#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/41/2214181.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2214181_Fobs loop_ _publ_author_name 'Shoukat, Noreen' 'Rauf, M. Khawar' 'Bolte, Michael' 'Badshah, Amin' _publ_section_title ; 1-(3-Chlorophenyl)-3-pivaloylthiourea ; _journal_coeditor_code EZ2082 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3207 _journal_volume 63 _journal_year 2007 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.1269 _cell_length_b 10.2848 _cell_length_c 21.1360 _exptl_crystal_F_000 568.00 _reflns_d_resolution_high 0.7193 _[local]_cod_data_source_file ez2082Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' rauf36 in P212121' _shelx_refln_list_code 4 _shelx_f_calc_maximum 127.86 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 29.32 24.80 1.11 o 4 0 0 2008.89 2090.67 39.93 o 6 0 0 292.50 269.89 7.70 o 8 0 0 2.89 3.87 1.02 o 1 1 0 653.46 570.17 6.57 o 2 1 0 631.77 630.51 9.59 o 3 1 0 1907.63 1905.33 27.52 o 4 1 0 1035.41 1037.65 13.67 o 5 1 0 14.69 15.91 0.62 o 6 1 0 31.34 38.38 0.77 o 7 1 0 41.34 38.23 0.74 o 8 1 0 48.68 42.99 0.85 o 0 2 0 1764.90 1595.11 16.03 o 1 2 0 4453.24 4290.42 38.26 o 2 2 0 2754.26 2689.59 27.72 o 3 2 0 1544.11 1606.11 22.16 o 4 2 0 187.24 186.30 1.94 o 5 2 0 165.34 174.32 6.38 o 6 2 0 93.25 97.02 1.15 o 7 2 0 300.48 296.12 5.32 o 8 2 0 0.14 0.89 0.73 o 1 3 0 5317.82 5208.80 76.35 o 2 3 0 17.18 23.11 0.71 o 3 3 0 5199.11 5531.48 65.00 o 4 3 0 764.64 776.29 9.61 o 5 3 0 2.94 4.98 0.70 o 6 3 0 18.99 21.57 0.71 o 7 3 0 13.56 12.85 0.69 o 8 3 0 22.62 19.96 0.87 o 0 4 0 3544.92 3631.45 67.28 o 1 4 0 1283.65 1310.35 18.23 o 2 4 0 908.89 940.90 13.43 o 3 4 0 691.56 685.53 8.26 o 4 4 0 296.33 299.68 4.93 o 5 4 0 54.44 65.38 2.15 o 6 4 0 73.46 75.99 0.93 o 7 4 0 329.44 313.65 12.69 o 8 4 0 11.09 9.43 0.92 o 1 5 0 443.13 434.72 6.41 o 2 5 0 10.22 18.60 1.12 o 3 5 0 453.62 449.22 4.57 o 4 5 0 3046.30 3103.80 51.97 o 5 5 0 920.81 942.42 16.56 o 6 5 0 108.59 117.59 2.68 o 7 5 0 0.21 0.74 0.84 o 0 6 0 1411.33 1370.48 25.83 o 1 6 0 1756.53 1793.39 23.58 o 2 6 0 942.32 934.89 5.20 o 3 6 0 32.93 42.25 0.94 o 4 6 0 1334.58 1346.28 18.63 o 5 6 0 273.03 260.07 3.15 o 6 6 0 5.95 9.17 0.77 o 7 6 0 1.06 0.46 0.86 o 1 7 0 395.33 443.25 5.70 o 2 7 0 322.32 310.38 4.20 o 3 7 0 131.31 151.06 2.83 o 4 7 0 70.67 73.98 0.93 o 5 7 0 36.14 37.17 1.06 o 6 7 0 134.05 129.20 2.08 o 7 7 0 1.32 1.66 0.81 o 0 8 0 283.74 308.84 8.10 o 1 8 0 4.46 6.84 0.66 o 2 8 0 770.35 756.72 9.26 o 3 8 0 24.07 32.52 0.71 o 4 8 0 173.52 172.31 2.66 o 5 8 0 263.63 266.34 5.22 o 6 8 0 0.02 1.31 0.67 o 7 8 0 148.22 117.20 4.08 o 1 9 0 500.20 507.91 9.93 o 2 9 0 7.36 4.81 0.65 o 3 9 0 23.10 22.59 0.71 o 4 9 0 9.36 8.69 0.63 o 5 9 0 511.40 513.89 8.75 o 6 9 0 9.63 8.19 0.86 o 0 10 0 60.26 52.42 1.19 o 1 10 0 838.87 825.66 12.51 o 2 10 0 94.77 110.19 2.11 o 3 10 0 66.87 67.50 2.39 o 4 10 0 23.81 21.16 0.90 o 5 10 0 66.31 71.29 1.89 o 6 10 0 18.19 14.45 0.94 o 1 11 0 297.03 289.77 4.16 o 2 11 0 352.03 359.33 6.68 o 3 11 0 10.38 15.17 0.76 o 4 11 0 13.65 15.84 0.72 o 5 11 0 82.12 80.09 1.98 o 0 12 0 8.72 10.31 1.08 o 1 12 0 167.81 165.39 3.54 o 2 12 0 30.31 34.17 1.17 o 3 12 0 9.21 8.63 0.75 o 4 12 0 59.42 53.92 1.58 o 1 13 0 23.46 20.46 0.76 o 2 13 0 64.78 62.71 1.17 o 3 13 0 9.05 9.69 0.81 o 0 14 0 295.47 289.07 5.05 o 1 14 0 27.97 26.02 1.40 o 1 0 1 93.33 82.21 2.36 o 2 0 1 8625.23 8807.40 65.12 o 3 0 1 964.85 997.51 10.97 o 4 0 1 502.26 568.18 8.66 o 5 0 1 53.50 64.87 1.09 o 6 0 1 908.33 910.01 14.82 o 7 0 1 109.46 107.93 2.46 o 8 0 1 29.86 30.53 1.15 o -8 1 1 55.36 54.49 1.43 o -7 1 1 24.46 23.82 0.67 o -6 1 1 92.45 88.28 1.93 o -5 1 1 352.12 362.82 4.72 o -4 1 1 738.62 709.84 6.81 o -3 1 1 61.15 54.80 1.05 o -2 1 1 6480.26 6472.15 71.77 o -1 1 1 3457.20 3257.81 42.01 o 1 1 1 3412.68 3206.87 39.78 o 2 1 1 6473.84 6530.26 69.26 o 3 1 1 50.70 45.75 0.80 o 4 1 1 738.14 706.37 10.08 o 5 1 1 348.53 366.60 5.55 o 6 1 1 93.71 92.07 1.98 o 7 1 1 23.92 22.59 0.63 o 8 1 1 54.39 51.26 2.03 o -8 2 1 86.56 81.96 1.62 o -7 2 1 40.31 39.03 0.75 o -6 2 1 144.97 149.02 2.06 o -5 2 1 334.19 323.11 3.34 o -4 2 1 270.40 278.84 2.74 o -3 2 1 477.05 492.78 6.87 o -2 2 1 820.74 803.58 8.16 o -1 2 1 16243.72 17976.59 567.72 o 0 2 1 1210.68 1044.81 12.54 o 1 2 1 16347.17 18556.20 327.44 o 2 2 1 811.11 792.45 7.76 o 3 2 1 481.44 488.16 5.07 o 4 2 1 264.08 274.97 3.78 o 5 2 1 342.73 329.16 7.01 o 6 2 1 145.46 149.92 2.33 o 7 2 1 39.79 37.51 0.75 o 8 2 1 86.68 81.01 2.56 o -8 3 1 17.19 16.23 0.81 o -7 3 1 151.06 157.78 3.77 o -6 3 1 139.59 148.19 1.11 o -5 3 1 759.50 770.62 17.95 o -4 3 1 32.19 29.36 0.68 o -3 3 1 2053.06 2070.54 22.42 o -2 3 1 434.13 400.51 2.49 o -1 3 1 1959.67 1809.11 41.61 o 0 3 1 266.54 230.50 5.02 o 1 3 1 1967.26 1834.43 18.86 o 2 3 1 441.91 407.55 3.39 o 3 3 1 2029.18 2025.17 28.59 o 4 3 1 31.38 30.86 0.99 o 5 3 1 763.49 804.42 10.65 o 6 3 1 138.69 141.20 2.55 o 7 3 1 152.54 162.83 3.48 o 8 3 1 17.56 16.67 0.82 o -8 4 1 10.65 8.83 0.89 o -7 4 1 112.31 114.86 2.13 o -6 4 1 20.32 23.25 0.79 o -5 4 1 62.74 59.70 1.14 o -4 4 1 111.10 101.33 1.27 o -3 4 1 2770.21 2768.96 26.26 o -2 4 1 2141.84 2247.03 27.42 o -1 4 1 812.53 768.54 10.78 o 0 4 1 18.04 15.75 0.64 o 1 4 1 823.42 780.94 9.26 o 2 4 1 2173.71 2268.14 19.09 o 3 4 1 2780.71 2768.20 25.49 o 4 4 1 104.23 95.33 1.92 o 5 4 1 61.36 59.48 1.12 o 6 4 1 22.23 25.77 0.73 o 7 4 1 114.25 113.16 2.19 o 8 4 1 11.28 8.73 0.82 o -7 5 1 60.83 62.53 1.30 o -6 5 1 163.28 165.42 2.35 o -5 5 1 37.67 41.33 1.59 o -4 5 1 163.97 166.81 4.05 o -3 5 1 541.25 544.70 9.93 o -2 5 1 3452.06 3549.98 36.12 o -1 5 1 2241.81 2412.39 32.82 o 0 5 1 2080.94 2144.55 27.39 o 1 5 1 2205.86 2308.67 21.89 o 2 5 1 3437.63 3500.04 47.61 o 3 5 1 562.11 579.55 5.76 o 4 5 1 174.90 177.79 2.29 o 5 5 1 38.47 40.06 1.10 o 6 5 1 158.38 168.20 2.26 o 7 5 1 60.34 60.56 1.57 o -7 6 1 7.09 7.21 1.06 o -6 6 1 660.17 641.67 17.62 o -5 6 1 14.04 14.43 0.70 o -4 6 1 222.67 226.65 3.72 o -3 6 1 677.86 666.09 7.30 o -2 6 1 601.98 618.41 8.25 o -1 6 1 219.62 218.33 3.56 o 0 6 1 1008.56 1025.97 18.25 o 1 6 1 214.37 205.84 3.21 o 2 6 1 611.50 629.44 4.89 o 3 6 1 679.58 651.66 7.83 o 4 6 1 238.73 240.82 3.79 o 5 6 1 16.88 18.45 0.71 o 6 6 1 654.40 660.48 12.45 o 7 6 1 7.41 8.27 0.81 o -7 7 1 12.18 13.75 0.91 o -6 7 1 291.19 306.43 7.31 o -5 7 1 415.73 418.02 7.29 o -4 7 1 133.63 122.71 1.79 o -3 7 1 9.42 11.63 0.60 o -2 7 1 152.73 145.25 1.91 o -1 7 1 35.20 34.04 0.67 o 0 7 1 1640.40 1551.34 27.08 o 1 7 1 38.61 37.43 0.70 o 2 7 1 155.45 147.01 0.99 o 3 7 1 7.83 10.29 0.62 o 4 7 1 138.67 125.89 1.78 o 5 7 1 428.76 439.18 6.33 o 6 7 1 293.10 302.22 4.37 o 7 7 1 12.38 13.62 0.84 o -7 8 1 19.28 17.03 1.05 o -6 8 1 52.65 47.47 1.01 o -5 8 1 157.52 154.18 4.88 o -4 8 1 242.28 237.03 2.85 o -3 8 1 769.13 797.09 12.93 o -2 8 1 451.60 432.22 5.26 o -1 8 1 263.87 262.97 4.35 o 0 8 1 10.42 9.85 0.53 o 1 8 1 267.82 271.58 4.15 o 2 8 1 449.84 426.86 4.81 o 3 8 1 768.61 780.04 10.70 o 4 8 1 239.78 228.68 2.72 o 5 8 1 155.46 157.24 1.79 o 6 8 1 52.93 51.88 1.15 o 7 8 1 18.87 16.13 0.98 o -6 9 1 39.12 39.27 1.35 o -5 9 1 25.51 24.22 0.80 o -4 9 1 38.46 38.49 1.31 o -3 9 1 43.75 44.12 0.78 o -2 9 1 188.03 186.20 2.12 o -1 9 1 267.68 271.09 3.24 o 0 9 1 23.26 22.18 0.61 o 1 9 1 268.93 272.25 4.16 o 2 9 1 192.12 190.09 2.71 o 3 9 1 44.23 45.48 1.33 o 4 9 1 39.66 41.10 0.78 o 5 9 1 26.27 25.04 0.93 o 6 9 1 39.55 40.13 1.39 o -6 10 1 42.00 36.60 1.35 o -5 10 1 16.67 16.71 0.78 o -4 10 1 157.90 163.17 2.00 o -3 10 1 338.95 343.70 7.48 o -2 10 1 320.47 327.15 3.53 o -1 10 1 6.75 6.88 0.60 o 0 10 1 11.76 13.73 0.66 o 1 10 1 6.12 6.36 0.66 o 2 10 1 312.50 321.17 3.77 o 3 10 1 338.40 342.78 6.48 o 4 10 1 159.70 166.10 2.84 o 5 10 1 16.17 16.03 0.75 o 6 10 1 40.64 32.88 0.98 o -5 11 1 126.53 129.72 4.08 o -4 11 1 121.05 127.59 2.83 o -3 11 1 71.07 71.09 2.14 o -2 11 1 282.15 276.53 4.97 o -1 11 1 214.42 214.65 3.75 o 0 11 1 258.25 261.20 5.37 o 1 11 1 212.10 216.25 3.32 o 2 11 1 278.52 275.59 3.34 o 3 11 1 69.52 68.86 1.87 o 4 11 1 122.13 129.24 2.69 o 5 11 1 123.69 119.13 4.57 o -4 12 1 118.29 113.97 3.63 o -3 12 1 15.02 17.02 0.86 o -2 12 1 41.17 39.43 0.90 o -1 12 1 33.77 34.62 0.82 o 0 12 1 2.57 2.70 0.64 o 1 12 1 31.14 32.45 1.07 o 2 12 1 41.76 41.05 0.87 o 3 12 1 15.30 16.11 0.83 o 4 12 1 119.44 115.93 3.54 o -3 13 1 4.95 6.27 0.69 o -2 13 1 129.92 122.91 2.84 o -1 13 1 151.57 145.08 2.20 o 0 13 1 129.77 132.40 2.48 o 1 13 1 153.11 147.17 2.61 o 2 13 1 132.54 127.67 1.92 o 3 13 1 4.96 5.29 0.78 o -1 14 1 36.72 34.62 0.90 o 0 14 1 3.25 5.16 0.78 o 1 14 1 35.90 37.92 1.02 o 1 0 2 4809.31 4552.33 43.69 o 2 0 2 171.72 163.96 1.75 o 3 0 2 419.22 420.86 4.38 o 4 0 2 135.33 120.82 3.18 o 5 0 2 231.22 243.66 4.29 o 6 0 2 39.31 32.74 0.71 o 7 0 2 17.49 17.27 0.64 o 8 0 2 0.31 1.77 0.71 o -8 1 2 140.29 122.37 3.18 o -7 1 2 11.80 11.66 0.63 o -6 1 2 103.59 105.02 1.14 o -5 1 2 257.35 231.16 4.08 o -4 1 2 293.03 285.79 3.11 o -3 1 2 282.32 271.73 3.71 o -2 1 2 2538.54 2449.08 30.93 o -1 1 2 2433.91 2265.06 17.79 o 1 1 2 2388.70 2195.11 27.35 o 2 1 2 2556.33 2480.97 30.58 o 3 1 2 282.16 284.89 4.09 o 4 1 2 283.67 272.64 3.53 o 5 1 2 262.15 239.43 4.24 o 6 1 2 109.56 111.32 2.18 o 7 1 2 11.18 10.24 0.64 o 8 1 2 138.08 120.95 3.13 o -8 2 2 58.70 51.45 1.81 o -7 2 2 80.31 76.73 1.55 o -6 2 2 150.80 156.07 2.65 o -5 2 2 212.93 203.14 3.35 o -4 2 2 607.17 635.13 6.92 o -3 2 2 1080.65 1184.37 12.23 o -2 2 2 510.76 446.08 4.85 o -1 2 2 199.80 182.25 6.23 o 0 2 2 1406.94 1255.21 5.93 o 1 2 2 206.95 182.79 4.74 o 2 2 2 546.27 482.64 4.84 o 3 2 2 1099.77 1213.71 18.05 o 4 2 2 615.39 657.89 8.22 o 5 2 2 215.20 208.83 3.01 o 6 2 2 153.01 158.88 2.30 o 7 2 2 83.97 84.56 1.01 o 8 2 2 57.09 47.97 1.40 o -8 3 2 21.07 19.60 0.76 o -7 3 2 15.83 17.89 0.88 o -6 3 2 57.78 57.17 0.88 o -5 3 2 206.40 206.38 1.35 o -4 3 2 186.89 185.85 1.69 o -3 3 2 229.55 220.51 1.50 o -2 3 2 67.46 89.77 0.96 o -1 3 2 5121.73 5051.70 69.28 o 0 3 2 72.51 76.25 1.16 o 1 3 2 5090.22 4871.80 70.03 o 2 3 2 78.27 101.06 1.72 o 3 3 2 231.49 220.74 2.26 o 4 3 2 184.80 184.57 1.85 o 5 3 2 216.18 218.66 3.40 o 6 3 2 59.48 57.45 0.99 o 7 3 2 17.21 20.38 0.94 o 8 3 2 20.59 17.00 0.74 o -8 4 2 15.08 14.93 0.91 o -7 4 2 204.24 193.05 5.38 o -6 4 2 21.36 22.82 1.19 o -5 4 2 1208.19 1246.53 15.53 o -4 4 2 106.91 108.86 1.33 o -3 4 2 820.73 810.13 9.55 o -2 4 2 125.74 120.65 1.21 o -1 4 2 541.33 513.11 8.64 o 0 4 2 32.47 27.19 0.64 o 1 4 2 528.04 500.26 4.65 o 2 4 2 129.75 127.52 1.62 o 3 4 2 816.99 824.41 8.32 o 4 4 2 111.97 113.37 1.69 o 5 4 2 1222.91 1246.36 16.30 o 6 4 2 19.87 21.58 0.73 o 7 4 2 203.68 202.06 5.34 o 8 4 2 14.17 13.22 0.91 o -7 5 2 7.16 6.59 0.87 o -6 5 2 175.39 182.94 2.36 o -5 5 2 79.50 80.56 1.57 o -4 5 2 475.83 478.37 5.04 o -3 5 2 46.50 49.93 0.76 o -2 5 2 60.84 56.75 0.90 o -1 5 2 262.19 220.04 4.44 o 0 5 2 1110.51 997.72 13.26 o 1 5 2 257.07 214.06 2.26 o 2 5 2 61.31 63.63 2.60 o 3 5 2 48.23 50.85 1.06 o 4 5 2 480.18 470.98 6.81 o 5 5 2 86.68 89.35 1.19 o 6 5 2 180.77 186.04 2.26 o 7 5 2 7.41 6.66 0.68 o -7 6 2 15.87 14.49 0.91 o -6 6 2 219.96 225.97 4.44 o -5 6 2 90.34 87.25 2.02 o -4 6 2 1504.81 1539.42 25.08 o -3 6 2 17.67 14.09 0.60 o -2 6 2 382.37 336.99 4.98 o -1 6 2 170.75 186.91 2.69 o 0 6 2 549.07 487.92 6.85 o 1 6 2 175.82 186.11 2.11 o 2 6 2 390.92 346.37 2.93 o 3 6 2 14.10 10.66 0.53 o 4 6 2 1477.22 1494.26 17.72 o 5 6 2 90.20 88.47 1.10 o 6 6 2 214.55 217.64 2.29 o 7 6 2 15.26 14.92 0.82 o -7 7 2 153.98 152.44 5.29 o -6 7 2 54.74 54.24 1.18 o -5 7 2 114.17 111.23 2.73 o -4 7 2 164.29 162.75 2.15 o -3 7 2 118.24 117.12 2.54 o -2 7 2 95.44 87.05 1.10 o -1 7 2 580.14 591.70 11.83 o 0 7 2 679.54 752.21 10.44 o 1 7 2 560.09 575.84 9.08 o 2 7 2 102.17 91.01 0.86 o 3 7 2 122.55 122.60 1.24 o 4 7 2 161.40 158.80 2.73 o 5 7 2 114.54 108.30 2.04 o 6 7 2 53.02 51.18 0.82 o 7 7 2 152.23 156.05 4.16 o -7 8 2 150.46 133.91 7.60 o -6 8 2 41.36 39.66 1.03 o -5 8 2 176.03 171.84 2.63 o -4 8 2 179.53 181.32 2.75 o -3 8 2 210.73 216.19 5.50 o -2 8 2 131.93 135.94 1.47 o -1 8 2 36.11 36.60 0.70 o 0 8 2 32.89 39.66 0.67 o 1 8 2 37.19 38.68 0.85 o 2 8 2 129.96 132.56 1.04 o 3 8 2 223.14 229.49 2.85 o 4 8 2 176.92 181.99 3.47 o 5 8 2 173.17 170.80 1.86 o 6 8 2 42.16 41.39 1.37 o 7 8 2 152.92 132.74 3.33 o -6 9 2 8.52 10.53 1.04 o -5 9 2 95.43 93.26 2.82 o -4 9 2 33.36 38.58 1.34 o -3 9 2 300.23 286.09 5.63 o -2 9 2 115.49 120.62 2.07 o -1 9 2 692.38 673.91 8.23 o 0 9 2 897.43 893.64 10.80 o 1 9 2 698.15 691.52 16.56 o 2 9 2 116.85 123.46 1.03 o 3 9 2 300.44 283.06 4.20 o 4 9 2 31.83 37.72 0.99 o 5 9 2 97.25 99.00 2.28 o 6 9 2 6.92 9.05 0.83 o -6 10 2 90.12 85.99 3.29 o -5 10 2 106.45 107.65 2.87 o -4 10 2 363.69 361.94 5.77 o -3 10 2 136.88 137.46 2.76 o -2 10 2 180.86 191.93 2.64 o -1 10 2 11.34 10.77 0.62 o 0 10 2 41.20 39.01 0.82 o 1 10 2 11.83 10.50 0.66 o 2 10 2 190.39 196.87 3.58 o 3 10 2 134.91 135.17 2.83 o 4 10 2 358.93 360.11 6.61 o 5 10 2 104.43 107.69 2.89 o 6 10 2 90.61 85.86 2.98 o -5 11 2 3.52 3.71 0.82 o -4 11 2 2.02 3.14 0.78 o -3 11 2 13.92 15.48 0.75 o -2 11 2 87.93 89.02 1.91 o -1 11 2 247.93 251.09 4.11 o 0 11 2 87.32 89.24 1.40 o 1 11 2 256.36 259.25 4.99 o 2 11 2 88.99 85.83 1.74 o 3 11 2 15.10 15.75 0.72 o 4 11 2 2.43 3.18 0.78 o 5 11 2 3.58 2.91 0.75 o -4 12 2 112.42 105.39 3.23 o -3 12 2 327.38 334.63 6.92 o -2 12 2 13.82 16.73 0.80 o -1 12 2 55.09 53.81 0.90 o 0 12 2 417.44 408.56 5.93 o 1 12 2 55.35 52.33 1.24 o 2 12 2 11.37 14.04 0.73 o 3 12 2 321.11 320.20 4.84 o 4 12 2 115.64 103.95 5.91 o -3 13 2 96.94 96.60 3.30 o -2 13 2 38.33 31.20 1.30 o -1 13 2 73.41 68.62 1.60 o 0 13 2 193.91 180.67 2.70 o 1 13 2 70.64 66.82 1.18 o 2 13 2 38.37 31.98 0.82 o 3 13 2 95.63 89.36 2.20 o -1 14 2 10.33 9.73 0.80 o 0 14 2 30.45 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