131.88 2.78 o -6 1 1 7.63 10.73 0.69 o -5 1 1 62.29 47.53 1.25 o -4 1 1 450.50 445.36 6.09 o -3 1 1 495.79 475.19 7.57 o -2 1 1 1579.71 1593.52 21.16 o -1 1 1 2806.11 2814.80 44.94 o 0 1 1 125.22 151.21 2.05 o 1 1 1 1015.27 1063.44 11.53 o 2 1 1 6.77 8.93 0.39 o 3 1 1 254.85 228.79 2.96 o 4 1 1 1402.53 1469.44 16.25 o 5 1 1 199.14 168.82 3.04 o 6 1 1 79.17 75.05 1.91 o 7 1 1 30.85 33.63 2.61 o 8 1 1 67.03 67.81 2.67 o -9 2 1 78.45 75.97 2.24 o -8 2 1 180.55 169.87 4.05 o -7 2 1 146.79 129.57 2.69 o -6 2 1 68.98 69.60 1.69 o -5 2 1 483.57 477.14 6.66 o -4 2 1 9.70 7.72 0.76 o -3 2 1 113.71 116.59 1.81 o -2 2 1 1972.92 1983.15 25.84 o -1 2 1 2979.29 2872.87 47.87 o 0 2 1 119.05 115.91 1.69 o 1 2 1 44.20 43.49 0.78 o 2 2 1 227.75 234.13 2.98 o 3 2 1 718.93 812.41 9.25 o 4 2 1 128.46 133.37 2.13 o 5 2 1 19.24 23.45 1.46 o 6 2 1 133.30 136.72 3.63 o 7 2 1 68.79 71.42 2.67 o -10 3 1 64.59 70.77 2.28 o -9 3 1 14.40 19.40 1.15 o -8 3 1 65.14 65.91 1.89 o -7 3 1 45.53 44.76 1.44 o -6 3 1 172.41 168.54 3.01 o -5 3 1 134.98 139.00 2.46 o -4 3 1 20.76 12.80 0.45 o -3 3 1 2612.46 2567.74 44.03 o -2 3 1 2982.90 2895.47 47.81 o -1 3 1 914.07 921.63 10.13 o 0 3 1 201.87 236.36 2.91 o 1 3 1 161.83 222.96 2.85 o 2 3 1 29.38 15.31 0.54 o 3 3 1 191.36 174.08 3.03 o 4 3 1 0.55 0.98 0.50 o 5 3 1 0.60 -0.19 0.51 o 6 3 1 63.49 72.27 2.63 o 7 3 1 44.05 52.66 3.26 o -10 4 1 50.93 50.40 1.88 o -9 4 1 60.91 59.91 1.91 o -8 4 1 60.82 60.85 1.79 o -7 4 1 88.38 86.90 2.08 o -6 4 1 394.89 412.76 6.05 o -5 4 1 197.81 205.00 2.88 o -4 4 1 207.23 207.13 2.76 o -3 4 1 3204.03 3500.49 37.48 o -2 4 1 2628.90 2761.30 30.11 o -1 4 1 404.51 432.54 5.08 o 0 4 1 105.36 114.09 1.70 o 1 4 1 205.86 235.00 3.08 o 2 4 1 179.65 180.35 3.57 o 3 4 1 40.48 42.65 1.58 o 4 4 1 7.91 9.44 0.81 o 5 4 1 44.47 42.63 1.95 o 6 4 1 40.94 47.31 3.16 o -10 5 1 20.53 20.66 1.23 o -9 5 1 38.53 41.95 1.58 o -8 5 1 37.90 40.04 1.44 o -7 5 1 31.19 38.57 1.31 o -6 5 1 21.95 20.54 0.89 o -5 5 1 25.72 19.63 0.68 o -4 5 1 452.16 436.39 5.30 o -3 5 1 1188.80 1177.99 13.10 o -2 5 1 125.23 104.43 1.65 o -1 5 1 136.35 112.57 2.40 o 0 5 1 107.95 104.54 2.38 o 1 5 1 171.32 169.56 3.94 o 2 5 1 137.01 122.47 2.54 o 3 5 1 35.35 32.75 1.30 o 4 5 1 82.76 73.14 2.53 o 5 5 1 65.87 68.64 2.65 o -10 6 1 12.35 13.04 1.98 o -9 6 1 30.65 28.42 1.72 o -8 6 1 166.38 164.58 2.91 o -7 6 1 14.33 15.81 1.01 o -6 6 1 13.06 12.99 0.74 o -5 6 1 96.00 105.56 3.80 o -4 6 1 1172.26 1207.36 13.56 o -3 6 1 634.82 648.66 11.24 o -2 6 1 4.18 4.47 0.37 o -1 6 1 271.51 274.04 4.33 o 0 6 1 135.01 144.13 2.76 o 1 6 1 92.44 95.99 2.21 o 2 6 1 0.43 0.60 0.45 o 3 6 1 20.15 22.30 1.15 o 4 6 1 69.27 70.40 2.65 o -9 7 1 55.20 55.70 4.30 o -8 7 1 16.14 19.76 1.41 o -7 7 1 9.29 9.43 1.00 o -6 7 1 70.91 73.86 2.42 o -5 7 1 136.28 147.51 2.93 o -4 7 1 549.35 557.82 11.89 o -3 7 1 34.69 36.80 1.74 o -2 7 1 2.71 2.53 0.99 o -1 7 1 1.78 2.96 1.03 o 0 7 1 0.39 -0.42 0.42 o 1 7 1 7.35 6.40 1.66 o 2 7 1 2.78 3.13 0.81 o 3 7 1 44.04 48.72 3.30 o -9 8 1 20.97 20.08 3.28 o -8 8 1 2.78 5.31 0.91 o -7 8 1 30.33 29.01 1.59 o -6 8 1 147.71 135.04 4.75 o -5 8 1 319.96 298.07 5.03 o -4 8 1 131.85 123.50 3.46 o -3 8 1 89.02 79.97 2.70 o -2 8 1 275.38 246.02 5.61 o -1 8 1 89.20 78.92 2.78 o 0 8 1 9.07 10.26 1.19 o 1 8 1 7.29 7.19 1.09 o -8 9 1 0.18 0.09 0.60 o -7 9 1 9.55 8.35 1.05 o -6 9 1 129.79 125.58 3.68 o -5 9 1 154.51 149.21 4.09 o -4 9 1 54.68 50.27 2.22 o -3 9 1 51.56 57.00 2.40 o -2 9 1 46.06 47.51 2.25 o -1 9 1 11.42 12.93 1.41 o 0 9 1 2.10 1.39 0.77 o -7 10 1 28.24 27.67 2.55 o -6 10 1 58.01 59.83 2.60 o -5 10 1 7.28 6.60 1.11 o -4 10 1 26.42 24.27 1.74 o -3 10 1 34.23 30.54 1.96 o 2 -10 2 7.57 10.93 2.66 o 3 -10 2 16.35 17.93 1.51 o 4 -10 2 52.24 55.64 2.41 o 5 -10 2 33.20 34.65 2.67 o 6 -10 2 3.81 5.76 1.02 o 0 -9 2 29.93 31.99 1.89 o 1 -9 2 30.02 32.11 1.81 o 2 -9 2 124.18 118.01 3.53 o 3 -9 2 75.20 69.48 2.57 o 4 -9 2 38.39 37.45 1.81 o 5 -9 2 25.69 27.72 3.52 o 6 -9 2 46.39 44.23 1.93 o 7 -9 2 114.41 114.63 3.35 o 8 -9 2 47.66 50.03 3.26 o -2 -8 2 19.64 21.91 1.29 o -1 -8 2 48.93 46.73 1.70 o 0 -8 2 1.14 1.92 0.60 o 1 -8 2 5.03 4.51 0.70 o 2 -8 2 66.07 63.91 2.34 o 3 -8 2 19.28 21.85 1.04 o 4 -8 2 20.32 26.27 1.12 o 5 -8 2 2.47 1.75 0.39 o 6 -8 2 98.99 101.12 2.38 o 7 -8 2 127.02 133.13 2.87 o 8 -8 2 20.96 23.20 1.47 o 9 -8 2 25.14 27.33 2.66 o -3 -7 2 12.22 17.21 1.49 o -2 -7 2 16.46 14.92 1.03 o -1 -7 2 86.15 86.92 2.96 o 0 -7 2 45.33 47.77 1.52 o 1 -7 2 210.70 210.13 3.71 o 2 -7 2 30.20 28.72 1.25 o 3 -7 2 3.19 4.11 0.83 o 4 -7 2 63.59 63.05 1.22 o 5 -7 2 21.71 24.23 0.86 o 6 -7 2 237.54 237.02 4.05 o 7 -7 2 126.13 125.62 2.74 o 8 -7 2 87.41 88.13 2.29 o 9 -7 2 47.26 46.46 2.87 o -4 -6 2 52.80 52.07 2.23 o -3 -6 2 65.36 62.73 1.91 o -2 -6 2 202.03 197.90 3.69 o -1 -6 2 89.36 86.89 2.94 o 0 -6 2 339.60 333.13 6.49 o 1 -6 2 622.87 624.07 8.64 o 2 -6 2 3.27 2.04 0.27 o 3 -6 2 2.73 5.79 0.43 o 4 -6 2 28.10 24.13 0.77 o 5 -6 2 186.63 183.25 2.43 o 6 -6 2 18.33 17.52 0.87 o 7 -6 2 10.32 9.11 0.74 o 8 -6 2 44.78 48.43 1.64 o 9 -6 2 109.39 117.12 3.49 o -5 -5 2 24.84 25.15 3.05 o -4 -5 2 9.60 11.72 1.10 o -3 -5 2 91.02 89.18 4.65 o -2 -5 2 116.22 119.78 2.48 o -1 -5 2 238.93 249.01 4.02 o 0 -5 2 1108.72 1223.04 15.85 o 1 -5 2 99.15 110.34 1.77 o 2 -5 2 42.15 50.65 1.18 o 3 -5 2 0.93 1.70 0.26 o 4 -5 2 287.10 307.62 3.94 o 5 -5 2 482.86 499.73 6.07 o 6 -5 2 336.37 344.58 5.29 o 7 -5 2 56.09 56.06 2.06 o 8 -5 2 132.19 120.86 2.73 o 9 -5 2 113.81 113.57 3.42 o 10 -5 2 7.82 7.51 1.13 o -6 -4 2 19.52 21.11 1.50 o -5 -4 2 11.63 13.72 1.14 o -4 -4 2 1.26 2.01 0.46 o -3 -4 2 222.77 221.56 3.77 o -2 -4 2 0.72 2.27 0.36 o -1 -4 2 591.22 540.28 7.43 o 0 -4 2 157.31 142.34 4.49 o 1 -4 2 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