#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2214127.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214127_Fobs loop_ _publ_author_name 'Saaidi, Pierre-Lo\"ic' 'Jeanneau, Erwann' 'Hasserodt, Jens' _publ_section_title ; Tris(1,1,1,3,3,3-hexafluoroisopropyl) phosphate ; _journal_coeditor_code CS2040 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3241 _journal_page_last o3242 _journal_volume 63 _journal_year 2007 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _audit_creation_date 07-04-20 _audit_creation_method CRYSTALS _cell_angle_alpha 90 _cell_angle_beta 107.044(5) _cell_angle_gamma 90 _cell_length_a 18.904(5) _cell_length_b 9.910(5) _cell_length_c 19.176(5) _[local]_cod_data_source_file cs2040Isup2.hkl _[local]_cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma _refln_observed_status 4 0 0 7211.50 7390.14 132.50 o 6 0 0 5783.50 6334.38 75.00 o 8 0 0 3492.80 3275.26 50.40 o 10 0 0 1100.70 1040.79 16.20 o 12 0 0 2094.80 2175.93 27.40 o 14 0 0 19.20 11.65 1.00 o 16 0 0 913.00 912.39 15.50 o 18 0 0 19.20 19.35 1.40 o 20 0 0 115.70 129.45 4.60 o 22 0 0 16.50 15.05 2.30 o 1 1 0 -0.25 0.00 0.10 < 3 1 0 526.65 0.00 7.76 x 5 1 0 7040.15 7804.47 145.41 o 7 1 0 13978.10 13224.74 317.91 o 9 1 0 818.45 841.77 12.32 o 11 1 0 401.95 408.23 6.77 o 13 1 0 18.35 16.80 1.06 o 15 1 0 150.00 151.22 3.58 o 17 1 0 433.15 432.21 9.65 o 19 1 0 0.20 0.04 1.82 < 21 1 0 28.95 26.78 2.50 o 23 1 0 66.15 65.46 3.90 o 0 2 0 19361.60 19716.62 619.60 o 2 2 0 699.80 763.72 11.10 o 4 2 0 11.65 8.00 0.60 o 6 2 0 694.90 717.03 10.36 o 8 2 0 413.00 418.15 6.58 o 10 2 0 220.70 232.09 4.12 o 12 2 0 1505.25 1418.02 23.12 o 14 2 0 85.45 96.15 2.36 o 16 2 0 6.55 12.13 1.06 o 18 2 0 27.70 34.63 1.86 o 20 2 0 7.15 7.81 1.80 o 22 2 0 0.10 0.01 2.60 < 1 3 0 3917.75 4071.31 71.90 o 3 3 0 528.05 529.25 9.31 o 5 3 0 61.95 72.22 1.73 o 7 3 0 1255.55 1305.04 18.91 o 9 3 0 194.05 253.80 3.72 o 11 3 0 322.85 282.50 6.02 o 13 3 0 175.75 166.72 3.88 o 15 3 0 73.40 83.01 2.41 o 17 3 0 8.65 10.34 1.25 o 19 3 0 23.40 33.93 2.77 o 21 3 0 118.45 111.81 5.60 o 23 3 0 45.70 54.33 3.26 o 0 4 0 154.85 155.29 4.88 o 2 4 0 5553.35 5605.52 95.18 o 4 4 0 657.70 648.67 12.72 o 6 4 0 3.80 4.06 0.61 o 8 4 0 2454.80 2292.22 36.16 o 10 4 0 2389.55 2305.85 36.01 o 12 4 0 618.80 611.35 11.21 o 14 4 0 1526.30 1486.35 27.60 o 16 4 0 51.55 66.90 1.96 o 18 4 0 0.75 1.77 2.08 < 20 4 0 5.80 5.17 3.45 < 22 4 0 0.85 0.00 1.79 < 1 5 0 661.55 655.97 13.10 o 3 5 0 1014.15 1150.10 19.45 o 5 5 0 1079.35 1125.39 20.06 o 7 5 0 214.85 205.48 4.46 o 9 5 0 293.75 278.23 5.87 o 11 5 0 31.85 35.94 1.35 o 13 5 0 65.60 80.43 2.35 o 15 5 0 10.65 13.20 1.15 o 17 5 0 98.60 97.46 5.42 o 19 5 0 19.65 17.33 3.30 o 21 5 0 26.80 21.75 4.15 o 0 6 0 1975.15 2073.18 48.63 o 2 6 0 1964.00 1823.50 35.25 o 4 6 0 242.45 201.55 5.96 o 6 6 0 810.95 836.59 15.39 o 8 6 0 263.25 231.11 6.17 o 10 6 0 16.55 21.65 1.46 o 12 6 0 51.60 60.51 2.33 o 14 6 0 109.25 129.80 3.50 o 16 6 0 71.50 61.45 5.20 o 18 6 0 10.65 10.00 3.95 < 20 6 0 6.15 1.76 3.85 < 1 7 0 85.40 78.34 2.89 o 3 7 0 632.20 602.02 12.49 o 5 7 0 95.85 94.67 3.28 o 7 7 0 3.40 4.51 1.17 < 9 7 0 384.85 390.10 9.08 o 11 7 0 1113.05 1043.22 21.75 o 13 7 0 4.50 1.59 2.03 < 15 7 0 110.05 107.96 7.00 o 17 7 0 15.10 15.58 3.81 o 19 7 0 30.80 28.35 4.40 o 0 8 0 119.60 89.81 4.91 o 2 8 0 777.45 755.74 15.50 o 4 8 0 1286.75 1167.18 24.14 o 6 8 0 333.40 348.11 8.61 o 8 8 0 92.50 94.40 3.53 o 10 8 0 722.00 693.31 17.18 o 12 8 0 88.35 88.75 4.95 o 14 8 0 217.55 216.74 11.25 o 16 8 0 148.05 123.07 10.05 o 18 8 0 19.55 16.49 4.53 o 1 9 0 136.15 139.69 4.32 o 3 9 0 422.05 406.39 9.87 o 5 9 0 63.60 70.77 2.89 o 7 9 0 7.60 9.43 1.43 o 9 9 0 47.30 51.32 3.59 o 11 9 0 18.60 23.17 3.67 o 13 9 0 34.80 33.90 4.46 o 15 9 0 3.80 2.25 2.96 < 17 9 0 59.55 64.14 6.15 o 0 10 0 263.90 253.57 10.58 o 2 10 0 3.15 1.40 1.49 < 4 10 0 2.55 2.79 1.76 < 6 10 0 1.80 0.70 1.71 < 8 10 0 9.85 10.43 2.15 o 10 10 0 20.40 22.93 3.75 o 12 10 0 50.90 46.31 5.23 o 14 10 0 18.60 18.28 4.16 o 1 11 0 2.85 0.64 1.90 < 3 11 0 2.45 0.16 2.08 < 5 11 0 12.60 14.30 2.35 o 7 11 0 52.00 56.79 5.41 o 9 11 0 50.35 52.87 5.02 o 11 11 0 2.90 0.61 2.60 < 0 12 0 173.10 175.03 11.30 o 2 12 0 82.95 83.16 5.46 o 4 12 0 28.10 23.78 3.10 o 6 12 0 4.20 5.87 3.67 < 8 12 0 4.80 2.97 3.70 < 1 13 0 15.50 17.73 3.30 o -23 1 1 11.70 9.87 2.20 o -21 1 1 476.80 427.08 14.20 o -19 1 1 13.80 17.88 1.66 o -17 1 1 642.45 629.32 12.53 o -15 1 1 189.35 192.86 4.25 o -13 1 1 2044.55 1988.58 30.37 o -11 1 1 128.60 187.27 3.00 o -9 1 1 710.70 766.79 11.13 o -7 1 1 3849.00 4019.75 54.80 o -5 1 1 2503.05 2625.27 36.71 o -3 1 1 161.95 0.00 2.82 x -1 1 1 4.40 0.00 1.63 < 1 1 1 27.80 0.00 1.20 x 3 1 1 4226.35 4646.50 53.05 o 5 1 1 5652.65 6070.17 82.07 o 7 1 1 4538.65 4454.47 59.65 o 9 1 1 3161.65 3071.01 43.71 o 11 1 1 44.30 48.93 1.46 o 13 1 1 5.50 4.64 0.92 o 15 1 1 658.30 678.08 12.22 o 17 1 1 134.25 137.95 3.90 o 19 1 1 142.60 144.07 5.45 o 21 1 1 47.60 49.84 3.15 o 23 1 1 4.30 10.84 2.40 < -22 2 1 10.30 10.53 1.80 o -20 2 1 13.35 20.44 1.88 o -18 2 1 184.85 186.06 5.10 o -16 2 1 4.70 3.85 1.02 o -14 2 1 718.80 677.56 12.25 o -12 2 1 932.90 880.78 14.66 o -10 2 1 240.70 258.23 4.38 o -8 2 1 2068.25 2024.84 28.53 o -6 2 1 2794.30 2839.71 37.05 o -4 2 1 23091.05 23021.84 520.35 o -2 2 1 1489.85 1665.46 30.58 o 0 2 1 398.65 470.31 6.85 o 2 2 1 1007.70 1063.51 15.60 o 4 2 1 686.20 721.87 10.00 o 6 2 1 66.70 83.28 1.56 o 8 2 1 6.10 9.65 0.65 o 10 2 1 1310.80 1200.80 19.47 o 12 2 1 921.60 892.71 15.03 o 14 2 1 55.80 61.17 1.92 o 16 2 1 18.70 26.83 1.40 o 18 2 1 116.75 118.46 5.25 o 20 2 1 79.30 77.03 4.70 o 22 2 1 133.00 128.46 6.15 o -23 3 1 49.10 49.21 3.31 o -21 3 1 7.50 10.80 1.98 o -19 3 1 124.65 118.06 4.85 o -17 3 1 86.55 79.61 2.65 o -15 3 1 268.95 273.05 5.71 o -13 3 1 59.05 63.96 1.77 o -11 3 1 5087.75 4768.04 69.99 o -9 3 1 644.90 623.82 9.50 o -7 3 1 1931.35 1890.15 26.50 o -5 3 1 766.25 761.12 12.21 o -3 3 1 618.70 661.26 11.75 o -1 3 1 7919.80 8310.64 150.94 o 1 3 1 7250.65 7594.03 116.23 o 3 3 1 683.35 700.37 11.45 o 5 3 1 1724.30 1742.83 25.23 o 7 3 1 168.75 144.10 3.70 o 9 3 1 2997.45 2956.07 42.35 o 11 3 1 618.60 649.44 10.31 o 13 3 1 115.65 118.33 2.97 o 15 3 1 115.15 106.72 3.30 o 17 3 1 52.55 50.60 2.66 o 19 3 1 323.65 292.21 12.30 o 21 3 1 21.65 23.60 2.41 o -22 4 1 14.80 14.51 2.53 o -20 4 1 26.20 30.60 2.21 o -18 4 1 146.25 159.99 5.07 o -16 4 1 2.85 1.36 1.06 < -14 4 1 3.70 0.05 0.85 o -12 4 1 101.45 106.70 2.65 o -10 4 1 447.20 430.77 8.02 o -8 4 1 1747.00 1639.95 26.09 o -6 4 1 485.10 490.25 8.97 o -4 4 1 383.60 401.77 8.05 o -2 4 1 8547.25 8678.91 163.71 o 0 4 1 8103.40 8134.89 155.42 o 2 4 1 2242.95 2294.24 37.99 o 4 4 1 99.30 97.62 2.45 o 6 4 1 1708.80 1746.08 25.61 o 8 4 1 376.75 355.40 6.91 o 10 4 1 26.30 38.87 1.25 o 12 4 1 54.35 60.34 1.90 o 14 4 1 166.65 164.60 4.45 o 16 4 1 52.70 59.39 2.07 o 18 4 1 0.60 0.21 2.62 < 20 4 1 37.30 33.44 4.00 o 22 4 1 23.60 28.55 3.76 o -21 5 1 103.90 112.79 7.95 o -19 5 1 143.10 137.44 8.20 o -17 5 1 22.45 18.63 3.20 o -15 5 1 1.20 0.24 0.93 < -13 5 1 149.45 164.65 4.05 o -11 5 1 313.25 316.77 5.95 o -9 5 1 431.95 438.15 9.30 o -7 5 1 153.80 168.03 3.75 o -5 5 1 7.05 5.44 0.92 o -3 5 1 945.70 936.63 17.47 o -1 5 1 23.40 23.83 1.20 o 1 5 1 462.70 434.69 9.81 o 3 5 1 5264.25 5068.74 85.83 o 5 5 1 7.55 2.83 0.91 o 7 5 1 1064.15 1088.71 17.12 o 9 5 1 1294.20 1282.61 21.55 o 11 5 1 1325.35 1242.93 22.43 o 13 5 1 9.35 13.13 1.15 o 15 5 1 49.20 47.65 2.22 o 17 5 1 244.05 224.34 12.21 o 19 5 1 49.95 43.39 24.04 < 21 5 1 1.65 0.90 4.68 < -20 6 1 4.00 4.85 3.62 < -18 6 1 74.05 79.13 5.46 o -16 6 1 652.80 647.07 22.01 o -14 6 1 560.30 568.28 11.96 o -12 6 1 183.45 187.91 4.80 o -10 6 1 131.85 146.09 4.90 o -8 6 1 38.90 45.27 1.71 o -6 6 1 706.60 697.18 13.77 o -4 6 1 256.95 252.71 5.59 o -2 6 1 618.10 575.30 11.64 o 0 6 1 363.35 358.75 7.55 o 2 6 1 267.20 260.30 6.41 o 4 6 1 1423.65 1402.33 26.38 o 6 6 1 95.95 97.32 2.79 o 8 6 1 44.15 40.60 1.71 o 10 6 1 2843.25 2734.01 47.51 o 12 6 1 431.30 405.98 9.50 o 14 6 1 2.55 3.99 1.15 < 16 6 1 10.00 8.54 3.30 o 18 6 1 10.65 13.37 3.21 o 20 6 1 117.15 115.19 8.60 o -19 7 1 20.40 20.78 3.80 o -17 7 1 40.55 46.00 4.65 o -15 7 1 21.20 21.74 3.67 o -13 7 1 582.45 586.95 16.10 o -11 7 1 48.35 44.44 2.24 o -9 7 1 3522.70 3248.64 64.06 o -7 7 1 242.45 244.72 5.91 o -5 7 1 45.15 47.72 2.03 o -3 7 1 1098.00 1031.33 20.02 o -1 7 1 1789.70 1723.00 31.19 o 1 7 1 37.65 49.29 1.75 o 3 7 1 1295.65 1171.70 24.86 o 5 7 1 39.40 45.58 2.07 o 7 7 1 23.75 38.17 2.18 o 9 7 1 1102.60 1031.92 23.45 o 11 7 1 89.80 96.80 3.38 o 13 7 1 166.60 197.50 7.33 o 15 7 1 190.20 199.07 9.81 o 17 7 1 233.30 226.75 13.70 o 19 7 1 10.80 7.96 3.60 o -18 8 1 66.95 64.79 6.60 o -16 8 1 5.40 1.93 3.06 < -14 8 1 0.45 0.02 3.30 < -12 8 1 4.70 3.73 2.01 < -10 8 1 624.55 600.79 14.67 o -8 8 1 509.55 479.58 11.47 o -6 8 1 18.85 22.97 1.86 o -4 8 1 571.50 596.33 12.17 o -2 8 1 36.55 40.17 1.92 o 0 8 1 164.20 169.59 4.41 o 2 8 1 3.80 1.62 1.06 o 4 8 1 516.15 518.95 12.10 o 6 8 1 506.10 483.27 12.47 o 8 8 1 73.30 78.55 4.24 o 10 8 1 23.25 25.43 1.94 o 12 8 1 53.35 47.97 3.62 o 14 8 1 0.65 0.78 2.47 < 16 8 1 10.55 12.19 3.20 o 18 8 1 -1.10 0.75 4.33 < -17 9 1 10.35 5.67 3.75 < -15 9 1 10.45 6.77 4.07 < -13 9 1 163.05 161.60 9.01 o -11 9 1 57.45 51.71 4.61 o -9 9 1 1.40 0.07 2.22 < -7 9 1 81.20 79.96 3.04 o -5 9 1 13.25 15.35 1.39 o -3 9 1 21.60 17.33 1.59 o -1 9 1 35.75 34.51 2.04 o 1 9 1 24.65 27.02 1.71 o 3 9 1 193.80 201.88 5.55 o 5 9 1 101.85 115.74 3.75 o 7 9 1 10.05 10.92 1.53 o 9 9 1 43.05 45.16 3.27 o 11 9 1 12.55 13.51 3.25 o 13 9 1 12.35 11.91 3.10 o 15 9 1 6.10 0.02 3.65 < -14 10 1 -0.95 0.58 2.88 < -12 10 1 15.45 15.99 4.30 o -10 10 1 75.55 85.43 5.61 o -8 10 1 206.05 188.98 9.34 o -6 10 1 -0.25 2.48 1.70 < -4 10 1 64.55 78.17 3.06 o -2 10 1 53.55 45.84 2.75 o 0 10 1 139.70 129.96 4.79 o 2 10 1 75.60 80.27 3.46 o 4 10 1 28.20 29.20 2.29 o 6 10 1 13.15 15.20 1.84 o 8 10 1 76.55 80.76 5.02 o 10 10 1 201.80 169.07 22.05 o 12 10 1 2.50 2.81 2.30 < 14 10 1 2.70 0.67 4.10 < -11 11 1 7.80 4.02 4.00 < -9 11 1 18.40 19.95 4.41 o -7 11 1 48.40 49.68 5.05 o -5 11 1 49.25 59.17 3.81 o -3 11 1 151.45 144.90 7.19 o -1 11 1 3.85 5.64 1.77 < 1 11 1 5.35 5.00 2.04 < 3 11 1 536.95 500.50 16.25 o 5 11 1 143.10 123.93 7.20 o 7 11 1 7.15 6.87 3.25 < 9 11 1 6.90 6.33 3.07 < 11 11 1 -1.05 0.24 2.82 < -8 12 1 3.80 0.64 5.85 < -6 12 1 16.45 15.60 4.02 o -4 12 1 49.50 41.40 4.20 o -2 12 1 15.35 12.60 2.79 o 0 12 1 1.90 0.42 2.40 < 2 12 1 18.20 25.86 3.40 o 4 12 1 73.80 82.63 6.11 o 6 12 1 13.00 5.97 3.60 o 8 12 1 22.80 19.15 4.10 o -1 13 1 6.30 5.36 4.70 < 1 13 1 6.40 19.98 4.30 < -24 0 2 44.40 45.98 3.10 o -22 0 2 136.90 134.36 5.90 o -20 0 2 64.20 58.56 3.20 o -18 0 2 1473.40 1376.84 27.20 o -16 0 2 22.00 20.09 1.30 o -14 0 2 58.60 59.65 1.70 o -12 0 2 732.40 678.43 11.80 o -10 0 2 454.30 487.06 7.00 o -8 0 2 67.10 71.47 1.40 o -6 0 2 1378.10 1515.05 18.50 o -4 0 2 200.70 202.73 3.20 o -2 0 2 155.80 0.00 5.70 x 0 0 2 0.60 0.00 0.46 < 2 0 2 4961.90 0.00 64.70 x 4 0 2 175.40 182.62 3.00 o 6 0 2 871.30 930.48 12.50 o 8 0 2 4547.80 4420.87 60.50 o 10 0 2 87.20 120.39 2.10 o 12 0 2 2236.10 2093.39 32.90 o 14 0 2 517.00 565.81 9.60 o 16 0 2 149.10 141.89 4.20 o 18 0 2 683.30 556.43 18.40 o 20 0 2 71.40 72.02 3.90 o 22 0 2 243.40 212.05 9.60 o -23 1 2 78.50 83.50 4.96 o -21 1 2 8.05 9.52 1.66 o -19 1 2 118.90 119.32 4.45 o -17 1 2 152.00 158.06 3.86 o -15 1 2 20.30 24.27 1.10 o -13 1 2 1533.75 1530.25 22.50 o -11 1 2 828.85 781.90 12.30 o -9 1 2 340.90 323.77 5.43 o -7 1 2 269.70 267.92 4.72 o -5 1 2 3351.55 3580.83 48.91 o -3 1 2 1778.65 0.00 42.79 x -1 1 2 326.80 0.00 6.50 x 1 1 2 5749.60 0.00 139.43 x 3 1 2 1473.30 1578.62 20.25 o 5 1 2 469.05 548.91 7.30 o 7 1 2 7283.70 7260.56 104.25 o 9 1 2 1932.90 1876.98 27.20 o 11 1 2 218.85 208.95 4.25 o 13 1 2 2294.05 2219.49 35.33 o 15 1 2 4.80 1.96 1.05 o 17 1 2 36.00 47.55 2.36 o 19 1 2 9.15 8.85 2.01 o 21 1 2 28.50 36.16 2.90 o 23 1 2 42.00 42.36 3.31 o -22 2 2 9.00 6.84 2.08 o -20 2 2 12.40 11.22 1.66 o -18 2 2 101.85 104.07 2.96 o -16 2 2 -0.30 0.03 1.05 < -14 2 2 59.85 66.53 1.77 o -12 2 2 111.15 122.32 2.46 o -10 2 2 516.00 490.83 9.55 o -8 2 2 3227.60 3184.97 47.47 o -6 2 2 6878.35 6909.65 117.61 o -4 2 2 7.25 1.66 0.35 o -2 2 2 713.20 749.48 14.10 o 0 2 2 90.55 87.42 1.90 o 2 2 2 259.20 282.13 4.94 o 4 2 2 2345.05 2477.39 33.54 o 6 2 2 11042.40 11023.24 192.47 o 8 2 2 3310.40 3165.21 45.71 o 10 2 2 1813.00 1680.93 26.65 o 12 2 2 1350.25 1289.45 21.51 o 14 2 2 110.80 132.72 3.11 o 16 2 2 80.80 88.94 2.65 o 18 2 2 19.15 20.29 2.80 o 20 2 2 32.85 35.03 3.41 o 22 2 2 8.90 8.58 2.45 o -23 3 2 21.75 22.31 4.26 o -21 3 2 9.00 10.17 2.56 o -19 3 2 31.90 31.54 2.02 o -17 3 2 1129.85 1093.26 20.09 o -15 3 2 68.95 88.67 2.10 o -13 3 2 78.15 81.49 2.01 o -11 3 2 41.65 39.35 2.13 o -9 3 2 443.60 462.23 7.73 o -7 3 2 303.25 318.31 5.81 o -5 3 2 1452.40 1395.03 24.21 o -3 3 2 204.75 233.89 4.31 o -1 3 2 2819.60 2760.28 46.33 o 1 3 2 7447.40 7644.53 119.80 o 3 3 2 2172.15 2151.67 32.80 o 5 3 2 6281.65 6249.50 87.53 o 7 3 2 3850.45 3641.59 57.95 o 9 3 2 1613.40 1614.99 25.13 o 11 3 2 7.15 2.54 1.00 o 13 3 2 23.65 23.57 1.30 o 15 3 2 72.55 91.00 2.51 o 17 3 2 229.10 225.48 8.35 o 19 3 2 11.35 9.75 2.72 o 21 3 2 4.70 3.62 2.26 < -22 4 2 159.75 149.57 10.65 o -20 4 2 142.55 138.25 5.65 o -18 4 2 19.95 24.41 1.96 o -16 4 2 5.35 4.27 1.05 o -14 4 2 373.45 375.23 8.96 o -12 4 2 33.70 33.63 1.25 o -10 4 2 2052.15 1970.23 33.03 o -8 4 2 39.40 17.03 1.32 o -6 4 2 32.80 39.72 1.24 o -4 4 2 73.55 65.62 1.98 o -2 4 2 3832.35 3726.77 74.23 o 0 4 2 528.45 484.88 10.23 o 2 4 2 123.50 132.75 2.80 o 4 4 2 753.00 805.04 12.80 o 6 4 2 3685.70 3736.14 53.13 o 8 4 2 9.25 14.50 0.90 o 10 4 2 15.15 13.83 1.10 o 12 4 2 876.20 859.31 15.68 o 14 4 2 66.20 66.62 2.50 o 16 4 2 329.70 306.96 8.77 o 18 4 2 3.35 4.39 2.52 < 20 4 2 198.15 171.20 12.40 o -21 5 2 6.40 4.33 3.66 < -19 5 2 108.20 115.45 6.75 o -17 5 2 27.60 15.69 3.07 o -15 5 2 167.05 161.06 5.02 o -13 5 2 315.35 313.37 6.85 o -11 5 2 410.40 413.12 8.73 o -9 5 2 125.65 114.14 3.47 o -7 5 2 2249.05 2266.07 38.54 o -5 5 2 29.45 35.37 1.30 o -3 5 2 778.60 767.42 14.17 o -1 5 2 1581.65 1714.72 28.06 o 1 5 2 2752.85 2538.96 46.53 o 3 5 2 1322.20 1331.47 22.41 o 5 5 2 4759.70 4608.57 71.46 o 7 5 2 23.40 24.06 1.10 o 9 5 2 234.25 235.73 5.06 o 11 5 2 540.60 557.18 11.00 o 13 5 2 1196.00 1090.58 22.50 o 15 5 2 103.60 106.89 3.45 o 17 5 2 -6.50 1.69 18.56 < 19 5 2 -14.35 0.05 31.26 < 21 5 2 18.15 14.53 4.36 o -20 6 2 16.50 3.59 4.30 o -18 6 2 50.30 60.27 5.05 o -16 6 2 12.95 17.41 3.00 o -14 6 2 242.15 257.69 6.06 o -12 6 2 346.80 356.62 8.67 o -10 6 2 44.70 42.73 1.84 o -8 6 2 429.35 438.85 8.95 o -6 6 2 941.35 928.69 16.04 o -4 6 2 674.75 706.43 12.59 o -2 6 2 1091.15 1076.32 19.91 o 0 6 2 30.65 19.50 2.21 o 2 6 2 52.25 49.01 2.75 o 4 6 2 21.35 8.99 1.47 o 6 6 2 560.25 562.46 10.41 o 8 6 2 1065.15 1022.61 18.27 o 10 6 2 206.15 208.76 5.30 o 12 6 2 161.00 151.94 4.66 o 14 6 2 130.35 141.09 5.06 o 16 6 2 15.45 12.02 3.27 o 18 6 2 133.15 131.86 8.75 o 20 6 2 18.85 21.83 4.83 o -19 7 2 68.40 60.94 6.43 o -17 7 2 34.15 34.89 4.50 o -15 7 2 215.75 208.29 11.16 o -13 7 2 1.80 0.02 1.21 < -11 7 2 855.95 803.05 18.20 o -9 7 2 261.10 251.49 6.32 o -7 7 2 295.60 303.99 6.49 o -5 7 2 338.20 348.52 7.45 o -3 7 2 1364.65 1224.28 24.19 o -1 7 2 2687.85 2507.45 45.03 o 1 7 2 2.90 0.59 1.52 < 3 7 2 35.15 42.46 1.94 o 5 7 2 86.85 93.60 3.22 o 7 7 2 143.95 149.35 5.76 o 9 7 2 566.55 515.81 12.20 o 11 7 2 332.70 322.59 8.84 o 13 7 2 31.25 27.11 3.17 o 15 7 2 100.10 106.56 22.73 o 17 7 2 25.65 26.48 4.46 o 19 7 2 53.85 52.32 5.91 o -18 8 2 21.75 21.45 4.46 o -16 8 2 23.60 21.39 4.55 o -14 8 2 14.10 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3 985.80 938.02 17.35 o -15 1 3 211.35 228.38 4.20 o -13 1 3 642.45 602.23 10.15 o -11 1 3 27.10 16.71 0.95 o -9 1 3 10.65 5.53 0.65 o -7 1 3 14.95 17.38 0.61 o -5 1 3 2832.85 3025.12 57.94 o -3 1 3 12604.95 12646.67 346.46 o -1 1 3 4113.05 0.00 66.36 x 1 1 3 5672.55 5979.82 81.00 o 3 1 3 16397.75 15991.20 369.69 o 5 1 3 8735.00 8971.37 112.85 o 7 1 3 595.60 571.79 9.30 o 9 1 3 3025.05 2986.34 42.00 o 11 1 3 84.15 73.14 2.25 o 13 1 3 1527.05 1504.70 24.20 o 15 1 3 562.95 597.05 11.49 o 17 1 3 3.35 0.75 1.40 < 19 1 3 10.05 12.75 2.10 o 21 1 3 2.55 0.66 2.07 < -24 2 3 123.45 136.31 7.49 o -22 2 3 218.45 209.04 8.65 o -20 2 3 3.75 8.50 1.53 < -18 2 3 191.15 198.94 4.66 o -16 2 3 343.95 349.35 7.06 o -14 2 3 759.00 790.09 13.95 o -12 2 3 1962.20 2047.50 31.30 o -10 2 3 289.85 347.42 5.22 o -8 2 3 444.55 384.66 6.96 o -6 2 3 158.30 155.25 3.06 o -4 2 3 364.35 334.47 9.84 o -2 2 3 424.30 393.97 7.71 o 0 2 3 4510.35 4746.25 66.36 o 2 2 3 7005.75 7191.80 106.67 o 4 2 3 35.50 45.20 0.95 o 6 2 3 158.25 190.00 2.95 o 8 2 3 1.20 0.11 0.93 < 10 2 3 2415.65 2337.40 35.07 o 12 2 3 503.30 468.63 9.29 o 14 2 3 152.15 188.73 4.07 o 16 2 3 4.70 6.80 1.39 o 18 2 3 3.20 2.96 1.93 < 20 2 3 0.30 0.44 4.60 < 22 2 3 353.75 310.31 13.45 o -23 3 3 36.30 37.76 4.60 o -21 3 3 2.85 4.33 1.43 < -19 3 3 210.05 219.16 6.41 o -17 3 3 19.05 23.29 1.36 o -15 3 3 19.20 19.29 1.22 o -13 3 3 113.10 107.27 3.08 o -11 3 3 292.85 270.26 5.70 o -9 3 3 2357.70 2300.62 39.01 o -7 3 3 1446.20 1496.61 24.28 o -5 3 3 15726.70 15122.89 295.70 o -3 3 3 563.75 534.21 12.36 o -1 3 3 13268.60 13450.01 303.01 o 1 3 3 658.70 715.27 10.90 o 3 3 3 1922.05 2025.95 30.04 o 5 3 3 1994.05 1960.08 29.49 o 7 3 3 18.70 19.25 1.00 o 9 3 3 106.30 104.83 2.71 o 11 3 3 1537.50 1426.18 24.00 o 13 3 3 172.90 153.67 4.31 o 15 3 3 18.85 18.13 1.40 o 17 3 3 4.00 0.50 3.03 < 19 3 3 222.30 201.90 9.65 o 21 3 3 17.05 19.28 3.59 o -22 4 3 3.70 1.67 3.41 < -20 4 3 388.60 356.69 11.55 o -18 4 3 32.60 34.66 1.94 o -16 4 3 1574.60 1573.18 25.68 o 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385.43 o -3 1 4 16.35 10.51 0.85 o -1 1 4 6737.40 6959.50 116.82 o 1 1 4 427.35 436.96 7.40 o 3 1 4 226.20 241.52 4.32 o 5 1 4 82.80 94.33 2.00 o 7 1 4 5909.60 5820.52 78.30 o 9 1 4 1.15 0.07 1.21 < 11 1 4 1.30 0.07 1.33 < 13 1 4 53.30 62.54 1.95 o 15 1 4 70.35 67.12 2.51 o 17 1 4 18.20 24.82 1.94 o 19 1 4 44.75 50.64 3.51 o 21 1 4 150.90 143.29 6.80 o -24 2 4 -2.10 0.44 3.52 < -22 2 4 2.20 3.75 1.88 < -20 2 4 3.10 4.50 1.32 < -18 2 4 53.55 61.46 2.05 o -16 2 4 355.50 374.85 7.75 o -14 2 4 439.15 436.05 7.90 o -12 2 4 29.95 22.27 1.02 o -10 2 4 1338.25 1277.29 20.31 o -8 2 4 1341.70 1359.16 28.59 o -6 2 4 8589.00 8786.67 191.63 o -4 2 4 3134.20 3263.20 60.17 o -2 2 4 311.90 344.48 6.60 o 0 2 4 164.55 166.79 3.30 o 2 2 4 19.80 25.23 0.85 o 4 2 4 78.40 64.48 1.96 o 6 2 4 2051.20 2065.71 30.22 o 8 2 4 16.40 14.98 0.90 o 10 2 4 810.40 809.58 12.51 o 12 2 4 1138.55 1074.53 19.14 o 14 2 4 553.10 576.47 11.85 o 16 2 4 18.15 16.21 1.73 o 18 2 4 226.60 226.69 9.28 o 20 2 4 6.60 7.72 2.80 < 22 2 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