#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/40/2214086.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214086_Fobs loop_ _publ_author_name 'Blaurock, Steffen' 'Scholz, Mario' 'Roesky, Herbert W.' 'Edelmann, Frank T.' _publ_section_title ; Dichloro(dimethylsulfoximino)phosphane ; _journal_coeditor_code BT2385 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3247 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 71.593 _cell_angle_beta 79.730 _cell_angle_gamma 78.255 _cell_length_a 5.9867 _cell_length_b 7.7230 _cell_length_c 8.7161 _exptl_crystal_F_000 196.00 _reflns_d_resolution_high 0.7688 _[local]_cod_data_source_file bt2385Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' maiden2 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 90.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas 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o -6 3 0 45.90 39.71 2.67 o -5 3 0 63.88 60.53 2.83 o -4 3 0 180.78 182.57 2.96 o -3 3 0 0.17 0.78 0.58 o -2 3 0 655.40 650.71 6.07 o -1 3 0 9.23 9.12 0.78 o 0 3 0 3.07 4.69 0.50 o 1 3 0 518.14 508.37 15.12 o 2 3 0 3.61 3.11 0.52 o 3 3 0 5.71 4.45 0.59 o 4 3 0 59.67 62.54 2.22 o 5 3 0 15.86 16.69 1.52 o 6 3 0 30.18 35.58 2.25 o 7 3 0 2.53 2.20 1.15 o -6 4 0 106.70 109.09 4.29 o -5 4 0 342.32 337.83 6.70 o -4 4 0 978.57 926.13 12.84 o -3 4 0 5.92 6.06 0.77 o -2 4 0 277.49 261.17 3.16 o -1 4 0 668.57 612.44 6.91 o 0 4 0 425.37 384.82 5.02 o 1 4 0 1653.98 1549.23 7.31 o 2 4 0 1803.22 1674.78 8.04 o 3 4 0 243.53 246.25 7.80 o 4 4 0 1216.00 1138.52 13.11 o 5 4 0 313.84 301.86 5.83 o 6 4 0 0.19 -0.89 0.99 o 7 4 0 160.70 168.26 5.34 o -5 5 0 280.26 280.17 6.54 o -4 5 0 78.21 73.07 3.64 o -3 5 0 34.82 38.81 1.55 o -2 5 0 323.54 315.59 3.81 o -1 5 0 568.94 535.72 4.81 o 0 5 0 351.58 347.33 7.40 o 1 5 0 1916.55 1797.58 20.25 o 2 5 0 55.35 50.57 1.94 o 3 5 0 191.15 173.76 2.81 o 4 5 0 71.57 69.10 2.25 o 5 5 0 37.16 35.98 1.63 o 6 5 0 4.84 4.76 1.36 o 7 5 0 159.81 165.91 5.28 o -5 6 0 18.50 22.65 2.25 o -4 6 0 19.28 21.12 1.46 o -3 6 0 28.45 32.28 1.91 o -2 6 0 5.47 4.30 1.67 o -1 6 0 22.60 25.06 1.26 o 0 6 0 3.37 4.45 0.70 o 1 6 0 155.36 146.83 3.74 o 2 6 0 49.95 49.79 1.66 o 3 6 0 179.38 166.93 2.98 o 4 6 0 53.81 45.46 1.78 o 5 6 0 42.71 36.39 2.38 o 6 6 0 3.51 2.51 1.31 o -4 7 0 88.12 88.24 3.79 o -3 7 0 16.83 19.16 1.44 o -2 7 0 23.54 24.46 1.41 o -1 7 0 7.70 6.40 0.94 o 0 7 0 10.94 10.09 2.15 o 1 7 0 84.34 85.36 4.73 o 2 7 0 35.90 36.02 1.53 o 3 7 0 58.34 64.55 2.05 o 4 7 0 35.47 36.93 1.72 o 5 7 0 49.72 51.63 3.77 o 6 7 0 0.86 -0.47 1.15 o -3 8 0 157.85 174.15 8.84 o -2 8 0 22.93 26.29 1.66 o -1 8 0 27.03 29.18 1.63 o 0 8 0 26.86 28.24 2.77 o 1 8 0 152.51 150.31 3.22 o 2 8 0 36.67 36.34 2.67 o 3 8 0 167.14 176.68 7.82 o 4 8 0 135.67 136.02 3.71 o 5 8 0 37.94 40.99 2.05 o -1 9 0 18.09 21.63 1.59 o 0 9 0 132.04 129.90 3.31 o 1 9 0 45.53 48.98 3.61 o 2 9 0 156.66 165.10 10.52 o 3 9 0 245.17 259.32 4.68 o -2 -9 1 32.03 35.17 1.92 o -1 -9 1 165.43 177.33 3.98 o 0 -9 1 2.63 1.12 1.67 o -4 -8 1 0.55 -1.49 1.54 o -3 -8 1 42.81 42.46 1.92 o -2 -8 1 48.95 54.63 3.03 o -1 -8 1 83.86 86.35 4.08 o 0 -8 1 127.42 137.17 3.18 o 1 -8 1 0.10 -0.16 1.99 o 2 -8 1 14.43 14.31 1.41 o -5 -7 1 0.03 -0.58 1.36 o -4 -7 1 3.39 3.90 0.96 o -3 -7 1 73.86 70.47 5.70 o -2 -7 1 8.05 6.53 0.94 o -1 -7 1 23.61 20.34 1.37 o 0 -7 1 0.99 1.04 1.65 o 1 -7 1 0.99 2.14 0.74 o 2 -7 1 18.82 23.42 1.48 o 3 -7 1 0.18 -0.39 0.75 o 4 -7 1 12.39 11.49 2.12 o -6 -6 1 1.86 0.94 1.26 o -5 -6 1 439.40 446.68 11.77 o -4 -6 1 120.43 125.52 2.83 o -3 -6 1 30.86 30.74 1.46 o -2 -6 1 102.21 111.86 2.44 o -1 -6 1 455.40 465.87 6.78 o 0 -6 1 77.42 77.23 2.03 o 1 -6 1 400.72 422.37 4.72 o 2 -6 1 328.47 319.85 7.51 o 3 -6 1 76.56 75.84 2.31 o 4 -6 1 293.17 280.69 10.12 o -6 -5 1 122.13 120.44 4.39 o -5 -5 1 275.74 265.42 7.14 o -4 -5 1 54.02 48.54 1.72 o -3 -5 1 24.51 24.59 2.25 o -2 -5 1 347.97 338.13 3.92 o -1 -5 1 672.10 633.05 8.84 o 0 -5 1 449.29 434.47 5.34 o 1 -5 1 1597.78 1512.49 29.35 o 2 -5 1 7.09 7.83 1.12 o 3 -5 1 621.10 600.48 9.65 o 4 -5 1 184.37 188.83 4.08 o 5 -5 1 1.58 2.72 1.15 o -7 -4 1 60.02 63.20 3.51 o -6 -4 1 7.08 8.21 1.57 o -5 -4 1 313.20 311.36 4.27 o -4 -4 1 42.68 41.59 1.55 o -3 -4 1 11.33 12.37 1.75 o -2 -4 1 84.39 75.98 1.70 o -1 -4 1 127.12 133.90 2.11 o 0 -4 1 436.00 423.41 3.68 o 1 -4 1 54.02 53.71 1.42 o 2 -4 1 341.14 326.72 8.61 o 3 -4 1 37.35 37.22 1.42 o 4 -4 1 248.27 231.23 6.36 o 5 -4 1 16.38 15.54 1.78 o 6 -4 1 0.00 1.36 1.26 o -7 -3 1 139.43 145.50 4.87 o -6 -3 1 189.77 193.43 5.02 o -5 -3 1 148.57 154.55 4.08 o -4 -3 1 86.07 80.46 1.92 o -3 -3 1 0.24 1.54 0.52 o -2 -3 1 3.70 4.27 0.55 o -1 -3 1 72.80 61.57 4.66 o 0 -3 1 197.66 188.22 3.85 o 1 -3 1 987.79 917.79 10.57 o 2 -3 1 102.23 110.95 2.59 o 3 -3 1 131.48 117.22 2.20 o 4 -3 1 27.39 26.90 2.43 o 5 -3 1 10.27 11.41 1.52 o 6 -3 1 0.37 -0.68 1.10 o -7 -2 1 5.25 7.43 1.62 o -6 -2 1 116.43 115.73 3.87 o -5 -2 1 748.87 781.81 9.00 o -4 -2 1 64.81 58.14 3.01 o -3 -2 1 1458.22 1464.68 7.39 o -2 -2 1 16.43 20.04 1.75 o -1 -2 1 2498.95 2494.79 11.54 o 0 -2 1 1544.25 1481.99 5.83 o 1 -2 1 3.58 8.48 0.55 o 2 -2 1 318.20 335.52 2.98 o 3 -2 1 955.88 873.89 5.60 o 4 -2 1 61.67 59.41 1.70 o 5 -2 1 292.01 274.42 5.55 o 6 -2 1 30.39 33.48 2.30 o 7 -2 1 16.03 15.64 2.04 o -7 -1 1 9.10 9.42 1.78 o -6 -1 1 849.47 884.36 10.57 o -5 -1 1 82.44 104.43 3.30 o -4 -1 1 1634.42 1718.64 8.99 o -3 -1 1 1864.87 2037.08 8.73 o -2 -1 1 25.54 31.42 0.89 o -1 -1 1 1921.68 1933.52 13.94 o 0 -1 1 5290.74 4366.14 14.60 o 1 -1 1 1021.78 1008.57 4.94 o 2 -1 1 1851.18 1647.97 6.77 o 3 -1 1 1728.29 1547.46 7.44 o 4 -1 1 384.92 372.49 4.32 o 5 -1 1 983.19 906.86 9.73 o 6 -1 1 104.32 96.22 3.51 o 7 -1 1 0.19 1.78 1.36 o -7 0 1 59.00 67.49 3.40 o -6 0 1 115.41 126.67 4.08 o -5 0 1 85.98 86.59 3.03 o -4 0 1 151.94 172.92 6.46 o -3 0 1 58.84 91.29 1.65 o -2 0 1 69.97 96.89 1.52 o -1 0 1 283.69 289.15 1.96 o 1 0 1 1484.44 1530.78 9.08 o 2 0 1 1664.16 1562.58 7.53 o 3 0 1 266.42 264.48 2.75 o 4 0 1 335.48 323.91 3.46 o 5 0 1 82.75 80.00 2.83 o 6 0 1 1.08 2.20 1.05 o 7 0 1 32.96 29.87 2.46 o -7 1 1 5.67 5.65 1.52 o -6 1 1 148.98 145.08 4.45 o -5 1 1 9.09 6.38 1.26 o -4 1 1 819.54 811.42 7.80 o -3 1 1 349.53 382.11 3.53 o -2 1 1 4.71 1.78 0.42 o -1 1 1 361.26 341.56 2.46 o 0 1 1 618.46 628.70 2.52 o 1 1 1 46.58 57.87 1.23 o 2 1 1 1269.51 1267.39 5.29 o 3 1 1 712.20 705.90 6.28 o 4 1 1 1000.87 1041.06 10.18 o 5 1 1 617.66 656.19 7.90 o 6 1 1 11.55 8.89 1.46 o 7 1 1 0.75 1.67 1.26 o -7 2 1 1.59 -1.10 1.10 o -6 2 1 5.29 4.45 1.20 o -5 2 1 0.03 3.66 1.05 o -4 2 1 236.44 235.03 3.40 o -3 2 1 128.88 129.40 2.09 o -2 2 1 947.86 953.18 16.14 o -1 2 1 1110.46 1056.57 5.18 o 0 2 1 408.24 433.00 2.80 o 1 2 1 616.73 562.73 3.00 o 2 2 1 1036.78 1008.21 4.88 o 3 2 1 66.58 80.28 1.53 o 4 2 1 5.79 8.37 1.91 o 5 2 1 302.00 301.68 5.39 o 6 2 1 24.59 27.89 2.04 o 7 2 1 171.28 170.82 5.18 o -6 3 1 14.65 13.66 1.83 o -5 3 1 685.15 669.27 8.95 o -4 3 1 1250.81 1204.74 35.05 o -3 3 1 164.37 159.91 2.52 o -2 3 1 2502.97 2270.83 9.56 o -1 3 1 25.22 14.35 1.28 o 0 3 1 2307.16 2104.13 18.02 o 1 3 1 1047.65 936.84 4.74 o 2 3 1 712.03 652.81 4.11 o 3 3 1 0.21 1.36 0.48 o 4 3 1 2349.79 2094.81 10.14 o 5 3 1 564.37 526.39 7.17 o 6 3 1 470.11 469.94 7.53 o 7 3 1 298.21 292.83 6.70 o -6 4 1 5.67 3.98 1.52 o -5 4 1 296.43 296.23 6.17 o -4 4 1 5.88 6.78 0.99 o -3 4 1 720.05 685.37 6.67 o -2 4 1 417.82 408.47 9.39 o -1 4 1 10.12 12.75 0.74 o 0 4 1 59.09 58.50 1.39 o 1 4 1 422.81 378.78 3.82 o 2 4 1 760.42 727.03 10.67 o 3 4 1 321.89 303.04 3.51 o 4 4 1 553.80 512.90 6.15 o 5 4 1 179.34 177.93 3.09 o 6 4 1 244.57 232.98 5.49 o 7 4 1 16.02 12.40 1.78 o -5 5 1 0.43 -0.99 0.99 o -4 5 1 98.82 93.66 2.50 o -3 5 1 0.18 2.97 1.67 o -2 5 1 296.36 282.17 3.57 o -1 5 1 1.86 2.46 0.59 o 0 5 1 496.28 493.72 5.05 o 1 5 1 119.34 120.06 2.07 o 2 5 1 31.39 27.92 1.15 o 3 5 1 15.18 15.78 1.00 o 4 5 1 209.03 201.96 3.12 o 5 5 1 7.97 6.29 1.15 o 6 5 1 189.81 187.10 5.08 o 7 5 1 5.05 4.66 1.41 o -5 6 1 6.81 4.13 1.41 o -4 6 1 0.72 -0.81 0.81 o -3 6 1 98.01 90.03 2.44 o -2 6 1 18.33 21.04 1.18 o -1 6 1 65.95 63.65 3.66 o 0 6 1 7.36 7.13 0.81 o 1 6 1 110.96 104.19 3.37 o 2 6 1 27.72 24.35 1.49 o 3 6 1 1.65 3.56 0.74 o 4 6 1 8.78 9.33 1.39 o 5 6 1 69.87 70.14 2.59 o 6 6 1 1.83 0.26 1.15 o -4 7 1 43.67 46.67 3.53 o -3 7 1 263.58 254.12 4.25 o -2 7 1 136.92 137.73 6.17 o -1 7 1 195.96 196.48 4.16 o 0 7 1 763.66 753.38 8.71 o 1 7 1 0.07 1.57 0.68 o 2 7 1 262.82 255.86 6.78 o 3 7 1 86.66 83.76 2.28 o 4 7 1 12.43 12.37 1.12 o 5 7 1 195.56 190.79 3.79 o 6 7 1 321.81 328.88 7.32 o -3 8 1 86.66 92.42 2.85 o -2 8 1 3.36 2.87 0.94 o -1 8 1 227.78 251.09 8.29 o 0 8 1 47.41 46.73 1.89 o 1 8 1 68.50 77.83 2.56 o 2 8 1 138.36 150.35 3.18 o 3 8 1 222.67 219.12 3.90 o 4 8 1 1.70 2.05 0.83 o 5 8 1 401.58 412.85 5.81 o -1 9 1 3.81 7.79 1.11 o 0 9 1 10.76 11.86 2.15 o 1 9 1 0.22 0.93 0.75 o 2 9 1 2.15 1.74 0.86 o 3 9 1 7.00 7.66 2.62 o 4 9 1 34.38 35.23 1.94 o -3 -8 2 7.74 6.98 1.14 o -2 -8 2 9.74 9.20 1.20 o -1 -8 2 17.58 19.12 1.41 o 0 -8 2 17.01 19.80 1.50 o 1 -8 2 0.06 0.31 0.84 o 2 -8 2 4.28 3.12 0.98 o -5 -7 2 132.69 127.97 6.83 o -4 -7 2 285.15 285.80 4.72 o -3 -7 2 33.23 30.31 1.91 o -2 -7 2 548.10 559.80 15.91 o -1 -7 2 16.89 16.11 1.46 o 0 -7 2 141.22 139.05 3.07 o 1 -7 2 101.47 110.61 3.90 o 2 -7 2 29.00 32.49 1.70 o 3 -7 2 91.26 95.26 3.48 o -5 -6 2 152.27 153.54 3.47 o -4 -6 2 0.03 -0.21 0.63 o -3 -6 2 333.35 333.83 7.38 o -2 -6 2 24.26 19.62 2.20 o -1 -6 2 118.79 122.47 4.63 o 0 -6 2 81.10 80.08 2.18 o 1 -6 2 195.45 192.57 8.71 o 2 -6 2 0.35 1.21 0.71 o 3 -6 2 293.15 294.15 4.51 o 4 -6 2 10.24 9.48 1.96 o -6 -5 2 0.10 0.31 1.20 o -5 -5 2 56.98 51.55 2.07 o -4 -5 2 296.70 302.06 4.25 o -3 -5 2 0.26 -0.01 1.05 o -2 -5 2 259.74 269.17 5.99 o -1 -5 2 2.61 2.62 0.99 o 0 -5 2 4.27 4.74 0.70 o 1 -5 2 47.29 43.24 1.53 o 2 -5 2 434.51 425.92 11.85 o 3 -5 2 11.64 14.85 2.93 o 4 -5 2 517.45 490.41 13.92 o 5 -5 2 36.76 39.61 2.67 o -6 -4 2 4.72 8.32 1.57 o -5 -4 2 167.92 176.23 5.81 o -4 -4 2 33.37 33.94 1.48 o -3 -4 2 330.50 322.76 3.83 o -2 -4 2 90.13 89.49 4.37 o -1 -4 2 0.01 1.10 0.48 o 0 -4 2 2.58 1.94 0.55 o 1 -4 2 686.20 666.50 7.46 o 2 -4 2 277.14 271.61 3.42 o 3 -4 2 295.72 289.40 3.79 o 4 -4 2 77.87 74.19 2.15 o 5 -4 2 60.55 53.37 2.93 o 6 -4 2 30.57 29.19 2.51 o -7 -3 2 74.03 80.36 3.82 o -6 -3 2 84.64 83.92 3.61 o -5 -3 2 4.01 0.89 1.10 o -4 -3 2 11.48 10.45 0.92 o -3 -3 2 704.02 706.03 5.47 o -2 -3 2 202.06 204.53 2.59 o -1 -3 2 2912.93 2877.98 31.86 o 0 -3 2 1840.35 1847.69 8.19 o 1 -3 2 431.31 427.64 3.63 o 2 -3 2 250.71 250.80 5.34 o 3 -3 2 49.68 48.63 1.53 o 4 -3 2 6.55 5.87 0.81 o 5 -3 2 180.59 178.15 4.76 o 6 -3 2 108.47 106.78 4.19 o -7 -2 2 134.99 139.75 4.81 o -6 -2 2 133.56 137.91 4.34 o -5 -2 2 1.76 2.46 1.05 o -4 -2 2 1160.77 1189.52 7.81 o -3 -2 2 2440.80 2503.40 26.11 o -2 -2 2 683.68 745.89 5.36 o -1 -2 2 3968.79 3765.62 12.71 o 0 -2 2 242.69 286.30 2.50 o 1 -2 2 457.30 484.43 3.49 o 2 -2 2 117.48 106.39 1.78 o 3 -2 2 241.32 228.81 6.33 o 4 -2 2 146.69 145.32 2.57 o 5 -2 2 739.92 692.19 8.89 o 6 -2 2 73.37 64.82 3.14 o 7 -2 2 83.70 81.46 3.82 o -7 -1 2 10.29 8.42 1.67 o -6 -1 2 3.30 2.62 1.15 o -5 -1 2 17.27 17.37 1.62 o -4 -1 2 132.40 154.53 2.76 o -3 -1 2 183.63 196.97 2.53 o -2 -1 2 1033.89 1146.88 5.79 o -1 -1 2 1577.80 1692.78 6.59 o 0 -1 2 1368.65 1451.68 5.62 o 1 -1 2 184.29 207.86 4.73 o 2 -1 2 69.03 75.47 2.72 o 3 -1 2 8.03 6.22 1.20 o 4 -1 2 64.83 68.83 1.76 o 5 -1 2 32.57 33.75 2.04 o 6 -1 2 135.35 125.20 4.03 o 7 -1 2 0.69 -1.05 1.05 o -7 0 2 68.17 72.31 3.56 o -6 0 2 1.98 1.26 1.15 o -5 0 2 57.38 62.26 2.72 o -4 0 2 128.55 145.16 2.48 o -3 0 2 2523.14 2678.47 10.88 o -2 0 2 0.81 2.82 0.55 o -1 0 2 2835.77 2796.32 8.90 o 0 0 2 7.65 9.46 0.63 o 1 0 2 409.40 473.43 2.72 o 2 0 2 1005.65 1117.98 5.27 o 3 0 2 546.60 618.09 4.44 o 4 0 2 168.24 173.51 4.97 o 5 0 2 759.91 713.38 8.42 o 6 0 2 47.38 43.95 2.56 o 7 0 2 93.45 86.07 3.77 o -7 1 2 83.99 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449.10 5.11 o 4 2 8 4.10 4.11 1.44 o 5 2 8 116.00 124.63 4.34 o 6 2 8 3.96 7.48 1.73 o -4 3 8 9.32 6.15 1.11 o -3 3 8 128.69 133.50 3.18 o -2 3 8 11.05 10.02 1.81 o -1 3 8 56.01 56.30 1.89 o 0 3 8 3.64 1.94 0.74 o 1 3 8 0.04 0.78 0.59 o 2 3 8 0.59 2.12 0.67 o 3 3 8 150.83 150.31 3.11 o 4 3 8 129.12 142.25 3.05 o 5 3 8 84.67 82.82 3.66 o 6 3 8 31.35 27.10 2.46 o -3 4 8 0.23 0.22 0.75 o -2 4 8 23.01 22.64 1.44 o -1 4 8 1.09 -0.10 0.67 o 0 4 8 20.11 18.35 1.22 o 1 4 8 142.42 142.43 3.27 o 2 4 8 4.08 2.77 0.74 o 3 4 8 184.40 195.12 3.42 o 4 4 8 27.60 27.38 1.83 o 5 4 8 59.88 59.16 2.88 o 6 4 8 18.61 16.85 1.99 o -3 5 8 60.63 61.11 2.37 o -2 5 8 118.90 118.86 3.92 o -1 5 8 448.93 460.47 7.93 o 0 5 8 11.72 10.79 1.91 o 1 5 8 173.74 171.27 3.18 o 2 5 8 120.75 125.19 2.77 o 3 5 8 100.56 100.17 2.53 o 4 5 8 10.08 10.26 1.07 o 5 5 8 432.98 448.13 16.66 o 6 5 8 2.00 1.26 1.26 o -2 6 8 390.99 391.72 5.49 o -1 6 8 205.30 203.60 3.79 o 0 6 8 34.39 35.77 1.66 o 1 6 8 145.84 146.77 3.07 o 2 6 8 124.52 132.08 4.24 o 3 6 8 0.54 1.35 0.75 o 4 6 8 588.08 601.65 6.53 o 5 6 8 268.15 273.06 5.08 o -2 7 8 1.73 0.50 1.75 o -1 7 8 104.39 95.71 8.32 o 0 7 8 5.46 4.68 0.92 o 1 7 8 7.26 6.99 2.80 o 2 7 8 35.28 34.96 1.72 o 3 7 8 2.27 3.23 1.28 o 4 7 8 67.90 68.77 2.40 o 5 7 8 24.18 25.89 1.66 o -1 8 8 1.99 0.13 1.70 o 0 8 8 59.69 61.54 2.37 o 1 8 8 2.26 2.92 0.89 o 2 8 8 13.51 15.55 1.60 o 3 8 8 10.15 8.55 1.16 o 4 8 8 40.48 40.31 2.02 o -1 -3 9 136.99 129.87 3.40 o 0 -3 9 10.41 10.38 1.52 o 1 -3 9 2.55 3.06 0.98 o -2 -2 9 257.66 244.72 4.57 o -1 -2 9 19.37 20.77 1.48 o 0 -2 9 24.66 26.25 1.66 o 1 -2 9 6.72 7.24 1.04 o 2 -2 9 63.21 56.62 2.29 o 3 -2 9 1.62 0.39 0.89 o -3 -1 9 0.08 1.31 0.86 o -2 -1 9 37.47 34.25 3.45 o -1 -1 9 8.27 8.51 1.11 o 0 -1 9 163.43 149.14 4.34 o 1 -1 9 0.07 -0.89 0.89 o 2 -1 9 136.15 133.16 5.70 o 3 -1 9 4.85 5.08 1.04 o 4 -1 9 6.56 7.42 1.23 o -3 0 9 168.84 161.33 3.73 o -2 0 9 176.57 167.98 6.91 o -1 0 9 270.46 267.72 4.45 o 0 0 9 408.12 401.97 5.40 o 1 0 9 29.72 29.96 2.98 o 2 0 9 83.08 88.63 2.51 o 3 0 9 131.99 139.01 3.20 o 4 0 9 111.83 105.09 2.94 o -3 1 9 157.35 152.23 6.88 o -2 1 9 70.95 73.74 2.46 o -1 1 9 473.48 445.61 7.77 o 0 1 9 5.11 3.20 0.84 o 1 1 9 52.71 52.11 2.04 o 2 1 9 0.07 0.86 0.70 o 3 1 9 43.27 42.26 2.64 o 4 1 9 8.52 8.51 1.26 o 5 1 9 109.53 115.57 4.55 o -3 2 9 57.89 58.16 2.51 o -2 2 9 242.56 245.82 8.61 o -1 2 9 220.03 219.67 3.87 o 0 2 9 526.74 498.72 5.66 o 1 2 9 39.20 35.76 2.38 o 2 2 9 118.20 115.92 2.77 o 3 2 9 37.36 37.27 2.33 o 4 2 9 33.21 32.25 4.45 o 5 2 9 21.74 18.00 2.15 o -3 3 9 126.30 120.71 7.38 o -2 3 9 0.09 -2.40 2.98 o -1 3 9 156.26 150.42 3.30 o 0 3 9 11.96 16.09 1.18 o 1 3 9 0.01 1.91 0.70 o 2 3 9 102.19 102.21 3.82 o 3 3 9 16.68 16.88 1.29 o 4 3 9 32.76 32.17 1.63 o 5 3 9 20.70 19.99 2.09 o -3 4 9 18.16 15.58 3.77 o -2 4 9 47.22 44.26 1.94 o -1 4 9 365.14 358.63 4.99 o 0 4 9 43.20 42.05 1.86 o 1 4 9 536.23 517.56 7.12 o 2 4 9 161.29 165.38 4.37 o 3 4 9 96.52 96.67 2.66 o 4 4 9 181.91 181.90 7.12 o 5 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2.51 o 2 1 10 271.48 279.04 8.63 o 3 1 10 127.44 125.90 3.27 o 4 1 10 40.54 41.26 2.03 o -2 2 10 41.30 40.70 2.02 o -1 2 10 11.84 9.12 1.15 o 0 2 10 64.93 64.17 4.92 o 1 2 10 17.33 20.44 2.43 o 2 2 10 15.46 17.51 1.37 o 3 2 10 30.58 27.70 2.38 o 4 2 10 9.33 9.47 1.20 o -2 3 10 188.92 176.81 8.19 o -1 3 10 23.98 22.48 1.52 o 0 3 10 7.17 6.82 1.28 o 1 3 10 113.95 109.03 3.22 o 2 3 10 173.25 170.09 3.50 o 3 3 10 126.69 129.28 4.29 o 4 3 10 527.54 491.72 6.31 o -2 4 10 0.34 1.46 0.92 o -1 4 10 26.84 24.84 2.56 o 0 4 10 28.94 27.27 1.66 o 1 4 10 144.18 147.24 3.38 o 2 4 10 0.01 0.16 0.74 o 3 4 10 332.42 329.16 6.93 o 4 4 10 9.69 10.79 2.28 o -1 5 10 0.08 0.13 1.81 o 0 5 10 0.02 1.54 0.85 o 1 5 10 2.27 2.96 0.81 o 2 5 10 169.10 169.36 5.55 o 3 5 10 2.23 0.93 0.77 o 4 5 10 371.98 370.21 5.53 o 0 6 10 3.75 3.02 0.94 o 1 6 10 137.47 126.59 3.33 o 2 6 10 99.73 96.33 2.81 o 3 6 10 115.34 110.17 4.71 o 4 6 10 43.86 46.33 2.38 o 1 7 10 17.67 16.64 1.48 o 2 7 10 32.35 36.06 1.92 o 3 7 10 45.30 47.37 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